CN107898747B - Natural camellia oleifera lip balm with nourishing and moisturizing effects - Google Patents

Abstract

The invention relates to a natural camellia oleifera lip balm with nourishing and moisturizing effects, and belongs to the technical field of daily chemical products. The main technical scheme is as follows: the feed is prepared from the following raw materials in parts by mass: 15-20 parts of camellia oil, 3-5 parts of beeswax, 4-6 parts of tea sweet essential oil, 4-6 parts of camellia oleifera polyphenol, 1-4 parts of honey, 2-3 parts of vitamin C, 1-4 parts of vitamin E essential oil and 2-3 parts of vitamin B; the preparation method of the tea sweet dew essential oil comprises the following steps: mixing green tea 8-10 parts, black tea 6-8 parts, and black tea 2-4 parts, drying at 50 deg.C, adding camellia oil 2-4 times the weight of the mixture, heating to boil with a simultaneous distillation and extraction device, distilling and extracting for 30min, circulating for 2 times, collecting and mixing the distillate to obtain tea nectar essential oil. The invention provides a natural mountain oil tea lip balm with nourishing and moisturizing effects, which has the characteristics of greenness, pure naturalness, food grade, uniform color and luster, and high moisturizing and moisturizing effects.

Description

Natural camellia oleifera lip balm with nourishing and moisturizing effects

Technical Field

The invention belongs to the technical field of daily chemical products, and particularly relates to a natural camellia oleifera lip balm with nourishing and moisturizing effects.

Background

The lip balm mainly plays a role in protecting lips without sebaceous glands and protective barriers, repairing damaged lip skins, moistening and maintaining the lip skins, and preventing the occurrence of poor lip problems such as dryness, desquamation and the like of the lips. Therefore, the lipstick with good quality and superior quality is strongly demanded by consumers.

The lip cosmetics are difficult to avoid entering the body by the mouth because the using part of the lip cosmetics is the lips, so the raw materials of the lip balm must be ensured to be non-toxic and harmless to the human body. At present, the main components of the existing lip balm are grease and wax, the used raw materials are mostly artificial or chemically synthesized grease, the wax body is mostly candelilla wax, paraffin or vaseline and the like, and the lip balm can generate adverse effects when contacting the skin of the lips for a long time and cause secondary damage to the lips. The safety and the functional value are worried about, and in addition, the existing lip care cream has poor moistening degree, poor moisturizing effect and insufficient and uniform gloss.

Disclosure of Invention

In order to make up the defects of the prior art, the invention provides the natural mountain oil tea lip balm with the nourishing and moisturizing effects, which has the characteristics of greenness, pure naturalness, food grade, uniform color and luster, and high moistening and moisturizing effects.

The technical scheme of the invention is as follows: a natural camellia oleifera lip balm with nourishing and moisturizing effects is prepared from the following raw materials in parts by weight: 15-20 parts of camellia oil, 3-5 parts of beeswax, 4-6 parts of tea sweet essential oil, 4-6 parts of camellia oleifera polyphenol, 1-4 parts of honey, 2-3 parts of vitamin C, 1-4 parts of vitamin E essential oil and 2-3 parts of vitamin B;

the preparation method of the tea sweet dew essential oil comprises the following steps: mixing green tea 8-10 parts, black tea 6-8 parts and black tea 2-4 parts, drying at 50 deg.C, pulverizing, sieving with 60 mesh sieve, adding camellia oil 2-4 times the weight of the mixture, ultrasonic treating for 15-20min, heating to boil with simultaneous distillation and extraction device, distilling and extracting for 30min, circulating for 2 times, collecting and mixing the distillate to obtain tea nectar essential oil.

Further, the feed is prepared from the following raw materials in parts by mass: 15 parts of camellia oil, 3 parts of beeswax, 4 parts of tea sweet essential oil, 4 parts of camellia polyphenol, 1 part of honey, 2 parts of vitamin C, 1 part of vitamin E essential oil and 2 parts of vitamin B.

