CN105411944B - Application and oil tea face mask cream of the oil tea in terms of beauty skin care product is prepared - Google Patents
Application and oil tea face mask cream of the oil tea in terms of beauty skin care product is prepared Download PDFInfo
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- CN105411944B CN105411944B CN201510977975.4A CN201510977975A CN105411944B CN 105411944 B CN105411944 B CN 105411944B CN 201510977975 A CN201510977975 A CN 201510977975A CN 105411944 B CN105411944 B CN 105411944B
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a kind of application of oil tea in terms of beauty skin care product is prepared and oil tea face mask cream.The present invention is applied to prepare beauty skin care product using oil tea Ultramicro-powder and oil tea flower extract as skin conditioning agent.By weight percentage, the face mask cream is formed by oil tea Ultramicro-powder 10~70%, oil tea flower extract 10~50%, tea oil 5~30% and the auxiliaries such as hyaluronic acid, Sodium Hyaluronate, collagen, milk, honey.Face mask cream of the present invention is using nutritious crude vegetal camellia and tea oil as primary raw material, the two active effect brings out the best in each other, the oxidation-resistant active ingredient being rich in can deep layer conditioning skin state, effectively discharge toxin and free radical, and be equipped with tea oil, there is provided more horn of plenty, be more easy to by the nutritional ingredient of percutaneous absorption.Face mask cream does not add any chemical composition, and property is gentle, non-stimulated and toxic side effect.Preparation technology of the present invention is simple, and technological parameter is easily controlled, and contributes to rational exploitation and utilization oil tea resource.
Description
Technical field
The present invention relates to skin nursing products technical field, and beauty and skin care is being prepared more particularly, to a kind of oil tea
Application and oil tea face mask cream in terms of product.
Background technology
As the improvement of people's living standards, requirement of consumer's especially female consumer to skin nursing is increasingly
Height, " back to nature ", " green consumption " turn into fashion；In addition, the cosmetic health product and nursing product of plant component are with the addition of, because
Its plant component molecular weight is smaller, the effect of rapidly permeating into skin and play its maintenance skin.Therefore, natural environmental-protective type adds
" the green cosmetics " of agent have welcome unprecedented opportunity to develop.
Facial mask is a kind of carrier of skin health products, and facial mask suppresses sebum secretion by obstructing contact of the skin with air
Skin temperature is increased with evaporation of perspiration, so as to stimulate circulation, beneficial to the active ingredient in facial mask penetrate into epidermis or
Deeper, wider array of place, after absorbing more juicy, nutrition elite and various active ingredients so as to skin, flesh can be effectively improved
Skin state.
Face mask cream is a kind of facial mask type emerging in recent years, and it can be close with skin site of action in the long period
Stick, so as to increase the keratoderma transit dose of effect material, nutritional ingredient is beneficial to absorb, cleaning, moisturizing, moist and other effects
It can give full play to；In addition, face mask cream can arbitrarily change applying amount, coating thickness, spreader portion according to the different demands of user
Position can voluntarily control with user；It is a kind of good facial mask form.
Oil tea is the accessory substance of oil tea resource, and oil tea is the distinctive woody oleiferous plants crop in China, mainly in China the Changjiang river
Basin and areas to the south's plantation, are distributed in 18 provinces such as Hunan, Jiangxi, Guangxi, Guangdong, Fujian, Anhui, Yunnan（Area）.Oil tea
It is cross pollinated species（Complete to pollinate mainly by insect）, bloom March annual October to next year, many oil teas do not award powder then
Do not form fruit, can also influence percentage of fertile fruit while wasting trunk infusion.So in order to ensure the lasting high yield of camellia oleifera fruit and
High-quality fruit, it can typically take and artificially remove the excessive flower in part, therefore oil tea resource is very abundant, and develop obvious
Hysteresis, cause the serious waste of natural resources.The applicant has found that oil tea is rich in plurality kinds of health care composition, such as through studying for a long period of time
Protein, amino acid, vitamin C, polyphenol, polysaccharide, flavones, anthocyanidin etc., there is anti-oxidant, anti-aging, improve immunity etc.
Physiological function, external application, which has, to be maintained good metabolism, keeps skin gloss, effectively remove free radical, repair impaired skin etc.
Effect.
Tea oil, also known as camellia seed oil,CamelliaOil, be fromTheaceae CamelliaPlant it is commonOil tea（Camellia
oleifera Abel）The pure natural high edible vegetable oil extracted in mature seed, golden yellow color or pale yellow, quality is pure, clear
It is clear bright, smell delicate fragrance, good taste.The ratio of saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid in tea oil
Example is 8:83:9, it is very close with the lipid of human body skin, meet very much the needs of human body, and be also rich in VE, the battalion such as squalene
Form point.
Have no at present and be applied to oil tea to prepare beauty skin care product, including face mask cream product.If oil tea can be developed
The beauty skin care product of flower and tea oil, can not only make full use of ignored oil tea resource, reach the purpose to turn waste into wealth,
And for exploitation natural component based on face mask cream, provide more more options for consumer, tool is of great significance.
The content of the invention
The technical problem to be solved in the present invention is the technology for filling up existing beauty skin care product and the oil tea utilization of resources
Deficiency, there is provided application of the oil tea in terms of beauty skin care product is prepared.
Another technical problem to be solved by the present invention is that specifically providing a kind of facial mask paste formulation, the face mask cream is naturally to plant
Raw material oil tea primary raw material, product property is gentle, it is non-stimulated, have no toxic side effect.
The invention solves an also technical problem be to provide the preparation method of the oil tea face mask cream.
The purpose of the present invention is achieved by the following technical programs：
A kind of application of oil tea in terms of beauty skin care product is prepared is provided, will be specifically prepared using oil tea
Oil tea Ultramicro-powder and oil tea flower extract, will both as main skin conditioning agent be applied to prepare beauty and skin care production
Product.
