CN107898747B - Natural camellia oleifera lip balm with nourishing and moisturizing effects - Google Patents
Natural camellia oleifera lip balm with nourishing and moisturizing effects Download PDFInfo
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- CN107898747B CN107898747B CN201711439082.XA CN201711439082A CN107898747B CN 107898747 B CN107898747 B CN 107898747B CN 201711439082 A CN201711439082 A CN 201711439082A CN 107898747 B CN107898747 B CN 107898747B
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- 241000526900 Camellia oleifera Species 0.000 title claims abstract description 22
- 239000007934 lip balm Substances 0.000 title claims abstract description 21
- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 14
- 244000269722 Thea sinensis Species 0.000 claims abstract description 72
- 235000013616 tea Nutrition 0.000 claims abstract description 57
- 239000000341 volatile oil Substances 0.000 claims abstract description 34
- 239000000203 mixture Substances 0.000 claims abstract description 27
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 27
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 27
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 22
- 238000002156 mixing Methods 0.000 claims abstract description 20
- 239000010495 camellia oil Substances 0.000 claims abstract description 19
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000009508 confectionery Nutrition 0.000 claims abstract description 18
- 238000010438 heat treatment Methods 0.000 claims abstract description 17
- 239000003921 oil Substances 0.000 claims abstract description 16
- 238000001035 drying Methods 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 12
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229930003270 Vitamin B Natural products 0.000 claims abstract description 11
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 11
- 235000013871 bee wax Nutrition 0.000 claims abstract description 11
- 239000012166 beeswax Substances 0.000 claims abstract description 11
- 238000004821 distillation Methods 0.000 claims abstract description 11
- 238000000605 extraction Methods 0.000 claims abstract description 11
- 235000012907 honey Nutrition 0.000 claims abstract description 11
- 235000019156 vitamin B Nutrition 0.000 claims abstract description 11
- 239000011720 vitamin B Substances 0.000 claims abstract description 11
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 11
- 239000011718 vitamin C Substances 0.000 claims abstract description 11
- 235000006468 Thea sinensis Nutrition 0.000 claims abstract description 9
- 229930003427 Vitamin E Natural products 0.000 claims abstract description 9
- 235000020279 black tea Nutrition 0.000 claims abstract description 9
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims abstract description 9
- 235000019165 vitamin E Nutrition 0.000 claims abstract description 9
- 229940046009 vitamin E Drugs 0.000 claims abstract description 9
- 239000011709 vitamin E Substances 0.000 claims abstract description 9
- 235000009569 green tea Nutrition 0.000 claims abstract description 7
- 238000002360 preparation method Methods 0.000 claims abstract description 3
- 238000007873 sieving Methods 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 10
- 238000002791 soaking Methods 0.000 claims description 10
- 238000010298 pulverizing process Methods 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 238000004587 chromatography analysis Methods 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 230000001954 sterilising effect Effects 0.000 claims description 5
- 238000004659 sterilization and disinfection Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 239000002932 luster Substances 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 3
- 235000013305 food Nutrition 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 7
- 244000062730 Melissa officinalis Species 0.000 description 4
- 235000010654 Melissa officinalis Nutrition 0.000 description 4
- 235000019225 fermented tea Nutrition 0.000 description 4
- 239000000865 liniment Substances 0.000 description 4
- 238000009210 therapy by ultrasound Methods 0.000 description 4
- 238000009835 boiling Methods 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 240000001548 Camellia japonica Species 0.000 description 2
- 239000004677 Nylon Substances 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 235000006708 antioxidants Nutrition 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 235000018597 common camellia Nutrition 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 229930003935 flavonoid Natural products 0.000 description 2
- 150000002215 flavonoids Chemical class 0.000 description 2
- 235000017173 flavonoids Nutrition 0.000 description 2
