CN106109284A - A kind of facial film and preparation method thereof - Google Patents

Abstract

The invention discloses a kind of facial film, it is characterised in that include the component of following parts by weight: 82 88 parts of water；Xanthan gum 0.1 0.35 parts；Hyaluronate sodium 0.01 0.1 parts；Butanediol 25 parts；Methyl gluceth 20 is 1.5 3.5 parts；Glycerol 14 parts；Nicotiamide 0.8 2.2 parts；EDETATE SODIUM 0.02 0.06 parts；Carnosine 0.04 0.2 parts；Pantothenylol 0.06 0.16 parts；Skin conditioning agent 2.5 3.5 parts；Wetting agent 14 parts；Preservative 0.1 0.5 parts；PEG 40 castor oil hydrogenated 0.1 0.8 parts；Tocopherol acetas 0.005 0.015 parts；Emollient 0.01 0.1 parts；Described skin conditioning agent includes that plant extract species and amino acids, the parts by weight of described plant extract species are 2.3 3 parts, and the parts by weight of described amino acids are 0.2 0.5 parts.

Description

A kind of facial film and preparation method thereof

Technical field

The present invention relates to daily cosmetics field, more specifically, it relates to a kind of facial film and preparation method thereof.

Background technology

Due to the change at age and the bad environmental factors of Long Term Contact, skin can gradually lose and pollute to external world and micro-life The safeguard function of thing, the harm to surrounding is the most sensitive, and skin adapts to the ability of environment worse and worse, the outward appearance of skin, physics Characteristic and physiological function change in every way, occur that fine rule and wrinkle, flexibility missing, sagging increase, solid sense lacks, color and luster Uniformity disappearance, superficial makings is coarse and the phenomenon such as the pigmentation of plaque-like.Less obvious but measurable old as skin Change occur or the change of experience chronic environmental insult includes that cell and organizational vitality general declines, cellular replication rate reduces, The ability that SkBF slows down, moisture reduces, error accumulation structurally and functionally and skin oneself rebuild and repair declines.

Facial film, as a kind of carrier of face beautifying health keeping product, its objective is to make up makeup removing and the still not enough cleaner that washes one's face Make, and coordinate other active component to realize replenishing water and preserving moisture, whitening and anti-aging, Sage Extract etc. maintenance function on this basis.

The Chinese patent that application publication number is CN104739746A, Shen Qing Publication day is on 07 01st, 2015 discloses one Kind of pure natural nanometer plant mask, is characterized in that: dispelled fat skin moistening and whitening anti-wrinkle mask by silk polypeplide, by following masses proportioning group Become: fibroin 2-6%；Silk peptide 1.5-4.5%；Sorbitol 1-3；Polyvinyl alcohol 4-12%；Sodium benzoate 0.1-0.3%；Titanium dioxide 1.5-4.5%；Porous aluminium hydrate powder 3-9%；Polyvinyl acetate emulsion 2-6%；Ethanol 3-9%；Essence 0.1-0.3%； The nano powder 5-15% that each Chinese medicine is made；Pure water adds to 100%；Wherein, the nano powder that each Chinese medicine is made includes Radix Angelicae Sinensis, ice Sheet, succinum, Radix Rehmanniae Preparata, Margarita powder, sulfur, Semen Armeniacae Amarum, Rhizoma Chuanxiong, Ganoderma spore body, Semen Coicis, Poria, Radix Arnebiae (Radix Lithospermi), tourmaline and wheat meal Stone, all kinds of nano powders mix according to equal amount.

