CN110711168A - Method for preparing amino acid skin care essence by using high essential amino acid rice saving - Google Patents
Method for preparing amino acid skin care essence by using high essential amino acid rice saving Download PDFInfo
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- CN110711168A CN110711168A CN201911205800.6A CN201911205800A CN110711168A CN 110711168 A CN110711168 A CN 110711168A CN 201911205800 A CN201911205800 A CN 201911205800A CN 110711168 A CN110711168 A CN 110711168A
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- amino acid
- essential amino
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- 150000001413 amino acids Chemical class 0.000 title claims abstract description 80
- 235000020776 essential amino acid Nutrition 0.000 title claims abstract description 60
- 239000003797 essential amino acid Substances 0.000 title claims abstract description 60
- 235000007164 Oryza sativa Nutrition 0.000 title claims abstract description 30
- 235000009566 rice Nutrition 0.000 title claims abstract description 30
- 238000000034 method Methods 0.000 title claims abstract description 23
- 240000007594 Oryza sativa Species 0.000 title claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 35
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 24
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims description 19
- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 claims description 19
- 229960003237 betaine Drugs 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 19
- 239000000463 material Substances 0.000 claims description 17
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 16
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims description 16
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 238000000605 extraction Methods 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 11
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 10
- 239000008367 deionised water Substances 0.000 claims description 9
- 229910021641 deionized water Inorganic materials 0.000 claims description 9
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims description 8
- MLSJBGYKDYSOAE-DCWMUDTNSA-N L-Ascorbic acid-2-glucoside Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O[C@@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)=C1O MLSJBGYKDYSOAE-DCWMUDTNSA-N 0.000 claims description 8
- 229930003427 Vitamin E Natural products 0.000 claims description 8
- 229960000458 allantoin Drugs 0.000 claims description 8
- 229940069521 aloe extract Drugs 0.000 claims description 8
- 229940067599 ascorbyl glucoside Drugs 0.000 claims description 8
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 8
- 235000019165 vitamin E Nutrition 0.000 claims description 8
- 229940046009 vitamin E Drugs 0.000 claims description 8
- 239000011709 vitamin E Substances 0.000 claims description 8
- 239000002671 adjuvant Substances 0.000 claims description 7
- 239000000171 lavandula angustifolia l. flower oil Substances 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 7
- 239000000243 solution Substances 0.000 claims description 7
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical compound CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 claims description 6
- 230000002421 anti-septic effect Effects 0.000 claims description 6
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 6
- 235000013379 molasses Nutrition 0.000 claims description 6
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 5
- 108010059820 Polygalacturonase Proteins 0.000 claims description 5
- 239000007853 buffer solution Substances 0.000 claims description 5
- 239000003729 cation exchange resin Substances 0.000 claims description 5
- 238000004945 emulsification Methods 0.000 claims description 5
- 108010093305 exopolygalacturonase Proteins 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 230000010355 oscillation Effects 0.000 claims description 5
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 239000008213 purified water Substances 0.000 claims description 5
- 238000007789 sealing Methods 0.000 claims description 5
- 238000002137 ultrasound extraction Methods 0.000 claims description 5
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 4
- 229960005323 phenoxyethanol Drugs 0.000 claims description 4
- 235000016068 Berberis vulgaris Nutrition 0.000 claims description 3
- 241000335053 Beta vulgaris Species 0.000 claims description 3
- 241000219310 Beta vulgaris subsp. vulgaris Species 0.000 claims description 3
