CN105726420A - Camellia flower essential oil skin care lotion and preparation technology thereof - Google Patents
Camellia flower essential oil skin care lotion and preparation technology thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A61Q17/02—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention belongs to the technical field of skin care products, and particularly relates to a camellia flower essential oil skin care lotion and a preparation technology thereof. The camellia flower essential oil skin care lotion is prepared from a camellia flower extracting solution, tea oil, prinsepia utilis royle oil and camellia flower essential oil. The skin care lotion is natural in fragrance and rich in natural nutritional ingredients such as unsaturated fatty acid, camellia dulcin, protein, barringtogenol, vitamin E and mineral substances including potassium, phosphorus, magnesium and calcium, can speed up repairing of a skin barrier function and can be applied to daily accidental skin damage to control inflammations and reduce secondary skin damage; in addition, the structure of the contained fatty acid is very close to that of the human body lipid, the very significant protection and anti-radiation effects on erythrocyte hemolysis caused by ultraviolet rays are achieved, and the significant effect on skin care is achieved.
Description
Technical field
The present invention relates to technical field of skin care, be specifically related to a kind of Flos Camelliae Japonicae quintessence oil cream for skin care and preparation technology thereof.
Background technology
Modern people are fast due to rhythm of life, and work, learning pressure are big, online for a long time in addition, play erratic living habit and the nutrient imbalances such as mobile phone and the factor such as do not get enough athletic exercise, and cause the problems such as senilism, easily sick, fatiguability.Thus, anti-aging product gets more and more people's extensive concerning for a long time, and current anti-aging product spininess is to middle-aged and elderly people, and effect is single.Exploitation is specifically designed for the anti-aging product that various crowd is all suitable for, and is just particularly important.
In human body skin, water content accounts for the 18%-20% of its weight.But, skin is to be easiest to hydropenia, after skin hydropenia, it is easy to sends out wrinkle, come off, and skin color is gloomy, shows the sign of aging.The skin histology seriously dried out, its epidermis cell metabolism is relatively slow, causes old epidermis cell constantly to be piled up, therefore seems coarse, lacks gloss.It is therefore prevented that moisture of skin excessively runs off, for keeping the health of good skin barrier function and skin to be very important.
Along with the development of society, the progress of science, health is increasingly paid attention to by people, pays close attention to the quality of life, from color, smell and taste emphatically to noting collocation, nutrition, health, safety.The Cosmetic Market of China is the emerging market that the whole world is maximum, and emerging in multitude of skin cosmetic makes people too plenty for the eye to take it all in, and people, except learning the cosmetics made good use of, also focus more on effect and the safety of cosmetics.Therefore the welcome of consumer is enjoyed in recent years about the theory such as " without adding cosmetics ", " vegetalization cosmetic ", " organise cosmetic ", " natural cosmetics ", " edible cosmetics ".But, most cosmetics on the market are difficult to allow consumer pack whole components of identification product from product at present, and it is difficult to judge effectiveness and the safety of product, even if declaring edible cosmetics, its formula is also that constituent part derives from food additive or animal and plant raw material.
The safety of cosmetics and stability are to ensure that the important prerequisite of cosmetics quality, and in formula system, the safety of cosmetics and stability can be had particularly important impact with using by the selection of oils and fats, preservative etc..Princepia utilis oil is from plateau plant kingdom Yunnan, and rich in unsaturated fatty acid, and its composition is close with human sebaceous's class, has skin regeneration technique and moisture-keeping function；Also there is extremely strong skin permeability simultaneously, the effect similar with azone can be played, there is good antiinflammation, can be used for daily unexpected skin injury and control inflammation, reduce secondary skin injury.Research display, Princepia utilis oil is rich in multivitamins such as vitamin A. D. E, K and beta-carotene；Amino acid contained A wide selection of colours and designs, total content reaches 46.97%, and wherein 7 kinds of essential amino acid content account for the 28.1% of total amino acid content；Institute's fatty acids has 13 kinds, and wherein unsaturated fatty acid content is high, and based on oleic acid and linoleic acid, satisfied fatty acid, monounsaturated fatty acid and polyunsaturated fatty acid proportion of composing are close to 0.7:1:1, and its nutrition of lipids structure comparison is suitable for human body needs.Oleum Camelliae is real fully natural green edible oil.Especially its contained abundant linolenic acid is needed by human and can not synthesize have significantly high nutritive value.