After all kinds of Chinese medicines are dried mix homogeneously by prior art, it is prepared as receiving after cracker for medicine processing, screen cloth screening Rice flour, then prepare facial film with other compositions after mixing homogeneously, this facial film has promotion cutaneous circulation and metabolic work With, skin of face can be made to keep moistening, reach whitening, the wrinkle resistant and effect of defying age.But, owing to growing environment is to Chinese medicine Impact, Chinese medicine may contain heavy metal, the Chinese medicine powder after all kinds of drying directly is broken into Chinese medicine nano powder and enters by prior art Exercising use, the heavy metal that wherein may contain can enter to along with the addition of Chinese medicine nano powder in the facial film of preparation, and Chinese medicine The large percentage that facial film shared by nano powder is overall, user when using facial film, heavy metal therein and contact skin, can endanger Skin health.Therefore, prepare a kind of moisturizing, whitening, crease-resistant and to human body non-hazardous facial film has certain production should By value.

Summary of the invention

The deficiency existed for prior art, the purpose of the present invention one is to provide a kind of facial film, which solves in facial film The Chinese medicine used may containing the problem of harmful heavy metal substance, make facial film that production obtains not only to human body without endangering Do harm to and have moisturizing, whitening, the crease-resistant and advantage of reparation damaged skin.

For achieving the above object one, the technical scheme is that

A kind of facial film, it is characterised in that include the component of following parts by weight:

Water 82-88 part；

Xanthan gum 0.1-0.35 part；

Hyaluronate sodium 0.01-0.1 part；

Butanediol 2-5 part；

Methyl gluceth-20 is 1.5-3.5 part；

Glycerol 1-4 part；

Nicotiamide 0.8-2.2 part；

EDETATE SODIUM 0.02-0.06 part；

Carnosine 0.04-0.2 part；

Pantothenylol 0.06-0.16 part；

Skin conditioning agent 2.5-3.5 part；

Wetting agent 1-4 part；

Preservative 0.1-0.5 part；

Cremophor RH40 0.1-0.8 part；

Tocopherol acetas 0.005-0.015 part；

Emollient 0.01-0.1 part；

Described skin conditioning agent includes that plant extract species and amino acids, the parts by weight of described plant extract species are 2.3- 3 parts, the parts by weight of described amino acids are 0.2-0.5 part.

Tocopherol acetas penetrates into horny layer, is covered in corneocyte surface, thus prevents cell membrane with thin The readily oxidizable substance such as intracellular unsaturated fatty acid are oxidized, thus protect the complete of cell membrane and prevent aging；Hyaluronate sodium is Nature moisturizing factor, can quickly be absorbed by the skin, and has mild dilation blood capillary, increases skin elasticity, delay skin aging. By similar compatibility principle, EDETATE SODIUM, xanthan gum, hyaluronate sodium, tocopherol acetas and plant extract apoplexy due to endogenous wind The composition such as unsaturated fatty acid, vitamin be combined with each other, and forms layer protecting film at skin surface, and intercept in external environment is thin The infringement to skin such as bacterium, heavy metal, dust and ultraviolet, and improve moistening effect；And penetrate into skin, promote blood Liquid circulation and the absorption to nutrient substance, accelerate cellular intermediary metabolism, make damaged skin heal；Meanwhile, reduce the generation of wrinkle, Reduce melanin to generate and to promote the melanin generated to be moved back by blood circulation scattered.Skin can be played sterilization and disappear by butanediol Scorching effect, and the metabolism such as protein in epithelial cell, lipid and saccharide can be promoted, thus stimulate the growth of epithelial cell, promote The skin healing of inflammation of setting out.It addition, butanediol, glycerol and amino acids material produce compounding effect, promote amino acids material It is absorbed by the skin.Nicotiamide can quickly pass through horny layer, improves the barrier action of skin, reduces transepidermal water loss rate.Pass through Similar compatibility principle, the aminoacid in pantothenylol, nicotiamide, carnosine is the most affine with the bioflavonoids of plant extract apoplexy due to endogenous wind, After being absorbed by the skin, the active oxygen making the fatty acid over oxidation of cell membrane during oxidative stress and formed can be removed freely Base, prevents cell senescence, thus forms protective barrier on corneocyte surface；Expansion blood vessel also promotes other compositions quickly quilt Skin absorption, suppression melanosome is transferred to keratinocyte from pigment cell, is reduced facial pigmentation deposition, regulate mucopolysaccharide Content, reduce wrinkle, play tender white, crease-resistant effect.More preferably: described emollient is preferably Oleum Hippophae.

