CN112957304A

CN112957304A - Plant composition for cosmetics, mixed extracting solution and preparation method

Info

Publication number: CN112957304A
Application number: CN202110266798.4A
Authority: CN
Inventors: 戴伟
Original assignee: Individual
Current assignee: Individual
Priority date: 2021-03-11
Filing date: 2021-03-11
Publication date: 2021-06-15

Abstract

The invention discloses a plant composition for cosmetics, a mixed extracting solution and a preparation method, wherein the plant composition comprises 4-6 g of red ginseng, 8-12 g of centella asiatica, 8-12 g of white mulberry root-bark, 6-10 g of cynomorium songaricum, 8-12 g of flastem milkvetch seed, 6-10 g of liquorice, 8-12 g of salvia miltiorrhiza, 10-14 g of bighead atractylodes rhizome, 5-7 g of pawpaw, 4-8 g of sea buckthorn, 4-8 g of lucid ganoderma, 8-12 g of giant knotweed, 8-12 g of pyracantha fortuneana fruit, 6-10 g of oat, 6-10 g of turmeric and 6-10 g of selaginella tamariscina. The preparation method of the mixed extracting solution comprises the following steps: s1, crushing the materials to be crushed and sieving the materials by a 20-mesh sieve to obtain material powder; mixing and stirring the sheared material fragments and powder uniformly; s2, adding cold water (the cold water is clear water at normal temperature) into the container, soaking the material mixture at normal temperature, and filtering to obtain primary supernatant; s3, soaking the fabric in constant-temperature water at 50 ℃ again, and filtering to obtain secondary supernatant; s4, repeating the step S3, and filtering to obtain a supernatant for three times; s5, mixing the supernatants to obtain a total supernatant, separating impurities from the total supernatant by a high-speed centrifuge, and filtering and concentrating by an ultrafiltration membrane to obtain the mixed extract of the plant composition for cosmetics.

Description

Plant composition for cosmetics, mixed extracting solution and preparation method

Technical Field

The invention relates to the technical field of cosmetics, in particular to a plant composition for cosmetics, a mixed extracting solution and a preparation method.

Background

The beauty is good for people, the pursuit of young and beautiful appearance is the wish of every person, China is a big consumer country of cosmetics, along with the improvement of the consumption level of people and the change of the consumption concept, green beauty is more and more attractive and appreciated by people, the existing cosmetics need to be endowed with various active ingredients to improve the functionality of the existing cosmetics, but the existing active ingredients for the cosmetics are generally directly blended by chemical substances, and the harm to the skin of a human body is great; the countries have sufficient plant resources, and the effective components in the plants are used as the effective components of the cosmetics, so that the cosmetics have lasting and stable efficacy, remarkable and mild effects and high safety, and therefore, the research on the aspect is needed.

Disclosure of Invention

The present invention has been made in view of the above problems, and an object of the present invention is to provide a plant composition, a mixed extract solution, and a method for producing the same, which have improved use effects without causing side effects.

In order to achieve the purpose, the technical scheme of the invention is as follows:

a plant composition for cosmetic comprises Ginseng radix Rubri, herba Centellae, cortex Mori, herba Cynomorii, semen astragali Complanati, Glycyrrhrizae radix, Saviae Miltiorrhizae radix, Atractylodis rhizoma, fructus Chaenomelis, fructus Hippophae, Ganoderma, rhizoma Polygoni Cuspidati, fructus Pyracanthae, herba Avenae Fatuae, Curcuma rhizome, and herba Selaginellae; each part of the plant composition contains 4-6 g of red ginseng, 8-12 g of centella asiatica, 8-12 g of white mulberry root-bark, 6-10 g of cynomorium songaricum, 8-12 g of flastem milkvetch seed, 6-10 g of liquorice, 8-12 g of salvia miltiorrhiza, 10-14 g of bighead atractylodes rhizome, 5-7 g of pawpaw, 4-8 g of sea buckthorn, 4-8 g of lucid ganoderma, 8-12 g of giant knotweed rhizome, 8-12 g of pyracantha fortuneana fruit, 6-10 g of oat, 6-10 g of turmeric and 6-10 g of selaginella tamariscina.

Furthermore, each part of the plant composition contains 5g of red ginseng, 10g of centella, 10g of white mulberry root-bark, 8g of cynomorium songaricum, 10g of flastem milkvetch seed, 8g of liquorice, 10g of salvia miltiorrhiza, 12g of bighead atractylodes rhizome, 6g of pawpaw, 6g of sea-buckthorn, 6g of lucid ganoderma, 10g of giant knotweed rhizome, 10g of pyracantha fortuneana fruit, 8g of oat, 8g of turmeric and 8g of selaginella tamariscina.

Further, the invention also provides a mixed extracting solution of the plant composition, and the mixed extracting solution at least contains ginsenoside Re and glycyrrhizic acid. Ginsenoside Re and glycyrrhizic acid are markers of the mixed extracting solution, the mass percent of the ginsenoside Re is 1.76-1.97%, and the mass percent of the glycyrrhizic acid is 0.81-0.95%.

Further, the invention relates to a preparation method of the extracting solution, which comprises the following steps:

s1, weighing the raw materials in the plant composition according to the required parts, and then crushing the raw materials to be crushed and sieving the crushed raw materials with a 20-mesh sieve to obtain material powder; placing the material powder and the sheared material fragments in a container, and uniformly mixing and stirring;

s2, adding cold water into the container, soaking the material mixture for 0.5-1 h at normal temperature, and filtering to obtain primary supernatant and primary filter residue;

s3, placing the primary filter residue in a heating container, soaking for 0.5-1 h in constant-temperature water at 50 ℃, and filtering to obtain secondary supernatant and secondary filter residue;

s4, placing the secondary filter residue in a heating container, soaking for 0.5-1 h in constant-temperature water at 50 ℃, and filtering to obtain a supernatant for three times;

s5, mixing the primary supernatant, the secondary supernatant and the tertiary supernatant uniformly to obtain a total supernatant, separating impurities from the total supernatant by a high-speed centrifuge, filtering by using ultrafiltration equipment, and concentrating to obtain a mixed extract of the plant composition for cosmetics.

