CN104206561B - A kind of preparation technology of peony seed oil microcapsule powder - Google Patents
A kind of preparation technology of peony seed oil microcapsule powder Download PDFInfo
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- CN104206561B CN104206561B CN201410462696.XA CN201410462696A CN104206561B CN 104206561 B CN104206561 B CN 104206561B CN 201410462696 A CN201410462696 A CN 201410462696A CN 104206561 B CN104206561 B CN 104206561B
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Abstract
The invention discloses the preparation technology of a kind of peony seed oil microcapsule powder, it is characterised in that in turn include the following steps: (1) dissolves wall material and emulsifying agent with warm water；(2) to dissolve after wall material and emulsifying agent in add peony seed oil, mixing and stirring；(3) mixed solution obtained in step (2) is carried out high pressure homogenize process, obtain the solution that emulsified state is good；(4) solution obtaining step (3) is spray-dried, and obtains peony seed oil microcapsule powder；Described wall material is sodium caseinate, starch sodium octenyl succinate, gelatin, arabic gum, the mixture of one or more in maltose syrup；Described emulsifying agent is single diglycerine fatty acid ester, sodium stearoyl lactate, the mixture of one or more in diacetyl tartarate monoglyceride.The peony seed oil embedding rate of this technique is high, fat content is high, and technological process is the most efficient, it is simple to large-scale production and application.
Description
Technical field
The present invention relates to food processing field, the preparation technology of a kind of peony seed oil microcapsule powder.
Background technology
The vegetable oil extracted by seed of Flos Moutan is the distinctive woody macadamia nut oil of China, nutritious and unique because of it,
Having again medical care effect, being referred to as " the most best oil, " by relevant expert is the treasure in vegetable oil,
Also it is Chinese exclusive health care edible oil and fat, obtains new resource food approval in March, 2011.
Peony seed oil unsaturated fatty acid content reaches more than 90%, and wherein polyunsaturated fatty acid is sub-
Fiber crops acid content, more than 40%, is 140 times of olive oil.Remaining many index is the most all higher than other oil and plants, again
It is difficult to oxide deposition at positions such as human vas wall, heart coronary arteries.These compositions make it in medical science and battalion
Play important function on Yanging and become preferable edible oil.
Microcapsule technology refer to naturally occurring or synthetic macromolecular material by solid, liquid, gas even they
Mixture embeds, and forms semipermeable membrane or the technology of closing membrane.The material that inside is wrapped by is referred to as core, outer layer
Film is then referred to as wall material, and the microcapsule granule particle diameter that embedding is formed is 1～1000 μm.Can change owing to having
Become the state of material, quality, volume and performance, protect sensitive composition, enhanced stability, control core and release
Put, reduce or cover disagreeable taste and reduce volatility, the isolation function such as component, microcapsule technology food,
The aspects such as medicine, weaving, coating, agricultural, cosmetics industry are widely used.
Patent now for peony seed oil is less, and majority concentrates on making oil with common edible, to Paeonia suffruticosa
It is rarer that seed oil carries out microcapsule embedded technology report, and only a small amount of patent has deeply adding peony seed oil
Work processes.The preparation technology of a kind of water solublity peony seed oil powder body as disclosed in CN103609751A, this
Bright core wall material is than for 1:5, and fat content is relatively low, embedding rate relatively low (application example embedding rate is 90.2%).
Microcapsule peony seed oil preparation technology as disclosed in CN103948035A, its preparation technology mainly have employed ferment
Female microcapsule method and rich cohesion microcapsule method, both approaches has technics comparing complicated, relatively low weak of production capacity
Point, unsuitable large-scale popularization, the most above-mentioned technique is the most inconspicuous to the prompting of peony seed oil embedding rate.
Summary of the invention
For above-mentioned the deficiencies in the prior art, the invention provides a kind of peony seed oil microcapsule powder
Preparation technology.The peony seed oil embedding rate of this technique is high, fat content is high, and technological process is succinctly efficient,
It is easy to large-scale production and application.