Containing large number of biological flavonoid in Oleum Hippophae, maintain the normal permeability of capillary wall；Soluble in water, for by force Reducing agent, has the antioxidation of excellence.Can Direct Acquisition superoxide radical, it is possible to can effectively prevent amino acids and flesh Amino in peptide is oxidized, protects skin and reduces the degree of aging of skin.

Wherein, possibly together with phospholipid molecule, hydrophilic one end is mutually tied with hydrophilic group in amino acids and hyaluronate sodium Closing, hyaluronate sodium promotes the skin absorption to phospholipid molecule, can make up the phospholipid of disappearance in the cell membrane of corneocyte, from And make corneocyte film have the ability of preferably opposing free radical harm, reduce skin aging degree, and reach reparation and be subject to Damage the effect of skin.

More preferably: described plant extract species selects Aloe vulgaris leaf extract, Radix Et Caulis Acanthopanacis Senticosi extract, Pueraria lobota One or more in root extract, yellow tang extract, Hamamelis virginiana extract, Stigma Croci extract.

Plant extract apoplexy due to endogenous wind contains a large amount of nature moisturizing factor, has the effect of skin moistening moisturizing to skin；Wherein contain The nutrient substance such as volatile oil, Syringa oblata Lindl. element, bioflavonoids, mcg vitamin, quintessence oil, can be absorbed by the skin, Simultaneous Stabilization or Maintain the material such as collagen, elastin, promote the synthesis of collagen protein, prevent wrinkle from producing, and make skin the most elastic.

More preferably: described amino acids chooses one or more in serine, arginine, glycine.

The aminoacid used in the application has good water solublity, is easily absorbed by the skin, can promote that corneocyte is new Old metabolism；Amino is combined with long chain methyl gluceth-20, and scalable methyl gluceth-20 is in this application Polarity degree so that it is be more soluble in water with other components, forms homogeneous and stable state.

More preferably: described wetting agent is the compound of Fructus Hordei Germinatus oligose glucoside, hydrogenated starch hydrolysate and water；Institute Stating Fructus Hordei Germinatus oligose glucoside 0.5-1.6 part, described hydrogenated starch hydrolysate 0.2-1.2 part, described water is 0.4-1.2 part.

Containing a large amount of hydrophilic hydroxyl groups in Fructus Hordei Germinatus oligose glucoside and hydrogenated starch hydrolysate, can be completely dissolved in water, tool There is the effect of water suction moisturizing；And Fructus Hordei Germinatus oligose glucoside and hydrogenated starch hydrolysate are attracted each other by the charges of different polarity, formed steady Fixed carrying structure, connects each effective constituents, when skin surface, each component can be made to embody moisturizing, U.S. in skin surface White and wrinkle resistant effect.

More preferably: described preservative is DMDM Hydantoin, iodine propilolic alcohol butyl mephenesin Carbamate, methyl-isothiazol Quinoline ketone and the compound of butanediol, the parts by weight of described DMDM Hydantoin are 0.02-0.08 part；Described iodine propilolic alcohol butyl The parts by weight of mephenesin Carbamate are 0.03-0.1 part；The parts by weight of described Methylisothiazolinone are 0.04-0.09 part, described Butanediol is 0.01-0.23 part.

DMDM Hydantoin, iodine propilolic alcohol butyl mephenesin Carbamate, Methylisothiazolinone dissolve in butanediol, compounding shape Becoming preservative, this preservative has extensive drug effect to multiple-microorganism in nature, and can be with plant extract species in the application Produce and combine, make stable system, prevent plant extract species from occurring putrid and deteriorated, and to human non-toxic's evil, gentleness does not stimulates.This Outward, the compounding preservative obtained is cheap, contributes to reducing production cost.

