CN101703181A - Functional type soy glycoproteins microcapsule - Google Patents
Functional type soy glycoproteins microcapsule Download PDFInfo
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- CN101703181A CN101703181A CN200910259536A CN200910259536A CN101703181A CN 101703181 A CN101703181 A CN 101703181A CN 200910259536 A CN200910259536 A CN 200910259536A CN 200910259536 A CN200910259536 A CN 200910259536A CN 101703181 A CN101703181 A CN 101703181A
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- lycopene
- lecithin
- lutein
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Abstract
The invention discloses a preparation method of a functional type soy glycoproteins microcapsule, belonging to the technical field of food. The preparation method is characterized by utilizing full water-soluble soy glycoproteins as main wall material, and lecithin or lutein or lycopene as core material to prepare the functional type microcapsule products. The full water-soluble soy glycoproteins has a plurality of excellent functional characteristics; and the lecithin, lutein, and lycopene are lipid-soluble matters with higher nutritive and health-care values, but the instability and water insolubility of the matters limit application thereof to certain degree. The preparation method has the advantages that the full water-soluble soy glycoproteins with emulsifying property is utilized as the wall material, and the microcapsule is obtained by spray drying; the microcapsule not only has multiple functions of the soy glycoproteins, but also can strengthen the stability of nutritive and health-care matters of the lecithin or lutein or lycopene and absorption thereof by human body, increases formulation manners, and well extends application fields thereof.
Description
Technical field
This method relates to a kind of preparation method of functional type soy glycoproteins microcapsule, and this method belongs to field of food industry.
Background technology
Full water-soluble sugar soybean protein is a kind of rising functional oligose class, indigestibility, and calorific value is low, the disease of can not causeing fat; Be again the good breeding material of Bifidobacterium, have a series of physiological functions the human body beneficial.Full water-soluble soybean glycoprotein can be widely used in food, beverage production, aspect medicine, the feed addictive tempting application prospect is being arranged.In addition, full water-soluble soybean glycoprotein also has under emulsification and emulsion stability, the acid condition graceful function characteristics such as the stabilization of protein body, anti-cohesiveness, filming performance and foam stabilities.
Microcapsules technology in the food industry is the experience and the technology of using in the medical industry, nutriment in the food and additive are carried out microencapsulation processing, improved anti-storage, the processing characteristics of these compositions on the one hand, can exempt the bitter taste of food on the other hand, peculiar smell, unfavorable factors such as color.
In " spray-drying prepares lycopene microcapsule " (people's " dry technology and equipment " such as Fang Jingyan 2005 the 3rd volumes the 1st interim production technology of having reported with the spray drying method for preparation lycopene microcapsule.With the lycopene oleoresin is core, and albumen NC and carbohydrate/ViA are the wall material, make lycopene microcapsule through homogeneous, spray-drying.
(people's " food industry science and technology " such as Qi Jinfeng 2009 the 30th volumes the 1st are interim has reported that with maltodextrin, casein be the wall material, prepares Xanthin micro-capsule with spray-drying, freeze drying respectively in " different Microencapsulation Method are to the Xanthophyll micro-capsule Effect on Performance ".
(people's " food science and technology " such as Wang Xingmin 2008 the 33rd volumes the 12nd interim research soluble soybean polysaccharide and gelatin reported condenses the method for preparing the phytase microcapsules again in " research for preparing the phytase microcapsules with the soluble soybean polysaccharide for the wall material ".
The present invention utilizes full water-soluble soybean glycoprotein to be the wall material by spray-dired method, is core with lutein, lycopene, lecithin respectively, preparation Mobyneb microcapsules.
Summary of the invention
The present invention utilizes full water-soluble soybean glycoprotein as main wall material, produces the functional form microcapsules that contain lecithin, lycopene and lutein.
Technical scheme of the present invention is: take by weighing full water-soluble soybean glycoprotein and other compatibility materials (as gelatin in 1: 1～5: 1 ratios, Arabic gum, beta cyclodextrin etc.) join in the beaker, add a certain proportion of water, stirring is until mixing, as the wall material.In core: 1: 6～1: 15 ratio weighing core materials of wall material (lecithin or lycopene or lutein) joins in another beaker, adds a certain proportion of solvent, and carries out ultrasonic dissolution, and the time is 5min～20min.Core solution is slowly joined in the wall material solution, and the back that stirs is ultrasonic short molten, and the time is 10～200min, forms homogeneous solution.The homogeneous solution that previous step makes is carried out spray-drying, and admission pressure is 0.15～0.45MPa.
