CN105028706A - Peony seed oil microcapsule and preparation method of peony seed oil microcapsule - Google Patents
Peony seed oil microcapsule and preparation method of peony seed oil microcapsule Download PDFInfo
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- CN105028706A CN105028706A CN201510488382.1A CN201510488382A CN105028706A CN 105028706 A CN105028706 A CN 105028706A CN 201510488382 A CN201510488382 A CN 201510488382A CN 105028706 A CN105028706 A CN 105028706A
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Abstract
The invention discloses a peony seed oil microcapsule and a preparation method of the peony seed oil microcapsule, and belongs to the technical field of food engineering. The peony seed oil microcapsule comprises a core material phase and a wall material phase. Through being metered by weight parts, the core material phase consists of 10 to 60 parts of peony seed oil and 0.5 to 5 parts of oil soluble emulsifiers; the wall material phase consists of 20 to 75 parts of wall materials, 5 to 50 parts of wall material connecting auxiliary agents, 20 to 150 parts of water, 1 to 8 parts of water-soluble emulsifiers and 0.5 to 5 parts of stabilizers. The pressure emulsification homogenizing is used, so that the particle diameter of an emulsion reaches the nanometer level, so that the particle size of an obtained product is uniform; the reconstitution capacity is good; the solubleness is good; the peony seed oil microcapsule can be dissolved in cold water; no precipitate and no floating object exist in a solution; no floating oil exists after the still standing for 48 hours; the solution can be compounded with other emulsions such as milk; the application range of the peony seed oil is expanded. The peony seed oil microcapsule and the preparation method have the advantages that the process is simple; the production cost is low; the product stability is greatly improved; and the nutrition activity of the peony seed oil is maintained.
Description
Technical field
The present invention relates to Food Engineering Development field, particularly a kind of peony seed oil microcapsules and preparation method thereof.
Background technology
Peony seeds is the elite crystallization of peony plant, has natural longevity gene.The vegetable oil extracted by peony seeds, unsaturated fatty acid content reaches more than 90%, and wherein polyunsaturated fatty acid-linolenic acid content is more than 40%, is 140 times of olive oil.Peony seeds has kind containing multiple nutritional labelings useful to human body such as vitamin E, phytosterol, squalene, trace elements simultaneously, anti-oxidant, protect the liver, reducing blood lipid, hypoglycemic, sun-proof etc. in there is outstanding effect, be the pure natural plant grease of great exploitation potential for its.
On March 22nd, 2011, peony seed oil obtained new resource food approval.At present, the extraction process of peony seed oil reaches its maturity, but deep processing research is fewer, rarely has report for the scientific paper of the microcapsule embedded technology of peony seed oil and patent of invention.Patent document 1(CN104206561A, denomination of invention is " a kind of preparation technology of peony seed oil microcapsule powder ") disclose a kind of preparation method of peony seed oil microcapsules.The stabilizing agent that the method does not add salt ion one class carrys out equilibrium water solution system, causes embedding rate to reduce (embodiment 2 embedding rate 95.1%), the very fast phenomenon (test example 3) occurring oil slick in the different time of the reconstituted milk after reconstituting.In addition, spray-dired EAT (110-170 DEG C) and leaving air temp (60-90 DEG C) too high, the loss of volatile flavor substance can be caused, affect mouthfeel.Although be instant product, must heating hot water (80 DEG C of test example 2), be difficult to accomplish instant in cold warm water.Because which limit its application in food, medicine.Patent document 2(CN103948035A, denomination of invention is " peony seed oil microcapsules, its preparation method and application ") disclose two kinds of preparation methods of peony seed oil microcapsules: yeast method and complex coacervation.Wherein, yeast method needs the deactivation of yeast purifying, and complex coacervation needs solidification, and finally also want vacuum drying or freeze-drying, the operating time is long, and energy consumption is high, complex process, and industrialization difficulty controls, and efficiency is low.
In a word, above method is in peony seed oil microcapsules preparation process, and suitability for industrialized production is more difficult, and product stability is poor, affects the utilization of product in food, medicine, cosmetics, health products etc.
Summary of the invention
In order to make up above deficiency, the invention provides a kind of epigranular, restoration is good, dissolubility is good, can dissolve in cold water, solution deposit-free and floating thing, nutriment lose few peony seed oil microcapsules and preparation method thereof.