- 235000021536 Sugar beet Nutrition 0.000 claims description 3
- 238000013375 chromatographic separation Methods 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 3
- 238000002425 crystallisation Methods 0.000 claims description 3
- 230000008025 crystallization Effects 0.000 claims description 3
- 230000001804 emulsifying effect Effects 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 claims description 3
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 3
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 claims description 3
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 claims description 3
- 229960002216 methylparaben Drugs 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 2
- 238000007873 sieving Methods 0.000 claims description 2
- 244000178870 Lavandula angustifolia Species 0.000 claims 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims 1
- 241000209094 Oryza Species 0.000 abstract description 27
- 230000003020 moisturizing effect Effects 0.000 abstract description 6
- 239000000654 additive Substances 0.000 abstract description 3
- 230000036620 skin dryness Effects 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 239000002537 cosmetic Substances 0.000 abstract description 2
- 229940024606 amino acid Drugs 0.000 description 59
- 206010013786 Dry skin Diseases 0.000 description 4
- 238000004090 dissolution Methods 0.000 description 4
- 239000003755 preservative agent Substances 0.000 description 3
- 230000002335 preservative effect Effects 0.000 description 3
- 206010040844 Skin exfoliation Diseases 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000035618 desquamation Effects 0.000 description 2
- 230000037336 dry skin Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000037303 wrinkles Effects 0.000 description 2
- AGPKZVBTJJNPAG-WHFBIAKZSA-N L-isoleucine Chemical compound CC[C@H](C)[C@H](N)C(O)=O AGPKZVBTJJNPAG-WHFBIAKZSA-N 0.000 description 1
- KDXKERNSBIXSRK-YFKPBYRVSA-N L-lysine Chemical compound NCCCC[C@H](N)C(O)=O KDXKERNSBIXSRK-YFKPBYRVSA-N 0.000 description 1
- FFEARJCKVFRZRR-BYPYZUCNSA-N L-methionine Chemical compound CSCC[C@H](N)C(O)=O FFEARJCKVFRZRR-BYPYZUCNSA-N 0.000 description 1
- COLNVLDHVKWLRT-QMMMGPOBSA-N L-phenylalanine Chemical compound OC(=O)[C@@H](N)CC1=CC=CC=C1 COLNVLDHVKWLRT-QMMMGPOBSA-N 0.000 description 1
- AYFVYJQAPQTCCC-GBXIJSLDSA-N L-threonine Chemical compound C[C@@H](O)[C@H](N)C(O)=O AYFVYJQAPQTCCC-GBXIJSLDSA-N 0.000 description 1
- QIVBCDIJIAJPQS-VIFPVBQESA-N L-tryptophane Chemical compound C1=CC=C2C(C[C@H](N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-VIFPVBQESA-N 0.000 description 1
- KZSNJWFQEVHDMF-BYPYZUCNSA-N L-valine Chemical compound CC(C)[C@H](N)C(O)=O KZSNJWFQEVHDMF-BYPYZUCNSA-N 0.000 description 1
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 1
- 239000004472 Lysine Substances 0.000 description 1
- AYFVYJQAPQTCCC-UHFFFAOYSA-N Threonine Natural products CC(O)C(N)C(O)=O AYFVYJQAPQTCCC-UHFFFAOYSA-N 0.000 description 1
- 239000004473 Threonine Substances 0.000 description 1
- QIVBCDIJIAJPQS-UHFFFAOYSA-N Tryptophan Natural products C1=CC=C2C(CC(N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-UHFFFAOYSA-N 0.000 description 1
- KZSNJWFQEVHDMF-UHFFFAOYSA-N Valine Natural products CC(C)C(N)C(O)=O KZSNJWFQEVHDMF-UHFFFAOYSA-N 0.000 description 1
- 235000014104 aloe vera supplement Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 229960000310 isoleucine Drugs 0.000 description 1
- AGPKZVBTJJNPAG-UHFFFAOYSA-N isoleucine Natural products CCC(C)C(N)C(O)=O AGPKZVBTJJNPAG-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 229930182817 methionine Natural products 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 230000005808 skin problem Effects 0.000 description 1
- 239000004474 valine Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of cosmetics, in particular to a method for preparing amino acid skin care essence by utilizing high essential amino acid to save rice. The method for preparing the amino acid skin-care essence by utilizing the high essential amino acid festival rice contains 0.1-12% of the high essential amino acid festival rice amino acid by weight percent, and the related skin-care product is the essence. The amino acid skin care essence prepared by the high essential amino acid and the rice saving does not contain harmful chemical additives, can moisten skin, has good moisturizing effect, fully increases the skin moisture, and improves the skin dryness.