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- YYGNTYWPHWGJRM-UHFFFAOYSA-N (6E,10E,14E,18E)-2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC=C(C)CCC=C(C)CCC=C(C)C YYGNTYWPHWGJRM-UHFFFAOYSA-N 0.000 description 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 240000006914 Aspalathus linearis Species 0.000 description 1
- 235000012984 Aspalathus linearis Nutrition 0.000 description 1
- 240000006833 Camellia sasanqua Species 0.000 description 1
- 235000002537 Camellia sasanqua Nutrition 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- 206010040844 Skin exfoliation Diseases 0.000 description 1
- BHEOSNUKNHRBNM-UHFFFAOYSA-N Tetramethylsqualene Natural products CC(=C)C(C)CCC(=C)C(C)CCC(C)=CCCC=C(C)CCC(C)C(=C)CCC(C)C(C)=C BHEOSNUKNHRBNM-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 235000010208 anthocyanin Nutrition 0.000 description 1
- 229930002877 anthocyanin Natural products 0.000 description 1
- 239000004410 anthocyanin Substances 0.000 description 1
- 150000004636 anthocyanins Chemical class 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013868 candelilla wax Nutrition 0.000 description 1
- 229940073532 candelilla wax Drugs 0.000 description 1
- 239000004204 candelilla wax Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000035618 desquamation Effects 0.000 description 1
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N dodecahydrosqualene Natural products CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 210000003746 feather Anatomy 0.000 description 1
- 150000007946 flavonol Chemical class 0.000 description 1
- HVQAJTFOCKOKIN-UHFFFAOYSA-N flavonol Natural products O1C2=CC=CC=C2C(=O)C(O)=C1C1=CC=CC=C1 HVQAJTFOCKOKIN-UHFFFAOYSA-N 0.000 description 1
- 235000011957 flavonols Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- IUJAMGNYPWYUPM-UHFFFAOYSA-N hentriacontane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC IUJAMGNYPWYUPM-UHFFFAOYSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 229960002969 oleic acid Drugs 0.000 description 1
- 229940056211 paraffin Drugs 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 150000007965 phenolic acids Chemical class 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 229940031439 squalene Drugs 0.000 description 1
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 1
- 229940099259 vaseline Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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Abstract
The invention relates to a natural camellia oleifera lip balm with nourishing and moisturizing effects, and belongs to the technical field of daily chemical products. The main technical scheme is as follows: the feed is prepared from the following raw materials in parts by mass: 15-20 parts of camellia oil, 3-5 parts of beeswax, 4-6 parts of tea sweet essential oil, 4-6 parts of camellia oleifera polyphenol, 1-4 parts of honey, 2-3 parts of vitamin C, 1-4 parts of vitamin E essential oil and 2-3 parts of vitamin B; the preparation method of the tea sweet dew essential oil comprises the following steps: mixing green tea 8-10 parts, black tea 6-8 parts, and black tea 2-4 parts, drying at 50 deg.C, adding camellia oil 2-4 times the weight of the mixture, heating to boil with a simultaneous distillation and extraction device, distilling and extracting for 30min, circulating for 2 times, collecting and mixing the distillate to obtain tea nectar essential oil. The invention provides a natural mountain oil tea lip balm with nourishing and moisturizing effects, which has the characteristics of greenness, pure naturalness, food grade, uniform color and luster, and high moisturizing and moisturizing effects.
Description
Technical Field
The invention belongs to the technical field of daily chemical products, and particularly relates to a natural camellia oleifera lip balm with nourishing and moisturizing effects.
Background
The lip balm mainly plays a role in protecting lips without sebaceous glands and protective barriers, repairing damaged lip skins, moistening and maintaining the lip skins, and preventing the occurrence of poor lip problems such as dryness, desquamation and the like of the lips. Therefore, the lipstick with good quality and superior quality is strongly demanded by consumers.
The lip cosmetics are difficult to avoid entering the body by the mouth because the using part of the lip cosmetics is the lips, so the raw materials of the lip balm must be ensured to be non-toxic and harmless to the human body. At present, the main components of the existing lip balm are grease and wax, the used raw materials are mostly artificial or chemically synthesized grease, the wax body is mostly candelilla wax, paraffin or vaseline and the like, and the lip balm can generate adverse effects when contacting the skin of the lips for a long time and cause secondary damage to the lips. The safety and the functional value are worried about, and in addition, the existing lip care cream has poor moistening degree, poor moisturizing effect and insufficient and uniform gloss.