The micron powder that the oil tea Ultramicro-powder crushes to obtain using drier oil camellia；The oil tea flower extract is to adopt
Extract to obtain with green oil camellia, with ethanol Extraction solvent.
Preferably, the particle diameter of the micron powder is less than 10 μm.
Preferably, the volume fraction of ethanol is 20~90%.
It is further preferred that the preparation of the oil tea Ultramicro-powder comprises the following steps：
S11. through the drying process that finishes after green oil camellia is cleaned using deionized water；
S12. the oil tea coarse crushing handled through step S11 is obtained into coarse powder；
S13. it will further be crushed using superfine technique through coarse powder obtained by step S12 and obtain fine powder, and reach fine powder
Micron order.
Preferably, the drying process that finished described in step S11 is that the moisture for drying oil tea to oil tea is less than 6%.
Preferably, the drying process that finished described in step S11 is carried out using the united mode of microwave vacuum, and process conditions are micro-
200~600W of wave power, 30~100kPa of vacuum, 10~60min of time.
Preferably, the particle diameter of coarse powder described in step S12 is 100~200 μm.
Preferably, the particle diameter of the micron powder described in step S13 is less than 10 μm.
Preferably, it is molten to extract using ethanol for raw material after the preparation of the oil tea flower extract is crushed with green oil camellia
Agent, it is concentrated to give again through cryogenic vacuum after ultrasonic assistant extracts.
The ultrasonic assistant extraction conditions are：It is 200~800 μm that green oil camellia, which is crushed to particle diameter, ethanol volume integral
Number is 20~90%, according to oil tea pollen and the g of ethanol 1:2~15mL ratio is mixed, ultrasonic power be 140~
560W, ul-trasonic irradiation time are 30~90min.
Preferably, the volume fraction of ethanol is 50%~70%.
Preferably, the mixed proportion of the oil tea pollen and ethanol is 1 g:5~8mL ethanol.
Preferably, the ultrasonic power is 300~500W.
Preferably, the ul-trasonic irradiation time is 40~60min.
It is further preferred that when being extracted using ultrasonic assistant, powder particle diameter is used as 200~400 μm of fresh oil tea
Flower, volume fraction of ethanol is 50%~70%, according to oil tea pollen and the g of ethanol 1:5~8mL ratio is mixed, ultrasonic wave work(
Rate is 300~500W, and extraction time is 40~60min, obtains oil tea extract solution.
Obtained oil tea extract solution will be extracted to concentrate by cryogenic vacuum, preferable cryogenic vacuum concentration condition for 40~
50 DEG C, 10~15kPa, finally give oil tea flower extract.The oil tea flower extract being prepared using extracting method of the present invention,
Wherein soluble solid content is 40~50%（Mass percent）, and the biology remained in oil tea of high degree is living
Property composition and color and luster, obtaining good application effect applied to when preparing beauty skin care product.
Preferably, described oil tea includes common white flower oil camellia and safflower oil camellia, including but not limited to including Zhejiang
River safflower oil camellia, Tengchong safflower oil camellia, C. semisererata are colored, as if field safflower oil camellia, Camellia gigantocarpa are colored and rattan
Big fruit oil tea in county etc..Select wherein that pattern is normal, petal is complete, the flower of no disease and pests harm；Remove blade, grass cuttings and badly broken
Flower；Then rinsed well with deionized water, obtain green oil camellia.
Application of the oil tea of the present invention in terms of beauty skin care product is prepared, it is preferable that the beauty skin care product
For oil tea face mask cream.
The present invention provides a kind of preferable oil tea face mask cream, using oil tea Ultramicro-powder and oil tea flower extract as main
Skin conditioning agent, the oil tea is prepared in compounding moisturizing grease, NMF, nourishing additive agent, thickener, solvent and auxiliary material
Flower face mask cream.
Preferably, the moisturizing grease selects tea oil.Tea oil is cooler, there is heat-clearing, removing toxic substances；It is unsaturated in tea oil
Content of fatty acid is up to 90%, rich in VE, the nutritional ingredient such as squalene, and saturated fatty acid in tea oil, monounsaturated fatty acids with
The ratio of polyunsaturated fatty acid is 8:83:9, it is very close with the lipid of human body skin, meet very much the needs of human body, with suitable
When ratio and oil tea pollen and oil tea flower extract compatibility after be applied to skin, be readily absorbed by, play nutrition moisturizing effect.
Preferably, the NMF selects hyaluronic acid, Sodium Hyaluronate and glycerine.Hyaluronic acid/sodium is protected as natural
The wet factor, in the present invention with reference to glycerine, strengthen moistening effect, maintain the water and oil balance of oil tea face mask cream, science ratio
The greasy feeling used using facial mask of the present invention is effectively reduced.
Preferably, the nourishing additive agent selects collagen, milk and honey.Collagen is to repair skin damage group
The important source material knitted, moisture, support Skin Cell can be pinned, improve the elastic and moist sense of skin.Compounded ox
Milk and honey, milk and honey collectively constitute natural nutrient substance with oil tea active ingredient, and bioactive ingredients pole is beneficial to quilt
Skin Cell absorbs, and is effectively improved the nutritional status of skin.
Preferably, the thickener selects pectin.Pectin is a kind of acidic polysaccharose material from plants such as fruit, as
Food raw material, it is common to play in facial mask of the present invention, being complemented each other with oil tea pollen, oil tea flower extract and tea oil
To protection skin, the effect of ultraviolet radiation, beautifying face and moistering lotion is prevented, and all belongs to pure natural pollution-free.
Preferably, the preparing raw material of the oil tea face mask cream includes each component of following percentage by weight：
Oil tea Ultramicro-powder 10~70%；
Oil tea flower extract 10~50%；
Tea oil 5~30%；
Hyaluronic acid 0.5~10%；
Sodium Hyaluronate 0.5~10%；
Collagen 0.5~5%；
Milk 0.5~5%；
Honey 0.5~5%；
Pectin 0.5~5%；
Glycerine 0.5~3%；
Propane diols 2~10%；
Essence 0.05~2%
Deionized water surplus.