Technical scheme of the present invention is:
A kind of peony seed oil microcapsules, comprise core phase and wall material phase, according to weight parts, described core is made up of 10-60 part peony seed oil and 0.5-5 part oil soluble emulsifying agent; Described wall material is connect auxiliary agent, 20-150 part water, 1-8 part water soluble emulsifier and 0.5-5 part stabilizing agent formed by 20-75 part wall material, 5-50 part wall material.
Preferably, described oil soluble emulsifying agent is one or more in sucrose ester, fatty glyceride, phosphatide.Described fatty glyceride is generally mono fatty acid glyceride, bis-fatty acid glyceride or its mixture (aliphatic acid list double glyceride).
Preferably, described water soluble emulsifier is one or more in caseinic acid, casein sodium, Caseins, potassium salts, water-soluble plant albumen.
Preferably, described stabilizing agent is one or more in citric acid, natrium citricum, potassium citrate, sodium hydrogen phosphate, dipotassium hydrogen phosphate.
Preferably, described wall material is one or more in malt syrup (dextrin), gelatin, Arabic gum, xanthans, protein, converted starch, cellulose derivative; Described wall material connection auxiliary agent is sucrose and/or glycerine.
The preparation method of described peony seed oil microcapsules, step is as follows:
1) preparation of core phase, adds 0.5-5 part oil soluble emulsifying agent, heating for dissolving in 10-60 part peony seed oil, obtained core phase;
2) preparation of wall material phase, to join 20-75 part wall material and 5-50 part wall material connection auxiliary agent in 20-150 part water and to be heated to 50-90 DEG C, then adding 1-8 part water soluble emulsifier and 0.5-5 part stabilizing agent, obtained wall material phase;
3) described core phase mixed mutually with wall material, emulsifying homogeneous becomes particle diameter to be the emulsion of 100-2000nm;
4) by described emulsion drying-granulating, obtained peony seed oil microcapsules.
Preferably, heating for dissolving described in step 1), is heated to 30-60 DEG C.
If step 2) in do not add wall material connection auxiliary agent, during step 4) drying-granulating, wall material has easily produced porous, easily causes core to leak, therefore gained microcapsules instability.Wall material connection auxiliary agent (sucrose and or glycerine) has mobility under the hot environment of spraying-fluid bed, and its mobility impels wall material tight, even to core parcel.
Preferably, described oil soluble emulsifying agent is one or more in sucrose ester, fatty glyceride, phosphatide; Described water soluble emulsifier is one or more in caseinic acid, casein sodium, Caseins, potassium salts, water-soluble plant albumen; Described stabilizing agent is one or more in citric acid, natrium citricum, potassium citrate, sodium hydrogen phosphate, dipotassium hydrogen phosphate; Described wall material is one or more in malt syrup, gelatin, Arabic gum, xanthans, protein, converted starch, cellulose derivative; Described wall material connection auxiliary agent is sucrose and/or glycerine.
Preferably, emulsifying homogeneous described in step 3) first shears pre-emulsification in high-speed shearing machine; Then further emulsifying in high pressure homogenizer, the pressure of high pressure homogenizer is set to 20-80MPa.In step 3), after high-speed shearing machine high speed shear pre-emulsification, use pressure emulsifying homogeneous method to carry out nanometer, thus overcome the uneven shortcoming such as cause reconstituted milk floating oil, wall material protected effect bad of the particle diameter caused in prior art.
Preferably, drying-granulating described in step 4) carries out at spraying-fluid bed, and spraying-fluid bed EAT is set to 80-120 DEG C, and leaving air temp is set to 10-60 DEG C.
Beneficial effect of the present invention is:
The method that the present invention prepares peony seed oil microcapsules adopts microcapsules technology by peony seed oil microencapsulation, the method utilizes macromolecular material that is natural or synthesis that peony seed oil is rolled into microcapsules, therefrom product water dissolubility and stability better, and energy suitability for industrialized production, thus the range of application overcoming prior art existence is narrower, the problem of less stable.Comprehensive, peony seed oil microcapsules of the present invention have following advantages:
1. the present invention uses pressure emulsifying homogeneous to make emulsion particle diameter reach nanoscale, thus the product granularity obtained is even, restoration is good, dissolubility is good, can dissolve in cold water, solution deposit-free and floating thing, leave standstill after 48 hours without oil slick, can be composite arbitrarily with other emulsions, as milk, milk beverage etc.Thus widened the range of application of peony seed oil;
2. the present invention adopts low temperature drying, decreases the loss of peony seed oil volatile materials, retains fragrance and mouthfeel specific to peony seed oil;
3. this particle has certain compressibility, can make an addition in tablet, there will not be oil leakage phenomenon through tabletting machine, may be used on milk sheet, buccal tablet etc.
