CN107714496A - A kind of dropper BB frosts and preparation method thereof - Google Patents
A kind of dropper BB frosts and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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Abstract
The present invention discloses a kind of dropper BB frosts, including following components：Dimethicone Crosspolymer, phenyl trimethicone, isononyl isononanoate, dimethyl silicone polymer, dimethiconol, cetyl dimethicone, ring five dimethyl silicone polymer, cyclohexasiloxane, the dimethyl silicone polymers of PEG 10, the bentonite of quaternary ammonium salt 18, HDI/ trihydroxy methyl hexyl Inner ester cross-linked polymers, silica, propylene glycol carbonate, titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, anti-ageing composition, isomery dodecane surplus.The present invention is made up of pure oil phase, prepares simplicity, and viscosity is low, easy to use, and makeup is frivolous uniformly, is advantageous to the stabilization of oxidizable raw material, and good skin-care effect can be achieved.
Description
Technical field
The present invention relates to cosmetic field, is specifically related to a kind of dropper BB frosts and preparation method thereof.
Background technology
BB frosts, are Blemish Balm abbreviations, and effect mainly hides the flaw, adjusts the colour of skin, be sun-proof, careful pore, can beat
Produce the sensation of Nude Look (nude look effect).After BB frosts are originally peeling or whitening (brightening), to skin that is impaired and damaging
Protection and maintenance used in regeneration frost.This regeneration frost can give to the problem of skin rapidly to be improved in time, can
The shortcomings that improving and making up skin, thus BB frosts of gaining the name.
BB frosts are generally cream shape, or air cushion BB, typically using two-phase emulsification structure, W/O or O/W types, emulsified body
Belong to metastable condition, the quality problems such as water-oil separating easily occur；And viscosity is high, skin sense is sticky；The presence of water causes easily
Generation microorganism pollution, the problems such as oxidizable raw material goes bad.
The content of the invention
A kind of the present invention is intended to provide dropper BB frosts and preparation method thereof.It is made up of pure oil phase, prepares easy, viscosity
Low, easy to use, makeup is frivolous uniformly, is advantageous to the stabilization of oxidizable raw material, and good skin-care effect can be achieved.
To achieve the above object, the present invention uses following technical scheme：
A kind of dropper BB frosts, include the component of following mass percent：
Dimethicone Crosspolymer 1-10%
Phenyl trimethicone 1-10%
Isononyl isononanoate 1-5%
Dimethyl silicone polymer 0.1-1%
Dimethiconol 0.1-1%
Cetyl dimethicone 1-10%
Ring five dimethyl silicone polymer 10-30%
Cyclohexasiloxane 5-15%
PEG-10 dimethyl silicone polymers 0.5-1.5%
The bentonite of quaternary ammonium salt -18 0.5-1.5%
HDI/ trihydroxy methyl hexyl Inner ester cross-linked polymers 0.5-3%
Silica 0.1-1%
Propylene glycol carbonate 0.1-1%
Isomery dodecane surplus
Titanium dioxide 10-20%
Iron oxide red 0.1-0.5%
Iron oxide black 0.1-0.5%
Iron oxide yellow 0.1-3%.
Further, the BB frosts also include 0.1-10% anti-ageing composition.
Further, the anti-ageing composition is prepared by the raw material of following weight parts：Motherwort 1-10 parts, masson pine
Pollen 1-10 parts, frankincense 1-10 parts, ginseng 1-10 parts, shaddock pericarp 1-10 parts.
Further, the anti-ageing composition is prepared via a method which to obtain：（1）By motherwort, Pollen of Masson Pine, breast
Perfume, ginseng, the mixing of shaddock pericarp, crush, sift out, obtain mixed material；（2）Deep-sea two is added into mixed material and saves shepherd's purse seed
Oil, soak 8-10 hours, the weight of its mesopelagic (200 meter Dao1000 meter Shui Shen) two section shepherd's purse seed oil is 4-5 times of mixed material；（3）In step（2）Gained mixes
Close in raw material and add petroleum ether in 10 30 mL/g ratio, Extracting temperature is 40 °C 80 °C, and ultrasonic power is
Under conditions of 100W 500W, the ultrasonic extraction time is 10 50min, vacuum filtration, is freeze-dried, is resisted after concentrated by rotary evaporation
Decline composition.