More preferably: in described facial film, also include essence, described essence is daily use chemicals essence, the weight of described essence Number is 0.02-0.1 part.

Daily use chemicals essence makes the application have pleasant fragrance, and user, during using the application, makes body and mind loosen, Contribute to each effective ingredient to be absorbed, and different users's demand to diverse fragrant flavour can be met.

More preferably: described plant extract is obtained by following preparation method:

Rinse and sterilizing: weigh appropriate raw material, rinse with 1-2 times amount water, remove flushing liquor, carry out infrared sterilization treatment；

Filter for the first time: add 12-16 times amount water, be heated to 90-100 DEG C, decoct and extract 0.5-1.5 hour, four layers of filtered through gauze；

Second time filters: the filtering residue after filtering for the first time is added 10-12 times amount water again, is heated to 90-100 DEG C, extracts 0.5- 1.5 hours, four layers of filtered through gauze；

Third time filters: the filtering residue after second time filters is added 8-10 times amount water again, is heated to 90-100 DEG C, extracts 0.5- 1.5 hours, four layers of filtered through gauze；

Concentrating: remove filtering residue, merge the filtrate filtered first, second, and third time, be warming up to backflow, distillation obtains extract；

Purify: extract is crossed chromatographic column, obtains the plant extract of purity >=99wt%.

By plant material by flushing, sterilizing, multiple times of filtration, concentrate and purify after, planting of purity >=99wt% can be obtained Thing extract.The solvent filtering employing in the application is water, does not destroy the natural component in plant material, and through multiple times of filtration, In plant material, active substance is fully dissolved out, and can be effectively improved purity, and the plant extract obtained is water solublity, contributes to skin Skin absorbs.

The purpose of the present invention two is to provide the preparation method of a kind of facial film, makes each effective ingredient in facial film be sufficiently mixed also Form combined effect, make facial film have moisturizing, whitening, crease-resistant and effect of reparation damaged skin.

For achieving the above object two, the technical scheme is that the preparation method of a kind of facial film, including following Step:

Step one: 0.1-0.35 part xanthan gum, 0.01-0.1 part hyaluronate sodium are mixed with 82-88 part water, is warming up to 75-85 DEG C and be incubated 20-40min, after cool to 20-45 DEG C；

Step 2: by abundant to 0.5-1.6 part Fructus Hordei Germinatus oligose glucoside, 0.2-1.2 part hydrogenated starch hydrolysate, 0.4-1.2 part water Mixing, prepares wetting agent；

Step 3: by 0.02-0.08 part DMDM Hydantoin, 0.03-0.1 part iodine propilolic alcohol butyl mephenesin Carbamate, 0.04-0.09 Part Methylisothiazolinone and 0.01-0.23 part butanediol are sufficiently mixed, and prepare preservative；

Step 4: in the mixture that step one is cooled add 2-5 part butanediol, 1.5-3.5 part methyl gluceth- 20,1-4 part glycerol, 2.3-3 part plant extract species, 0.2-0.5 part amino acids, 0.8-2.2 part nicotiamide, 0.02-0.06 Part EDETATE SODIUM, 0.04-0.2 part carnosine, 0.06-0.16 part pantothenylol, the wetting agent of step 2 acquisition and step 3 obtain Preservative mix homogeneously；

Step 5: by 0.1-0.8 part Cremophor RH40,0.005-0.015 part tocopherol acetas, 0.01-0.1 part profit Skin agent is sufficiently mixed；

Step 6: step 4 is sufficiently mixed through the mixture of acquisition and the mixture of step 5 acquisition, pick test, filters out Material, prepares.