4. the peony seed oil microcapsules particulate obtained by the method for the invention has good mobility, therefore facilitates it and uses, transports and storage;
5. preparation method of the present invention is simple, and route is reasonable, safe and reliable, maintains the nutritional activities of peony seed oil, thus has remarkable advantage.
Detailed description of the invention
Embodiment 1
3g sucrose ester is joined in 60g peony seed oil, is stirred and heated to 60 DEG C, is stirred to dissolving, obtained core phase.By 5g gelatin, 15g converted starch and 5g sucrose, add in 100mL water, be heated to 90 DEG C, stir and make Gelatin; Add 2g casein sodium and 3g citric acid, be stirred to dissolving, obtained wall material phase.Core phase is mixed mutually with wall material, first in high-speed shearing machine pre-emulsification, then by high pressure homogenizer at the emulsified homogeneous of 80MPa, form emulsion, the particle diameter of emulsion reaches 200nm.Under the condition of EAT 120 DEG C, leaving air temp 10 DEG C by described emulsion through spraying-fluidized bed drying, thus obtained peony seed oil microcapsules particulate.
Obtain 98.4g peony seed oil microcapsules particulate by the method, wherein surface starch adhesive capacity is 7%, and the embedding rate of peony seed oil is 99.4%.
Observed by screening, 80 mesh sieves crossed by the peony seed oil microcapsules particulate of 90%, and 100 mesh sieves crossed by the peony seed oil microcapsules particulate of 5%, prove that powder size is even.
By gained peony seed oil microcapsules particulate 10g, join 200ml, in 26 DEG C of water, rock (without the need to stirring) gently and timing, namely 11s visually observes less than particle, and peony seed oil microcapsules are dissolved in the water well, and solution presents homogeneous translucent emulsion, and leave standstill deposit-free and floating thing after 48 hours, prove that it has good dissolubility and restoration.
Embodiment 2
0.5kg phosphatide is joined in 10kg peony seed oil, is heated to 30 DEG C, is stirred to dissolving, obtained core phase.In 4kg Arabic gum, 10kg converted starch, 44kg malt syrup and 15kg glycerine, add 90L water, be heated to 50 DEG C, stir and make it to dissolve; Add 1kg caseinic acid and 0.5kg sodium hydrogen phosphate, be stirred to dissolving, obtained wall material phase.Core phase is mixed mutually with wall material, first in high-speed shearing machine pre-emulsification, then by high pressure homogenizer at the emulsified homogeneous of 20MPa, form stable emulsion, the particle diameter of emulsion reaches 350nm.Then under the condition of EAT 90 DEG C, leaving air temp 60 DEG C by emulsion through spraying-fluidized bed drying, thus obtained peony seed oil microcapsules particulate.
Obtain 99.3kg peony seed oil particulate by the method, wherein surface starch adhesive capacity is 15%, peony seed oil embedding rate 99.6%.
Observed by screening, 80 mesh sieves crossed by the peony seed oil microcapsules particulate of 90%, and the peony seed oil microscapsule powder of 5% crosses 100 mesh sieves, proves that powder size is even.
By gained peony seed oil microcapsules particulate 100g, join 2000ml, in 26 DEG C of water, rock (without the need to stirring) gently and timing, namely 10s visually observes less than particle, and peony seed oil microcapsules are dissolved in the water well, and solution presents homogeneous translucent emulsion, and leave standstill deposit-free and floating thing after 48 hours, prove that it has good dissolubility and restoration.
Embodiment 3
0.5kg mono fatty acid glyceride and 3.5kg sucrose ester join in 30kg peony seed oil, are heated to 50 DEG C and are stirred to dissolving, obtained core phase.In 15kg converted starch, 17kg dextrin and 20kg sucrose, 10kg glycerine, add 100L water, be heated to 50 DEG C, stir and make it to dissolve; Add 2.5kg Caseins, potassium salts and 1.5kg dipotassium hydrogen phosphate, be stirred to dissolving, obtained wall material phase.Core phase is mixed mutually with wall material, first in high-speed shearing machine pre-emulsification, then by high pressure homogenizer at the emulsified homogeneous of 40MPa, form emulsion, the particle diameter of emulsion reaches 230nm.Obtain stable emulsion through triple effect evaporator evaporation recycling design, then under the condition of EAT 200 DEG C, leaving air temp 100 DEG C by emulsion through spraying-fluidized bed drying, thus obtained peony seed oil microcapsules particulate.