Disclosure of Invention
In order to make up the defects of the prior art, the invention provides the natural mountain oil tea lip balm with the nourishing and moisturizing effects, which has the characteristics of greenness, pure naturalness, food grade, uniform color and luster, and high moistening and moisturizing effects.
The technical scheme of the invention is as follows: a natural camellia oleifera lip balm with nourishing and moisturizing effects is prepared from the following raw materials in parts by weight: 15-20 parts of camellia oil, 3-5 parts of beeswax, 4-6 parts of tea sweet essential oil, 4-6 parts of camellia oleifera polyphenol, 1-4 parts of honey, 2-3 parts of vitamin C, 1-4 parts of vitamin E essential oil and 2-3 parts of vitamin B;
the preparation method of the tea sweet dew essential oil comprises the following steps: mixing green tea 8-10 parts, black tea 6-8 parts and black tea 2-4 parts, drying at 50 deg.C, pulverizing, sieving with 60 mesh sieve, adding camellia oil 2-4 times the weight of the mixture, ultrasonic treating for 15-20min, heating to boil with simultaneous distillation and extraction device, distilling and extracting for 30min, circulating for 2 times, collecting and mixing the distillate to obtain tea nectar essential oil.
Further, the feed is prepared from the following raw materials in parts by mass: 15 parts of camellia oil, 3 parts of beeswax, 4 parts of tea sweet essential oil, 4 parts of camellia polyphenol, 1 part of honey, 2 parts of vitamin C, 1 part of vitamin E essential oil and 2 parts of vitamin B.
Further, the feed is prepared from the following raw materials in parts by mass: 20 parts of camellia oil, 5 parts of beeswax, 6 parts of tea sweet essential oil, 6 parts of camellia polyphenol, 4 parts of honey, 3 parts of vitamin C, 4 parts of vitamin E essential oil and 3 parts of vitamin B.
Further, the feed is prepared from the following raw materials in parts by mass: 18 parts of camellia oil, 4 parts of beeswax, 5 parts of tea sweet essential oil, 5 parts of camellia oleifera polyphenol, 3 parts of honey, 3 parts of vitamin C, 2 parts of vitamin E essential oil and 2 parts of vitamin B.
Tea polyphenol is a general term for polyphenol substances in tea, comprises anthocyanin, flavonoid, flavonol, phenolic acid and the like, and is a main component for forming the color, the aroma and the health-care function of the tea. The tea polyphenol has strong antioxidation, can prolong the storage period of the product, prevent the product from fading, improve the stability of the product and effectively protect various nutritional ingredients of the product.
The invention has the following beneficial effects:
(1) the natural camellia oleifera lip balm produced by the method disclosed by the invention is green and purely natural, is food-grade, uniform in color and luster, high in moisture and humidity, and has the effect of creating tender Q-shaped elastic lips. Compared with the products in the prior art, the product has greatly improved sense, practicability, safety, stability and controllability, and the raw materials all adopt pure natural components to accord with the development trend of the lip balm;
(2) the raw material camellia oil used by the invention contains oleic acid, squalene, vitamins and other components which are easily absorbed by skin, and has good skin-care and lip-protecting effects; the lipstick contains antioxidant components such as flavonoids and tea polyphenol, can protect color and fade lip wrinkles, and simultaneously prolongs the shelf life of the lipstick;
(3) the tea nectar essential oil used as the raw material of the lipstick mainly contains tea polyphenol which is a natural rare antioxidant and fresh-keeping color-protecting component, has a strong inhibition effect on rancidity of grease, can greatly prolong the quality guarantee period of the lipstick, and greatly improves the functional effect of the lipstick due to the addition of the tea nectar essential oil and the oil tea polyphenol.
Detailed Description
The present invention will be further described with reference to specific embodiments, and the raw materials used in the present invention are commercially available unless otherwise specified.
Example 1
(1) Extracting tea sweet dew essential oil: mixing 8 parts of green tea, 6 parts of black tea and 2 parts of dark tea uniformly, drying at 50 ℃, crushing, sieving with a 60-mesh sieve, adding camellia oil 2 times of the mixture in mass, performing ultrasonic treatment for 15min, heating to boil by using a simultaneous distillation and extraction device, performing distillation and extraction for 30min, circulating for 2 times, collecting and combining distillate to obtain tea nectar essential oil;
(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 4 times of anhydrous ethanol, ultrasonic treating for 20min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure (0.06Mpa) to obtain dried product, i.e. tea polyphenols;
(3) adding 3 parts of beeswax into 15 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 1 part of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;
(4) adding 4 parts of prepared tea sweet oil and 4 parts of oil tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;
(5) adding 2 parts of vitamin C, 2 parts of vitamin B and 1 parts of essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.