Further, in the step S1, the material processed into thin pieces in the previous stage is cut into pieces of 0.5 to 1 square centimeter.

Further, in the step S2, the mass ratio of the sum of the mass of the material powder and the sheared material pieces to the water is 1: 10.

Further, in step S5, the ultrafiltration apparatus is an ultrafiltration membrane device.

Compared with the prior art, the invention has the advantages and positive effects that:

the plant composition for the cosmetics is formed by combining various plant raw materials, has a strict formula structure and an obvious effect, overcomes the defects of unobvious effect and single effect of certain compositions, has reasonable compatibility of various substances, has complementary effects and fully exerts the whole effect of a group of formulas. The formula of the plant composition has no incompatibility, has no banned substances specified by the state, and has sufficient safety; after the plant composition is extracted, the obtained mixed extracting solution is used as an effective component to be added into cosmetics, so that the cosmetics have the effects of whitening, moisturizing, resisting wrinkles (flattening and reducing fine lines), lightening spots (including acne marks), lightening scars (acne scars), thinning faces and the like after being used, can completely meet the use requirements of people, and have wide market prospect and social benefit.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived from the embodiments of the present invention by a person skilled in the art without any creative effort, should be included in the protection scope of the present invention.

Example 1, this example discloses a botanical composition for cosmetics, wherein the raw materials of the botanical composition include red ginseng, centella asiatica, cortex mori radicis, cynomorium songaricum, semen astragali complanati, liquorice, salvia miltiorrhiza, bighead atractylodes rhizome, pawpaw, sea buckthorn, ganoderma lucidum, polygonum cuspidatum, pyracantha fortuneana, oat, turmeric, selaginella tamariscina; each part of the plant composition comprises 4g of red ginseng, 8g of centella, 8g of white mulberry root-bark, 6g of cynomorium songaricum, 8g of flastem milkvetch seed, 6g of liquorice, 8g of salvia miltiorrhiza, 10g of bighead atractylodes rhizome, 5g of pawpaw, 4g of sea-buckthorn, 4g of lucid ganoderma, 8g of giant knotweed, 8g of pyracantha fortuneana fruit, 6g of oat, 6g of turmeric and 6g of selaginella tamariscina.

Example 2, this example discloses a botanical composition for cosmetics, wherein the raw materials of the botanical composition include red ginseng, centella asiatica, cortex mori radicis, cynomorium songaricum, semen astragali complanati, liquorice, salvia miltiorrhiza, bighead atractylodes rhizome, pawpaw, sea buckthorn, ganoderma lucidum, polygonum cuspidatum, pyracantha fortuneana, oat, turmeric, selaginella tamariscina; each part of the plant composition contains 5g of red ginseng, 10g of centella, 10g of white mulberry root-bark, 8g of cynomorium songaricum, 10g of flastem milkvetch seed, 8g of liquorice, 10g of salvia miltiorrhiza, 12g of bighead atractylodes rhizome, 6g of pawpaw, 6g of sea-buckthorn, 6g of lucid ganoderma, 10g of giant knotweed, 10g of pyracantha fortuneana fruit, 8g of oat, 8g of turmeric and 8g of selaginella tamariscina.

Example 3, this example discloses a botanical composition for cosmetics, wherein the raw materials of the botanical composition for cosmetics include red ginseng, centella asiatica, white mulberry root-bark, cynomorium songaricum, flastem milkvetch seed, licorice, salvia miltiorrhiza, atractylodes macrocephala, papaya, sea buckthorn, ganoderma lucidum, polygonum cuspidatum, pyracantha fortunei, oat, turmeric, selaginella tamariscina; each part of the plant composition for cosmetics comprises 6g of red ginseng, 12g of centella asiatica, 12g of white mulberry root-bark, 10g of cynomorium songaricum, 12g of flastem milkvetch seed, 10g of liquorice, 12g of salvia miltiorrhiza, 14g of bighead atractylodes rhizome, 7g of pawpaw, 8g of sea-buckthorn, 8g of lucid ganoderma, 12g of giant knotweed rhizome, 12g of pyracantha fortuneana fruit, 10g of oat, 10g of turmeric and 10g of selaginella tamariscina.

The brief introduction of the efficacy of each component in the combined formula is as follows:

(1) red ginseng

The main components are as follows: ginsenoside, polysaccharide, volatile oil, amino acids, trace elements, polypeptide, etc.

The red ginseng can inhibit harmful active oxygen increase and has an antioxidant effect on lipid, various active ingredients in the red ginseng, such as amino acid and peptide substances, can be slowly absorbed by skin, can enhance the elasticity of the skin, promote blood circulation, prevent skin aging and wrinkle generation, resist harmful stimulation of the external environment to the skin, deeply moisten the skin, inhibit the reduction of melanin, clear oxygen free radicals, effectively improve pruritus and desquamation phenomena, enable the face to be fine and smooth, enable the skin to be pure white and tender, and is a good product for skin care and beauty.

(2) Centella asiatica

The centella asiatica is subjected to related detection, research, separation and identification, and contains -sitosterol, daucosterol, asiaticoside and madecassoside, asiatic acid and vanillic acid; in addition, amino acids, flavonols, fatty acids, alkaloids, etc.

Centella asiatica can inhibit fibroblast from various sources, especially inhibit growth of fibroblast from scar source, and has the functions of reducing activity of transamidase, reducing acid mucopolysaccharide and collagen content, and inhibiting excessive proliferation of connective tissue matrix and fibrous component, so as to reduce scar. In addition, the asiaticoside can increase the content of hydroxyproline in the skin, promote the formation of collagen in the dermis, regenerate and reconnect fibrin, and achieve the effects of tightening and smoothing the skin.

The asiaticoside can inhibit the growth of fat cells (face thinning effect), prevent skin edema, and avoid obesity. Centella asiatica is applied to cosmetics and is suitable for various skin types.

(3) Cortex Mori

The main components are as follows: umbelliferone, scopoletin, flavone component, cyclosanguinin, morin, morine, cyclosanguinin, -sitosterol, daucosterol, etc.