The present invention is prepared anti-ageing using the anti-ageing composition material of the section shepherd's purse seed oil immersion bubble of deep-sea two and ultrasonic extraction combination
Composition, because deep-sea two is saved, shepherd's purse seed oil oxidation stability is good, and skin sense silk is sliding, pleasant, rich in skin nutrition composition:OMEGA-3,
Anti-ageing composition made from immersion is while with senile-resistant efficacy, moreover it is possible to increases oxidation resistance and the increase of dropper BB frosts
Use the fragrance of rear skin sense.
Further, the titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow are surface treatment toner, described
Surface conditioning agent is triethoxy octyl group silane.
Further, the toner can be premix mill base, and the preparation method of the mill base is：（1）Each toner is put into
3-5 minutes are ground in dry type toner grinder, obtain mixed-powder；（2）Toner dispersant is added into mixed-powder, stirring is equal
Even acquisition mixture；（3）Said mixture is added to circular grinding 3-5 times in anhydrous clean three-roll grinder, to slurry
Uniform and smooth, you can.
Yet further, the toner dispersant is by ring five dimethyl silicone polymer, PEG/PPG-18/18 poly dimethyl silicon
Oxygen alkane forms, and the addition of the toner dispersant is the 20-50% of mixed-powder weight.
Further, the ring five dimethyl silicone polymer, the quality of PEG/PPG-18/18 dimethyl silicone polymers it
Than for（1-10）：（1-10）.
The present invention also provides a kind of preparation method of dropper BB frosts, comprises the following steps：
1）By A phases raw material mix, stir 20-30 minutes, be uniformly dispersed, the A phases be Dimethicone Crosspolymer,
The poly- diformazan of phenyl trimethicone, isononyl isononanoate, dimethyl silicone polymer, dimethiconol, cetyl
Radical siloxane, ring five dimethyl silicone polymer, cyclohexasiloxane, PEG-10 dimethyl silicone polymers, the bentonite of quaternary ammonium salt -18
, HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer, silica, propylene glycol carbonate, isomery dodecane, anti-ageing composition it is mixed
Close；
2）B phases raw material is used in advance 3-5 minutes are ground in dry type toner grinder, obtained mixed-powder and then add mixed-powder
Enter in A phases, homogeneous 10-15 minutes, be uniformly dispersed to toner, the B phases are titanium dioxide, iron oxide red, iron oxide black and oxygen
Change the mixing of iron oxide yellow.
The present invention has advantageous effect in that relative to prior art：
（1）Titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow are prepared into dispersion pulp by the present invention can make it in BB frosts
In formula system evenly, color and luster is more fine and smooth, and makeup effect is more frivolous；
（2）The present invention is made up of pure oil phase, can solve the problem that the incident demulsification problem of W/O or O/W types in the prior art, and then
Trigger the quality problems such as water-oil separating；And the presence that pure oil phase also solves water causes incidental microorganism pollution, easily
The problems such as oxidic raw materials go bad；The present invention is advantageous to the stabilization of oxidizable raw material, and brewed using the section shepherd's purse seed oil immersion of deep-sea two
The anti-ageing composition obtained is while with senile-resistant efficacy, moreover it is possible to after the oxidation resistance and the increase use that increase dropper BB frosts
The fragrance of skin sense.
（3）The present invention uses dropper mode, easy to use, prepares simplicity, and viscosity is low, and makeup is frivolous uniformly, is advantageous to easily
The stabilization of oxidic raw materials, good skin-care effect can be achieved.
Embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical scheme will be carried out below
Detailed description.Obviously, described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are resulting on the premise of creative work is not made to be owned
Other embodiment, belong to the scope that the present invention is protected.
Motherwort is labiate LeonurusheterohyllusSweet. Nen Stems leaves.Motherwort Nen Stems leaves contain
The multiple nutritional components such as protein, carbohydrate.Nature and flavor work hard it is cool, have promoting blood circulation, stagnation resolvation, menstruation regulating, disappear water the effect of.Treatment
Water, hematuria under irregular menstruation, edema, rush down blood, dysentery, hemorrhoid.Motherwort contains various trace elements.With enhancing immunocyte
Vigor, the generation for relaxing atherosclerosis and the effect for improving human body defence function of diseases system；Can anti-oxidant, health care
Always, hyperplasia that is antifatigue and suppressing cancer cell.
Pollen pini also known as pine are yellow, are China pinaceae plant masson pine, Chinese pine or the dry pollen for belonging to several plants together, are us
The pollen class Chinese medicine of state's tradition medicine-food two-purpose, there are abundant nutritive value and multiple biological activities.Pollen pini contain protein,
The multiple nutritional components such as amino acid, mineral matter, vitamin, enzyme and coenzyme, fat, flavones, nucleic acid, monose, polysaccharide, phosphatide, tool
It is improved immunity, anti-aging, antifatigue, beautifying face and moistering lotion and other effects.
Boswellia carterii is widely grown in drying, and hilly India is widely grown in drying, hilly India.In ancient times
Generation, olibanum resin have turned into important adjustment, the modern medicines such as scent, medical treatment, cosmetics, perfume and have shown contained masticinic acid in frankincense
And other obvious mitigation wrinkles of organic acid tool, anti-aging, anti-inflammatory, analgesic activity.
Shaddock pericarp is the pericarp of shaddock, rich in naringin, can reduce the stickiness of blood, Cucumber Extract, improve skin
Elasticity.
Embodiment 1
A kind of dropper BB frosts, include the component of following mass percent：Dimethicone Crosspolymer 5%, phenyl poly- three
Methylsiloxane 5%, isononyl isononanoate 2.5%, dimethyl silicone polymer 0.5%, dimethiconol 0.5%, cetyl
Dimethyl silicone polymer 5%, ring five dimethyl silicone polymer 20%, cyclohexasiloxane 10%, PEG-10 dimethyl silicone polymers 1%,
The bentonite of quaternary ammonium salt -18 1%, HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer 1.5%, silica 0.5%, propylene glycol carbonate
0.5%th, titanium dioxide 15%, iron oxide red 0.35%, iron oxide black 0.25%, iron oxide yellow 1.5%, anti-ageing composition 5%, isomery ten
Dioxane surplus.
Wherein, anti-ageing composition is prepared by the raw material of following weight parts：5 parts of motherwort, 5 parts of Pollen of Masson Pine, breast
Fragrant 5 parts, 5 parts of ginseng, 5 parts of shaddock pericarp.
The preparation method of above-mentioned dropper BB frosts, comprises the following steps：
1）A phases raw material is mixed, stirs 25 minutes, is uniformly dispersed, the A phases are Dimethicone Crosspolymer, benzene
The poly- trimethicone of base, isononyl isononanoate, dimethyl silicone polymer, dimethiconol, cetyl poly dimethyl
Siloxanes, ring five dimethyl silicone polymer, cyclohexasiloxane, PEG-10 dimethyl silicone polymers, the bentonite of quaternary ammonium salt -18,
The mixing of HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer, silica, propylene glycol carbonate, isomery dodecane, anti-ageing composition；
Wherein, anti-ageing composition is prepared via a method which to obtain：（1）Motherwort, Pollen of Masson Pine, frankincense, ginseng, shaddock pericarp are mixed
Close, crush, sift out, obtain mixed material；（2）Deep-sea two is added into mixed material and saves shepherd's purse seed oil, is soaked 9 hours, wherein
The weight that shepherd's purse seed oil is saved at deep-sea two is 4 times of mixed material；（3）In step（2）In 20 mL/g ratio in gained mixed material
Petroleum ether is added, Extracting temperature is 60 °C, and under conditions of ultrasonic power is 300W, the ultrasonic extraction time is 30min, vacuum
Filter, be freeze-dried after concentrated by rotary evaporation, obtain anti-ageing composition.