Example 2
(1) Extracting tea sweet dew essential oil: mixing 10 parts of green tea, 8 parts of red tea and 4 parts of dark tea uniformly, drying at 50 ℃, crushing, sieving with a 60-mesh sieve, adding camellia oil with the mass of 4 times of that of the mixture, carrying out ultrasonic treatment for 20min, heating to boiling by using a simultaneous distillation and extraction device, carrying out distillation and extraction for 30min, circulating for 2 times, collecting and combining distillate to obtain tea nectar essential oil;
(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 4 times of anhydrous ethanol, ultrasonic treating for 20min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure to obtain dried product to obtain tea polyphenols;
(3) adding 5 parts of beeswax into 20 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 4 parts of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;
(4) adding 6 parts of prepared tea sweet dew essential oil and 6 parts of tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;
(5) adding 3 parts of vitamin C, 3 parts of vitamin B and 4 parts of vitamin E essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.
Example 3
(1) Extracting tea sweet dew essential oil: mixing 9 parts of green tea, 7 parts of black tea and 3 parts of dark tea uniformly, drying at 50 ℃, crushing, sieving with a 60-mesh sieve, adding camellia oil with the mass of 3 times of that of the mixture, carrying out ultrasonic treatment for 18min, heating to boiling by using a simultaneous distillation and extraction device, carrying out distillation and extraction for 30min, circulating for 2 times, collecting and combining distillate to obtain tea nectar essential oil;
(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 3 times of anhydrous ethanol, ultrasonic treating for 18min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure to obtain dried product to obtain pure product of tea polyphenols;
(3) adding 4 parts of beeswax into 20 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 3 parts of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;
(4) adding 5 parts of prepared tea sweet oil and 6 parts of oil tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;
(5) adding 3 parts of vitamin C, 2 parts of vitamin B and 2 parts of vitamin E essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.
Example 4
(1) Extracting tea sweet dew essential oil: mixing 9 parts of green tea, 7 parts of black tea and 3 parts of dark tea, drying at 50 ℃, crushing, sieving with a 60-mesh sieve, adding camellia oil 2-4 times of the mixture in mass, performing ultrasonic treatment for 18min, heating to boiling by using a simultaneous distillation and extraction device, performing distillation and extraction for 30min, circulating for 2 times, collecting and combining distillate to obtain tea nectar essential oil;
(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 3 times of anhydrous ethanol, ultrasonic treating for 18min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure to obtain dried product to obtain pure product of tea polyphenols;
(3) adding 4 parts of beeswax into 18 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 3 parts of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;
(4) adding 5 parts of prepared tea sweet oil and 5 parts of oil tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;
(5) adding 3 parts of vitamin C, 2 parts of vitamin B and 4 parts of vitamin E essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.
EXAMPLE 4 lipstick Properties determination
1. Temperature resistance test
The lipstick body changes were observed by taking 4 lipsticks prepared in examples 1 to 4 as an experimental group and a brand of similar products on the market as a control group, setting the experimental temperature to-40 + -5 ℃ and the experimental temperature to 40 + -5 ℃ for 24 hours respectively according to the air temperature conditions all the year round, and the results are shown in Table 2.
TABLE 2 lipstick temperature resistance test results
Sample (I) | Control group | Example 1 | Example 2 | Example 3 | Example 4 |
Crack by desiccation | Is free of | Is free of | Is free of | Is free of | Is free of |
Deformation of | Light and slight | Is free of | Is free of | Is free of | Is free of |
As can be seen from the results in Table 2, the four lipsticks of examples 1-4 did not crack, break or deform, while the commercially available lipstick deformed slightly at 40 + -5 deg.C; therefore, the lipstick prepared by the invention has excellent temperature resistance, is easy to store, and can better adapt to temperature change all the year round. 2. Moisture test
The 4 lipsticks prepared in examples 1 to 4 were used as an experimental group, a brand of the same kind of commercially available product was used as a control group, 5 women were found at room temperature (25 ℃), and the 5 lipsticks were coated in such a manner that the upper and lower lips were coated twice from left to right, respectively, and the prepared sheet-like feathers of uniform size were touched with both lips, and the experimental results are shown in Table 3.