The main wall material that the present invention uses is a full water-soluble soybean glycoprotein, full water-soluble soybean glycoprotein has the one-tenth membrane stability of good emulsifying and emulsion stability, water retentivity, the strong fragrant effect of seasoning and optimization. because full water-soluble soybean glycoprotein itself has good emulsifying stability, so can add or not add other emulsifying agent in process of production on a small quantity.
The core that the present invention adopts is lecithin or lycopene or lutein, lecithin, lutein and lycopene are the liposoluble substances with higher healthy nutritive value, but the unstability of this type of material and water-insoluble have limited their application to a certain extent.The present invention is by being that the wall material carries out microencapsulation to above-mentioned three kinds of materials with the full water-soluble soybean glycoprotein, make it not only have the multiple function of soy glycoproteins, and enhancing lecithin or lutein or lycopene nourishing healthy Stability of Substance and absorption of human body, increase composite mode, expand its application better.
The compatibility material of using among the present invention is gelatin, Arabic gum, beta cyclodextrin etc., also can not add the compatibility material, and according to preparation technology, parameter is adjusted to some extent.
Utilize the emulsification property of full water-soluble soybean glycoprotein among the present invention, but, also can add other emulsifying agent on a small quantity according to different requirements.
Description of drawings
Fig. 1: embodiment 1 product
Fig. 2: embodiment 2 products
Fig. 3: embodiment 3 products
The specific embodiment
Embodiment 1: with full water-soluble glycoprotein is main wall material, and lecithin is that core is produced the functional microcapsule product
(1) takes by weighing 4g soybean polyoses and 4g gelatin and join in the beaker of 100mL, add 50mL water, stir until mixing, as the wall material.(2) take by weighing 0.8g lecithin, join in the beaker of 20mL, add 30mL water, and carry out ultrasonic dissolution, as core, ultrasonic power is 400W, and the time is 5min.(3) core is added drop-wise in the wall material solution while stirring lentamente, the back that stirs is ultrasonic short molten, and ultrasonic power is 400W, and the time is 10min, forms homogeneous solution.(4) homogeneous solution that previous step is made is carried out spray-drying, and admission pressure is 0.24MPa, and feed rate is 12mL/min, promptly obtains pulverous lecithin product.
Embodiment 2: with full water-soluble glycoprotein is main wall material, and lutein is that core is produced the functional microcapsule product
(1) takes by weighing 2.5g soybean polyoses and 1.25g gelatin and join in the beaker of 100mL, add 50mL water, stir until mixing, as the wall material.(2) take by weighing 0.5g lutein, join in the beaker of 10mL, add 1mL soybean oil ultrasonic dissolution, as core, ultrasonic power is 500W, and the time is 5min.(3) core is joined in the wall material solution while stirring lentamente, the back that stirs is ultrasonic short molten, and ultrasonic power is 500W, and the time is 10min, forms homogeneous solution.
(4) homogeneous solution that previous step is made is carried out spray-drying, and admission pressure is 0.24MPa, and feed rate is 12mL/min, promptly obtains pulverous lutein product.
Embodiment 3: with full water-soluble glycoprotein is main wall material, and lycopene is that core is produced the functional microcapsule product
(1) takes by weighing 4g soybean polyoses and 2g gelatin and join in the beaker of 100mL, add 50mL water, stir, add class 80 of 0.09g department and 0.41g Tween 80 again, as the wall material until mixing.(2) take by weighing the 0.4g lycopene, join in the beaker of 10mL, add 10mL ethyl acetate ultrasonic dissolution, as core, ultrasonic power is 700W, and the time is 10min.
(3) lentamente core is added drop-wise in the wall material solution while stirring, ultrasonic short molten after stirring, ultrasonic power is 700W, time is 20min, form homogeneous solution. (4) carry out spray-drying to the homogeneous solution that previous step makes, admission pressure is 0.24MPa, and feed rate is 12mL/min, promptly obtains pulverous lycopene product.
Claims (4)
1. the preparation method of a functional type soy glycoproteins microcapsule, this method comprises:
1) takes by weighing full water-soluble glycoprotein in 1: 1～5: 1 ratio and other compatibility materials (as gelatin, Arabic gum, beta cyclodextrin etc.) join in the beaker, add a certain proportion of water, stir until mixing, as the wall material.
2) in core: 1: 6～1: 15 ratio weighing core materials of wall material (lecithin, lycopene or lutein) joins in another beaker, adds a certain proportion of solvent, and carries out ultrasonic dissolution, and the time is 5min～20min.
3) core is slowly joined in the wall material solution, the back that stirs is ultrasonic short molten, and the time is 10～200min, forms homogeneous solution.
4) homogeneous solution that previous step is made is carried out spray-drying, and admission pressure is 0.15～0.45MPa.
2. method according to claim 1, it is characterized in that: full water-soluble soybean glycoprotein is as main wall material.