2）B phases raw material is used in dry type toner grinder in advance and ground 4 minutes, obtains mixed-powder then by mixed-powder
Add in A phases, homogeneous 13 minutes, be uniformly dispersed to toner, the B phases are titanium dioxide, iron oxide red, iron oxide black and oxidation
The mixing of iron oxide yellow, wherein titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow can be made as premixing mill base, the mill base
Preparation method be：（1）Titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow are put into dry type toner grinder and ground
Mill 4 minutes, obtain mixed-powder；（2）It is 5 that mass ratio is added into mixed-powder：5 ring five dimethyl silicone polymer, PEG/
PPG-18/18 dimethyl silicone polymers, are uniformly dispersed, and produce dispersion pulp, the addition of the toner dispersant is powder weight
30%；（3）Said mixture is added to circular grinding 4 times in anhydrous clean three-roll grinder, to slurry uniform and smooth,
.
Embodiment 2
A kind of dropper BB frosts, include the component of following mass percent：Dimethicone Crosspolymer 1%, phenyl poly- three
Methylsiloxane 10%, isononyl isononanoate 1%, dimethyl silicone polymer 1%, dimethiconol 0.1%, cetyl poly- two
Methylsiloxane 10%, ring five dimethyl silicone polymer 10%, cyclohexasiloxane 15%, PEG-10 dimethyl silicone polymers 0.5%,
The bentonite of quaternary ammonium salt -18 1.5%, HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer 0.5%, silica 1%, propylene glycol carbonate
0.1%th, titanium dioxide 20%, iron oxide red 0.1%, iron oxide black 0.1%, iron oxide yellow 3%, anti-ageing composition 0.1%, isomery 12
Alkane surplus.
Wherein, anti-ageing composition is prepared by the raw material of following weight parts：1 part of motherwort, 10 parts of Pollen of Masson Pine, breast
Fragrant 1 part, 10 parts of ginseng, 1 part of shaddock pericarp.
The preparation method of above-mentioned dropper BB frosts, comprises the following steps：
1）A phases raw material is mixed, stirs 20 minutes, is uniformly dispersed, the A phases are Dimethicone Crosspolymer, benzene
The poly- trimethicone of base, isononyl isononanoate, dimethyl silicone polymer, dimethiconol, cetyl poly dimethyl
Siloxanes, ring five dimethyl silicone polymer, cyclohexasiloxane, PEG-10 dimethyl silicone polymers, the bentonite of quaternary ammonium salt -18,
The mixing of HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer, silica, propylene glycol carbonate, isomery dodecane, anti-ageing composition；
Wherein, anti-ageing composition is prepared via a method which to obtain：（1）Motherwort, Pollen of Masson Pine, frankincense, ginseng, shaddock pericarp are mixed
Close, crush, sift out, obtain mixed material；（2）Deep-sea two is added into mixed material and saves shepherd's purse seed oil, is soaked 8 hours, wherein
The weight that shepherd's purse seed oil is saved at deep-sea two is 5 times of mixed material；（3）In step（2）In 10 mL/g ratio in gained mixed material
Petroleum ether is added, Extracting temperature is 70 °C, and under conditions of ultrasonic power is 500W, the ultrasonic extraction time is 50min, vacuum
Filter, be freeze-dried after concentrated by rotary evaporation, obtain anti-ageing composition.