TABLE 3 lipstick moisturization test results
Sample (I) | Control group | Example 1 | Example 2 | Example 3 | Example 4 |
Root number of | 0 | 1 | 2 | 2 | 2 |
As can be seen from Table 3, the lip balms of examples 1-4 had a higher moisturization than the control, and also met the standard moisturization of lip balms, had a suitable degree of stickiness, and had a more comfortable, silky and moist feel on the lips.
3. Ductility test
The 4 lipsticks prepared in examples 1 to 4 were used as an experimental group, a commercially available similar product of a certain brand was used as a control group, a ductility test was conducted, 0.3cm of a lipstick in a tube of the same specification was uniformly applied to nylon cloth having a length of 50cm and a width of 2cm, respectively, the length of a lipstick retaining mark of the nylon cloth was measured, and continuity of the lipstick mark was observed. The test results are shown in Table 4 below.
TABLE 4 lipstick extensibility test results
Sample (I) | Control group | Example 1 | Example 2 | Example 3 | Example 4 |
Length (cm) | 30.2 | 35.3 | 37.1 | 40.5 | 40.2 |
Paste mark | With discontinuity | Continuous | Continuous | Continuous | Continuous |
As can be seen from Table 4, the lip balms of examples 1-4 had higher extensibility than the control, continuous and uniform coating, comfortable feeling in use, and high practicability.
4. Moisture retention test
The 4 lipsticks prepared in examples 1 to 4 were used as an experimental group, a commercially available similar product of a certain brand was used as a control group, a moisture retention test was conducted, and the same quality of the lipstick was placed at room temperature under the same conditions for 24 hours, and the quality thereof was measured. The test results are shown in Table 5 below.
TABLE 5 lipstick moisturization test results
As is apparent from Table 5, the lip balms of examples 1 to 4 had higher moisturizing properties than the control, and had higher lip nourishing and moisturizing properties and higher durability after coating.
The natural camellia sasanqua lip balm prepared in example 2 was subjected to trial effect evaluation, and the results are shown in table 6 below;
table 6 trial effect evaluation table
As shown in Table 6, the natural camellia oleifera lip balm prepared by the invention has the advantages of uniform color, soft and shiny luster, normal smell, elegant tea fragrance, harmonious aftertaste, no peculiar smell, smooth surface, no air holes, fine paste, and no cracking or softening after being cut.
Claims (1)
1. The natural camellia oleifera lip balm with nourishing and moisturizing effects is characterized by being prepared from the following raw materials in parts by mass: 15-20 parts of camellia oil, 3-5 parts of beeswax, 4-6 parts of tea sweet essential oil, 4-6 parts of camellia oleifera polyphenol, 1-4 parts of honey, 2-3 parts of vitamin C, 1-4 parts of vitamin E essential oil and 2-3 parts of vitamin B;
(1) the preparation method of the tea sweet dew essential oil comprises the following steps: mixing green tea 8-10 parts, black tea 6-8 parts and black tea 2-4 parts, drying at 50 deg.C, pulverizing, sieving with 60 mesh sieve, adding camellia oil 2-4 times the weight of the mixture, ultrasonic treating for 15-20min, heating to boil with simultaneous distillation and extraction device, distilling and extracting for 30min, circulating for 2 times, collecting and mixing the distillate to obtain tea nectar essential oil;
(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 4 times of anhydrous ethanol, ultrasonic treating for 20min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure of 0.06Mpa to obtain dried product, i.e. tea polyphenols;
(3) adding 3 parts of beeswax into 15 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 1 part of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;
(4) adding 4 parts of prepared tea sweet oil and 4 parts of oil tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;
(5) adding 2 parts of vitamin C, 2 parts of vitamin B and 1 parts of essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.
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