CN104206561A - Preparation process of peony seed oil micro-capsule powder - Google Patents
Preparation process of peony seed oil micro-capsule powder Download PDFInfo
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- CN104206561A CN104206561A CN201410462696.XA CN201410462696A CN104206561A CN 104206561 A CN104206561 A CN 104206561A CN 201410462696 A CN201410462696 A CN 201410462696A CN 104206561 A CN104206561 A CN 104206561A
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Abstract
The invention discloses a preparation process of peony seed oil micro-capsule powder. The preparation process is characterized by sequentially comprising the following steps: (1) dissolving a wall material and an emulsifying agent by using warm water; (2) adding peony seed oil into the dissolved wall material and emulsifying agent, and uniformly mixing and stirring to obtain a mixed solution; (3) homogenizing the mixed solution obtained in the step (2) under high pressure to obtain a solution in a good emulsification state; and (4) spray-drying the solution obtained in the step (3) to obtain the peony seed oil micro-capsule powder, wherein the wall material is one or a mixture of more of sodium caseinate, starch sodium octenylsuccinate, gelatin, arabic gum and malt syrup, and the emulsifying agent is one or a mixture of more of mono-and diglycerides of fatty acids, sodium stearyl lactate and diacetyl monostearin tartrate. The peony seed oil micro-capsule powder prepared by virtue of the process is high in peony seed oil embedding rate and high in grease content; the process flow is simple and efficient, and facilitates large-scale production and application.
Description
Technical field
The present invention relates to food processing field, particularly a kind of preparation technology of peony seed oil microcapsule powder.
Background technology
The vegetable oil extracted by peony seeds is the distinctive woody macadamia nut oil of China, nutritious and unique because of it, there is medical care effect again, by relevant expert is called " oil best in the world; " it is the treasure in vegetable oil, also be Chinese exclusive health care edible oil and fat, obtain new resource food approval in March, 2011.
Peony seed oil unsaturated fatty acid content reaches more than 90%, and especially wherein polyunsaturated fatty acid-linolenic acid content is more than 40%, is 140 times of olive oil.All the other many indexs also all higher than other oil plant, again not easily oxide deposition at positions such as human vas wall, heart coronary arteries.These compositions make it in medical science and nutrition, play important function and become desirable edible oil.
Microcapsules technology to refer to natural or synthesized polymer material, by even their the mixture embedding of solid, liquid, gas, form the technology of pellicle or closing membrane.The material that inside is wrapped by is called core, and outer membrane is then called wall material, and the microcapsule granule particle diameter that embedding is formed is 1 ~ 1000 μm.Owing to having state, quality, volume and the performance that can change material; protection sensitive composition; strengthen stability; control Release of core material; reduce or cover disagreeable taste and reduce volatility; the functions such as isolation component, microcapsules technology is widely used in food, medicine, weaving, coating, agricultural, cosmetics industry etc.
Now less for the patent of peony seed oil, majority concentrates on and makes on oil with common edible, carries out microcapsule embedded technology report rarer to peony seed oil, only has a small amount of patent to have deep processing process to peony seed oil.A kind of preparation technology of water-soluble peony seed oil powder disclosed in CN103609751A, this invention core wall material is than being 1:5, and fat content is lower, embedding rate lower (application example embedding rate is 90.2%).Microcapsules peony seed oil preparation technology disclosed in CN103948035A, its preparation technology mainly have employed yeast microcapsule method and rich cohesion microcapsule method, these two kinds of methods have technics comparing complicated, the weakness that production capacity is lower, unsuitable large-scale popularization, above-mentioned technique is also not obvious to the prompting of peony seed oil embedding rate in addition.
Summary of the invention
For above-mentioned the deficiencies in the prior art, the invention provides a kind of preparation technology of peony seed oil microcapsule powder.The peony seed oil embedding rate of this technique is high, fat content is high, and technological process is succinctly efficient, is convenient to large-scale production and application.
The preparation technology of a kind of peony seed oil microcapsule powder provided by the invention, in turn includes the following steps:
(1) wall material and emulsifying agent is dissolved with 60-80 DEG C of warm water;
(2) in the wall material after dissolving and emulsifying agent, peony seed oil is added, mixing and stirring;
(3) high-pressure homogeneous process is carried out to the mixed solution obtained in step (2), obtain the solution that emulsified state is good;
(4) spraying dry is carried out to the solution that step (3) obtains, obtain peony seed oil microcapsule powder;
Described wall material is casein sodium, starch Sodium Octenyl Succinate, gelatin, Arabic gum, the mixture of one or more in malt syrup;
Described emulsifying agent is single diglycerine fatty acid ester, stearoyl lactate, the mixture of one or more in diacetyl tartarate monoglyceride.
Described peony seed oil, wall material, emulsifying agent shared mass percent in peony seed oil microcapsule powder is followed successively by: peony seed oil 5-70%, wall material 25-93%, emulsifying agent 2-5%.