The mulberry white skin can promote the metabolism of human skin, make the skin of people whiten, can also dispel scars left by acnes, has good effect of removing facial blackheads, can repair damaged histiocytes, fade scars, nourish and whiten the skin, make the skin of women whiten, and has very good effect on the facial skin.

The composition has effects of removing pockmark, fading scar and whitening.

(4) Cynomorium songaricum

Cynomorium songaricum is reputed by desert ginseng, and contains various amino acids, daucosterol and Cynomorium songaricum polysaccharide (D-galactose).

The latest research finds that the cynomorium songaricum polysaccharide can promote the regeneration and metabolism of human cells, enhance the activity of superoxide dismutase (SOD), effectively remove oxygen radicals, inhibit tyrosinase, improve the activity of peroxidized lipase and have obvious anti-aging effect. And the cynomorium songaricum can improve the capability of skin for absorbing oxygen molecules, thereby playing a role in whitening.

(5) Semen astragali Complanati

The main components are as follows: flavonoids, triterpenes, organic acids, amino acids, polypeptides, sterols, proteins, tannins and the like.

The functional substances contained in the product can remove chloasma, freckle, and senile plaque, remove wrinkle, and care skin. The flavonoids contained in the flatstem milkvetch seed are effective free radical scavengers, can reduce the accumulation of lipofuscin in cells, clear the deposition of facial melanin, improve the elasticity of skin, reduce facial wrinkles and enable the facial skin to be moist and flexible; the unsaturated fatty acid contained in the skin care product can smooth and moisten the skin, and the sterol contained in the skin care product has good permeability to the skin, can keep moisture on the surface of the skin, promotes skin metabolism, inhibits skin inflammation, and prevents sunburn, red spots and skin aging. The contained substances of iron, copper, zinc, selenium and the like can prevent sallow complexion, maintain the normal color of the skin and delay the aging of the skin.

It has effects of reducing speckle, maintaining skin flexibility and moisture, and preventing sunburn.

(6) Licorice root, radix Glycyrrhizae

The Glycyrrhrizae radix contains glycyrrhizin, glycyrrhizic acid, liquiritin, and licoflavonoid.

Licoflavone has strong effect in inhibiting tyrosinase activity and scavenging oxygen free radicals, and licoflavone has whitening effect by inhibiting tyrosinase and dopachrome tautomerase (TRP-2) activity and inhibiting polymerization of 5.6-dihydroxyindole (DH1) to prevent melanin formation, thereby whitening skin. The component with sunscreen effect in Glycyrrhrizae radix extract is generally flavone compound, and can strongly absorb ultraviolet and visible light due to conjugation of molecular structure of Glycyrrhrizae radix flavone compound. Molecules absorbing high-energy ultraviolet rays can transit from a ground state to an activated state and then return from the activated state to the ground state, and harmless low-energy rays are released; compared with synthetic sunscreen agent, the licorice extract used as sunscreen agent does not need antioxidant in the formula, does not irritate skin, and has strong stable absorption capacity. The Glycyrrhrizae radix extract can effectively improve moisture-keeping ability of skin care product, and has antihistaminic and vasodilatation effects. Dipotassium glycyrrhizinate contained in licorice has wide compatibility in cosmetics, and can be frequently used together with other active agents to accelerate skin absorption of the dipotassium glycyrrhizinate and other active agents.

The liquorice added into the cosmetics can maintain the emulsified state of the product for a long time and prevent oxidative deterioration, and is a name of natural preservatives.

(7) Root of red-rooted salvia

The chemical components of the salvia miltiorrhiza mainly comprise fat-soluble components and water-soluble components, namely, a plurality of liposoluble tanshinone components, water-soluble protocatechuic phenol aldehyde and catechol derivatives and the like, and the contained salvianolic acid components are effective components in cosmetics, can clear oxygen free radicals and inhibit lipid peroxidation, and have strong antioxidation, wherein particularly, the effect of the salvianolic acid A is remarkable, namely the salvianolic acid A has the effect which is hundreds to thousands times stronger than that of vitamin E under the same concentration, can effectively protect the activity of SOD (superoxide dismutase), and is one of the natural products with the strongest antioxidation in the prior art.

Because the salvia miltiorrhiza has the function of cooling blood, the salvia miltiorrhiza is beneficial to fading facial color spots and can effectively inhibit excessive secretion of sebaceous glands so as to inhibit the growth of acne with exuberant secretion. The salvia miltiorrhiza is made into a mask and a cosmetic, which is helpful for eliminating and reducing skin wrinkles, and the salvia miltiorrhiza lipid-clearing factor can permeate the bottom layer of the skin, clear excess fat, condition pulse qi, promote blood circulation and naturally whiten the skin.

(8) White atractylodes rhizome

The chemical components of the atractylodes macrocephala koidz are mainly volatile oil and polysaccharide, the volatile oil is atractylone, atractylol and the like, and the atractylodes macrocephala koidz polysaccharide is an important biological high molecular compound and is also one of important active ingredients of plants, so that the research on the atractylodes macrocephala koidz is important. In addition, Atractylodis rhizoma also contains glutamic acid vitamin A etc.

The beauty treatment effect of the white atractylodes rhizome has the effects of whitening skin, removing pox and fading spots, the Li Shizhen Biaozhu dipping wine (or vinegar) has the extremely cause of treating freckles, and the records in the Ming-generation 16 th century medical work 'medical entry': the white atractylodes rhizome can tonify qi and blood, whiten skin and is suitable for rough and sallow skin caused by deficiency-cold of qi and blood. The white atractylodes rhizome can retain youthful looks and remove freckles, enables the face to look glossy, and is mainly used for delaying skin aging (because of the effect of removing oxygen radicals, the effect is enhanced when the white atractylodes rhizome is used together with the liquorice), expanding blood vessels, fading black spots and freckles, whitening the skin and the like. It can be added into cosmetics and facial mask for preventing skin aging.

(9) The pawpaw is rich in vitamins, carotene and papain. The chemical components are as follows: demethylpentacyclic triterpenoid saponins, lignanoid glycosides, flavonoids and phenolic components.