It is further preferred that the preparing raw material of the oil tea face mask cream includes each component of following percentage by weight：
Oil tea Ultramicro-powder 20~40%；
Oil tea flower extract 20~30%；
Tea oil 5~20%；
Hyaluronic acid 2~5%；
Sodium Hyaluronate 2~5%；
Collagen 1~3%；
Milk 0.5~2%；
Honey 0.5~2%；
Pectin 0.5~2%；
Glycerine 2~3%；
Propane diols 2~6%；
Essence 0.05~0.5%
Deionized water surplus.
Not only stability, thickening degree are good for the face mask cream being prepared under formula of the present invention；And moisturizing, moisturizing
Effect is good, and greasy feeling is also weaker；The compositions such as anti-oxidant, nourishing whitening therein can be good at by percutaneous absorption, deep layer conditioning
Skin state, discharge toxin and free radical are played, strengthen skin metabolism, soft brilliant white and other effects.
The present invention also provides the preparation method of the oil tea face mask cream raw material simultaneously, in foregoing wherein primary raw material component oil
Camellia Ultramicro-powder, oil tea flower extract preferable preparation method on the basis of, it is further provided the preferable preparation method of tea oil：Institute
It is using the camellia seed kernel after shelling as raw material, using ultrasonic assistant aqueous enzymatic extraction to state tea oil.Methods described extracts what is obtained
Tea oil purity is high, and content of phospholipid, acid number and peroxide value are low, and lighter color, smell is good, and pollution is few, reaches and is better than first-level tea oil
Standard, meet external preparation for skin.Moreover, the tea oil fully remains neutraceutical active ingredients, wherein unsaturated fatty acid content
It is 200~220mg/Kg up to 85%~90%, VE contents, squalene content is 150~180 mg/Kg.
The enzyme that the aqueous enzymatic method uses can be protease, cellulase, pectase, alpha-amylase or complex enzyme etc. its
In one or more.Most preferably, the complex enzyme combined when extracting tea oil in the present invention using protease with cellulase, it is excellent
Sortilin enzyme:The ratio of cellulase is 4:1.
The ultrasonic assistant aqueous enzymatic extraction condition is：New camellia seed kernel and water enzyme ratio 1:（3~10）（g/mL）, enzyme
Dosage 1%~5%, 30 DEG C~80 DEG C, enzymolysis time 1h~8h of hydrolysis temperature, enzymolysis pH4~9, ultrasonic power 100W~600W,
Ultrasonic time 10min~60min.
The camellia seed kernel grinding particle size preferably 20~60 mesh.
When preferably, using ultrasonic assistant aqueous enzymatic extraction tea oil, camellia seed kernel pulverizes and sieves 20~40 mesh, solid-liquid ratio
1:（5~8）（g/mL）, enzyme dosage 2~4%, 50 DEG C~60 DEG C, enzymolysis time 5h~7h of hydrolysis temperature, digest pH6~7, ultrasound
Wave power 300W~500W, ultrasonic time 30min~40min.
Specifically, the present invention provides the preparation method of the oil tea face mask cream, is the oil tea ultra micro that will be prepared
Powder, oil tea flower extract and tea oil are mixed in proportion, and collagen, hyaluronic acid, Sodium Hyaluronate, fruit are added according still further to formula
Glue, milk, honey, glycerine, propane diols and deionized water are abundant with Homogenized emulsifier then under 300~600r/min of rotating speed
Stirring, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, stirs discharge bubble, and cooling is
Obtain oil tea face mask cream.
The invention has the advantages that：
The invention provides a kind of new opplication of oil tea, and oil tea Ultramicro-powder and oil tea flower extract are adjusted as skin
Agent is managed, by dermal sensitivity test, oil tea property is gentle, and skin is had no stimulation, and is to make external application cosmetic health product
Desirable feedstock.In addition, oil tea and another resource tea oil compatibility of oil tea, therefore, the present invention is with crude vegetal camellia and tea oil
For primary raw material, coordinate appropriate auxiliary material, develop that a kind of safety is gentle, the non-stimulated, facial mask that has no toxic side effect.It is not only fully sharp
With ignored oil tea resource, reach the purpose to turn waste into wealth, and develop the face mask cream based on natural component, be consumer
More more options are provided, tool is of great significance.After testing, various nutritional ingredients in the oil tea flower extract, anti-oxidant
Component content enriches, and protein content is 4% ~ 10%, and amino acid content is 2% ~ 5%, VCContent is 2% ~ 5%, polyphenol content 10%
~ 15%, polyoses content is 10% ~ 20%, and flavones content is 38% ~ 45%, and anthocyanidin content is 8% ~ 12%；And there is very strong removing
Free radical ability, more than 95% is all reached to the clearance rate of the free radicals such as DPPH, OH and O2-.Oil tea Ultramicro-powder and oil
Both Flos Camelliae Japonicae extracts complement each other, brought out the best in each other, and are applied to skin and are readily absorbed by；There is preferable beauty and health care work(to skin
Effect.
Further, other selected key components of the present invention, face mask cream of the present invention is based on pure plant oil tea
The NMF such as nourishing additive agent, hyaluronic acid/sodium, glycerine such as raw material, comprehensive tea oil, milk, honey, collagen is wanted to make jointly
For skin, the effect of playing beauty and health care.Main component is oil tea Ultramicro-powder, oil tea flower extract in face mask cream of the present invention
And tea oil, the nutrition and antioxidant content enriched in oil tea can effectively discharge skin toxins, prevent free radical from attacking, effectively
Improve skin metabolism, strengthen skin updating ability；Saturated fatty acid, monounsaturated fatty acids and how unsaturated fat in tea oil
The ratio of fat acid and the lipid of human body skin are closely similar, are applied to skin and are easily absorbed by the skin, and tea oil is rich in VEWith
The materials such as angle alkene shark, play anti-aging, improve skin immunity and other effects.