2）B phases raw material is used in dry type toner grinder in advance and ground 3 minutes, obtains mixed-powder then by mixed-powder
Add in A phases, homogeneous 15 minutes, be uniformly dispersed to toner, the B phases are titanium dioxide, iron oxide red, iron oxide black and oxidation
The mixing of iron oxide yellow, wherein titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow can be made as premixing mill base, the mill base
Preparation method be：（1）Titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow are put into dry type toner grinder and ground
Mill 3 minutes, obtain mixed-powder；（2）It is 3 that mass ratio is added into mixed-powder：7 ring five dimethyl silicone polymer, PEG/
PPG-18/18 dimethyl silicone polymers, are uniformly dispersed, and produce dispersion pulp, the addition of the toner dispersant is powder weight
20%；（3）Said mixture is added to circular grinding 3 times in anhydrous clean three-roll grinder, to slurry uniform and smooth,
.
Embodiment 3
A kind of dropper BB frosts, include the component of following mass percent：Dimethicone Crosspolymer 10%, phenyl gather
Trimethicone 1%, isononyl isononanoate 5%, dimethyl silicone polymer 0.1%, dimethiconol 1%, cetyl gather
Dimethyl siloxane 1%, ring five dimethyl silicone polymer 30%, cyclohexasiloxane 5%, PEG-10 dimethyl silicone polymers 1.5%,
The bentonite of quaternary ammonium salt -18 0.5%, HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer 3%, silica 0.1%, propylene glycol carbonate
1%th, titanium dioxide 10%, iron oxide red 0.5%, iron oxide black 0.5%, iron oxide yellow 0.1%, anti-ageing composition 10%, isomery 12
Alkane surplus.
Wherein, anti-ageing composition is prepared by the raw material of following weight parts：10 parts of motherwort, 1 part of Pollen of Masson Pine, breast
Fragrant 10 parts, 1 part of ginseng, 10 parts of shaddock pericarp.
The preparation method of above-mentioned dropper BB frosts, comprises the following steps：
1）A phases raw material is mixed, stirs 30 minutes, is uniformly dispersed, the A phases are Dimethicone Crosspolymer, benzene
The poly- trimethicone of base, isononyl isononanoate, dimethyl silicone polymer, dimethiconol, cetyl poly dimethyl
Siloxanes, ring five dimethyl silicone polymer, cyclohexasiloxane, PEG-10 dimethyl silicone polymers, the bentonite of quaternary ammonium salt -18,
The mixing of HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer, silica, propylene glycol carbonate, isomery dodecane, anti-ageing composition；
Wherein, anti-ageing composition is prepared via a method which to obtain：（1）Motherwort, Pollen of Masson Pine, frankincense, ginseng, shaddock pericarp are mixed
Close, crush, sift out, obtain mixed material；（2）Deep-sea two is added into mixed material and saves shepherd's purse seed oil, is soaked 10 hours, its
The weight that shepherd's purse seed oil is saved in mesopelagic (200 meter Dao1000 meter Shui Shen) two is 4 times of mixed material；（3）In step（2）30 mL/g ratio is pressed in gained mixed material
Example adds petroleum ether, and Extracting temperature is 40 °C, and under conditions of ultrasonic power is 100W, the ultrasonic extraction time is 10min, vacuum
Filter, be freeze-dried after concentrated by rotary evaporation, obtain anti-ageing composition.
2）B phases raw material is used in dry type toner grinder in advance and ground 5 minutes, obtains mixed-powder then by mixed-powder
Add in A phases, homogeneous 15 minutes, be uniformly dispersed to toner, the B phases are titanium dioxide, iron oxide red, iron oxide black and oxidation
The mixing of iron oxide yellow, wherein titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow can be made as premixing mill base, the mill base
Preparation method be：（1）Titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow are put into dry type toner grinder and ground
Mill 3 minutes, obtain mixed-powder；（2）It is 1 that mass ratio is added into mixed-powder：10 ring five dimethyl silicone polymer, PEG/
PPG-18/18 dimethyl silicone polymers, are uniformly dispersed, and produce dispersion pulp, the addition of the toner dispersant is powder weight
40%；（3）Said mixture is added to circular grinding 5 times in anhydrous clean three-roll grinder, to slurry uniform and smooth,
.