Pawpaw has important nutrient substances for beautifying skin, can be eaten by pawpaw, can also be externally used for protecting skin, and has the function of improving skin color because the pawpaw contains enzyme which is related to papain and carotene contained in pawpaw, the enzyme is an important medium for decomposing protein by a human body, the papain can play a role of removing cutin by dissolving and decomposing protein in dead cells, and the pawpaw contains abundant carotene and vitamin C which are natural antioxidants and can effectively remove oxygen radicals to delay the aging of the face. The extract can be added into skin care cosmetics and facial masks to make the product of the skin care cosmetics and facial masks of the products of the skin care cosmetics to be of a higher grade.

(10) Sea-buckthorn

Seabuckthorn contains hundreds of active substances, wherein 14 kinds of vitamins, 12 kinds of organic acids and monosaccharides, 22 kinds of amino acids and amides, 7 kinds of fatty acids, 32 kinds of lipids, 30 kinds of phenols and flavonoids and 29 kinds of trace elements are contained. The content of the vitamin C is about 6-1294 mg/100g, which is 2-3 times of that of kiwi fruit, the sea-buckthorn contains quite stable vitamin C because the sea-buckthorn does not contain ascorbic acid oxidase, the content of the vitamin E in the sea-buckthorn is in the top position in fruit trees, the content of alpha-tocopherol in each 100g of sea-buckthorn oil is 206.9mg measured by liquid phase chromatography, and the result is similar to the results reported in foreign countries, and the content of the vitamin E in each 100g of pulp oil is 100-160 mg.

The vitamin E rich in the sea buckthorn has stronger functions of resisting oxidation and removing oxygen free radicals, and the carotene, the carotenoid, the unsaturated fatty acid and the like contained in the sea buckthorn can inhibit the activity of tyrosinase and prevent the formation of melanin, thereby playing the effects of maintaining beauty, keeping young and lightening spots.

Sea buckthorn is rich in vitamin C, which is called as the king of vitamin C, and vitamin C is a natural in-vivo whitening agent, can effectively inhibit the deposition of abnormal pigments on the skin and the activity of tyrosinase, and is helpful for the reduction of dopachrome (an intermediate for converting tyrosine into melanin), so that the formation of melanin is reduced, and the skin is effectively whitened.

The sea buckthorn contains various amino acids, various vitamins, trace elements, unsaturated fatty acid, SOD and the like, can prevent skin aging, lighten senile plaque and chloasma, effectively activate skin, promote cell metabolism, promote epithelial tissue regeneration, prevent melanin formation, help skin to resist ultraviolet ray damage and whiten skin.

Sea buckthorn is rich in superoxide dismutase (SOD), an enzyme that can be converted into oxygen and hydrogen peroxide by disproportionation reactions. It is widely used in various animals, plants and microbes, and is an important antioxidant, and can protect cells exposed to oxygen and remove free radicals of human body, thereby achieving the special effect of anti-aging. Is really an rare additive in cosmetics and facial masks.

(11) Glossy ganoderma

Ganoderma contains various chemical components such as polysaccharide, triterpenes, nucleosides, sterols, alkaloids, amino acids, microelements, etc., and has biological activities of regulating immunity, resisting aging, etc.

The action mechanism of ganoderma lucidum in the aspect of maintaining beauty and keeping young is as follows: the effective components contained in the ganoderma lucidum can delay the aging of organisms and effectively remove oxygen free radicals, thereby achieving the effects of maintaining beauty and keeping young. The rich amino acids contained in Ganoderma are natural moisturizing factors, such as 15 times of glycerol, 2 times of propylene glycol and 6 times of sorbitol, which can keep and regulate the water content of skin, recover the elasticity of skin, and keep skin moist and fine; and can inhibit the formation of melanin in skin, lighten color spots, and make face achieve the effects of moistening and brightening.

The ganoderma lucidum polysaccharide serving as an effective component in ganoderma lucidum can effectively inhibit the formation of free radicals, resist oxidation and aging, increase the content of collagen in skin, effectively promote the formation of hyaluronic acid, and keep the skin tender and smooth so as to achieve the optimal state.

The ganoderma polypeptide has five skin care effects, effectively replenishes water, moisturizes, whitens, repairs and relieves, so that the nutrition of the ganoderma directly permeates into a skin layer, the texture of the skin is improved, the repair and moisturizing capability of the skin is improved, and the skin is comprehensively protected from being damaged by years. The ganoderma lucidum is used in cosmetics and facial masks, and various cosmetic effects contained in the ganoderma lucidum can improve the grade of the cosmetics and the facial masks, so that the ganoderma lucidum is a good product for beautifying.

(12) Giant knotweed rhizome:

the chemical components of the giant knotweed are as follows: resveratrol and emodin are main functional components in giant knotweed rhizome, and research shows that resveratrol and emodin have wide antioxidant properties, such as LDL cholesterol oxidation and lipid peroxidation. In addition, rhizoma Polygoni Cuspidati is rich in tannin and flavonoids.

The giant knotweed extract has a good inhibition effect on the activity of melanocytes, and in addition, the giant knotweed extract has a promotion effect on the activity of macrophages, and the macrophages can phagocytose melanin in cell culture, so that the giant knotweed extract can reduce the content of melanin through two aspects, and can be used for whitening cosmetics.

(13) Pyracantha fortuneana fruit

The main components are as follows: contains 18 amino acids including 7 essential amino acids for human body, 2 essential amino acids for infants, and further contains rutin and quercetin compounds, bioactive polysaccharides, fatty acids, volatile aroma components, crude protein, carotene, pectin, vitamin B1, B2, PP, C, E, and 9 mineral elements.

The activity of enzymes such as SOD in the pyracantha fortuneana is strong, the processing and application of the pyracantha fortuneana fruit in foreign countries are mainly focused on the development of cosmetics, clinical experiments prove that the pyracantha fortuneana fruit has a magical whitening effect, can inhibit histamine from stimulating pigment mother cells to generate excessive melanin, has magical effects of lightening the melanine pigment and preserving moisture, and meanwhile, the pyracantha fortuneana fruit is rich in flavonoid compounds such as rutin, hyperin and the like, and can obviously delay the extraction of fluorescent substances by active oxygen radicals. The pyracantha fortuneana fruit skin-whitening cosmetic has strong antioxidant effect and anti-catastrophe effect, plays a very good role in moisturizing and moisturizing while whitening skin, has the effects of supplementing nutrition and trace elements to human skin, accelerating metabolism, promoting epidermal cell growth, removing cutin and wrinkles, and removing spots and tendering skin, and is an rare cosmetic additive.