Oil tea face mask cream stability of the present invention, viscosity are good, and lotion is moist, and color and luster is suitable, and fragrance is clear
Feel well and have the distinctive fragrance of oil tea, smear favorable dispersibility and without greasy feeling, there is very strong moisturizing, soft effect to skin.
The face mask cream is heat-resisting, cold-resistant, light fastness is qualified；PH is in faintly acid, close to the pH value of human body skin；Property is gentle, stingless
Sharp and toxic side effect, suitable for various skin quality, it is especially suitable for sensitive skin.
The performances such as organoleptic indicator, physical and chemical index to oil tea face mask cream of the present invention are measured.After testing, present invention oil
Stability, the viscosity of camellia are good, and lotion is moist, and stretchability is preferable, and color and luster is in light yellow, slightly micro- red, and fragrance is clear
Refreshing suitable and have the peculiar fragrance of oil tea, humidity-preserving type is stronger.Observed by measure, oil tea face mask cream of the present invention is heat-resisting, resistance to
It is cold, light fastness is qualified, pH value is in faintly acid, close to the pH of human body skin.
Embodiment
With reference to embodiment, the present invention is described in further detail, but embodiments of the present invention be not limited to it is described
Embodiment.Unless stated otherwise, the present invention uses raw material, apparatus and method for this area usual sources and the raw material used,
Apparatus and method.
The preparation of the oil tea face mask cream primary raw material of the present invention of embodiment 1
The preparation technology flow of several primary raw material compositions specifically includes following steps in oil tea face mask cream：
S11. feedstock oil camellia is plucked, selected：The present embodiment using Camellia chekiangoleosa flower as raw material, select no disease and pests harm,
Pattern is scarlet, the complete oil tea of petal, and removes the blade and blemished flowers being wherein mingled with, and is rinsed well with deionized water；
S12. feedstock oil camellia drying process：The green oil camellia for taking a part to rinse well, suitably removes surface moisture
Afterwards, fixing drying process is carried out using microwave vacuum associated form, parameter setting is：Microwave power 400W, vacuum 75kPa,
Time 30min；Dry oil tea moisture is finally measured as 5.8%；
S13. oil tea Ultramicro-powder is prepared：Take dried oil tea first to carry out coarse crushing using medicinal herb grinder, cross 60
Mesh sieve, then the corase meal after sieving is carried out being crushed to micron order using oscillatory type super fine machine.
The preparation of the oil tea face mask cream primary raw material of the present invention of embodiment 2
The preparation technology flow of several primary raw material compositions specifically includes following steps in oil tea face mask cream：
S11. feedstock oil camellia is plucked, selected：The present embodiment using C. semisererata flower as raw material, select no disease and pests harm,
Big and gorgeous, the complete oil tea of petal is spent, and removes the blade and blemished flowers being wherein mingled with, is rinsed well with deionized water；
S12. feedstock oil camellia drying process：The green oil camellia for taking a part to rinse well, suitably removes surface moisture
Afterwards, fixing drying process is carried out using microwave vacuum associated form, parameter setting is：Microwave power 200W, vacuum 100kPa,
Time 60min；Dry oil tea moisture is finally measured as 5.3%；
S13. oil tea Ultramicro-powder is prepared：Take dried oil tea first to carry out coarse crushing using medicinal herb grinder, cross 60
Mesh sieve, then the corase meal after sieving is carried out being crushed to micron order using oscillatory type super fine machine.
The preparation of the oil tea face mask cream primary raw material of the present invention of embodiment 3
The preparation technology flow of several primary raw material compositions specifically includes following steps in oil tea face mask cream：
S11. feedstock oil camellia is plucked, selected：The present embodiment using common white flower oil camellia as raw material, select no disease and pests harm,
Pattern is pure white, the complete oil tea of flower pattern, and removes the blade and blemished flowers being wherein mingled with, and is rinsed well with deionized water；
S12. feedstock oil camellia drying process：The green oil camellia for taking a part to rinse well, suitably removes surface moisture
Afterwards, fixing drying process is carried out using microwave vacuum associated form, parameter setting is：Microwave power 600W, vacuum 200kPa,
Time 45min；Dry oil tea moisture is finally measured as 5.1%；
S13. oil tea Ultramicro-powder is prepared：Take dried oil tea first to carry out coarse crushing using medicinal herb grinder, cross 100
Mesh sieve, then the corase meal after sieving is carried out being crushed to micron order using oscillatory type super fine machine.
Embodiment 4 prepares oil tea flower extract
40 mesh sieves crushed as raw material using green oil camellia, using 60% ethanol as Extraction solvent, according to 1g:6mL ratio
Mixing, is extracted, processing parameter setting is by ultrasonic assistant：Ultrasonic power 400W, ul-trasonic irradiation time 50min；Carry
The extract solution obtained is concentrated by cryogenic vacuum, temperature 50 C, vacuum 13kPa, finally gives required oil tea extraction
Thing, it is 43.7% to measure wherein soluble solid content.After testing, wherein protein content is 4%~10%, amino acid content
For 2%~5%, VCContent be 2%~5%, polyphenol content be 10%~15%, polyoses content be 10%~20%, flavones content be 38%~
45%, anthocyanidin content is 8%~12%.
Embodiment 5 prepares oil tea flower extract
40 mesh sieves crushed as raw material using green oil camellia, using 50% ethanol as Extraction solvent, according to 1g:6mL ratio
Mixing, is extracted, processing parameter setting is by ultrasonic assistant：Ultrasonic power 400W, ul-trasonic irradiation time 50min；Carry
The extract solution obtained is concentrated by cryogenic vacuum, temperature 50 C, vacuum 13kPa, finally gives required oil tea extraction
Thing, it is 42.5% to measure wherein soluble solid content.After testing, wherein protein content is 4%~10%, amino acid content
For 2%~5%, VCContent be 2%~5%, polyphenol content be 10%~15%, polyoses content be 10%~20%, flavones content be 38%~
45%, anthocyanidin content is 8%~12%.