The preparation technology of a kind of peony seed oil microcapsule powder that the present invention provides, in turn includes the following steps:
(1) wall material and emulsifying agent are dissolved with 60-80 DEG C of warm water；
(2) to dissolve after wall material and emulsifying agent in add peony seed oil, mixing and stirring；
(3) mixed solution obtained in step (2) is carried out high pressure homogenize process, obtain emulsified state
Good solution；
(4) solution obtaining step (3) is spray-dried, and obtains peony seed oil microcapsule powder；
Described wall material is sodium caseinate, starch sodium octenyl succinate, gelatin, arabic gum, Fructus Hordei Germinatus
The mixture of one or more in syrup；
Described emulsifying agent is single diglycerine fatty acid ester, sodium stearoyl lactate, diacetyl tartarate monoglyceride
In the mixture of one or more.
Described peony seed oil, wall material, emulsifying agent shared mass percent in peony seed oil microcapsule powder depends on
Secondary it is: peony seed oil 5-70%, wall material 25-93%, emulsifying agent 2-5%.
Described wall material is the mixture of sodium caseinate, starch sodium octenyl succinate and maltose syrup, three
The weight ratio of person is sodium caseinate: starch sodium octenyl succinate: maltose syrup=(1-4): (3-12):
(12-87)。
Preferably, the weight ratio of described sodium caseinate, starch sodium octenyl succinate and maltose syrup is
Sodium caseinate: starch sodium octenyl succinate: maltose syrup=(1-2): (3-12): (44-87)..
Described emulsifying agent is that single diglycerine fatty acid ester, sodium stearoyl lactate and diacetyl tartarate list are double sweet
The mixture of grease, the mass ratio of three is single diglycerine fatty acid ester: sodium stearoyl lactate: biacetyl
Tartaric acid list double glyceride=2:1:(0-1)～10:1:(0-1).
Preferably, described emulsifying agent is single diglycerine fatty acid ester and the mixture of sodium stearoyl lactate, two
The mass ratio of person is single diglycerine fatty acid ester: sodium stearoyl lactate=2:1～4:1.
The pressure that high pressure homogenize in described step (3) processes is divided into the two-stage, first order pressure to be
10-30MPa, preferably 15-20MPa, second level pressure is 5-10MPa, preferably 5-6MPa, all
Matter number of times 1-5 time.
In the drying process with atomizing of described step (4), inlet temperature is 110-170 DEG C, preferably 120 DEG C
-150 DEG C, leaving air temp is 60-90 DEG C, preferably 65 DEG C-75 DEG C.
The preparation technology of peony seed oil microcapsule powder that the present invention provides, by temperature in production process,
The technological parameters such as pressure strict control and wall material and the scientific and reasonable compatibility of emulsifier component and join
Ratio so that the embedding rate of peony seed oil is reached more than 95%, effectively prevents the unsaturation in peony seed oil
Fatty acid contacts with the oxygen in air and oxidized, loses or reduces its peculiar effect；Embedding oils and fats is total
Amount also can select in the range of 5%-70% according to actual production demand.Additionally, obtained peony seed oil
Microcapsule powder also has good instant capacity and stability so that it is application is no longer limited to oil with common edible fat,
Solid beverage based food can also be applied to, bake based food etc..
Detailed description of the invention
In order to make those skilled in the art be more fully understood that technical scheme, below in conjunction with specifically
The present invention is described in further detail for embodiment.
Embodiment 1
Prepare peony seed oil microcapsule powder (microcapsule powder is in terms of 100g) the most as follows:
(1) 60 DEG C of warm water dissolves wall material, emulsifying agent；Wherein, wall material is sodium caseinate 2g, octenyl
The mixture of succinic acid starch sodium 12g, maltose syrup 44g (calculating with solid content), emulsifier is
2g, wherein single diglycerine fatty acid ester is 1.5g, and sodium stearoyl lactate is 0.5g.