Flos Camelliae Japonicae is graceful because of its plant shape appearance, and flower-shape is gorgeous in riotous profusion, and is subject to valuing of world's gardening circle, is the ornamental flower of Chinese tradition, one of Yi Shi world famous flower and tree.In Flos Camelliae Japonicae, floral leaf, alabastrum are rich in each seed amino acid, multivitamin and multiple rare trace element, especially its contained abundant Flos Camelliae Japonicae quintessence oil is natural and is synthetic, fragrance persistently, can easily be absorbed by skin, deep layer bactericidal antiphlogistic, skin nursing nutrient, hyaluronic acid etc. in collocation, moreover it is possible to effectively lock the moisture of skin surface cell are provided, make skin surface recover water profit vigor, there is significantly high skin protection and be worth.
Summary of the invention
It is an object of the invention to solve defect of the prior art, a kind of Flos Camelliae Japonicae quintessence oil cream for skin care is provided, this cream for skin care not only fragrance is natural, rich in natural nutrient components such as unsaturated fatty acid, Flos Camelliae Japonicae dulcin, protein, Barringtonia racemosa (L.) B L.ex Do. alcohol, vitamin E, mineral potassium, phosphorus, magnesium, calcium, the reparation of skin barrier function can be accelerated, and can be applicable to daily unexpected skin injury and control inflammation, reduce secondary skin injury；And contained fatty acid structure is with human body papery closely, the erythrocyte hemolysis caused by ultraviolet has the protection radiation resistance of highly significant, the nursing of skin is had remarkable result.Flos Camelliae Japonicae quintessence oil cream for skin care formula uses natural bacteriostatic composition and the Natural antioxidant, and compatibility is good, and cutaneous safety test is non-stimulated, is a kind of gentleness, safe and stable and can the cosmetics of permanent moisturizing.
Another object of the present invention is to provide the preparation technology of a kind of above-mentioned Flos Camelliae Japonicae quintessence oil cream for skin care.
For achieving the above object, technical scheme is as follows: a kind of Flos Camelliae Japonicae quintessence oil cream for skin care, is made up of Flos Camelliae Japonicae extracting solution, Oleum Camelliae, Princepia utilis oil, Flos Camelliae Japonicae essential oil component.
Preferably, described each component is calculated by weight as: Flos Camelliae Japonicae extracting solution 30 ~ 35 parts, Oleum Camelliae 50 ~ 60 parts, Princepia utilis oil 9.5 ~ 18.5 parts, Flos Camelliae Japonicae quintessence oil 0.5 ~ 1.5 part.
In Flos Camelliae Japonicae quintessence oil cream for skin care formula disclosed by the invention, Flos Camelliae Japonicae quintessence oil is rich in having each seed amino acid, multivitamin and multiple rare trace element, especially its contained natural plants aromatic substance, fragrance unique, persistently, can easily be absorbed by skin, deep layer bactericidal antiphlogistic；Oleum Camelliae is rich in natural nutrient components such as unsaturated fatty acid, Flos Camelliae Japonicae dulcin, protein, Barringtonia racemosa (L.) B L.ex Do. alcohol, vitamin E, mineral potassium, phosphorus, magnesium, calcium；Fatty acid structure contained by Princepia utilis oil with human body papery closely, is described as " eatable cosmetics ", the erythrocyte hemolysis caused by ultraviolet has the protection radiation resistance of highly significant, especially the nursing of skin is had remarkable result；Flos Camelliae Japonicae extract water-soluble active ingredient can Substitute For Partial deionized water, it is possible to keep the transparency of product and the refractive index of balance aqueous phase.