Further, the feed is prepared from the following raw materials in parts by mass: 20 parts of camellia oil, 5 parts of beeswax, 6 parts of tea sweet essential oil, 6 parts of camellia polyphenol, 4 parts of honey, 3 parts of vitamin C, 4 parts of vitamin E essential oil and 3 parts of vitamin B.

Further, the feed is prepared from the following raw materials in parts by mass: 18 parts of camellia oil, 4 parts of beeswax, 5 parts of tea sweet essential oil, 5 parts of camellia oleifera polyphenol, 3 parts of honey, 3 parts of vitamin C, 2 parts of vitamin E essential oil and 2 parts of vitamin B.

Tea polyphenol is a general term for polyphenol substances in tea, comprises anthocyanin, flavonoid, flavonol, phenolic acid and the like, and is a main component for forming the color, the aroma and the health-care function of the tea. The tea polyphenol has strong antioxidation, can prolong the storage period of the product, prevent the product from fading, improve the stability of the product and effectively protect various nutritional ingredients of the product.

The invention has the following beneficial effects:

(1) the natural camellia oleifera lip balm produced by the method disclosed by the invention is green and purely natural, is food-grade, uniform in color and luster, high in moisture and humidity, and has the effect of creating tender Q-shaped elastic lips. Compared with the products in the prior art, the product has greatly improved sense, practicability, safety, stability and controllability, and the raw materials all adopt pure natural components to accord with the development trend of the lip balm;

(2) the raw material camellia oil used by the invention contains oleic acid, squalene, vitamins and other components which are easily absorbed by skin, and has good skin-care and lip-protecting effects; the lipstick contains antioxidant components such as flavonoids and tea polyphenol, can protect color and fade lip wrinkles, and simultaneously prolongs the shelf life of the lipstick;

(3) the tea nectar essential oil used as the raw material of the lipstick mainly contains tea polyphenol which is a natural rare antioxidant and fresh-keeping color-protecting component, has a strong inhibition effect on rancidity of grease, can greatly prolong the quality guarantee period of the lipstick, and greatly improves the functional effect of the lipstick due to the addition of the tea nectar essential oil and the oil tea polyphenol.

Detailed Description

The present invention will be further described with reference to specific embodiments, and the raw materials used in the present invention are commercially available unless otherwise specified.

Example 1

(1) Extracting tea sweet dew essential oil: mixing 8 parts of green tea, 6 parts of black tea and 2 parts of dark tea uniformly, drying at 50 ℃, crushing, sieving with a 60-mesh sieve, adding camellia oil 2 times of the mixture in mass, performing ultrasonic treatment for 15min, heating to boil by using a simultaneous distillation and extraction device, performing distillation and extraction for 30min, circulating for 2 times, collecting and combining distillate to obtain tea nectar essential oil;

(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 4 times of anhydrous ethanol, ultrasonic treating for 20min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure (0.06Mpa) to obtain dried product, i.e. tea polyphenols;

(3) adding 3 parts of beeswax into 15 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 1 part of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;

(4) adding 4 parts of prepared tea sweet oil and 4 parts of oil tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;

(5) adding 2 parts of vitamin C, 2 parts of vitamin B and 1 parts of essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.

Example 2

(1) Extracting tea sweet dew essential oil: mixing 10 parts of green tea, 8 parts of red tea and 4 parts of dark tea uniformly, drying at 50 ℃, crushing, sieving with a 60-mesh sieve, adding camellia oil with the mass of 4 times of that of the mixture, carrying out ultrasonic treatment for 20min, heating to boiling by using a simultaneous distillation and extraction device, carrying out distillation and extraction for 30min, circulating for 2 times, collecting and combining distillate to obtain tea nectar essential oil;

(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 4 times of anhydrous ethanol, ultrasonic treating for 20min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure to obtain dried product to obtain tea polyphenols;

(3) adding 5 parts of beeswax into 20 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 4 parts of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;

(4) adding 6 parts of prepared tea sweet dew essential oil and 6 parts of tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;

(5) adding 3 parts of vitamin C, 3 parts of vitamin B and 4 parts of vitamin E essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.