(2) to dissolve after wall material and emulsifying agent in add peony seed oil 40g be stirred mixing, until
Obtain the solution of stable homogeneous system；
(3) step (2) gained solution being carried out high pressure homogenize process, first order pressure is 20MPa,
Second level pressure 5MPa, homogenization cycles 2 times, obtain the solution that emulsified state is good；
(4) solution is spray-dried, wherein inlet temperature 140 DEG C, leaving air temp 70 DEG C, obtains
Peony seed oil microcapsule powder in good condition；
Embodiment 2
Prepare seed of Flos Moutan oil meal (microcapsule powder is in terms of 100g) the most as follows:
(1) 80 DEG C of warm water dissolves wall material, emulsifying agent；Wherein, wall material is sodium caseinate 4g, octenyl
The mixture of succinic acid starch sodium 10g, maltose syrup 12g (calculating with solid content), emulsifier is
4g, component and weight proportion in emulsifying agent be: single diglycerine fatty acid ester: sodium stearoyl lactate: double second
Acyl tartaric acid list double glyceride=2:1:0.5；
(2) wall material and emulsifying agent after dissolving add peony seed oil 70g and are stirred mixing；Until
Solution to stable homogeneous system；
(3) solution carrying out high pressure homogenize process, first order pressure is 20MPa, second level pressure 5MPa,
Homogenization cycles 2 times, obtains the solution that emulsified state is good；
(4) solution is spray-dried, wherein inlet temperature 140 DEG C, leaving air temp 70 DEG C, obtains
Peony seed oil microcapsule powder in good condition；
Embodiment 3
Prepare seed of Flos Moutan oil meal (microcapsule powder is in terms of 100g) the most as follows:
(1) 70 DEG C of warm water dissolves wall material, emulsifying agent；Wherein, wall material is sodium caseinate 1g, octenyl
The mixture of succinic acid starch sodium 3g, maltose syrup 87g (calculating with solid content), emulsifier is
1g, wherein, single diglycerine fatty acid ester is 0.8g, and sodium stearoyl lactate is 0.2g；
(2) in the wall material dissolved and emulsifying agent, add peony seed oil 8g and be stirred mixing；Until obtaining
The solution of stable homogeneous system；
(3) solution carrying out high pressure homogenize process, first order pressure is 20MPa, second level pressure 5MPa,
Homogenization cycles 2 times, obtains the solution that emulsified state is good；
(4) solution is spray-dried, wherein inlet temperature 140 DEG C, leaving air temp 70 DEG C, obtains
Peony seed oil microcapsule powder in good condition.
Test example 1
The embedding rate of the seed of Flos Moutan oil meal preparing embodiment 1-3 is tested, and result is as follows:
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Embedding rate (%) | 97.8 | 95.1 | 99.2 |
Test example 2
The instant capacity of the seed of Flos Moutan oil meal preparing the present invention is evaluated: method is as follows: with the water of 80 DEG C
Seed of Flos Moutan oil meal is reconstituted, obtains the seed of Flos Moutan oil meal solution of 10%, with spoon at the uniform velocity agitating solution,
Start to record the time, during until the little granule being visible by naked eyes in solution.Test result is as follows:
| Project | Seed of Flos Moutan oil meal prepared by the present invention |
| Liquid is visible by naked eyes little granule required time (s) | 10s |
As seen from the above table, the seed of Flos Moutan oil meal instant capacity that the present invention provides is good.
Test example 3
The evaluation of seed of Flos Moutan oil meal prepared by the present invention: method is as follows: with the water of 80 DEG C
Seed of Flos Moutan oil meal is reconstituted, obtains the seed of Flos Moutan oil meal solution of 10%, with spoon at the uniform velocity agitating solution,
After solution stirring is uniform, observes surface and the time of oil slick occurs.Test result is as follows:
| Sample | 10% peony seed oil solution-stabilized time (min) |
| Embodiment 1 | ＞ 60 |
| Embodiment 2 | ＞ 45 |
| Embodiment 3 | ＞ 120 |
Above the preparation technology of a kind of peony seed oil microcapsule powder provided by the present invention is carried out in detail
Introduce.Principle and the embodiment of the present invention are set forth by specific case used herein, above
The explanation of embodiment is only intended to help to understand the core concept of the present invention.It should be pointed out that, for this technology
For the those of ordinary skill in field, under the premise without departing from the principles of the invention, it is also possible to the present invention
Carry out some improvement and modification.These improve and modify and should also be as falling into the protection model of the claims in the present invention
In enclosing.