Further, the preparation technology of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care, described preparation technology specifically comprises the following steps that
S1. Flos Camelliae Japonicae extract and deionized water are added in stirring container and be sufficiently stirred for, carry out high-speed stirred afterwards and produce eddy current to stirring container；
S2., after step S1 stirring produces eddy current, it is sequentially added into Oleum Camelliae, Princepia utilis oil, mix and blend heat temperature raising；
S3. under step S2 constant temperature stirs, adding Flos Camelliae Japonicae quintessence oil, after mix and blend in suction emulsifying pot, open homogenizing, homogenizing speed is 3000rpm, mixes modified to complete emulsifying in emulsifying pot；
S4., after the complete emulsifying of step S3, regulate pH value to neutral with edible sodium bicarbonate or citric acid solution, be cooled to suitable subpackage temperature, stir, sterilization, sterilizing, fill, obtain Flos Camelliae Japonicae quintessence oil cream for skin care.
Further, in described step S1, mixing time is 30 ~ 50min.
Further, in described step S2, mixing time is 20 ~ 30min, and temperature is 70 DEG C ~ 75 DEG C.
Further, the Oleum Camelliae in described step S2 is that white flower oil Camellia sinensis camellia oleosa seed selects through air-dry color, shells, steaming and decocting, squeezing, high-pressure filteration step prepare.
Further, in described step S3, mixing time is 20 ~ 30min, and homogenizing time is 10～30min, and emulsifying temperature is 70 DEG C ~ 75 DEG C.
Technical scheme gives full play to Flos Camelliae Japonicae natural plant resource, does not have the participation of any industrial chemicals in the whole course of processing；Effect is notable, no side effects, is suitable for each age group crowd and uses；Technique is simple, input cost is low.
Have employed the technical scheme of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care of the present invention and preparation technology thereof, compared with prior art, the Flos Camelliae Japonicae quintessence oil cream for skin care of the present invention has the advantages that
(1) the Flos Camelliae Japonicae quintessence oil cream for skin care of the present invention has good percutaneous permeability, and effect skin has moisturizing, replenishing the calcium can repair impaired skin barrier.Meanwhile, there is effects of antiinflammation and bacteriostasis, be applied to daily unexpected skin injury (scald, scratch, dampen, moth bites) and can play and control inflammation, reduce secondary skin injury.
(2) the Flos Camelliae Japonicae quintessence oil cream for skin care of the present invention is rich in unsaturated fatty acid, multivitamin and multiple rare trace element, has the effects such as defying age, anticancer and anticancer growth.
(3) the Flos Camelliae Japonicae quintessence oil cream for skin care of the present invention also there is moisturizing simultaneously, UV resistance, only mosquito sting itch, the effect such as blood circulation promoting and blood stasis dispelling.
(4) the Flos Camelliae Japonicae quintessence oil each raw material of cream for skin care recipe ingredient disclosed by the invention all adopts pure natural raw material, derives from edible raw material, safe and non-stimulating, even if eating by mistake, without human body produces damage and potential safety hazard.
(5) Flos Camelliae Japonicae quintessence oil cream for skin care permeability disclosed by the invention is strong, can improve cutin and degenerate, have the effect such as moisturizing, anticracking.To prevention xerosis cutis crowfoot cracks, keep moisture of skin, keep skin tender, degree of depth conditioning skin, promote cutaneous circulation, regulate sebum secretion and skin metabolism, improve dim Huang, coarse, wrinkle, pimpled skin quality, make skin more healthy moist；Antiinflammatory Shu Min, uvioresistant, improve circulation free radical resisting anoxia enduring and resist strenuously scorching antibacterial.