Described wall material is the mixture of casein sodium, starch Sodium Octenyl Succinate and malt syrup, and the weight ratio of three is casein sodium: starch Sodium Octenyl Succinate: malt syrup=(1-4): (3-12): (12-87).
Preferably, the weight ratio of described casein sodium, starch Sodium Octenyl Succinate and malt syrup is casein sodium: starch Sodium Octenyl Succinate: malt syrup=(1-2): (3-12): (44-87).。
Described emulsifying agent is single diglycerine fatty acid ester, the mixture of stearoyl lactate and diacetyl tartarate list double glyceride, the mass ratio of three is single diglycerine fatty acid ester: stearoyl lactate: diacetyl tartarate list double glyceride=2:1:(0-1) ~ 10:1:(0-1).
Preferably, described emulsifying agent is the mixture of single diglycerine fatty acid ester and stearoyl lactate, and both mass ratioes are single diglycerine fatty acid ester: stearoyl lactate=2:1 ~ 4:1.
The pressure of the high-pressure homogeneous process in described step (3) is divided into two-stage, and first order pressure is 10-30MPa, and be preferably 15-20MPa, second level pressure is 5-10MPa, is preferably 5-6MPa, homogenization cycles 1-5 time.
In the drying process with atomizing of described step (4), EAT is 110-170 DEG C, and be preferably 120 DEG C-150 DEG C, leaving air temp is 60-90 DEG C, is preferably 65 DEG C-75 DEG C.
The preparation technology of peony seed oil microcapsule powder provided by the invention, by to the technological parameter such as temperature, pressure in production process strict control and wall material and the scientific and reasonable compatibility of emulsifier component and proportioning, make to reach more than 95% to the embedding rate of peony seed oil, effectively prevent the unrighted acid in peony seed oil from contacting with the oxygen in air and oxidized, lose or reduce its peculiar effect; Embedding grease total amount also can be selected within the scope of 5%-70% according to actual production demand.In addition, the peony seed oil microcapsule powder obtained also has good instant capacity and stability, makes it apply and is no longer confined to oil with common edible fat, can also be applied to solid beverage based food, bake based food etc.
Detailed description of the invention
In order to make those skilled in the art person understand technical scheme of the present invention better, below in conjunction with detailed description of the invention, the present invention is described in further detail.
Embodiment 1
Prepare peony seed oil microcapsule powder (microcapsule powder is in 100g) successively as follows:
(1) 60 DEG C of warm water dissolves wall material, emulsifying agent; Wherein, wall material is casein sodium 2g, starch Sodium Octenyl Succinate 12g, the mixture of malt syrup 44g (calculating with solid content), and emulsifier is 2g, and wherein single diglycerine fatty acid ester is 1.5g, and stearoyl lactate is 0.5g.
(2) in the wall material after dissolving and emulsifying agent, add peony seed oil 40g to be uniformly mixed, until obtain the solution of stable homogeneous system;
(3) carry out high-pressure homogeneous process to step (2) gained solution, first order pressure is 20MPa, second level pressure 5MPa, and homogenization cycles 2 times, obtains the solution that emulsified state is good;
(4) spraying dry is carried out to solution, wherein EAT 140 DEG C, leaving air temp 70 DEG C, obtain peony seed oil microcapsule powder in good condition;
Embodiment 2
Prepare peony seeds oil-bound distemper (microcapsule powder is in 100g) successively as follows:
(1) 80 DEG C of warm water dissolves wall material, emulsifying agent; Wherein, wall material is casein sodium 4g, starch Sodium Octenyl Succinate 10g, the mixture of malt syrup 12g (calculating with solid content), emulsifier is 4g, and the component in emulsifying agent and weight proportion are: single diglycerine fatty acid ester: stearoyl lactate: diacetyl tartarate list double glyceride=2:1:0.5;
(2) add peony seed oil 70g to the wall material after dissolving and emulsifying agent to be uniformly mixed; Until obtain the solution of stable homogeneous system;
(3) carry out high-pressure homogeneous process to solution, first order pressure is 20MPa, second level pressure 5MPa, and homogenization cycles 2 times, obtains the solution that emulsified state is good;
(4) spraying dry is carried out to solution, wherein EAT 140 DEG C, leaving air temp 70 DEG C, obtain peony seed oil microcapsule powder in good condition;
Embodiment 3
Prepare peony seeds oil-bound distemper (microcapsule powder is in 100g) successively as follows:
(1) 70 DEG C of warm water dissolves wall material, emulsifying agent; Wherein, wall material is casein sodium 1g, starch Sodium Octenyl Succinate 3g, the mixture of malt syrup 87g (calculating with solid content), and emulsifier is 1g, and wherein, single diglycerine fatty acid ester is 0.8g, and stearoyl lactate is 0.2g;
(2) in the wall material dissolved and emulsifying agent, add peony seed oil 8g to be uniformly mixed; Until obtain the solution of stable homogeneous system;
(3) carry out high-pressure homogeneous process to solution, first order pressure is 20MPa, second level pressure 5MPa, and homogenization cycles 2 times, obtains the solution that emulsified state is good;
(4) spraying dry is carried out to solution, wherein EAT 140 DEG C, leaving air temp 70 DEG C, obtain peony seed oil microcapsule powder in good condition.