Embodiment 6 prepares oil tea flower extract
40 mesh sieves crushed as raw material using green oil camellia, using 70% ethanol as Extraction solvent, according to 1g:6mL ratio
Mixing, is extracted, processing parameter setting is by ultrasonic assistant：Ultrasonic power 400W, ul-trasonic irradiation time 50min；Carry
The extract solution obtained is concentrated by cryogenic vacuum, temperature 50 C, vacuum 13kPa, finally gives required oil tea extraction
Thing, it is 44.3% to measure wherein soluble solid content.After testing, wherein protein content is 4%~10%, amino acid content
For 2%~5%, VCContent be 2%~5%, polyphenol content be 10%~15%, polyoses content be 10%~20%, flavones content be 38%~
45%, anthocyanidin content is 8%~12%.
Embodiment 7 prepares oil tea flower extract
80 mesh sieves crushed as raw material using green oil camellia, using 60% ethanol as Extraction solvent, according to 1g:2mL ratio
Mixing, is extracted, processing parameter setting is by ultrasonic assistant：Ultrasonic power 500W, ul-trasonic irradiation time 40min；Carry
The extract solution obtained is concentrated by cryogenic vacuum, 40 DEG C, vacuum 15kPa of temperature, finally gives required oil tea extraction
Thing, it is 46.8% to measure wherein soluble solid content.After testing, wherein protein content is 4%~10%, amino acid content
For 2%~5%, VCContent be 2%~5%, polyphenol content be 10%~15%, polyoses content be 10%~20%, flavones content be 38%~
45%, anthocyanidin content is 8%~12%.
Embodiment 8 prepares oil tea flower extract
20 mesh sieves crushed as raw material using green oil camellia, using 60% ethanol as Extraction solvent, according to 1g:15mL ratio
Example mixing, is extracted, processing parameter setting is by ultrasonic assistant：Ultrasonic power 300W, ul-trasonic irradiation time 60min；
Extract obtained extract solution to concentrate by cryogenic vacuum, temperature 45 C, vacuum 10kPa, finally give required oil tea and carry
Thing is taken, it is 41.4% to measure wherein soluble solid content.After testing, wherein protein content is 4%~10%, and amino acid contains
Measure as 2%~5%, VCContent is 2% ~ 5%, and polyphenol content is 10%~15%, and polyoses content is 10%~20%, flavones content 38%
~45%, anthocyanidin content is 8%~12%.
Embodiment 9 prepares tea oil
The camellia seed kernel of 20 mesh sieves is crushed to peel off（It is conventional）For raw material, solid-liquid ratio 1g:5mL, enzyme dosage 3%（Albumen
Enzyme：Cellulase=4：1）, 53 DEG C, enzymolysis time 6h of hydrolysis temperature, digest pH6.5, ultrasonic power 400W, ultrasonic time
30min, obtain required tea oil.Neutraceutical active ingredients in tea oil are measured, unrighted acid mass fraction is 87.5%, VEContain
It is 115.3mg/kg to measure as 205.6mg/Kg, squalene content.
Embodiment 10 prepares tea oil
The camellia seed kernel of 40 mesh sieves is crushed to peel off（It is conventional）For raw material, solid-liquid ratio 1g:6mL, enzyme dosage 2%（Albumen
Enzyme：Cellulase=4：1）, 55 DEG C, enzymolysis time 5h of hydrolysis temperature, digest pH6.5, ultrasonic power 300W, ultrasonic time
35min, obtain required tea oil.Neutraceutical active ingredients in tea oil are measured, unrighted acid mass fraction is 85.2%, VEContain
It is 128.5mg/kg to measure as 210.4mg/Kg, squalene content.
Embodiment 11 prepares tea oil
The camellia seed kernel of 40 mesh sieves is crushed to peel off（It is conventional）For raw material, solid-liquid ratio 1g:6mL, enzyme dosage 4%（Albumen
Enzyme：Cellulase=4：1）, 50 DEG C, enzymolysis time 7h of hydrolysis temperature, digest pH6.5, ultrasonic power 500W, ultrasonic time
30min, obtain required tea oil.Neutraceutical active ingredients in tea oil are measured, unrighted acid mass fraction is 87.8%, VEContain
It is 140.6mg/kg to measure as 205.3mg/Kg, squalene content.
The preparation of the oil tea face mask cream of embodiment 12
The present embodiment provides a kind of oil tea face mask cream, and by weight percentage, it includes formula as below：Oil tea ultra micro
Powder 30%, oil tea flower extract 30%, tea oil 5%, collagen 1%, hyaluronic acid 1%, Sodium Hyaluronate 1%, pectin 0.5%, milk
2%th, honey 1%, glycerine 3%, propane diols 2% and essence 0.1%, remaining is deionized water.
Randomly selected in product made from oil tea Ultramicro-powder from embodiment 1 to embodiment 4, the oil tea flower extract from
Randomly selected in product made from embodiment 5 to embodiment 8, the tea oil obtained from embodiment 9 to embodiment 11 can produce
Randomly selected in product, conventional tea oil product purchased in market can also be used, its neutraceutical active ingredients standard can refer to embodiment implementation
Example 9 is to embodiment 11.
Oil tea Ultramicro-powder, oil tea flower extract and tea oil are mixed in proportion, according still further to formula addition collagen, thoroughly
Bright matter acid, Sodium Hyaluronate, pectin, milk, honey, glycerine, propane diols and deionized water, then in 300~600r/ of rotating speed
Under min, it is sufficiently stirred with Homogenized emulsifier, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, fully stirs
Uniformly discharge bubble is mixed, cools down and produces oil tea face mask cream.
The preparation of the oil tea face mask cream of embodiment 13
The present embodiment provides a kind of oil tea face mask cream, and by weight percentage, it includes formula as below：Oil tea ultra micro
Powder 20%, oil tea flower extract 20%, tea oil 10%, collagen 2%, hyaluronic acid 1.5%, Sodium Hyaluronate 1%, pectin 1%, ox
Milk 1%, honey 1.5%, glycerine 2%, propane diols 3%, essence 0.05%, remaining is deionized water.