The use of pyracantha fortuneana in the combination can achieve different effects, so that the grade of the cosmetic is improved.

(14) Oat

The main components are as follows: oat protein, oat peptide, oat glucan, oat oil and the like.

The melanin inhibiting capability of oat is close to that of arbutin which is a commonly used whitening agent of the current cosmetics, which shows that the efficacy of oat extract is equivalent to that of arbutin. The substances can reduce the formation of melanin, lighten color spots, increase the activity of skin, delay skin aging, whiten skin, preserve heat, regulate water and oil balance, promote fibroblasts to synthesize collagen, repair damaged skin cells, change proteins in the skin cells into a plurality of small fragments, namely 'cytokines', transmit signals into the skin and promote the skin to generate fresh cells. The protein component extracted from oat is very similar to the cell factor, and the skin often judges the oat protein component as the cell factor by mistake, so that the production of cells is spontaneously accelerated, the whole metabolism is promoted, and the skin is activated.

Currently oats and their derivatives are among the only natural ingredients regulated by the FDA in the united states.

The oat in the combination can exert natural functional effect, and can be combined with other functional substances in other varieties to exert the beauty effect, so that the effect is enhanced.

(15) Turmeric root tuber

The main components are as follows: curcumin and its volatile oil, polysaccharides, flavonoids, sterols, etc.

Curcuma rhizome has effects of promoting qi circulation, promoting blood circulation, resisting oxidation, scavenging free radicals, relieving inflammation and relieving pain. The turmeric is rich in natural plant antioxidants beneficial to the skin, is helpful for reducing aging marks, protecting the skin from the invasion of free radicals, keeping the skin smooth, balancing water and oil, showing beautiful skin color, and can be used as an antioxidant to be added into beauty and skin care cosmetics.

The composition can enhance scavenging oxygen free radicals, and can balance water and oil.

(16) Herba Selaginellae (Thunb.) Selaginella

The main components are as follows: contains flavone, lignan, alcohol polysaccharide, alkaloid, fatty acid, amino acid, inorganic salt, selaginin B, selaginin C, adenosine, arbutin, guanosine, etc.

The selaginella tamariscina or the senecio cannabifolius which is also called as the eriodictyotis sinensis has extremely strong vitality, the selaginella tamariscina extract has strong repairing capability and also called as moisturizing holy hands, has strong moisturizing capability, deeply moisturizes the skin, effectively locks water, can moisturize the skin of the face for a long time, can make the face smooth and beautiful by mixing the selaginella tamariscina dry powder and the egg white and applying the selaginella tamariscina dry powder and the egg white to the face, can reduce the occurrence of skin inflammation, has the effects of removing acnes and whitening the skin by frequent application, and can be added into.

The herba Selaginellae is used in the composition to moisten and whiten human face by combining the strong moisturizing effect of herba Selaginellae and other effective substances.

The plant composition for cosmetics is prepared by crushing, sieving, soaking, filtering, centrifuging to remove impurities, and concentrating to obtain mixed extractive solution containing at least ginsenoside Re and glycyrrhizic acid. Ginsenoside Re and glycyrrhizic acid are markers of the mixed extracting solution, the mass percent of the ginsenoside Re is 1.76-1.97%, and the mass percent of the glycyrrhizic acid is 0.81-0.95%.

The preparation method of the mixed extracting solution comprises the following steps:

weighing the raw materials in the plant composition according to the required parts, and then crushing the raw materials to be crushed and sieving the crushed raw materials with a 20-mesh sieve to obtain material powder. The sheet component processed in the previous stage is cut into pieces with the size of about 0.5-1 square centimeter. (in actual operation, plant components are not excessively crushed, the plant components are not easy to filter after being soaked and are easy to block sieve pores) are soaked in a container at normal temperature for 0.5-1 h according to the ratio of 1:10, primary supernatant is obtained through filtering, filter residues are placed in a heating container and soaked in constant-temperature water of 50 ℃ for 0.5-1 h, the steps are repeated for 2 times, and then 2 nd supernatant and 3 rd supernatant are obtained, the primary supernatant and the 2 nd supernatant and the 3 rd supernatant are mixed to obtain total supernatant, impurities of the total supernatant are separated through a high-speed centrifugal machine, and then the total supernatant is filtered and concentrated through an ultrafiltration device (ultrafiltration membrane) to obtain mixed extracting solution of the plant composition.

It is necessary to describe the advantages of the extraction method and the steps:

the soaking method adopts a creative one-cooling two-hot soaking method, and the theoretical basis is as follows: the plant composition crushing components are mixed with the starch, resin, pectin and other components, the starch, resin, pectin and other components are attached to plant cell membranes, the precipitation of effective components in cells is influenced, after the plant composition crushing components are soaked in clean water at normal temperature for the first time, a large number of ineffective components attached to the cell membranes are diluted, the permeability of the plant composition crushing components is increased, the precipitation of the effective components is facilitated, the effective components are heated to 50 ℃ for two times and soaked at constant temperature, the motion amount of effective substance molecules is increased, the precipitation amount of the effective components is increased, and relevant analysis is performed: the molecular motion speed increases about 2-4 times for every 10 degrees of temperature increase. The one-cold-two-hot dipping method is superior to the three-cold dipping method and the three-50-degree constant-temperature hot dipping method, and a point is emphasized that if the 50-degree hot dipping method is used in the whole process, the starch, the resin and the pectin in the mixed components can cause viscosity increase due to high water temperature, particularly after the first soaking, the ineffective components are attached to cell membranes and are not easy to fall off, so that the precipitation of the effective components is influenced.