Description
Technical Field
The invention relates to the technical field of cosmetic production, in particular to a method for preparing amino acid skin care essence by utilizing high essential amino acid to save rice.
Background
Nowadays, factors such as temperature change and pressure caused by environmental pollution and season change, skin aging and metabolism slowing down cause skin water loss, make skin rough and dry wrinkles, and further cause various skin problems, so that the moisturizing and moisturizing facial skin is very important.
The rice with high essential amino acid is rich in nutrition and contains eight essential amino acids which can not be synthesized by the human body; lysine, tryptophan, phenylalanine, methionine, threonine, isoleucine and valine, and fills the blank of human body requirements. When the rice with high essential amino acid is produced, a byproduct of saving rice with high essential amino acid is generated. The amino acid has the effects of moisturizing, softening skin, resisting wrinkle, whitening, refreshing and the like in the skin care product. However, no research on the preparation of the amino acid skin care essence by using the high essential amino acid festival rice is reported at present.
Disclosure of Invention
In view of the above technical problems, the present invention aims to provide a method for preparing amino acid skin care essence by using high essential amino acid rice saving, wherein the amino acid skin care essence prepared by using high essential amino acid rice saving can moisten skin, enhance skin wettability and improve skin vitality.
In order to achieve the purpose, the invention adopts the following technical scheme:
the method for preparing the amino acid skin care essence by utilizing the high essential amino acid rice-saving technology comprises the following steps:
(1) putting water, 1-4% of glycerol, 0.5-2% of ascorbyl glucoside, 2-5% of betaine, 0.1-0.3% of lavender oil and 0.1-0.2% of allantoin in a weight ratio into an emulsifying tank, stirring uniformly, and heating to 80-85 ℃ for complete dissolution;
(2) cooling to 50-55 deg.C, adding premixed propylene glycol 1-4%, amino acid 0.1-12% and adjuvants 0.1-5%, stirring and dispersing; wherein the amino acid is the amino acid with high essential amino acid content, and the extraction method of the amino acid with high essential amino acid content comprises the steps of crushing the amino acid with high essential amino acid content, sieving the crushed amino acid with a sieve, and drying the crushed amino acid with high essential amino acid content until the moisture content is lower than 10% to obtain the amino acid with high essential amino acid content; adding a buffer solution into the high essential amino acid festival powder, adjusting the pH to 5.0, adding pectinase which is 3.5 percent of the total mass of the high essential amino acid festival powder, and carrying out water bath oscillation enzymolysis for 1.5h at the temperature of 55 ℃ to obtain a mixed initial material; after the enzymolysis is finished, adding purified water into the mixed initial material according to the material-liquid ratio of 1:30, placing the mixture into ultrasonic equipment for ultrasonic extraction, wherein the ultrasonic power is 500w, and the extraction time is 35min, so as to obtain crude amino acid extraction liquid; then adjusting the pH value of the crude amino acid extract to 3.0, and purifying the crude amino acid extract by using a cation exchange resin column or activated carbon to obtain the amino acid extract.
(3) Cooling to 35-43 deg.C, adding antiseptic 0.3-1%, stirring, filtering, sealing and packaging to obtain essence containing high essential amino acids and amino acids.
Further, the auxiliary materials are vitamin E and aloe extract.
Preferably, the preservative is any one of phenoxyethanol, p-hydroxyacetophenone and methylparaben.
Further, the auxiliary materials are vitamin E and aloe extract; the preservative is phenoxyethanol.
Preferably, the preparation method of the betaine comprises the following steps: extracting sugar beet with hot water, cleaning juice, evaporating, crystallizing, and separating sugar, beet pulp and molasses; carrying out primary desugaring separation treatment on the molasses to obtain a first mixture; and carrying out chromatographic separation and evaporative crystallization on the first mixture to extract the betaine.
Further, the water is deionized water.