Embodiment 4
A kind of dropper BB frosts, include the component of following mass percent：Dimethicone Crosspolymer 3%, phenyl poly- three
Methylsiloxane 7%, isononyl isononanoate 4%, dimethyl silicone polymer 0.3%, dimethiconol 0.8%, cetyl gather
Dimethyl siloxane 8%, ring five dimethyl silicone polymer 25%, cyclohexasiloxane 7%, PEG-10 dimethyl silicone polymers 0.9%,
The bentonite of quaternary ammonium salt -18 0.8%, HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer 2%, silica 0.6%, propylene glycol carbonate
0.7%th, titanium dioxide 14%, iron oxide red 0.2%, iron oxide black 0.4%, iron oxide yellow 2%, anti-ageing composition 7%, isomery dodecane
Surplus.
Wherein, anti-ageing composition is prepared by the raw material of following weight parts：8 parts of motherwort, 2 parts of Pollen of Masson Pine, breast
Fragrant 3 parts, 7 parts of ginseng, 4 parts of shaddock pericarp.
The preparation method of above-mentioned dropper BB frosts, comprises the following steps：
1）A phases raw material is mixed, stirs 23 minutes, is uniformly dispersed, the A phases are Dimethicone Crosspolymer, benzene
The poly- trimethicone of base, isononyl isononanoate, dimethyl silicone polymer, dimethiconol, cetyl poly dimethyl
Siloxanes, ring five dimethyl silicone polymer, cyclohexasiloxane, PEG-10 dimethyl silicone polymers, the bentonite of quaternary ammonium salt -18,
The mixing of HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer, silica, propylene glycol carbonate, isomery dodecane, anti-ageing composition；
Wherein, the anti-ageing composition is prepared via a method which to obtain：（1）By motherwort, Pollen of Masson Pine, frankincense, ginseng, shaddock fruit
Skin mixes, and crushes, sifts out, obtain mixed material；（2）Deep-sea two is added into mixed material and saves shepherd's purse seed oil, is soaked 9 hours,
The weight of its mesopelagic (200 meter Dao1000 meter Shui Shen) two section shepherd's purse seed oil is 4 times of mixed material；（3）In step（2）By 25mL/g's in gained mixed material
Ratio adds petroleum ether, and Extracting temperature is 50 °C, and under conditions of ultrasonic power is 400W, the ultrasonic extraction time is 20min,
It is filtered by vacuum, is freeze-dried after concentrated by rotary evaporation, obtains anti-ageing composition.
2）B phases raw material is used in dry type toner grinder in advance and ground 5 minutes, obtains mixed-powder then by mixed-powder
Add in A phases, homogeneous 10 minutes, be uniformly dispersed to toner, the B phases are titanium dioxide, iron oxide red, iron oxide black and oxidation
The mixing of iron oxide yellow, wherein titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow can be made as premixing mill base, the mill base
Preparation method be：（1）Titanium dioxide, iron oxide red, iron oxide black and iron oxide yellow are put into dry type toner grinder and ground
Mill 5 minutes, obtain mixed-powder；（2）It is 10 that mass ratio is added into mixed-powder：1 ring five dimethyl silicone polymer, PEG/
PPG-18/18 dimethyl silicone polymers, are uniformly dispersed, and produce dispersion pulp, the addition of the toner dispersant is powder weight
50%；（3）Said mixture is added to circular grinding 5 times in anhydrous clean three-roll grinder, to slurry uniform and smooth,
.
Comparative example 1
The difference of comparative example 1 and embodiment 1 is comparative example 1 not comprising motherwort, Pollen of Masson Pine.
Comparative example 2
The difference of comparative example 1 and embodiment 1 is comparative example 1 not comprising frankincense, ginseng, shaddock pericarp.