Markers in the total supernatant of each of the three soaking methods were measured by high performance liquid chromatography: and (3) content determination and comparison of ginsenoside Re and glycyrrhizic acid:

and (3) determination of ginsenoside Re: the method comprises the following steps: a chromatographic column: c18 column mobile phase: performing gradient elution by acetonitrile-water; detection wavelength: 203nm, column temperature 35 ℃, flow rate: 1.0 ml.min-1; the sample amount is 10 ul; linear range: 0.504-252 ug (r > 0.999);

and (3) glycyrrhizic acid determination: the method comprises the following steps: a chromatographic column: c18 column mobile phase: methanol 2moL/L ammonium acetate-glacial acetic acid (66:34: 1); detection wavelength: 252 nm; column temperature: 22 degrees; flow rate: 10 ml.min-1; sample introduction amount: 10 ul; linear range: 0.1033-1.0330 ug (r is 0.9999);

table 1:

as can be seen from table 1, the cold-hot soaking method is superior to the full-process cold soaking and the full-process hot soaking method in terms of precipitation of plant active ingredients, thereby proving that the above theory holds. The method saves the amount of raw materials, thereby reducing the cost and saving the fund.

In addition, a membrane separation technology is adopted in the extraction process, namely: the Ultrafiltration (UF) membrane separation technology keeps the effective components of plants to the maximum extent, the diameter of the separation membrane is 1-20 nm (nanometer), the relative molecular mass of the effective components of the plants is mostly not more than 1000, and the relative molecular mass of the ineffective components such as starch, resin and other impurities is more than 50000, so the effective components of the plants can be separated by using an ultrafiltration membrane with the molecular weight cutoff of less than 50000, the quality of the extracting solution is ensured, bacteria and pyrogen can be removed while the separation is carried out, the storage time is prolonged, the energy consumption is low, the ultrafiltration membrane can be produced at normal temperature, the continuous and automatic operation can be realized, the requirements of modern production of the mixed extracting solution of the plants are met, and the separation and extraction technology exceeds the actual effects of a cold ethanol extraction method, a percolation method and other extraction methods, and has good development prospects. The temperature does not exceed 50 ℃ during the whole extraction process! The effective heat-sensitive components in the plant, such as effective components of vitamins and the like, are fully reserved.

The mixed extract of the present invention was added to the cream for testing;

preparing cream:

raw material ratio (parts by mass)

Phase A:

phase B:

and C phase:

the preparation steps are as follows:

1. weighing each raw material according to the requirement

1.1 adding the following components into an oil phase pretreatment pot:

ceteareth-21, cetearyl alcohol, caprylic/capric triglyceride, dimethicone, cetyl dimethicone, isopropyl palmitate; stirring and heating to 90-95 ℃, and maintaining for 20 minutes for sterilization to obtain an oil phase substance.

1.2 adding the following components into a water phase pretreatment pot:

butanediol, dipropylene glycol, sodium stearyl glutamate and ionized water; stirring and heating to 90-95 ℃, and maintaining for 20 minutes for sterilization to obtain a water phase substance.

1.3 sucking the filtered oil phase substances into a preheated emulsifying pot, sucking the water phase substances, starting a scraper plate in sequence for stirring, quickly stirring and homogenizing for 10-20 minutes, keeping the temperature in the emulsifying pot not lower than 85 ℃, carrying out vacuum emulsification, then carrying out heat preservation stirring for 10-15 minutes, when the temperature of the A.B two phases is cooled to 70-80 ℃, sequentially adding a co-emulsifier and a thickening agent within 5-15 minutes, continuing stirring, cooling to 50 ℃ by using jacket circulating water, adding a plant mixed extracting solution, when the temperature is 40 ℃, sequentially adding a preservative and essence, continuing stirring to room temperature, and discharging to obtain a finished product.

Note: the blank sample for the test was not added with the plant mixed extract, and the rest of the procedure was the same.

The cosmetic skin cream added with the plant mixed extract has the effects of whitening, speckle lightening, scar (acne scar), wrinkle resistance, moisture retention and face thinning. The facial mask has the advantages of moistening and firming facial skin, comfortable and smooth skin feel and no peculiar smell, can improve the unpleasant odor of a human body, plays the roles of beautifying and modifying the skin, can improve the negative image caused by the problem skin by frequent use, and promotes the beautifying index of an individual. The extractive solution can also be added into facial mask, skin care lotion, essence, etc. to exert its effects.

In order to verify the efficacy of the plant mixed extract added to cosmetics, the following series of tests were performed:

1. the test purpose is as follows: skin whiteness, moisture, oil content and elasticity test reflect the effects of whitening, moisturizing, conditioning grease, tightening, resisting wrinkles and thinning the skin after the cosmetic is used.

1.1 method: testing an instrument; the skin tester M-6602 manufactured by Shenzhen Fuhentong science and technology Limited is used.

1.2 test population screening: the age is 20-55 years, the gender is female, and the number of people is 50.

1.3 meets the standard: the skin is healthy, has no skin allergy history and no visceral diseases, is not in the lactation period of pregnancy, meets the standard of the test requirement of using the instrument, and is a volunteer.

1.4 site selection: the selected application part is the part close to the wrist on the inner sides of the left and right front arms of the same person, so the skin is similar to the skin on the face. The left side is blank control and the right side is efficacy test.

1.5 test time and methods: the test part is cleaned every day and then smeared once for 28 days, and the part is smeared uniformly and gently rubbed each time until the part is fully absorbed. The data of day 0, day 7, day 14, day 21 and day 28 were tested, and the test items included: 4 groups of data including white degree, moisture, oil and elasticity are obtained, then the average value of each time period in the measured data of each group is obtained, and finally (day 28) the final average value of each group is obtained in a gathering way.

1.6 test evaluation standard parameters: the white degree is 36-75 (natural value), which is dark below the natural value and white above the natural value. Moisture (%) is 32 to 47 (natural value), and below this value, drying is performed, and above this value, moisture retention is performed. The oil content (%) is 37 to 49 (natural value), and a value lower than this means that the oil content is low, and a value higher than this means that the oil is secreted much. Elasticity (%) is 53-70 (natural value), and a value lower than this is skin relaxation and a value higher than this is skin firmness.

Table 2:

test site	Test subject (example)	Degree of whitening	Moisture (%)	Oil content (%)	Elasticity (%)
						Curved side of left forearm	50 examples of	31	28％	30％	55％
Curved side of right forearm	50 examples of	80	55％	41％	73％

Table 2 shows the final results of the subjects on day 28:

blank control group:

1. there was no increase in whiteness, in the low data state, suggesting that skin darkness did not improve.