Preferably, the betaine and the deionized water are dissolved in an emulsification tank according to the weight ratio of 1: 1 to prepare betaine solution with the weight ratio of 50%, then the allantoin is added and fully stirred until the betaine solution is completely dissolved, and then the rest deionized water, the glycerol, the ascorbyl glucoside and the lavender oil are added and stirred uniformly.
Further, the heating mode is water bath heating.
Preferably, the auxiliary materials comprise 0.1-1% of vitamin E and 0.5-2% of aloe extract by weight.
Compared with the prior art, the invention has the following beneficial effects: the amino acid skin care essence prepared by naturally utilizing the highly essential amino acid and saving the rice does not contain harmful chemical additives, can moisten the skin, has good moisturizing effect, fully increases the skin moisture and improves the skin dryness.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In this embodiment, the adjuvants are vitamin E, aloe vera extract.
In this embodiment, the preservative is any one of phenoxyethanol, p-hydroxyacetophenone, and methylparaben.
In this example, the preparation method of betaine is: extracting sugar beet with hot water, cleaning juice, evaporating, crystallizing, and separating sugar, beet pulp and molasses; carrying out primary desugaring separation treatment on the molasses to obtain a first mixture; and carrying out chromatographic separation and evaporative crystallization on the first mixture to extract the betaine.
In this embodiment, the water is deionized water.
In the present embodiment: dissolving betaine and deionized water in an emulsifying tank according to the weight ratio of 1: 1 to prepare betaine solution with the weight ratio of 50%, adding allantoin, stirring fully until the betaine solution is completely dissolved, and then adding the rest deionized water, glycerol, ascorbyl glucoside and lavender oil, and stirring uniformly.
In this embodiment, the heating manner is water bath heating.
Example 1
The preparation method comprises the following steps:
(1) putting water, 1% of glycerol, 0.5% of ascorbyl glucoside, 2% of betaine, 0.1% of lavender oil and 0.1% of allantoin in a weight ratio into an emulsification tank, stirring uniformly, and heating to 80-85 ℃ for complete dissolution;
(2) cooling to 50-55 deg.C, adding premixed propylene glycol 1%, amino acid 0.1% and adjuvants 0.1%, stirring and dispersing; the amino acid is the amino acid with high essential amino acid in the rice, and the extraction method of the amino acid with high essential amino acid in the rice is that the amino acid with high essential amino acid in the rice is crushed and then is sieved, and the crushed amino acid is dried until the moisture content is lower than 10 percent, so that the amino acid with high essential amino acid in the rice is obtained; adding a buffer solution into the high essential amino acid festival powder, adjusting the pH to 5.0, adding pectinase which is 3.5 percent of the total mass of the high essential amino acid festival powder, and carrying out water bath oscillation enzymolysis for 1.5h at the temperature of 55 ℃ to obtain a mixed initial material; after the enzymolysis is finished, adding purified water into the mixed initial material according to the material-liquid ratio of 1:30, placing the mixture into ultrasonic equipment for ultrasonic extraction, wherein the ultrasonic power is 500w, and the extraction time is 35min, so as to obtain crude amino acid extraction liquid; then adjusting the pH value of the crude amino acid extract to 3.0, and purifying the crude amino acid extract by using a cation exchange resin column or activated carbon to obtain the amino acid extract.
(3) Cooling to 35-43 deg.C, adding antiseptic 0.3%, stirring, filtering, sealing and packaging to obtain essence containing high essential amino acids and amino acids.
The weight ratio of the auxiliary materials is 0.1 percent of vitamin E and 0.5 percent of aloe extract.