Obtain 99.6kg peony seed oil particulate by the method, surface starch adhesive capacity is 10%, and wherein the embedding rate of peony seed oil is 99.7%.
Observed by screening, 80 mesh sieves crossed by the peony seed oil microcapsules particulate of 90%, and the peony seed oil microscapsule powder of 6% crosses 100 mesh sieves, proves that powder size is even.
By gained peony seed oil microcapsules particulate 10g, join 200ml, in 15 DEG C of water, rock (without the need to stirring) gently and timing, namely 16s visually observes less than particle, and peony seed oil microcapsules are dissolved in the water well, and solution presents homogeneous translucent emulsion, and leave standstill deposit-free and floating thing after 48 hours, prove that it has good dissolubility and restoration.
In the particle diameter of emulsion, " particle diameter " refers to median particle diameter D50, and it can directly be measured by laser particle analyzer.
Claims (10)
1. peony seed oil microcapsules, comprise core phase and wall material phase, it is characterized in that: according to weight parts, and described core is made up of 10-60 part peony seed oil and 0.5-5 part oil soluble emulsifying agent; Described wall material is connect auxiliary agent, 20-150 part water, 1-8 part water soluble emulsifier and 0.5-5 part stabilizing agent formed by 20-75 part wall material, 5-50 part wall material.
2. peony seed oil microcapsules as claimed in claim 1, is characterized in that: described oil soluble emulsifying agent is one or more in sucrose ester, fatty glyceride, phosphatide.
3. peony seed oil microcapsules as claimed in claim 1, is characterized in that: described water soluble emulsifier is one or more in caseinic acid, casein sodium, Caseins, potassium salts, water-soluble plant albumen.
4. peony seed oil microcapsules as claimed in claim 1, is characterized in that: described stabilizing agent is one or more in citric acid, natrium citricum, potassium citrate, sodium hydrogen phosphate, dipotassium hydrogen phosphate.
5. peony seed oil microcapsules as claimed in claim 1, is characterized in that: described wall material is one or more in malt syrup, gelatin, Arabic gum, xanthans, protein, converted starch, cellulose derivative; Described wall material connection auxiliary agent is sucrose and/or glycerine.
6. the preparation method of peony seed oil microcapsules as claimed in claim 1, it is characterized in that, step is as follows:
1) preparation of core phase, adds 0.5-5 part oil soluble emulsifying agent, heating for dissolving in 10-60 part peony seed oil, obtained core phase;
2) preparation of wall material phase, to join 20-75 part wall material and 5-50 part wall material connection auxiliary agent in 20-150 part water and to be heated to 50-90 DEG C, then adding 1-8 part water soluble emulsifier and 0.5-5 part stabilizing agent, obtained wall material phase;
3) described core phase mixed mutually with wall material, emulsifying homogeneous becomes particle diameter to be the emulsion of 100-2000nm;
4) by described emulsion drying-granulating, obtained peony seed oil microcapsules.
7. peony seed oil microcapsules as claimed in claim 6 and preparation method thereof, is characterized in that: heating for dissolving described in step 1), is heated to 30-60 DEG C.
8. peony seed oil microcapsules as claimed in claim 6 and preparation method thereof, is characterized in that: described oil soluble emulsifying agent is one or more in sucrose ester, fatty glyceride, phosphatide; Described water soluble emulsifier is one or more in caseinic acid, casein sodium, Caseins, potassium salts, water-soluble plant albumen; Described stabilizing agent is one or more in citric acid, natrium citricum, potassium citrate, sodium hydrogen phosphate, dipotassium hydrogen phosphate; Described wall material is one or more in malt syrup, gelatin, Arabic gum, xanthans, protein, converted starch, cellulose derivative; Described wall material connection auxiliary agent is sucrose and/or glycerine.
9. peony seed oil microcapsules as claimed in claim 6 and preparation method thereof, is characterized in that: emulsifying homogeneous described in step 3) first shears pre-emulsification in high-speed shearing machine; Then further emulsifying in high pressure homogenizer, the pressure of high pressure homogenizer is set to 20-80MPa.