The application uses the method for distributed rendering to be prepared.Xanthan gum and hyaluronate sodium is made to fill by a liter gentle insulation Divide soluble in water, by similar compatibility principle, be sufficiently formed the colloidal state of stable homogeneous；In advance wetting agent and preservative are divided Do not compound so that Fructus Hordei Germinatus oligose glucoside and hydrogenated starch hydrolysate in wetting agent form stable carrying structure, make Preservative stably and to human non-toxic's evil is well-dispersed in the application, mixes with other compositions, former by similar compatibility Reason, is connected with other compositions.Cremophor RH40 and emollient similar compatibility, make both preferably with tocopherol acetas Molten it is integrated；In use, in the application, each composition is dispersed in skin surface, embody moisturizing, whitening, wrinkle resistant and Repair the effect of damaged skin.More preferably: described step 6 has been also added with essence.

The final stage relatively low in temperature adds essence, can be effectively retained the perfume ingredient in the application.

In sum, the method have the advantages that

1, EDETATE SODIUM, xanthan gum, hyaluronate sodium, tocopherol acetas and the unsaturated fatty acids of plant extract apoplexy due to endogenous wind The compositions such as acid, vitamin be combined with each other, and form layer protecting film at skin surface, stop that heavy metal and ultraviolet etc. are to skin Infringement, reaches moisturizing, whitening, the wrinkle resistant and effect of reparation damaged skin.

2, butanediol, glycerol produce compounding effect with amino acids material, promote that amino acids material is absorbed by the skin, make Skin more moistening effect.

3, the aminoacid in pantothenylol, nicotiamide, carnosine is the most affine with the bioflavonoids of plant extract apoplexy due to endogenous wind, at angle Matter confluent monolayer cells surface forms protective barrier, removes free radical, prevents cell senescence；Expansion blood vessel also promotes other compositions quickly quilt Skin absorption, suppression melanosome is transferred to keratinocyte from pigment cell, is reduced facial pigmentation deposition, regulate mucopolysaccharide Content, reduce wrinkle, play tender white, crease-resistant effect.

4, hyaluronate sodium is the most affine with phospholipid molecule in Oleum Hippophae, promotes the skin absorption to phospholipid molecule, from And make up the phospholipid of disappearance in the cell membrane of corneocyte, make corneocyte film have preferably opposing free radical harm Ability, makes skin quickly absorb the nutrient substance in the application, keep skin moisturizing and tender in vain, reduce wrinkle and produce, and reach Repair the effect of damaged skin.

Detailed description of the invention

Below in conjunction with embodiment, describe the present invention.

Composition and the consumption of embodiment 1-10 are as shown in table 1.

The component of table 1 embodiment 1-10 and parts by weight

The extracting method of plant extract species in embodiment 1-10:

Rinse and sterilizing: weigh appropriate raw material, rinse with 1-2 times amount water, remove flushing liquor, carry out infrared sterilization treatment；

Filter for the first time: add 12-16 times amount water, be heated to 90-100 DEG C, decoct and extract 0.5-1.5 hour, four layers of filtered through gauze；

Second time filters: the filtering residue after filtering for the first time is added 10-12 times amount water again, is heated to 90-100 DEG C, extracts 0.5- 1.5 hours, four layers of filtered through gauze；

Third time filters: the filtering residue after second time filters is added 8-10 times amount water again, is heated to 90-100 DEG C, extracts 0.5- 1.5 hours, four layers of filtered through gauze；

Concentrating: remove filtering residue, merge the filtrate filtered first, second, and third time, be warming up to backflow, distillation obtains extract；

Purify: extract is crossed chromatographic column, obtains the plant extract of purity >=99wt%.