Example 2
The preparation method comprises the following steps:
(1) putting water, 4% of glycerol, 2% of ascorbyl glucoside, 5% of betaine, 0.3% of lavender oil and 0.2% of allantoin according to the weight ratio into an emulsification tank, stirring uniformly, and heating to 80-85 ℃ for complete dissolution;
(2) cooling to 50-55 deg.C, adding premixed propylene glycol 4%, amino acid 12% and adjuvants 5%, stirring and dispersing; the amino acid is the amino acid with high essential amino acid in the rice, and the extraction method of the amino acid with high essential amino acid in the rice is that the amino acid with high essential amino acid in the rice is crushed and then is sieved, and the crushed amino acid is dried until the moisture content is lower than 10 percent, so that the amino acid with high essential amino acid in the rice is obtained; adding a buffer solution into the high essential amino acid festival powder, adjusting the pH to 5.0, adding pectinase which is 3.5 percent of the total mass of the high essential amino acid festival powder, and carrying out water bath oscillation enzymolysis for 1.5h at the temperature of 55 ℃ to obtain a mixed initial material; after the enzymolysis is finished, adding purified water into the mixed initial material according to the material-liquid ratio of 1:30, placing the mixture into ultrasonic equipment for ultrasonic extraction, wherein the ultrasonic power is 500w, and the extraction time is 35min, so as to obtain crude amino acid extraction liquid; then adjusting the pH value of the crude amino acid extract to 3.0, and purifying the crude amino acid extract by using a cation exchange resin column or activated carbon to obtain the amino acid extract.
(3) Cooling to 35-43 deg.C, adding antiseptic 1%, stirring, filtering, sealing and packaging to obtain essence containing high essential amino acids and amino acids.
The weight ratio of the auxiliary materials is that vitamin E1 percent and aloe extract 2 percent.
Example 3
The preparation method comprises the following steps:
(1) putting water, 3% of glycerol, 1% of ascorbyl glucoside, 3% of betaine, 0.2% of lavender oil and 0.15% of allantoin according to the weight ratio into an emulsification tank, stirring uniformly, and heating to 80-85 ℃ for complete dissolution;
(2) cooling to 50-55 deg.C, adding premixed propylene glycol 3%, amino acid 6% and adjuvants 3%, stirring and dispersing; the amino acid is the amino acid with high essential amino acid in the rice, and the extraction method of the amino acid with high essential amino acid in the rice is that the amino acid with high essential amino acid in the rice is crushed and then is sieved, and the crushed amino acid is dried until the moisture content is lower than 10 percent, so that the amino acid with high essential amino acid in the rice is obtained; adding a buffer solution into the high essential amino acid festival powder, adjusting the pH to 5.0, adding pectinase which is 3.5 percent of the total mass of the high essential amino acid festival powder, and carrying out water bath oscillation enzymolysis for 1.5h at the temperature of 55 ℃ to obtain a mixed initial material; after the enzymolysis is finished, adding purified water into the mixed initial material according to the material-liquid ratio of 1:30, placing the mixture into ultrasonic equipment for ultrasonic extraction, wherein the ultrasonic power is 500w, and the extraction time is 35min, so as to obtain crude amino acid extraction liquid; then adjusting the pH value of the crude amino acid extract to 3.0, and purifying the crude amino acid extract by using a cation exchange resin column or activated carbon to obtain the amino acid extract.
(3) Cooling to 35-43 deg.C, adding antiseptic 0.8%, stirring, filtering, sealing and packaging to obtain essence containing high essential amino acids and amino acids.
The weight ratio of the auxiliary materials is 0.5 percent of vitamin E and 1 percent of aloe extract.
Evaluation of efficacy of use
50 persons are selected and randomly divided into 5 groups, and the experimental group comprises examples 1 to 3, 10 examples 1, 10 examples 2, 10 examples 3, 10 blank control groups and 10 experimental control groups.
The experimental control group is smeared on the face by adopting the common essence on the market.
Blank control group, without any product.
Experimental group, each example group was applied to the face with the amino acid skin care essence prepared from the highly essential amino acid festival rice of examples 1 to 3, respectively.
Three groups all take half a month as an observation period, and the times of the occurrence of dry skin and desquamation are respectively recorded in the observation period.
In the experimental group, the skin of the testee in the example 1 is dry and the number of desquamation people is 0; example 2 subjects had dry skin and 0 skin peels; example 3 the skin of the test subjects was dry and peeled 0 people.