10. peony seed oil microcapsules as claimed in claim 6 and preparation method thereof, it is characterized in that: drying-granulating described in step 4) carries out at spraying-fluid bed, spraying-fluid bed EAT is set to 80-120 DEG C, and leaving air temp is set to 10-60 DEG C.
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106106728A (en) * | 2016-06-17 | 2016-11-16 | 郑州师范学院 | Flos Chrysanthemi Yoghourt and preparation method thereof |
| CN106387916A (en) * | 2016-09-12 | 2017-02-15 | 云南农业大学 | Oral microencapsulated porcupine oil and preparation method thereof |
| CN106693845A (en) * | 2016-07-13 | 2017-05-24 | 东莞市恩科化工有限公司 | Preparation method of natural essential oil microcapsule |
| CN106900885A (en) * | 2017-02-27 | 2017-06-30 | 山东省科学院生物研究所 | A kind of microencapsulation peony seed oil, complex composition and preparation method thereof |
| CN107136511A (en) * | 2017-05-25 | 2017-09-08 | 山东省科学院生物研究所 | A kind of peony seed oil composition for promoting cranial nerve development, Peony-seed-oil soft capsule and preparation method thereof |
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| CN114431472A (en) * | 2022-02-15 | 2022-05-06 | 晨日不老莓(辽宁)大健康有限责任公司 | Aronia melanocarpa seed oil microcapsule powder and preparation method thereof |
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| CN106106728A (en) * | 2016-06-17 | 2016-11-16 | 郑州师范学院 | Flos Chrysanthemi Yoghourt and preparation method thereof |
| CN106693845A (en) * | 2016-07-13 | 2017-05-24 | 东莞市恩科化工有限公司 | Preparation method of natural essential oil microcapsule |
| CN106387916A (en) * | 2016-09-12 | 2017-02-15 | 云南农业大学 | Oral microencapsulated porcupine oil and preparation method thereof |
| CN106900885A (en) * | 2017-02-27 | 2017-06-30 | 山东省科学院生物研究所 | A kind of microencapsulation peony seed oil, complex composition and preparation method thereof |
| CN107136511A (en) * | 2017-05-25 | 2017-09-08 | 山东省科学院生物研究所 | A kind of peony seed oil composition for promoting cranial nerve development, Peony-seed-oil soft capsule and preparation method thereof |
| CN107519025A (en) * | 2017-08-23 | 2017-12-29 | 中山大学惠州研究院 | A kind of hydrophobic sun-proof microcapsules and preparation method thereof |
| CN108277085A (en) * | 2017-12-18 | 2018-07-13 | 云南中烟工业有限责任公司 | A kind of compound with slow-release function, preparation method and application |
| CN108271865A (en) * | 2017-12-29 | 2018-07-13 | 河南洛阳红牡丹产业研发有限公司 | A kind of production method of tree peony fresh milk |
| CN108902503A (en) * | 2018-07-26 | 2018-11-30 | 湖南普菲克生物科技有限公司 | A kind of functional powder grease and its preparation and application |
| CN109700030A (en) * | 2019-01-28 | 2019-05-03 | 江南大学 | The preparation method and product of a kind of Seabuckthorm Seed Oil microcapsules and its application in sea-buckthorn chewing tablet |
| CN109700030B (en) * | 2019-01-28 | 2022-05-20 | 江南大学 | Preparation method of sea buckthorn seed oil microcapsule, product and application of sea buckthorn seed oil microcapsule in sea buckthorn chewable tablet |
| CN111560771A (en) * | 2019-05-24 | 2020-08-21 | 安徽农业大学 | Embroidery anticorrosion and antioxidation method for three-dimensional pattern |
| CN111560771B (en) * | 2019-05-24 | 2021-07-09 | 安徽农业大学 | Embroidery anticorrosion and antioxidation method for three-dimensional pattern |
| CN113262728A (en) * | 2021-06-08 | 2021-08-17 | 山东天美生物技术有限公司 | Production process of peony seed diglyceride microcapsule powder |
| CN114307582A (en) * | 2021-12-30 | 2022-04-12 | 福建恒安集团有限公司 | Microcapsule natural deodorant |
| CN114431472A (en) * | 2022-02-15 | 2022-05-06 | 晨日不老莓(辽宁)大健康有限责任公司 | Aronia melanocarpa seed oil microcapsule powder and preparation method thereof |
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Application publication date: 20151111 |