The preparation method of embodiment 1:

Step one: the corresponding xanthan gum of parts by weight, hyaluronate sodium are mixed with water, is warming up to 75-85 DEG C and is incubated 20- 40min, after cool to 20-45 DEG C；

Step 2: the corresponding Fructus Hordei Germinatus oligose glucoside of parts by weight, hydrogenated starch hydrolysate, water are sufficiently mixed, prepare moisturizing Agent；

Step 3: by the corresponding DMDM Hydantoin of parts by weight, iodine propilolic alcohol butyl mephenesin Carbamate, Methylisothiazolinone and Butanediol is sufficiently mixed, and prepares preservative；

Step 4: add in the mixture that step one is cooled the corresponding butanediol of parts by weight, methyl gluceth- 20, glycerol, plant extract species, amino acids, nicotiamide, EDETATE SODIUM, carnosine, pantothenylol, step 2 obtain wetting agent with And the preservative mix homogeneously that step 3 obtains；

Step 5: the corresponding Cremophor RH40 of parts by weight, tocopherol acetas, emollient are sufficiently mixed；

Step 6: step 4 is sufficiently mixed through the mixture of acquisition and the mixture of step 5 acquisition, pick test, filters out Material, prepares.

The preparation method of embodiment 2-10:

On the basis of the preparation method of embodiment 1, add the essence of corresponding parts by weight in step 6, prepare.

Comparative example 1 moistening effect is tested

Test specimen: the sample prepared with embodiment 1,4 and 7 is respectively test sample 1,2 and 3；Group in control sample 1-10 Divide as shown in table 2 with parts by weight.

In control sample, the extracting method of plant extract species is with reference to the extracting method of plant extract species in embodiment 1-10；

The preparation method of control sample 1-9 is with reference to the preparation method of embodiment 2-10；

The preparation method of control sample 10: directly by each component mix homogeneously, prepares.

Test method: choose the same area, be all 30 years old women white collar 520 of Combination skin quality, be divided into 13 groups, Often group 40.The sample that test sample 1-3 and control sample 1-10 obtain is used and fully soaks with money non-woven fabrics face paper, divide afterwards Do not give 1-13 group experimenter to use.Before using, every experimenter all uses same procedure to carry out facial cleansing, and uses RUNVE shellfish think the moisture of buccal skin is detected by HL611 skin test device, record data.1-3 group experimenter divides Shi Yong not test the facial film that sample 1-3 obtains, 4-13 group experimenter uses the facial film that control sample 1-10 obtains respectively.520 tested Person's face mask film is 20min often, sits quietly in same room with them after using facial film, and room temperature is 20 DEG C-25 DEG C, and relative humidity is 40%-60%.After face mask film terminates when 1h, 4h, 7h and 10h, every experimenter all uses RUNVE shellfish to think to obtain HL611 skin Buccal skin is tested by skin tester, records moisture, and the data before and after often group experimenter's facial film uses are passed through respectively Average treatment, analysis.

The instrument that process of the test uses: RUNVE shellfish thinks to obtain HL611 skin test device.

Result of the test: before and after 1-13 group experimenter's application facial film, skin moisture content situation of change is as shown in table 3.By table 3 Understanding, before face mask film, the mean difference of the skin moisture content often organizing experimenter is less；The often group corresponding facial film of experimenter's application After 1h, 4h, 7h and 10h survey skin moisture content change the most obvious.Use in the 1-3 group experimenter of test sample, 10h Inner skin moisture content change is less, illustrates that testing sample 1-3 has preferable moisturizing and skin moistening effect；Use the 1-10 of control sample Group experimenter, 1-h inner skin moisture content change is relatively big, illustrates to increase over time, and application facial film adds to the battalion in skin Moisture cannot be pinned by foster material so that moisture loss in skin, it is impossible to reaches good moistening effect.Produce the former of this phenomenon Because: facial film component lacks one or more in hyaluronate sodium, Oleum Hippophae, amino acids, butanediol, glycerol, or The above component of person is not up to area requirement.

The component of table 2 control sample 1-10 and parts by weight

Skin moisture content situation of change before and after table 3 1-13 group experimenter's application facial film

Comparative example 2 whitening skin and preserving moisture repairing test

Test specimen: respectively test sample with the sample that embodiment 7 prepares；Component in control sample 1-3 and weight portion thereof Number is as shown in table 4.