Randomly selected in product made from oil tea Ultramicro-powder from embodiment 1 to embodiment 4, the oil tea flower extract from
Randomly selected in product made from embodiment 5 to embodiment 8, the tea oil obtained from embodiment 9 to embodiment 11 can produce
Randomly selected in product.
Oil tea Ultramicro-powder, oil tea flower extract and tea oil are mixed in proportion, according still further to formula addition collagen, thoroughly
Bright matter acid, Sodium Hyaluronate, pectin, milk, honey, glycerine, propane diols and deionized water, then in 300~600r/ of rotating speed
Under min, it is sufficiently stirred with Homogenized emulsifier, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, fully stirs
Uniformly discharge bubble is mixed, cools down and produces oil tea face mask cream.
The preparation of the oil tea face mask cream of embodiment 14
The present embodiment provides a kind of oil tea face mask cream, and by weight percentage, it includes formula as below：Oil tea ultra micro
Powder 40%, oil tea flower extract 25%, tea oil 10%, collagen 2%, hyaluronic acid 2%, Sodium Hyaluronate 4%, pectin 1%, milk
2%th, honey 2%, glycerine 3%, propane diols 3%, essence 0.05%, remaining is deionized water.
Randomly selected in product made from oil tea Ultramicro-powder from embodiment 1 to embodiment 4, the oil tea flower extract from
Randomly selected in product made from embodiment 5 to embodiment 8, the tea oil obtained from embodiment 9 to embodiment 11 can produce
Randomly selected in product.
Oil tea Ultramicro-powder, oil tea flower extract and tea oil are mixed in proportion, according still further to formula addition collagen, thoroughly
Bright matter acid, Sodium Hyaluronate, pectin, milk, honey, glycerine, propane diols and deionized water, then in 300~600r/ of rotating speed
Under min, it is sufficiently stirred with Homogenized emulsifier, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, fully stirs
Uniformly discharge bubble is mixed, cools down and produces oil tea face mask cream.
The preparation of the oil tea face mask cream of embodiment 15
The present embodiment provides a kind of oil tea face mask cream, and by weight percentage, it includes formula as below：Oil tea ultra micro
Powder 35%, oil tea flower extract 30%, tea oil 5%, collagen 2%, hyaluronic acid 2%, Sodium Hyaluronate 4%, pectin 2%, milk
2%th, honey 2%, glycerine 2%, propane diols 4%, essence 2%, remaining is deionized water.
Randomly selected in product made from oil tea Ultramicro-powder from embodiment 1 to embodiment 4, the oil tea flower extract from
Randomly selected in product made from embodiment 5 to embodiment 8, the tea oil obtained from embodiment 9 to embodiment 11 can produce
Randomly selected in product.
Oil tea Ultramicro-powder, oil tea flower extract and tea oil are mixed in proportion, according still further to formula addition collagen, thoroughly
Bright matter acid, Sodium Hyaluronate, pectin, milk, honey, glycerine, propane diols and deionized water, then in 300~600r/ of rotating speed
Under min, it is sufficiently stirred with Homogenized emulsifier, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, fully stirs
Uniformly discharge bubble is mixed, cools down and produces oil tea face mask cream.
The preparation of the oil tea face mask cream of embodiment 16
The present embodiment provides a kind of oil tea face mask cream, and by weight percentage, it includes formula as below：Oil tea ultra micro
Powder 70%, oil tea flower extract 10%, tea oil 5%, collagen 0.5%, hyaluronic acid 0.5%, Sodium Hyaluronate 0.5%, pectin
0.5%th, milk 0.5%, honey 0.5%, glycerine 3%, propane diols 2%, essence 0.05%, remaining is deionized water.
Randomly selected in product made from oil tea Ultramicro-powder from embodiment 1 to embodiment 4, the oil tea flower extract from
Randomly selected in product made from embodiment 5 to embodiment 8, the tea oil obtained from embodiment 9 to embodiment 11 can produce
Randomly selected in product.
Oil tea Ultramicro-powder, oil tea flower extract and tea oil are mixed in proportion, according still further to formula addition collagen, thoroughly
Bright matter acid, Sodium Hyaluronate, pectin, milk, honey, glycerine, propane diols and deionized water, then in 300~600r/ of rotating speed
Under min, it is sufficiently stirred with Homogenized emulsifier, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, fully stirs
Uniformly discharge bubble is mixed, cools down and produces oil tea face mask cream.
The preparation of the oil tea face mask cream of embodiment 17
The present embodiment provides a kind of oil tea face mask cream, and by weight percentage, it includes formula as below：Oil tea ultra micro
Powder 20%, oil tea flower extract 20%, tea oil 30%, collagen 1%, hyaluronic acid 1%, Sodium Hyaluronate 1%, pectin 5%, milk
0.5%th, honey 0.5%, glycerine 2%, propane diols 8%, essence 1.5%, remaining is deionized water.
Randomly selected in product made from oil tea Ultramicro-powder from embodiment 1 to embodiment 4, the oil tea flower extract from
Randomly selected in product made from embodiment 5 to embodiment 8, the tea oil obtained from embodiment 9 to embodiment 11 can produce
Randomly selected in product.
Oil tea Ultramicro-powder, oil tea flower extract and tea oil are mixed in proportion, according still further to formula addition collagen, thoroughly
Bright matter acid, Sodium Hyaluronate, pectin, milk, honey, glycerine, propane diols and deionized water, then in 300~600r/ of rotating speed
Under min, it is sufficiently stirred with Homogenized emulsifier, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, fully stirs
Uniformly discharge bubble is mixed, cools down and produces oil tea face mask cream.