Example 3

(1) Extracting tea sweet dew essential oil: mixing 9 parts of green tea, 7 parts of black tea and 3 parts of dark tea uniformly, drying at 50 ℃, crushing, sieving with a 60-mesh sieve, adding camellia oil with the mass of 3 times of that of the mixture, carrying out ultrasonic treatment for 18min, heating to boiling by using a simultaneous distillation and extraction device, carrying out distillation and extraction for 30min, circulating for 2 times, collecting and combining distillate to obtain tea nectar essential oil;

(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 3 times of anhydrous ethanol, ultrasonic treating for 18min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure to obtain dried product to obtain pure product of tea polyphenols;

(3) adding 4 parts of beeswax into 20 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 3 parts of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;

(4) adding 5 parts of prepared tea sweet oil and 6 parts of oil tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;

(5) adding 3 parts of vitamin C, 2 parts of vitamin B and 2 parts of vitamin E essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.

Example 4

(1) Extracting tea sweet dew essential oil: mixing 9 parts of green tea, 7 parts of black tea and 3 parts of dark tea, drying at 50 ℃, crushing, sieving with a 60-mesh sieve, adding camellia oil 2-4 times of the mixture in mass, performing ultrasonic treatment for 18min, heating to boiling by using a simultaneous distillation and extraction device, performing distillation and extraction for 30min, circulating for 2 times, collecting and combining distillate to obtain tea nectar essential oil;

(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 3 times of anhydrous ethanol, ultrasonic treating for 18min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure to obtain dried product to obtain pure product of tea polyphenols;

(3) adding 4 parts of beeswax into 18 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 3 parts of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;

(4) adding 5 parts of prepared tea sweet oil and 5 parts of oil tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;

(5) adding 3 parts of vitamin C, 2 parts of vitamin B and 4 parts of vitamin E essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.

EXAMPLE 4 lipstick Properties determination

1. Temperature resistance test

The lipstick body changes were observed by taking 4 lipsticks prepared in examples 1 to 4 as an experimental group and a brand of similar products on the market as a control group, setting the experimental temperature to-40 + -5 ℃ and the experimental temperature to 40 + -5 ℃ for 24 hours respectively according to the air temperature conditions all the year round, and the results are shown in Table 2.

TABLE 2 lipstick temperature resistance test results

Sample (I)	Control group	Example 1	Example 2	Example 3	Example 4
						Crack by desiccation	Is free of	Is free of	Is free of	Is free of	Is free of
Deformation of	Light and slight	Is free of	Is free of	Is free of	Is free of

As can be seen from the results in Table 2, the four lipsticks of examples 1-4 did not crack, break or deform, while the commercially available lipstick deformed slightly at 40 + -5 deg.C; therefore, the lipstick prepared by the invention has excellent temperature resistance, is easy to store, and can better adapt to temperature change all the year round. 2. Moisture test

The 4 lipsticks prepared in examples 1 to 4 were used as an experimental group, a brand of the same kind of commercially available product was used as a control group, 5 women were found at room temperature (25 ℃), and the 5 lipsticks were coated in such a manner that the upper and lower lips were coated twice from left to right, respectively, and the prepared sheet-like feathers of uniform size were touched with both lips, and the experimental results are shown in Table 3.

TABLE 3 lipstick moisturization test results

Sample (I)	Control group	Example 1	Example 2	Example 3	Example 4
						Root number of	0	1	2	2	2

As can be seen from Table 3, the lip balms of examples 1-4 had a higher moisturization than the control, and also met the standard moisturization of lip balms, had a suitable degree of stickiness, and had a more comfortable, silky and moist feel on the lips.