(6) Flos Camelliae Japonicae quintessence oil cream for skin care formula disclosed by the invention, its Flos Camelliae Japonicae extracting solution, Oleum Camelliae, Princepia utilis oil, Flos Camelliae Japonicae quintessence oil raw material compatibility require higher, in this formula system, good stability, safety are good.And can allow each component that ordinary consumer is easier in identification formula according to general knowledge the safety of each component of principium identification.
Detailed description of the invention
Below in conjunction with embodiment, technical scheme is described further.
Embodiment 1
A kind of Flos Camelliae Japonicae quintessence oil cream for skin care, is made up of Flos Camelliae Japonicae extracting solution, Oleum Camelliae, Princepia utilis oil, Flos Camelliae Japonicae essential oil component, and described each component is calculated by weight as: Flos Camelliae Japonicae extracting solution 30 parts, Oleum Camelliae 50 parts, Princepia utilis oil 9.5 parts, Flos Camelliae Japonicae quintessence oil 0.5 part.
Embodiment 2
A kind of Flos Camelliae Japonicae quintessence oil cream for skin care, is made up of Flos Camelliae Japonicae extracting solution, Oleum Camelliae, Princepia utilis oil, Flos Camelliae Japonicae essential oil component, and described each component is calculated by weight as: Flos Camelliae Japonicae extracting solution 32 parts, Oleum Camelliae 55 parts, Princepia utilis oil 14 parts, Flos Camelliae Japonicae quintessence oil 1 part.
Embodiment 3
A kind of Flos Camelliae Japonicae quintessence oil cream for skin care, is made up of Flos Camelliae Japonicae extracting solution, Oleum Camelliae, Princepia utilis oil, Flos Camelliae Japonicae essential oil component, and described each component is calculated by weight as: Flos Camelliae Japonicae extracting solution 35 parts, Oleum Camelliae 60 parts, Princepia utilis oil 18.5 parts, Flos Camelliae Japonicae quintessence oil 1.5 parts.
Embodiment 1,2, the physical and chemical index of 3 one kind of Flos Camelliae Japonicae quintessence oil cream for skin care as follows:
1, character
This product is that viscosity is suitable for, the transparency emulsion that stretchability is good.
2, pH value measures
Weighing embodiment 1,2, the 3 each 1.0g of sample respectively, and be separately added in 10ml distilled water, and be stirred continuously, heating, to 40 DEG C, is cooled to room temperature, and recording pH value is 6.8-7.3.
3, stability
(1) heat resistant test
First electro-heating standing-temperature cultivator is adjusted to (40 ± 1) DEG C, then respectively embodiment 1,2,3 is respectively taken two parts of samples, a copy of it is placed in electro-heating standing-temperature cultivator and keeps after 24h, take out, compare with another part of sample after recovering room temperature, the phenomenons such as nothing layering emulsifying is spoiled.
(2) low temperature resistant test
First electric refrigerator is adjusted to (-5-15) DEG C ± 1 DEG C, then respectively embodiment 1,2,3 is respectively taken two parts of samples, a copy of it is placed in electric refrigerator and keeps after 24h, take out, compare with another part of sample after recovering room temperature, the phenomenons such as nothing layering emulsifying is spoiled.
(3) centrifugal test
The sample respectively taken from embodiment 1,2,3 is placed in centrifuge, after the speed test 30min of (2000-4000) r/min, without lamination.
4, irritation test
The sample of Example 1,2,3, is applied in volunteer (18-60 year, 100 people) gesture and facial expression in right amount, observes without rubescent after spending 30 minutes, dermexanthesis, foaming phenomena.
Embodiment 1,2,3 one kind of Flos Camelliae Japonicae quintessence oil cream for skin care, treat for following clinical:
1, treatment target
Randomly selecting the age tests the crowd of 18～55 years old, it is low that the crowd chosen shows as skin histology jaundice, dry and cracked, decline and physiological function: 1) skin histology decline person: showing as epidermis cell karyokinesis increases, melanin also increases, and the colour of skin becomes brownish black more.Skin surface is hardening, tarnishes.Subcutaneous fat reduces, and produces with wrinkle with cutis laxa.2) physiological function is low: sebaceous gland, sweat gland deterioration, and perspiration and sebum are got rid of and reduced, skin lose gradually in the past gloss and become dry., with the nutrition of supplementary skin necessity, there is more difficult healing during wound in blood circulation hypofunction.