Test method: choose the same area, be all Combination skin quality and have pox to print 18-35 year women white collar 400, flat It is divided into 4 groups, numbering A group, B group, C group and D group.The sample that test sample and control sample 1-3 obtain is used with money non-woven fabrics Face paper fully soaks, after give respectively A-D group experimenter use.Every experimenter uses phase with week-night 8:00 on every Wendesdays With application facial film 20min after face cleaning mode, continue 12 months, relative analysis skin conditions.

Result of the test: in A group, the pox print of 96% experimenter's face substantially desalinates the even disappearance of part pox print, skin moisturizing； In B-D group, the pox print desalination of only 15% experimenter's face, skin moisturizing degree is slightly better than the year before.Produce the reason of this result Predominantly: the facial film that control sample prepares lacks EDETATE SODIUM, xanthan gum, hyaluronate sodium, tocopheryl acetate sodium, plant extract One or more in species, or above component is not up to area requirement.

The component of table 4 control sample 1-3 and parts by weight thereof

Comparative example 3 whitening anti-wrinkling effect test

Test specimen: respectively test sample with the sample that embodiment 10 prepares；The component of control sample 1-3 and parts by weight thereof As shown in table 5.

In control sample, the extracting method of plant extract species is with reference to the extracting method of plant extract species in embodiment 1-10；

The preparation method of control sample 1-3 is with reference to the preparation method of embodiment 2-10；

Test method: choose the same area, 50 years old women 400 that skin aging degree is similar, is equally divided into 4 groups, numbered A Group, B group, C group and D group.The sample that test sample and control sample 1-3 obtain is used and fully soaks with money non-woven fabrics face paper, Rear give respectively A-D group experimenter use.Every experimenter uses with week-night 8:00 on every Wendesdays and applies after identical face cleaning mode Use facial film 20min, continue 12 months, relative analysis skin conditions.

Result of the test: in A group, the skin of 100% experimenter is improved, wherein, 98% experimenter's facial wrinkles is bright Showing thin out even to disappear, skin becomes delicate and moistens, high resilience；In B-D group, only the facial wrinkles of 20% experimenter is slightly Thin out, skin condition with do not use before slightly take a turn for the better but change inconspicuous.Produce the reason of this phenomenon predominantly: control sample prepares Facial film in lack one or more in pantothenylol, nicotiamide, carnosine, or above component is not up to area requirement.

The component of table 5 control sample 1-3 and parts by weight thereof

The above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-mentioned enforcement Example, all technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that, for the art Those of ordinary skill for, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications are also Should be regarded as protection scope of the present invention.

Claims (10)

1. a facial film, it is characterised in that include the component of following parts by weight:

Water 82-88 part；

Xanthan gum 0.1-0.35 part；

Hyaluronate sodium 0.01-0.1 part；

Butanediol 2-5 part；

Methyl gluceth-20 is 1.5-3.5 part；

Glycerol 1-4 part；

Nicotiamide 0.8-2.2 part；

EDTA disodium 0.02-0.06 part；

Carnosine 0.04-0.2 part；

Pantothenylol 0.06-0.16 part；

Skin conditioning agent 2.5-3.5 part；

Wetting agent 1-4 part；

Preservative 0.1-0.5 part；

Cremophor RH40 0.1-0.8 part；

Tocopherol acetas 0.005-0.015 part；

Emollient 0.01-0.1 part；

Described skin conditioning agent includes that plant extract species and amino acids, the parts by weight of described plant extract species are 2.3- 3 parts, the parts by weight of described amino acids are 0.2-0.5 part.

A kind of facial film the most according to claim 1, it is characterised in that described emollient is preferably Oleum Hippophae.

A kind of facial film the most according to claim 1, it is characterised in that described plant extract species selects Aloe Barbadensis Miller In extract, Radix Et Caulis Acanthopanacis Senticosi extract, Radix Puerariae extract, yellow tang extract, Hamamelis virginiana extract, Stigma Croci extract One or more.

A kind of facial film the most according to claim 1, it is characterised in that described amino acids chooses serine, arginine, sweet One or more in propylhomoserin.