In the experimental control group, the skin of the testee is dry for 3 times and 5 times, and the skin of the testee is peeled for 2 times and 4 times.
In the blank control group, the skin of the test subject is dried 9 times and 18 times, and the skin of the test subject is peeled 6 times and 10 times.
In conclusion, the amino acid skin care essence prepared by the high essential amino acid rice saving method does not contain harmful chemical additives, can moisten skin, has a good moisturizing effect, fully increases the skin wettability and improves the skin dryness.
Claims (8)
1. The method for preparing the amino acid skin care essence by using the high essential amino acid rice-saving is characterized by comprising the following steps: the preparation method comprises the following steps:
(1) according to the weight ratio, putting water, 1-4% of glycerol, 0.5-2% of ascorbyl glucoside, 2-5% of betaine, 0.1-0.3% of lavender oil and 0.1-0.2% of allantoin into an emulsification tank, stirring uniformly, heating to 80-85 ℃ and dissolving completely;
(2) cooling to 50-55 deg.C, adding premixed propylene glycol 1-4%, amino acid 0.1-12% and adjuvants 0.1-5%, stirring and dispersing; the amino acid with high essential amino acid content is obtained by crushing the amino acid with high essential amino acid content, sieving with a sieve, and drying until the water content is lower than 10%; adding a buffer solution into the high essential amino acid festival powder, adjusting the pH to 5.0, adding pectinase which is 3.5 percent of the total mass of the high essential amino acid festival powder, and carrying out water bath oscillation enzymolysis for 1.5h at the temperature of 55 ℃ to obtain a mixed initial material; after the enzymolysis is finished, adding purified water into the mixed initial material according to the material-liquid ratio of 1:30, placing the mixture into ultrasonic equipment for ultrasonic extraction, wherein the ultrasonic power is 500w, and the extraction time is 35min, so as to obtain crude amino acid extraction liquid; then adjusting the pH value of the crude amino acid extract to 3.0, and purifying the crude amino acid extract by using a cation exchange resin column or activated carbon to obtain the amino acid extract.
(3) Cooling to 35-43 deg.C, adding antiseptic 0.3-1%, stirring, filtering, sealing and packaging to obtain essence containing high essential amino acids and amino acids.
2. The method for preparing amino acid skin care essence by using high essential amino acid rice-saving according to claim 1, wherein the method comprises the following steps: the adjuvants are vitamin E and Aloe extract.
3. The method for preparing amino acid skin care essence by using high essential amino acid rice-saving according to claim 1, wherein the method comprises the following steps: the antiseptic is any one of phenoxyethanol, p-hydroxyacetophenone and methylparaben.
4. The method for preparing amino acid skin care essence by using high essential amino acid rice saving as claimed in claim 1, wherein the method for preparing betaine comprises: extracting sugar beet with hot water, cleaning juice, evaporating, crystallizing, and separating sugar, beet pulp and molasses; carrying out primary desugaring separation treatment on the molasses to obtain a first mixture; and carrying out chromatographic separation and evaporative crystallization on the first mixture to extract the betaine.
5. The method for preparing amino acid skin care essence by using high essential amino acid rice-saving according to claim 1, wherein the method comprises the following steps: the water is deionized water.
6. The method for preparing amino acid skin care essence by using high essential amino acid rice-saving according to claim 1, wherein the method comprises the following steps: dissolving betaine and deionized water in an emulsifying tank according to the weight ratio of 1: 1 to prepare 50% betaine solution, adding allantoin, stirring to dissolve completely, adding the rest deionized water, glycerol, ascorbyl glucoside and oleum Lavandula Angustifolia, and stirring.
7. The method for preparing amino acid skin care essence by using high essential amino acid rice-saving according to claim 1, wherein the method comprises the following steps: the heating mode is water bath heating.
8. The method for preparing amino acid skin care essence by using high essential amino acid rice saving according to claim 2, wherein the method comprises the following steps: the auxiliary materials comprise 0.1-1% of vitamin E and 0.5-2% of aloe extract by weight ratio.
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