2. The water content does not reach the normal data range, which indicates that the skin is in a dry and water-deficient state.

3. The oil content data is lower than the normal standard, which indicates that the skin oil content is low; in direct proportion to moisture, dry skin is indicated.

4. The elasticity is slightly increased but still at a low value, indicating that the skin is in a relaxed state.

Efficacy test group:

1. the data of the white degree is in a high value state, which shows that the extracting solution has good whitening effect.

2. The water content data is high, which indicates that the extracting solution has good moisturizing effect.

3. The oil content data is in a normal range, which indicates that the extracting solution has good efficacy of conditioning oil secretion.

4. The elasticity data is high, which indicates that the extracting solution can increase the content of collagen in the skin, make the skin compact and smooth fine lines (anti-wrinkle) and has the effect of inhibiting the proliferation of fat cells (face thinning effect).

In summary, the test results show that the mixed extract of the botanical composition has: whitening skin, keeping moisture, controlling oil, resisting wrinkle, and thinning face.

2. Spot (acne marks) lightening efficacy test:

2.1, method: the subjects filled out the use feedback opinion tables and concluded by statistical analysis.

2.2 test population screening: the age is 25-60 years, the number of gender women is 200, the number is 4, and each group is 50 (according to chloasma, freckle, senile plaque and acne mark).

2.3 meets the standard: the face of the subject has chloasma, freckles, senile plaques and acne marks with different degrees, the skin is dark yellow, the skin has no history of allergy and visceral diseases, and the subject is not in the lactation period of pregnancy and meets the voluntary selection condition of the subject.

2.4 test methods: after the face of the subject is cleaned, the cream with the extracting solution is uniformly applied to the face and gently kneaded with the palm until the cream is fully absorbed, and the face is used for 1 time respectively in the morning and at night and is continuously used for 8 weeks. Follow-up was 1 time each at week 2, week 4, week 6 and week 8 before and after use.

2.5 evaluation criteria:

(1) the healing is realized, the visual color spots or acne marks basically disappear, the skin is glossy and fine, and the skin color is obviously improved.

(2) Has obvious effect, the color spots or the acne marks are faded by more than 50 percent by naked eyes, the skin is glossy, and the skin color is improved.

(3) The color of the color spot or the acne mark is faded by more than 10 percent when the color spot or the acne mark is seen by naked eyes, or the color of the color spot and the acne mark is lightened, and the skin is glossy.

(4) No effect, no obvious change before and after use.

The significant efficiency is (the number of cure cases + the number of significant cases)/the total number of cases x 100%

The total effective rate is (number of cure cases + number of obvious cases + number of improvement cases)/the total number of cases x 100%

Evaluation results were as follows:

table 3:

as can be seen from table 3, the skin care cream added with the mixed extract has good effects of promoting healing and obviously improving chloasma, freckles, senile plaques and acne sequela acne marks, can well improve dark yellow complexion, enables the skin to be glossy and fine, and the highest efficiency of the implementation group 1 shows that the extract has obvious effect on the chloasma, and all subjects have no adverse conditions such as body discomfort, skin allergy and pruritus, and skin redness and swelling in the test process.

3. Acne scar lightening efficacy test:

3.1 method: half face is compared with makeup effect, and the self-vision evaluation method is adopted.

3.2 test population screening: the age is 25-55 years, the gender is female, and the number of people is 50.

3.3 meets the standard: both sides of the face of the subject have acne scars with dark yellow skin, no allergic history of the skin and no visceral diseases, are not in the lactation period of pregnancy and meet the voluntary selection condition of the subject.

3.4 test methods: by using the questionnaire form, the subjects evaluated the degree of improvement of the acne scars before and after the product was used.

The left half face was used as a blank control group and the right half face was used as an efficacy test group. The product is used by washing face with warm water before application, and uniformly applying the product to the part with acne scar 1 times respectively in the morning and evening for 8 weeks before and after application, and is followed by 2 weeks, 4 weeks, 6 weeks and 8 weeks before and after application.

3.5 evaluation criteria: 1. the acne scar is healed, the acne scar is obviously shallow, and the acne scar is reduced and basically invisible. 2. The acne scar is shallow or reduced to a greater extent, and the effect degree reaches 50% or more than before the product is used. 3. The improvement is slight, and the acne scar is slightly shallow or reduced, and the improvement degree is 10% or more than before using the product.

4. No effect, no change of acne scar before and after using the product.

Evaluation results were as follows:

table 4:

as can be seen from Table 4, the blank control group only improves the skin dark yellow, the effect group has very obvious effect on acne scars, the significant efficiency and the total effective rate respectively reach more than 80% and 90%, and the effect on the skin dark yellow is very good (the effect is shown in Table 3), the plant composition and the mixed extract thereof are fully verified to have very good effect on improving the face acne scars, the face skin is well repaired while the acne scars are improved, and the face skin is glossy and beautified and modified.