Skin histology jaundice, dry and cracked, decline and physiological function low person totally 100 example, be randomly divided into treatment group and matched group, often organize each 50 examples.
2, Therapeutic Method
Treatment group: every morning, 8:00-9:00 smeared the Flos Camelliae Japonicae quintessence oil cream for skin care of embodiment 1,2,3 after washing one's face, and each consumption is that 0.5-1.0g is advisable.
Matched group: every morning, 8:00-9:00 smeared commercial vitamin E moisturizer after washing one's face.
3, clinical treatment outcome
Flos Camelliae Japonicae quintessence oil cream for skin care clinical therapeutic efficacy provided by the invention: treatment group effective percentage is 98%, and matched group effective percentage is 40%.After clinical treatment 30 days, it is moistening, flexible that the jaundice for the treatment of group, dry and cracked skin become, melanin reduces, and skin deliquescing, simultaneously pool, skin pass are greatly improved, wrinkle of skin reduces, and originally has the skin of senile plaque also to reduce to some extent, skin becomes more smooth simultaneously, improving the degeneration of skin keratin, repair coarse skin, skin physiology function is improved, and matched group is after clinical observation 30 days, there is not obvious change in skin characteristic.
4, conclusion
The aspects such as the present invention provides Flos Camelliae Japonicae quintessence oil cream for skin care antagonism yellowing of the skin, dry and cracked, old and feeble, regulation of skin physiological function, its effect is better than matched group.And the present invention provides Flos Camelliae Japonicae quintessence oil cream for skin care effect notable, no side effects, it is suitable for each age group crowd and uses.
Embodiment 4
The preparation technology of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care, described preparation technology specifically comprises the following steps that
S1. Flos Camelliae Japonicae extract and deionized water are added after stirring container is sufficiently stirred for 30min, carry out high-speed stirred and produce eddy current to stirring container；
S2. produce after eddy current in step S1 stirring, be sequentially added into Oleum Camelliae, Princepia utilis oil, mix and blend 20min, and be heated to 70 DEG C ~ 75 DEG C, described Oleum Camelliae be white flower oil Camellia sinensis camellia oleosa seed select through air-dry color, shell, steaming and decocting, squeezing, high-pressure filteration step prepared；
S3. under step S2 constant temperature stirs, adding Flos Camelliae Japonicae quintessence oil, after mix and blend 20min in suction emulsifying pot, open homogenizing, homogenizing speed is 3000rpm, at 70 DEG C ~ 75 DEG C homogenizing 10min, mixes modified to complete emulsifying in emulsifying pot；
S4., after the complete emulsifying of step S3, regulate pH value to neutral with edible sodium bicarbonate or citric acid solution, be cooled to suitable subpackage temperature, stir, sterilization, sterilizing, fill, obtain Flos Camelliae Japonicae quintessence oil cream for skin care.
Embodiment 5
The preparation technology of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care, described preparation technology specifically comprises the following steps that
S1. Flos Camelliae Japonicae extract and deionized water are added after stirring container is sufficiently stirred for 40min, carry out high-speed stirred and produce eddy current to stirring container；
S2. produce after eddy current in step S1 stirring, be sequentially added into Oleum Camelliae, Princepia utilis oil, mix and blend 25min, and be heated to 70 DEG C ~ 75 DEG C, described Oleum Camelliae be white flower oil Camellia sinensis camellia oleosa seed select through air-dry color, shell, steaming and decocting, squeezing, high-pressure filteration step prepared；
S3. under step S2 constant temperature stirs, adding Flos Camelliae Japonicae quintessence oil, after mix and blend 25min in suction emulsifying pot, open homogenizing, homogenizing speed is 3000rpm, at 70 DEG C ~ 75 DEG C homogenizing 20min, mixes modified to complete emulsifying in emulsifying pot；
S4., after the complete emulsifying of step S3, regulate pH value to neutral with edible sodium bicarbonate or citric acid solution, be cooled to suitable subpackage temperature, stir, sterilization, sterilizing, fill, obtain Flos Camelliae Japonicae quintessence oil cream for skin care.