The preparation of the oil tea face mask cream of embodiment 18
The present embodiment provides a kind of oil tea face mask cream, and by weight percentage, it includes formula as below：Oil tea ultra micro
Powder 10%, oil tea flower extract 10%, tea oil 5%, collagen 5%, hyaluronic acid 10%, Sodium Hyaluronate 10%, pectin 5%, milk
1%th, honey 10%, glycerine 10%, propane diols 10%, essence 0.1%, remaining is deionized water.
Randomly selected in product made from oil tea Ultramicro-powder from embodiment 1 to embodiment 4, the oil tea flower extract from
Randomly selected in product made from embodiment 5 to embodiment 8, the tea oil obtained from embodiment 9 to embodiment 11 can produce
Randomly selected in product.
Oil tea Ultramicro-powder, oil tea flower extract and tea oil are mixed in proportion, according still further to formula addition collagen, thoroughly
Bright matter acid, Sodium Hyaluronate, pectin, milk, honey, glycerine, propane diols and deionized water, then in 300~600r/ of rotating speed
Under min, it is sufficiently stirred with Homogenized emulsifier, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, fully stirs
Uniformly discharge bubble is mixed, cools down and produces oil tea face mask cream.
It is prepared by the oil tea face mask cream that comparative example 1 does not contain oil tea flower extract
This comparative example provides another oil tea face mask cream, and oil tea flower extract is not contained in formula.Remaining formula components
It is by weight percentage：Oil tea Ultramicro-powder 40%, tea oil 10%, collagen 5%, hyaluronic acid 5%, Sodium Hyaluronate 5%,
Pectin 2%, milk 2%, honey 2%, glycerine 10%, propane diols 10%, essence 0.1%, remaining is deionized water.
Randomly selected in product made from oil tea Ultramicro-powder from embodiment 1 to embodiment 4, the tea oil can be from implementation
Randomly selected in product made from example 9 to embodiment 11.
Oil tea Ultramicro-powder and tea oil are mixed in proportion, collagen, hyaluronic acid, hyalomitome are added according still further to formula
Sour sodium, pectin, milk, honey, glycerine, propane diols and deionized water, then under 300~600r/min of rotating speed, use homogenized milk
Change device to be sufficiently stirred, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, stirs discharge gas
Bubble, cools down and produces oil tea face mask cream.
It is prepared by the oil tea face mask cream that comparative example 2 does not contain oil tea Ultramicro-powder
This comparative example provides another oil tea face mask cream, and oil tea Ultramicro-powder is not contained in formula.Remaining formula components
It is by weight percentage：Oil tea flower extract 30%, tea oil 10%, collagen 5%, hyaluronic acid 5%, Sodium Hyaluronate 5%,
Pectin 2%, milk 2%, honey 2%, glycerine 10%, propane diols 10%, essence 0.1%, remaining is deionized water.
Randomly selected in product made from oil tea flower extract from embodiment 5 to embodiment 8, the tea oil can be from implementation
Randomly selected in product made from example 9 to embodiment 11.
Oil tea flower extract and tea oil are mixed in proportion, collagen, hyaluronic acid, hyalomitome are added according still further to formula
Sour sodium, pectin, milk, honey, glycerine, propane diols and deionized water, then under 300~600r/min of rotating speed, use homogenized milk
Change device to be sufficiently stirred, 5~20min of mixing time；Thing to be mixed adds essence after being down to room temperature, stirs discharge gas
Bubble, cools down and produces oil tea face mask cream.
The performance evaluation of the oil tea face mask cream of the present invention of embodiment 19
Organoleptic properties, physical and chemical index, storage stabilization are carried out to the oil tea face mask cream being prepared using inventive formulation
Property etc. is tested.
1. oil tea face mask cream human skin smears experiment
Trial method：Take face mask cream product appropriate, carry on the back careful smearing in the palm, skin after observation is smeared dispersiveness and smeared
Oiliness.Allow from volunteer's list 10 triers randomly selected to adhere to using one week or so, product efficacy is provided specifically
Evaluation.Its lotion sophistication, smoothness to be observed, toughness, greasy feeling is whether there is, sees color and luster, smelling, each best result 10 divides,
Minimum point 0 point.
Adhere to that one tries out to bimestrial, several triers reflect that the product not only makes skin show moist, tender, light
Sliding, refrigerant sensation, and pachylosis can be mitigated, spot on desalination face.Product property is gentle, non-stimulated, toxic side effect, without on probation
Person shows the uncomfortable reaction such as allergy；The product is applied to various skin quality, is especially suitable for sensitive skin quality and uses.Ten triers comment
Valency result total score situation is shown in Table 1：
Table 1
| Embodiment | Lotion sophistication | Smoothness | Toughness | Whether there is greasy feeling | Color and luster | Smell |
| 12 | 95 | 97 | 100 | 95 | 93 | 95 |
| 13 | 95 | 95 | 98 | 93 | 93 | 95 |
| 14 | 100 | 100 | 99 | 99 | 98 | 98 |
| 15 | 99 | 99 | 97 | 98 | 95 | 92 |
| 16 | 92 | 93 | 99 | 93 | 92 | 96 |
| 17 | 93 | 99 | 95 | 93 | 95 | 92 |
| 18 | 92 | 93 | 93 | 92 | 90 | 92 |
| Comparative example 1 | 88 | 90 | 86 | 90 | 90 | 90 |
| Comparative example 2 | 90 | 90 | 85 | 90 | 90 | 86 |
2nd, oil tea face mask cream physical and chemical index detects
Heat resistant test：Face mask cream product of the present invention is placed into 24 h under the conditions of 40 DEG C, it was observed that the equal oil-free moisture of lotion
From phenomenon.
Low temperature resistant test：Face mask cream product of the present invention is placed into 24 h under the conditions of -5 DEG C, cream is observed after recovering to room temperature
Body is without water-oil separating phenomenon.
Light Resistance Test：Face mask cream product of the present invention is placed into 24 h in the sun, it was observed that face mask cream shows as surface
It is glossy, smooth, pore-free and heterochromatic spot, uniformity.