3. Ductility test

The 4 lipsticks prepared in examples 1 to 4 were used as an experimental group, a commercially available similar product of a certain brand was used as a control group, a ductility test was conducted, 0.3cm of a lipstick in a tube of the same specification was uniformly applied to nylon cloth having a length of 50cm and a width of 2cm, respectively, the length of a lipstick retaining mark of the nylon cloth was measured, and continuity of the lipstick mark was observed. The test results are shown in Table 4 below.

TABLE 4 lipstick extensibility test results

Sample (I)	Control group	Example 1	Example 2	Example 3	Example 4
						Length (cm)	30.2	35.3	37.1	40.5	40.2
Paste mark	With discontinuity	Continuous	Continuous	Continuous	Continuous

As can be seen from Table 4, the lip balms of examples 1-4 had higher extensibility than the control, continuous and uniform coating, comfortable feeling in use, and high practicability.

4. Moisture retention test

The 4 lipsticks prepared in examples 1 to 4 were used as an experimental group, a commercially available similar product of a certain brand was used as a control group, a moisture retention test was conducted, and the same quality of the lipstick was placed at room temperature under the same conditions for 24 hours, and the quality thereof was measured. The test results are shown in Table 5 below.

TABLE 5 lipstick moisturization test results

As is apparent from Table 5, the lip balms of examples 1 to 4 had higher moisturizing properties than the control, and had higher lip nourishing and moisturizing properties and higher durability after coating.

The natural camellia sasanqua lip balm prepared in example 2 was subjected to trial effect evaluation, and the results are shown in table 6 below;

table 6 trial effect evaluation table

As shown in Table 6, the natural camellia oleifera lip balm prepared by the invention has the advantages of uniform color, soft and shiny luster, normal smell, elegant tea fragrance, harmonious aftertaste, no peculiar smell, smooth surface, no air holes, fine paste, and no cracking or softening after being cut.

Claims (1)

1. The natural camellia oleifera lip balm with nourishing and moisturizing effects is characterized by being prepared from the following raw materials in parts by mass: 15-20 parts of camellia oil, 3-5 parts of beeswax, 4-6 parts of tea sweet essential oil, 4-6 parts of camellia oleifera polyphenol, 1-4 parts of honey, 2-3 parts of vitamin C, 1-4 parts of vitamin E essential oil and 2-3 parts of vitamin B;

(1) the preparation method of the tea sweet dew essential oil comprises the following steps: mixing green tea 8-10 parts, black tea 6-8 parts and black tea 2-4 parts, drying at 50 deg.C, pulverizing, sieving with 60 mesh sieve, adding camellia oil 2-4 times the weight of the mixture, ultrasonic treating for 15-20min, heating to boil with simultaneous distillation and extraction device, distilling and extracting for 30min, circulating for 2 times, collecting and mixing the distillate to obtain tea nectar essential oil;

(2) extracting the camellia oleifera tea polyphenol: drying oil tea at 80 deg.C, pulverizing, sieving with 60 mesh sieve, adding 4 times of anhydrous ethanol, ultrasonic treating for 20min, heating to boil, distilling and concentrating, circulating for 3 times, and collecting and mixing concentrated solution; concentrating the concentrated solution again, extracting, filtering, purifying with chromatography column, and concentrating under reduced pressure of 0.06Mpa to obtain dried product, i.e. tea polyphenols;

(3) adding 3 parts of beeswax into 15 parts of camellia oil, soaking for 2 hours at 20 ℃ by using ultrasonic waves, mixing uniformly, adding 1 part of honey, and soaking for 1 hour at 90 ℃ by using ultrasonic waves to obtain a mixture I;

(4) adding 4 parts of prepared tea sweet oil and 4 parts of oil tea polyphenol into the mixture obtained in the step (3), and heating at 80 ℃ for 5min to obtain a mixture II;

(5) adding 2 parts of vitamin C, 2 parts of vitamin B and 1 parts of essential oil into the mixture II, uniformly stirring, naturally cooling to 40 ℃, keeping for 20min, pouring into a sterilization apparatus, and cooling at-7 ℃ for 15min to obtain the natural camellia oleifera lip balm.