Comparative example 3
The difference of comparative example 3 and embodiment 1 in comparative example 2 toner be not prepared into dispersion pulp.
The dropper BB frosts using effect of experimental example 1 is tested
Each 20 of Example 1-4, comparative example 1-2 BB frost respectively, recruits healthy volunteer 20, respectively using 28 days above-mentioned 6
Kind BB frosts are tested.Using actual use sense organ and visual assessment, 5 points represent, 4 points represent preferable, and 3 points represent general, 2
Divide and represent poor, 1 point of expression is poor;Record data after 20 people evaluation, averages.Such as table 1 below is commented after use：
Table 1
| Trial target | Makeup effect is frivolous | Hide the flaw | It is easy to use | Viscosity | Skin elasticity |
| Embodiment 1 | 5.0 | 4.7 | 4.8 | 4.7 | 5.0 |
| Embodiment 2 | 4.8 | 4.5 | 4.6 | 4.9 | 4.9 |
| Embodiment 3 | 4.5 | 4.3 | 4.7 | 4.8 | 4.7 |
| Embodiment 4 | 4.6 | 4.2 | 4.1 | 4.5 | 4.8 |
| Comparative example 1 | 2.4 | 2.6 | 2.5 | 2.8 | 2.0 |
| Comparative example 2 | 2.3 | 25 | 2.4 | 2.7 | 2.1 |
| Comparative example 3 | 2.8 | 2.7 | 2.8 | 3.0 | 3.0 |
According to the test result shown in above-mentioned table 1, it can be seen that the dropper BB frosts of embodiments of the invention 14 have significant
Makeup effect is frivolous, hides the characteristics of flaw is good, easy to use, viscosity is low, skin elasticity is good.
The foregoing is only a preferred embodiment of the present invention, not makees any formal limitation to the present invention；It is all
The those of ordinary skill of the industry can be described in by specification and described above and swimmingly implement the present invention；It is but all familiar
Professional and technical personnel without departing from the scope of the present invention, makes using disclosed above technology contents
A little variation, modification and evolution equivalent variations, be the present invention equivalent embodiment；Meanwhile all realities according to the present invention
Variation, modification and evolution of any equivalent variations that matter technology is made to above example etc., still fall within the technology of the present invention
Within the protection domain of scheme.
Claims (8)
1. a kind of dropper BB frosts, it is characterised in that include the component of following mass percent：
Dimethicone Crosspolymer 1-10%
Phenyl trimethicone 1-10%
Isononyl isononanoate 1-5%
Dimethyl silicone polymer 0.1-1%
Dimethiconol 0.1-1%
Cetyl dimethicone 1-10%
Ring five dimethyl silicone polymer 10-30%
Cyclohexasiloxane 5-15%
PEG-10 dimethyl silicone polymers 0.5-1.5%
The bentonite of quaternary ammonium salt -18 0.5-1.5%
HDI/ trihydroxy methyl hexyl Inner ester cross-linked polymers 0.5-3%
Silica 0.1-1%
Propylene glycol carbonate 0.1-1%
Titanium dioxide 10-20%
Iron oxide red 0.1-0.5%
Iron oxide black 0.1-0.5%
Iron oxide yellow 0.1-3%
Isomery dodecane surplus.
2. a kind of dropper BB frosts according to claim 1, it is characterised in that the BB frosts are also anti-ageing including 0.1-10%
Composition, the anti-ageing composition are prepared by the raw material of following weight parts：Motherwort 1-10 parts, Pollen of Masson Pine 1-10
Part, frankincense 1-10 parts, ginseng 1-10 parts, shaddock pericarp 1-10 parts.