Centrifugal test：Take face mask cream product of the present invention to centrifuge 30min under the conditions of 4000r/min, find the equal nothing of face mask cream
Lamination.
PH value：After measured, mask product cream pH value of the present invention is between 5.0~7.0, in faintly acid.
3rd, oil tea face mask cream bin stability is evaluated
Face mask cream product of the present invention is placed in color-comparison tube, respectively in 40 ± 1 DEG C of constant incubators and -10 DEG C of ice
48 h are placed in case, recover to room temperature to observe, sends out phenomenon thick without any water-oil separating and lotion, illustrates oil tea facial mask of the present invention
The heat-resisting cold tolerance of cream is qualified.
Claims (11)
1. application of the oil tea in terms of beauty skin care product is prepared, it is characterised in that will be prepared using oil tea
Oil tea Ultramicro-powder and oil tea flower extract are applied to prepare beauty skin care product as skin conditioning agent；
The micron powder that the oil tea Ultramicro-powder crushes to obtain using drier oil camellia；The oil tea flower extract is using new
Fresh fried flour is colored, extracts to obtain using ethanol water as Extraction solvent.
2. application according to claim 1, it is characterised in that the preparation of the oil tea Ultramicro-powder comprises the following steps：
S11. through the drying process that finishes after green oil camellia is cleaned；
S12. coarse powder is obtained by the oil tea pollen handled through step S11 is broken；
S13. will crush using superfine communication technique to obtain micron order Ultramicro-powder through coarse powder obtained by step S12；The oil tea is super
The particle diameter of the micron powder of micro mist is less than 10 μm.
3. application according to claim 2, it is characterised in that in the preparation of oil tea Ultramicro-powder, fixing described in step S11
Drying process is that the moisture for drying oil tea to oil tea is less than 6%；Drying process is finished described in step S11 using micro-
The vacuum combined mode of ripple is carried out, and process conditions are 200~600W of microwave power, 30~100kPa of vacuum, and the time 10~
60min；The particle diameter of coarse powder described in step S12 is 100~200 μm.
4. application according to claim 1, it is characterised in that the preparation of the oil tea flower extract is with green oil camellia pollen
It is raw material after broken, using the aqueous solution of ethanol as Extraction solvent, is concentrated to give again through cryogenic vacuum after ultrasonic assistant extracts；
The ultrasonic assistant extraction conditions are：It is 200~800 μm that green oil camellia, which is crushed to granularity, in the aqueous solution of ethanol
Volume fraction of ethanol is 20~90%, according to oil tea pollen and ethanol 1g:2~15mL ratio is mixed, ultrasonic power
For 140~560W, the ul-trasonic irradiation time is 30~90min；
The cryogenic vacuum concentration condition is 40~50 DEG C, 10~15kPa.
5. application according to claim 4, it is characterised in that in the aqueous solution of ethanol volume fraction of ethanol be 50%~
70%；The oil tea pollen is with ethanol according to 1g:5~8mL ratio；The ultrasonic power is 300~500W；The ultrasound
Ripple action time is 40~60min.
6. a kind of oil tea face mask cream, it is characterised in that by the oil tea Ultramicro-powder and power described in any one of claims 1 to 3
Profit requires that the oil tea flower extract described in 1,4 or 5 any one adds as skin conditioning agent, compounding moisturizing grease, NMF, nutrition
Agent, thickener, solvent and auxiliary material is added to be prepared.
7. oil tea face mask cream according to claim 6, it is characterised in that the moisturizing grease selects tea oil；The moisturizing
Hyaluronic acid, Sodium Hyaluronate and glycerine are selected in agent；The nourishing additive agent selects collagen, milk and honey；The increasing
Thick dose is selected pectin.
8. oil tea face mask cream according to claim 7, it is characterised in that the preparation method of the tea oil be to shell after
Camellia seed kernel is raw material, using ultrasonic assistant aqueous enzymatic extraction；The enzyme is protease, cellulase, pectase, alphalise starch
One or more in enzyme or complex enzyme；
The ultrasonic assistant aqueous enzymatic extraction condition is：Camellia seed kernel and water enzyme ratio 1g:3~10mL, enzyme dosage 1%~
5%, 30 DEG C~80 DEG C, enzymolysis time 1h~8h of hydrolysis temperature, digest pH4~9, ultrasonic power 100W~600W, when ultrasonic
Between 10min~60min.
9. oil tea face mask cream according to claim 7, it is characterised in that the preparing raw material of the oil tea face mask cream includes
The each component of following percentage by weight：
10. oil tea face mask cream according to claim 9, it is characterised in that the preparing raw material bag of the oil tea face mask cream
Include each component of following percentage by weight：
11. the preparation method of any one of claim 6 to the 10 oil tea face mask cream, it is characterised in that be that oil tea is super
Micro mist, oil tea flower extract and tea oil mix in proportion, add collagen, hyaluronic acid, Sodium Hyaluronate, pectin, milk,
Honey, glycerine, propane diols and deionized water, emulsifying under 300~600r/min of rotating speed, thing to be mixed add after being down to room temperature
Essence, discharge bubble is stirred, cool down and produce oil tea face mask cream.
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| CN105104361A (en) * | 2015-06-30 | 2015-12-02 | 中国林业科学研究院亚热带林业研究所 | Camellia oleifera pollen ultra low temperature storage method |
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| JP2010083786A (en) * | 2008-09-30 | 2010-04-15 | Maruzen Pharmaceut Co Ltd | Anti-aging agent and skin cosmetic |
| CN103689740A (en) * | 2013-12-12 | 2014-04-02 | 华南农业大学 | Extractive of camellia oleifera flowers and application of extractive in preparation of health-care drink |
| CN103800241A (en) * | 2014-02-21 | 2014-05-21 | 普洱联众生物资源开发有限公司 | Plukenetia volubilis Linneo facial mask paste |
| CN105104361A (en) * | 2015-06-30 | 2015-12-02 | 中国林业科学研究院亚热带林业研究所 | Camellia oleifera pollen ultra low temperature storage method |
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