3. method according to claim 1 is characterized in that: water-soluble soybean glycoprotein solution is equipped with homogeneous solution with lecithin, lycopene and lutein solution mixing system respectively.
4. method according to claim 1 is characterized in that: above-mentioned homogeneous solution is carried out microencapsulation with spray-drying.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910259536A CN101703181A (en) | 2009-12-18 | 2009-12-18 | Functional type soy glycoproteins microcapsule |
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| CN200910259536A CN101703181A (en) | 2009-12-18 | 2009-12-18 | Functional type soy glycoproteins microcapsule |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107047964A (en) * | 2017-05-31 | 2017-08-18 | 贵州江口绿源水产发展有限公司 | A kind of Chinese medicine compounded fish feed and preparation method thereof |
| CN107048093A (en) * | 2017-05-31 | 2017-08-18 | 贵州江口绿源水产发展有限公司 | A kind of fish feed additive and preparation method thereof |
| CN107079853A (en) * | 2017-06-02 | 2017-08-22 | 贵州江口绿源水产发展有限公司 | A kind of prevention and controls of fin rot |
| CN107155978A (en) * | 2017-06-07 | 2017-09-15 | 贵州江口绿源水产发展有限公司 | A kind of prevention and controls of trichodinasis |
| CN107347749A (en) * | 2017-06-28 | 2017-11-17 | 贵州江口绿源水产发展有限公司 | A kind of prevention and controls of anchor head pulicosis |
| CN107347750A (en) * | 2017-07-12 | 2017-11-17 | 贵州江口绿源水产发展有限公司 | A kind of cultural method using herbal control fish saprolegniasis |
| CN107410117A (en) * | 2017-06-07 | 2017-12-01 | 贵州江口绿源水产发展有限公司 | A kind of disease prevention and cure method of rice field fish culture |
| CN107439433A (en) * | 2017-07-14 | 2017-12-08 | 贵州江口绿源水产发展有限公司 | A kind of cultural method using herbal control fish bacterial enteritis disease |
| CN107594597A (en) * | 2017-07-31 | 2018-01-19 | 浙江新维普添加剂有限公司 | A kind of fat soluble nutrient microcapsules and preparation method thereof |
| CN115069180A (en) * | 2022-07-20 | 2022-09-20 | 浙江惠嘉生物科技股份有限公司 | Secondary cross-linking type plant essential oil microcapsule as well as preparation method and application thereof |
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2009
- 2009-12-18 CN CN200910259536A patent/CN101703181A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107047964A (en) * | 2017-05-31 | 2017-08-18 | 贵州江口绿源水产发展有限公司 | A kind of Chinese medicine compounded fish feed and preparation method thereof |
| CN107048093A (en) * | 2017-05-31 | 2017-08-18 | 贵州江口绿源水产发展有限公司 | A kind of fish feed additive and preparation method thereof |
| CN107079853A (en) * | 2017-06-02 | 2017-08-22 | 贵州江口绿源水产发展有限公司 | A kind of prevention and controls of fin rot |
| CN107155978A (en) * | 2017-06-07 | 2017-09-15 | 贵州江口绿源水产发展有限公司 | A kind of prevention and controls of trichodinasis |
| CN107410117A (en) * | 2017-06-07 | 2017-12-01 | 贵州江口绿源水产发展有限公司 | A kind of disease prevention and cure method of rice field fish culture |
| CN107347749A (en) * | 2017-06-28 | 2017-11-17 | 贵州江口绿源水产发展有限公司 | A kind of prevention and controls of anchor head pulicosis |
| CN107347750A (en) * | 2017-07-12 | 2017-11-17 | 贵州江口绿源水产发展有限公司 | A kind of cultural method using herbal control fish saprolegniasis |
| CN107439433A (en) * | 2017-07-14 | 2017-12-08 | 贵州江口绿源水产发展有限公司 | A kind of cultural method using herbal control fish bacterial enteritis disease |
| CN107594597A (en) * | 2017-07-31 | 2018-01-19 | 浙江新维普添加剂有限公司 | A kind of fat soluble nutrient microcapsules and preparation method thereof |
| CN107594597B (en) * | 2017-07-31 | 2020-05-12 | 浙江新和成股份有限公司 | Fat-soluble nutrient microcapsule and preparation method thereof |
| CN115069180A (en) * | 2022-07-20 | 2022-09-20 | 浙江惠嘉生物科技股份有限公司 | Secondary cross-linking type plant essential oil microcapsule as well as preparation method and application thereof |
| CN115069180B (en) * | 2022-07-20 | 2022-11-04 | 浙江惠嘉生物科技股份有限公司 | Secondary cross-linking type plant essential oil microcapsule as well as preparation method and application thereof |
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Open date: 20100512 |