Test example 1
Test the embedding rate of peony seeds oil-bound distemper prepared by embodiment 1-3, result is as follows:
Project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
Embedding rate (%) | 97.8 | 95.1 | 99.2 |
Test example 2
The instant capacity of peony seeds oil-bound distemper prepared by the present invention is evaluated: method is as follows: with the water of 80 DEG C, peony seeds oil-bound distemper is reconstituted, obtain the peony seeds oil-bound distemper solution of 10%, with spoon at the uniform velocity agitating solution, start writing time, until in solution without macroscopic granule time.Test result is as follows:
Project | Peony seeds oil-bound distemper prepared by the present invention |
Without visible granule required time (s) of naked eyes in liquid | 10s |
As seen from the above table, peony seeds oil-bound distemper instant capacity provided by the invention is good.
Test example 3
Evaluation to peony seeds oil-bound distemper prepared by the present invention: method is as follows: peony seeds oil-bound distemper is reconstituted with the water of 80 DEG C, obtain the peony seeds oil-bound distemper solution of 10%, with spoon at the uniform velocity agitating solution, after solution stirs, observe the time that oil slick appears in surface.Test result is as follows:
Sample | 10% peony seed oil solution-stabilized time (min) |
Embodiment 1 | >60 |
Embodiment 2 | >45 |
Embodiment 3 | >120 |
Above the preparation technology of a kind of peony seed oil microcapsule powder provided by the present invention is described in detail.Apply specific case herein to set forth principle of the present invention and embodiment, the explanation of above embodiment just understands core concept of the present invention for helping.It should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention, some improvement and modification can also be carried out to the present invention.These improve and modify and also should fall in the protection domain of the claims in the present invention.
Claims (8)
1. a preparation technology for peony seed oil microcapsule powder, is characterized in that, in turn includes the following steps:
(1) wall material and emulsifying agent is dissolved with warm water;
(2) in the wall material after dissolving and emulsifying agent, peony seed oil is added, mixing and stirring;
(3) high-pressure homogeneous process is carried out to the mixed solution obtained in step (2), obtain the solution that emulsified state is good;
(4) spraying dry is carried out to the solution that step (3) obtains, obtain peony seed oil microcapsule powder;
Described wall material is casein sodium, starch Sodium Octenyl Succinate, gelatin, Arabic gum, the mixture of one or more in malt syrup;
Described emulsifying agent is single diglycerine fatty acid ester, stearoyl lactate, the mixture of one or more in diacetyl tartarate monoglyceride.
2. the preparation technology of peony seed oil microcapsule powder according to claim 1, it is characterized in that, described peony seed oil, wall material, emulsifying agent shared mass percent in peony seed oil microcapsule powder is followed successively by: peony seed oil 5-70%, wall material 25-93%, emulsifying agent 2-5%.
3. the preparation technology of peony seed oil microcapsule powder according to claim 1 and 2, it is characterized in that, described wall material is the mixture of casein sodium, starch Sodium Octenyl Succinate and malt syrup, and the weight ratio of three is casein sodium: starch Sodium Octenyl Succinate: malt syrup=(1-4): (3-12): (12-87).
4. the preparation technology of peony seed oil microcapsule powder according to claim 3, it is characterized in that, the weight ratio of described casein sodium, starch Sodium Octenyl Succinate and malt syrup is casein sodium: starch Sodium Octenyl Succinate: malt syrup=(1-2): (3-12): (44-87).
5. the preparation technology of peony seed oil microcapsule powder according to claim 1 and 2, it is characterized in that, described emulsifying agent is single diglycerine fatty acid ester, the mixture of stearoyl lactate and diacetyl tartarate list double glyceride, the mass ratio of three is single diglycerine fatty acid ester: stearoyl lactate: diacetyl tartarate list double glyceride=2:1:(0-1) ~ 10:1:(0-1).
6. the preparation technology of peony seed oil microcapsule powder according to claim 1 and 2, it is characterized in that, described emulsifying agent is the mixture of single diglycerine fatty acid ester and stearoyl lactate, and both mass ratioes are single diglycerine fatty acid ester: stearoyl lactate=2:1 ~ 4:1.
7. the preparation technology of peony seed oil microcapsule powder according to claim 1, it is characterized in that, the pressure of the high-pressure homogeneous process in described step (3) is divided into two-stage, and first order pressure is 10-30MPa, second level pressure is 5-10MPa, homogenization cycles 1-5 time.
8. the preparation technology of peony seed oil microcapsule powder according to claim 1, is characterized in that, in the drying process with atomizing of described step (4), EAT is 110-170 DEG C, and leaving air temp is 60-90 DEG C.
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CN104920642A (en) * | 2015-07-03 | 2015-09-23 | 山东省分析测试中心 | Food-grade peony seed blend oil microemulsion and preparing method thereof |
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