Claims (4)
1. the preparation technology of a peony seed oil microcapsule powder, it is characterised in that in turn include the following steps:
(1) wall material and emulsifying agent are dissolved with warm water；
(2) to dissolve after wall material and emulsifying agent in add peony seed oil, mixing and stirring；
(3) mixed solution obtained in step (2) is carried out high pressure homogenize process, obtain emulsified state good
Good solution；
(4) solution obtaining step (3) is spray-dried, and obtains peony seed oil microcapsule powder；
Described peony seed oil, wall material, emulsifying agent mass percent shared by peony seed oil microcapsule powder is successively
For: peony seed oil 5-70%, wall material 25-93%, emulsifying agent 2-5%；
Described wall material is the mixture of sodium caseinate, starch sodium octenyl succinate and maltose syrup, three
Weight ratio be sodium caseinate: starch sodium octenyl succinate: maltose syrup=(1-4): (3-12):
(12-87)；
Described emulsifying agent is single diglycerine fatty acid ester, sodium stearoyl lactate and diacetyl tartarate list diglycerol
The mixture of ester, the mass ratio of three is single diglycerine fatty acid ester: sodium stearoyl lactate: diacetyl tartaric
Single double glyceride=the 2:1:(0-1 of acid)～10:1:(0-1)；Or described emulsifying agent is single diglycerine fatty acid ester
With the mixture of sodium stearoyl lactate, both mass ratioes are single diglycerine fatty acid ester: sodium stearoyl lactate
=2:1～4:1.
The preparation technology of peony seed oil microcapsule powder the most according to claim 1, it is characterised in that
The weight ratio of described sodium caseinate, starch sodium octenyl succinate and maltose syrup is sodium caseinate: pungent
Starch alkenyl succinate sodium: maltose syrup=(1-2): (3-12): (44-87).
The preparation technology of peony seed oil microcapsule powder the most according to claim 1, it is characterised in that
The pressure that high pressure homogenize in described step (3) processes is divided into two-stage, first order pressure to be 10-30MPa,
Second level pressure is 5-10MPa, homogenization cycles 1-5 time.
The preparation technology of peony seed oil microcapsule powder the most according to claim 1, it is characterised in that
In the drying process with atomizing of described step (4), inlet temperature is 110-170 DEG C, and leaving air temp is 60-90 DEG C.
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| CN104920642B (en) * | 2015-07-03 | 2017-12-12 | 山东省分析测试中心 | Food-grade peony seeds mediation oil Microemulsions For Use and preparation method thereof |
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| CN103564065B (en) * | 2013-10-30 | 2014-12-17 | 广州绿萃生物科技有限公司 | Preparation method of purple perilla seed oil microcapsule |
| CN103609751A (en) * | 2013-12-02 | 2014-03-05 | 东北林业大学 | Preparation process of water-soluble peony seed oil powder |
| CN103948035B (en) * | 2014-05-05 | 2016-09-07 | 李�杰 | A kind of preparation method of peony seed oil microcapsule |
| CN104000196B (en) * | 2014-06-04 | 2016-03-16 | 李�杰 | Compound tree peony seed oil formulation and preparation method and application |
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Denomination of invention: Preparation of peony seed oil microcapsule powder Effective date of registration: 20220610 Granted publication date: 20160817 Pledgee: Haidian Beijing science and technology enterprise financing Company limited by guarantee Pledgor: BEIJING ALCHEMIST TECHNOLOGY CO.,LTD. Registration number: Y2022110000120 |