Embodiment 6
The preparation technology of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care, described preparation technology specifically comprises the following steps that
S1. Flos Camelliae Japonicae extract and deionized water are added after stirring container is sufficiently stirred for 50min, carry out high-speed stirred and produce eddy current to stirring container；
S2. produce after eddy current in step S1 stirring, be sequentially added into Oleum Camelliae, Princepia utilis oil, mix and blend 30min, and be heated to 70 DEG C ~ 75 DEG C, described Oleum Camelliae be white flower oil Camellia sinensis camellia oleosa seed select through air-dry color, shell, steaming and decocting, squeezing, high-pressure filteration step prepared；
S3. under step S2 constant temperature stirs, adding Flos Camelliae Japonicae quintessence oil, after mix and blend 30min in suction emulsifying pot, open homogenizing, homogenizing speed is 3000rpm, at 70 DEG C ~ 75 DEG C homogenizing 30min, mixes modified to complete emulsifying in emulsifying pot；
S4., after the complete emulsifying of step S3, regulate pH value to neutral with edible sodium bicarbonate or citric acid solution, be cooled to suitable subpackage temperature, stir, sterilization, sterilizing, fill, obtain Flos Camelliae Japonicae quintessence oil cream for skin care.
Flos Camelliae Japonicae quintessence oil cream for skin care prepared by embodiment 4-6 carries out performance detection, including stability test, anti-corrosion function test, security test and moisture of skin test.
1, stability test
Flos Camelliae Japonicae quintessence oil cream for skin care prepared by the above-mentioned embodiment 4-6 prepared carries out study on the stability, product stability investigates reference standard QB/T1857-2004 " skin moistening cream ", in order to obtain more stable product, condition of investigating requires higher than QB/T1857-2004, successively at-15 DEG C, 5 DEG C, at 40 DEG C and 49 DEG C, test 15 days, 30 days respectively, 45 days, 60 days and 90 days, the stability of the gentle protective skin cream of the test present invention, stability test result of the test is as shown in table 1:
In table 1, stability test result of the test shows: Flos Camelliae Japonicae quintessence oil cream for skin care prepared by embodiment 4-6, (40 ~ 49) DEG C heat-resisting investigation, recovering to room temperature without the layering phenomenons such as emulsifying is spoiled, (-5 ~-15) are DEG C cold-resistant to be investigated, recover to room temperature with test before without obvious Traits change.Therefore the Flos Camelliae Japonicae quintessence oil cream for skin care that prepared by the present invention has good formula compatibility and constant product quality.
2, anti-corrosion function test
Tested by preservation challenge and carry out preservative efficacy evaluation.The method is with reference to the test of American Pharmacopeia USP28 version antimicrobial preservative efficacy.The Flos Camelliae Japonicae quintessence oil cream for skin care prepared by embodiment 4-6 is mixed in the cell culture substrate of identical type respectively, then the fungus of disposable access standard volume and mycete, sample is deposited at the temperature of 37 DEG C, regular sampling Detection residual therein fungus number and residual fungi count, and the antibacterial effect of sample is evaluated according to the situation of change remaining fungus number and residual fungi count.
Criterion: the residual being detected in sample at the 28th day bacterial population alive and the equal < 1.0 × 103CFU/g (ml) of fungus number of living；From the 14th day, the residual being detected in the sample of the 21st day and the 28th day lived bacterial population and fungus number of living all can not be further added by.