3. a kind of dropper BB frosts according to claim 2, it is characterised in that the anti-ageing composition is made by the following method
It is standby to obtain：（1）Motherwort, Pollen of Masson Pine, frankincense, ginseng, shaddock pericarp are mixed, is crushed, is sifted out, obtain mixed material；
（2）Deep-sea two is added into mixed material and saves shepherd's purse seed oil, is soaked 8-10 hours, the weight of its mesopelagic (200 meter Dao1000 meter Shui Shen) two section shepherd's purse seed oil is mixed
Close raw material 4-5 times；（3）In step（2）In gained mixed material petroleum ether, extraction temperature are added in 10 30 mL/g ratio
Spend for 40 DEG C 80 DEG C, under conditions of ultrasonic power is 100W 500W, the ultrasonic extraction time is 10 50min, vacuum
Filter, be freeze-dried after concentrated by rotary evaporation, obtain anti-ageing composition.
4. a kind of dropper BB frosts according to claim 1, it is characterised in that the titanium dioxide, iron oxide red, iron oxide
Black and iron oxide yellow is the toner of surface treatment, and the surface conditioning agent is triethoxy octyl group silane.
5. a kind of dropper BB frosts according to claim 4, it is characterised in that the toner is to premix mill base, the mill base
Preparation method be：（1）Each toner is put into grinding 3-5 minutes in dry type toner grinder, obtains mixed-powder；（2）To mixed
Close and toner dispersant is added in powder, stir and obtain mixture；（3）Said mixture is added to anhydrous three clean rollers
Circular grinding 3-5 times in grinder, to slurry uniform and smooth, you can.
6. a kind of dropper BB frosts according to claim 5, it is characterised in that the toner dispersant is by the poly dimethyl of ring five
Siloxanes, PEG/PPG-18/18 dimethyl silicone polymers composition, the addition of the toner dispersant is mixed-powder weight
20-50%。
7. a kind of dropper BB frosts according to claim 6, it is characterised in that the ring five dimethyl silicone polymer, PEG/
The mass ratio of PPG-18/18 dimethyl silicone polymers is（1-10）：（1-10）.
A kind of 8. method of a kind of dropper BB frosts prepared as described in claim any one of 1-7, it is characterised in that including following
Step：
1）By A phases raw material mix, stir 20-30 minutes, be uniformly dispersed, the A phases be Dimethicone Crosspolymer,
The poly- diformazan of phenyl trimethicone, isononyl isononanoate, dimethyl silicone polymer, dimethiconol, cetyl
Radical siloxane, ring five dimethyl silicone polymer, cyclohexasiloxane, PEG-10 dimethyl silicone polymers, the bentonite of quaternary ammonium salt -18
, HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer, silica, propylene glycol carbonate, isomery dodecane, anti-ageing composition it is mixed
Close；
2）B phases raw material is used in advance 3-5 minutes are ground in dry type toner grinder, obtained mixed-powder and then add mixed-powder
Enter in A phases, homogeneous 10-15 minutes, be uniformly dispersed to toner, the B phases are titanium dioxide, iron oxide red, iron oxide black and oxygen
Change the mixing of iron oxide yellow.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710979316.3A CN107714496A (en) | 2017-10-19 | 2017-10-19 | A kind of dropper BB frosts and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710979316.3A CN107714496A (en) | 2017-10-19 | 2017-10-19 | A kind of dropper BB frosts and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108888524A (en) * | 2018-08-10 | 2018-11-27 | 广州市科能化妆品科研有限公司 | Concealing composition and preparation method thereof |
| EP4129416A4 (en) * | 2020-04-01 | 2024-04-24 | Kao Corp | Topical skin preparation composition |
-
2017
- 2017-10-19 CN CN201710979316.3A patent/CN107714496A/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108888524A (en) * | 2018-08-10 | 2018-11-27 | 广州市科能化妆品科研有限公司 | Concealing composition and preparation method thereof |
| CN108888524B (en) * | 2018-08-10 | 2021-06-18 | 广州市科能化妆品科研有限公司 | Concealer composition and process for producing the same |
| EP4129416A4 (en) * | 2020-04-01 | 2024-04-24 | Kao Corp | Topical skin preparation composition |
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