A kind of facial film the most according to claim 1, it is characterised in that described wetting agent is Fructus Hordei Germinatus oligose glucoside, hydrogenation Glucidtemns and the compound of water；Described Fructus Hordei Germinatus oligose glucoside 0.5-1.6 part, described hydrogenated starch hydrolysate 0.2-1.2 Part, described water is 0.4-1.2 part.

A kind of facial film the most according to claim 1, it is characterised in that described preservative is DMDM Hydantoin, iodine propine Alcohol butyl mephenesin Carbamate, Methylisothiazolinone and the compound of butanediol, the parts by weight of described DMDM Hydantoin are 0.02-0.08 part；The parts by weight of described iodine propilolic alcohol butyl mephenesin Carbamate are 0.03-0.1 part；Described Methylisothiazolinone Parts by weight be 0.04-0.09 part, described butanediol is 0.01-0.23 part.

A kind of facial film the most according to claim 1, it is characterised in that also including essence in described facial film, described essence is Daily use chemicals essence, the parts by weight of described essence are 0.02-0.1 part.

A kind of facial film the most according to claim 1, it is characterised in that described plant extract is obtained by following preparation method :

Rinse and sterilizing: weigh appropriate raw material, rinse with 1-2 times amount water, remove flushing liquor, carry out infrared sterilization treatment；

Filter for the first time: add 12-16 times amount water, be heated to 90-100 DEG C, decoct and extract 0.5-1.5 hour, four layers of filtered through gauze；

Second time filters: the filtering residue after filtering for the first time is added 10-12 times amount water again, is heated to 90-100 DEG C, extracts 0.5- 1.5 hours, four layers of filtered through gauze；

Third time filters: the filtering residue after second time filters is added 8-10 times amount water again, is heated to 90-100 DEG C, extracts 0.5-1.5 hour, four layers of filtered through gauze；

Concentrating: remove filtering residue, merge the filtrate filtered first, second, and third time, be warming up to backflow, distillation obtains extract；

Purify: extract is crossed chromatographic column, obtains the plant extract of purity >=99wt%.

9. the preparation method of a kind of facial film as described in claim 1-8 any one, it is characterised in that include following step Rapid:

Step one: 0.1-0.35 part xanthan gum, 0.01-0.1 part hyaluronate sodium are mixed with 82-88 part water, is warming up to 75-85 DEG C and be incubated 20-40min, after cool to 20-45 DEG C；

Step 2: by abundant to 0.5-1.6 part Fructus Hordei Germinatus oligose glucoside, 0.2-1.2 part hydrogenated starch hydrolysate, 0.4-1.2 part water Mixing, prepares wetting agent；

Step 3: by 0.02-0.08 part DMDM Hydantoin, 0.03-0.1 part iodine propilolic alcohol butyl mephenesin Carbamate, 0.04-0.09 Part Methylisothiazolinone and 0.01-0.23 part butanediol are sufficiently mixed, and prepare preservative；

Step 4: in the mixture that step one is cooled add 2-5 part butanediol, 1.5-3.5 part methyl gluceth- 20,1-4 part glycerol, 2.3-3 part plant extract species, 0.2-0.5 part amino acids, 0.8-2.2 part nicotiamide, 0.02-0.06 Part EDETATE SODIUM, 0.04-0.2 part carnosine, 0.06-0.16 part pantothenylol, the wetting agent of step 2 acquisition and step 3 obtain Preservative mix homogeneously；

Step 5: by 0.1-0.8 part Cremophor RH40,0.005-0.015 part tocopherol acetas, 0.01-0.1 part profit Skin agent is sufficiently mixed；

Step 6: step 4 is sufficiently mixed through the mixture of acquisition and the mixture of step 5 acquisition, pick test, filters out Material, prepares.

The preparation method of a kind of facial film the most according to claim 9, it is characterised in that be also added with in described step 6 Essence.