Preservative efficacy test result is as shown in table 2:
By table 2 preservative efficacy test result it can be seen that when the 7th day, the residual being detected in Flos Camelliae Japonicae quintessence oil cream for skin care sample prepared by embodiment 4-6 is lived the equal < 1.0 × 10 of bacterial population3CFU/g, when the 14th day, the equal < 1.0 × 10 of remaining bacteria number3CFU/g, and clump count all do not increase.Therefore the Flos Camelliae Japonicae quintessence oil cream for skin care that prepared by the present invention has good preservative efficacy.
3, security test
Security test includes acute skin irritation test and acute eye irritation test.
(1) acute skin irritation test:
Flos Camelliae Japonicae quintessence oil cream for skin care prepared by embodiment 4-6 carries out acute skin irritation test, and each embodiment all selects 5 albino guinea-pigs to test, test chamber temperature: 20-24 DEG C, relative humidity: 60-70%.Spinal column both sides, laboratory animal back are cut by test precontract 24h by hair, and unhairing scope is respectively 2cm × 3cm, application area 2.5cm × 2.5cm.Taking tested material to be about 0.5mL and spread upon on the skin of side, when tested material uses the preparation of nonirritant solvent, opposite side is coated with solvent as comparison, smears every day 1 time, smears 14 days continuously.From second day, before smearing, answer cropping every time, remain tested material, observed result after a hour with water or nonirritant solvent cleaning.Irritant reaction evaluation is carried out with reference to " cosmetics health specification (2007 editions) " regulation.
Acute skin irritation test result is as shown in table 3:
By the acute skin irritation test result of table 3 it can be seen that the Flos Camelliae Japonicae quintessence oil cream for skin care prepared of the embodiment 4-6 acute skin irritation test to Cavia porcellus, it is showed no irritative response.Therefore the Flos Camelliae Japonicae quintessence oil cream for skin care that prepared by the present invention, acute skin irritation test result shows do not have skin irritation.
(2) acute eye irritation test
Flos Camelliae Japonicae quintessence oil cream for skin care prepared by embodiment 4-6 carries out acute eye irritation test, and each embodiment all selects 3 healthy adult white rabbit to test, test chamber temperature: 20-24 DEG C, relative humidity: 60-70%.Before test, animal at least to adapt to 3 day time in experimental animal room environment.Pull open a palpebra inferior for hairy rat side eyes gently, tested material 0.1mL (100mg) is instilled in (or being painted into) conjunctival sac, makes upper and lower eyelid passively close 1s, to prevent tested material from losing.Opposite side eyes do not process makes own control.Eyes are not rinsed in 24 hours after instilling tested material.If thinking necessary, can be rinsed when 24h.If above-mentioned result of the test display tested material is irritant, need to selecting else and be rinsed effect test with 3 rabbit, after namely instilling tested material to rabbit eyes, 30s comparatively fast but will not cause the current that animal eye is damaged to rinse at least 30s with enough, flow velocity.Animal eyes was checked in 1,24,48,72 hours and the 4th and the 7th after instilling tested material.If 72 hours irritant reaction do not occur, get final product termination test.If it find that involve cornea or have other Eye irritation effect, not recuperator in 7 days, observing time need to be extended for the reversibility or irreversibility determining this infringement, be usually no more than 21 days.Irritant reaction evaluation is carried out with reference to " cosmetics health specification (2007 editions) " regulation.
Acute ocular stimulates test result as shown in table 4:
By the acute ocular stimulation test result of table 4 it can be seen that the eye irritation of rabbit is tested and had no irritative response by Flos Camelliae Japonicae quintessence oil cream for skin care prepared by embodiment 4-6.Therefore the Flos Camelliae Japonicae quintessence oil cream for skin care of the present invention, acute eye irritation test shows do not have acute ocular zest.
4, moisture of skin test
Using Germany CK company moisture of skin tester MPA10, during test, moisture measurement probe vertical is pressed in tested inner forearm skin surface, probe top is pushed back a segment distance, keeps the pressure of 0.16N, just demonstrates result in one second on main frame.Test condition is temperature 25 ± 2 DEG C, humidity 50 ± 10%.Test result is as shown in Figure 1.
From the moisture of skin test result of Fig. 1, Flos Camelliae Japonicae quintessence oil cream for skin care prepared by embodiment 4-6 all after smearing 30min reach best moistening effect, after 90min, moisture rate of increase is all higher than 0, explanation moistening effect is good, and there is stronger lasting moisture-retaining capacity, wherein the effect of embodiment 6 is best.
In sum, the Flos Camelliae Japonicae quintessence oil cream for skin care of the preparation of the present invention, its each raw material all adopts pure natural raw material, derive from edible raw material, formula uses natural bacteriostatic composition and the Natural antioxidant, compatibility is good, and cutaneous safety test is non-stimulated, is a kind of health, gentleness, safe and stable and can the cosmetic product of permanent moisturizing.
Obviously, the above embodiment of the present invention is only for clearly demonstrating example of the present invention, and is not the restriction to embodiments of the present invention；For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description, here without also cannot all of embodiment be given exhaustive；All any amendment, equivalent replacement and improvement etc. made within the spirit and principles in the present invention, should be included within the protection domain of the claims in the present invention.
Claims (7)
1. a Flos Camelliae Japonicae quintessence oil cream for skin care, it is characterised in that be made up of Flos Camelliae Japonicae extracting solution, Oleum Camelliae, Princepia utilis oil, Flos Camelliae Japonicae essential oil component.
2. a kind of Flos Camelliae Japonicae quintessence oil cream for skin care according to claim 1, it is characterised in that described each component is calculated by weight as: Flos Camelliae Japonicae extracting solution 30 ~ 35 parts, Oleum Camelliae 50 ~ 60 parts, Princepia utilis oil 9.5 ~ 18.5 parts, Flos Camelliae Japonicae quintessence oil 0.5 ~ 1.5 part.
3. the preparation technology of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care according to claim 1 and 2, it is characterised in that described preparation technology specifically comprises the following steps that
S1. Flos Camelliae Japonicae extract and deionized water are added in stirring container and be sufficiently stirred for, carry out high-speed stirred afterwards and produce eddy current to stirring container；
S2., after step S1 stirring produces eddy current, it is sequentially added into Oleum Camelliae, Princepia utilis oil, mix and blend heat temperature raising；
S3. under step S2 constant temperature stirs, adding Flos Camelliae Japonicae quintessence oil, after mix and blend in suction emulsifying pot, open homogenizing, homogenizing speed is 3000rpm, mixes modified to complete emulsifying in emulsifying pot；
S4., after the complete emulsifying of step S3, regulate pH value to neutral with edible sodium bicarbonate or citric acid solution, be cooled to suitable subpackage temperature, stir, sterilization, sterilizing, fill, obtain Flos Camelliae Japonicae quintessence oil cream for skin care.
4. the preparation technology of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care according to claim 3, it is characterised in that in described step S1, mixing time is 30 ~ 50min.
5. the preparation technology of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care according to claim 3, it is characterised in that in described step S2, mixing time is 20 ~ 30min, and temperature is 70 DEG C ~ 75 DEG C.
6. the preparation technology of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care according to claim 3, it is characterised in that the Oleum Camelliae in described step S2 is that white flower oil Camellia sinensis camellia oleosa seed selects through air-dry color, shells, steaming and decocting, squeezing, high-pressure filteration step prepare.
7. the preparation technology of a kind of Flos Camelliae Japonicae quintessence oil cream for skin care according to claim 3, it is characterised in that in described step S3, mixing time is 20 ~ 30min, and homogenizing time is 10～30min, and emulsifying temperature is 70 DEG C ~ 75 DEG C.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110384649A (en) * | 2019-07-18 | 2019-10-29 | 吕利民 | A kind of Chinese medicine cytothesis facial treatment essence liquid |
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