The plant composition has reasonable formula structure, excellent selected materials and no incompatibility among the materials, active ingredients of all the substances in the formula are matched and supplemented with each other, red ginseng is used in the formula, the red ginseng contains a plurality of active substances beneficial to human skin, the first component is ginsenoside, amino acid, polypeptide and other substances, the active ingredients can be combined with other functional substances in the formula, such as ganoderma polypeptide in ganoderma lucidum and asiaticoside in asiatic pennywort herb, the function of repairing damaged skin cells can be fully exerted, the elasticity of skin can be enhanced, the damaged skin cells can be regenerated, the active substances of the red ginseng can be combined with flavone in flastem milkvetch seed and active substances such as licoflavone in liquorice, the restoring capability of melanin can be fully inhibited, the skin is white and smooth, the skin is a skin-care cosmetic upper product, cynomorium songaricum which is wild in desert Gobi is also named as desert ginseng, is a pure natural desert plant, the whitening cream is rich in various active ingredients, amino acids, cynomorium songaricum polysaccharide and other substances beneficial to human skin, has a good whitening effect when being matched with licorice flavonoids, mulberry flavone, white atractylodes rhizome polysaccharide and other substances, has a good effect of improving rough skin, darkness, spots and the like caused by deficiency-cold of qi and blood, improves the yellow-dark complexion of volunteer subjects in tables 3 and 4, wherein the success of the white atractylodes rhizome is not limited! The active ingredients of the largehead atractylodes rhizome are matched with functional substances in the formula, such as carotene in sea buckthorn, amino acid in lucid ganoderma, arbutin-like substances in oat and flavonoid substances in flastem milkvetch seed, so that the largehead atractylodes rhizome has good effects of resisting oxidation and lightening skin pigment spots, can effectively lighten and dispel chloasma, freckles, age spots (senile plaques) and acne marks, and can whiten and smoothen the skin, and the pyracantha fortuneana fruit on the loess plateau is rich in various functional cosmetic substances, such as various amino acids and various vitamins necessary for a human body; it can be combined with carotene and vitamin C in fructus Chaenomelis, various amino acids and vitamin C contained in fructus Hippophae, and salvianolic acid in Saviae Miltiorrhizae radix to effectively remove oxygen free radicals, sufficiently increase activity of superoxide dismutase (SOD), delay skin aging, and make skin elastic, moist, and beautiful. The giant knotweed rhizome is mainly used for lifting loose skin in the formula to tighten the skin of the face, the effective components of the giant knotweed rhizome are combined with asiaticoside in the formula to fully increase the content of collagen in the skin, and the content of the collagen in the skin can be increased to 25-30% after the combined effective components are applied to the skin of a human body through measurement, so that the effects of tightening the skin and smoothening fine wrinkles in a crowd experiment are related to the effect. The rhizoma Polygoni Cuspidati extract, asiaticoside and Saviae Miltiorrhizae radix lipid cleaning factor have strong inhibiting effect on lipase, and can be used in cosmetics for reducing weight (thinning face). The ingredients of the mulberry bark, such as flavone, the cyclomori radicis and the mulberry element, can effectively fade and remove acne scars, and the effect is enhanced after the mulberry bark is combined with asiaticoside and papain. The effective components in the turmeric can play a role in regulating water and oil balance, can improve dark yellow aging marks left by years, and has enhanced effect when being used with the flastem milkvetch seeds. The selaginella tamariscina is also called as the gerbera, has the main moisturizing effect in the formula, contains effective components which can have strong moisturizing and moisture-keeping capabilities, deeply moisturizes the skin and effectively locks water, and can be combined with the effective moisturizing components in lucid ganoderma, sea buckthorn, liquorice, pawpaw and the like to enable the face to be in a moisturizing and moisture-tendering state for a long time, and the peak value of the effective moisturizing state can reach 8 hours after the combined compatibility is tested.

The plant composition for the cosmetics has a strict structure and an obvious effect, overcomes the defects of unobvious effect and single effect of certain combined formulas, has reasonable compatibility of various substances, has complementary effects, and fully exerts the whole effect of a group of formulas. The composition has no incompatibility and no forbidden substances regulated by the state, and the mixed extract is used as an effective component to be added into cosmetics, so that the effects of whitening, moisturizing, resisting wrinkles (flattening and reducing fine lines), fading scars (acne scars) including acne marks, thinning face and the like can be achieved after the cosmetic is used. It can be added into cosmetics for providing multifunctional effects of caring skin, repairing, beautifying, and modifying.

The practical effects of the new concepts and the substances provided by the invention after matching are obtained by actual research, test and experience of researchers, which are not possessed by the prior art at present, the composition of the formula and the dosage required by each substance in the formula are obtained through long-time repeated test, and the preparation process of the formula mixed extracting solution and the process are obtained through deep thought and repeated practice, so the invention has great creativity, thereby having wide market prospect and social benefit.

In addition, some modifications made by the researchers without departing from the subject matter of the present disclosure should be covered by the protection scope of the patent.

Claims

1. A botanical composition for use in cosmetics, characterized by: the raw materials of the plant composition comprise red ginseng, centella, cortex mori radicis, cynomorium songaricum, semen astragali complanati, liquorice, salvia miltiorrhiza, bighead atractylodes rhizome, pawpaw, sea buckthorn, lucid ganoderma, polygonum cuspidatum, pyracantha fortunei, oat, turmeric and selaginella tamariscina; each part of the plant composition contains 4-6 g of red ginseng, 8-12 g of centella asiatica, 8-12 g of white mulberry root-bark, 6-10 g of cynomorium songaricum, 8-12 g of flastem milkvetch seed, 6-10 g of liquorice, 8-12 g of salvia miltiorrhiza, 10-14 g of bighead atractylodes rhizome, 5-7 g of pawpaw, 4-8 g of sea buckthorn, 4-8 g of lucid ganoderma, 8-12 g of giant knotweed rhizome, 8-12 g of pyracantha fortuneana fruit, 6-10 g of oat, 6-10 g of turmeric and 6-10 g of selaginella tamariscina.

2. The plant composition for cosmetics according to claim 1, characterized in that: each part of the plant composition contains 5g of red ginseng, 10g of centella, 10g of white mulberry root-bark, 8g of cynomorium songaricum, 10g of flastem milkvetch seed, 8g of liquorice, 10g of salvia miltiorrhiza, 12g of bighead atractylodes rhizome, 6g of pawpaw, 6g of sea-buckthorn, 6g of lucid ganoderma, 10g of giant knotweed, 10g of pyracantha fortuneana fruit, 8g of oat, 8g of turmeric and 8g of selaginella tamariscina.

3. A mixed extract of a botanical composition as claimed in claim 1 or claim 2 wherein: the mixed extracting solution at least contains ginsenoside Re and glycyrrhizic acid; the mass percent of the ginsenoside Re is 1.76-1.97%, and the mass percent of the glycyrrhizic acid is 0.81-0.95%.

4. A method for preparing the mixed extract solution according to claim 3, wherein: the preparation method of the mixed extracting solution comprises the following steps:

5. The method for preparing a mixed extract of a plant composition for cosmetics according to claim 4, wherein: in the step S1, the material which is processed into slices in the previous stage is cut into pieces of 0.5-1 square centimeters.

6. The method for preparing a mixed extract of a plant composition for cosmetics according to claim 4, wherein: in the step S2, the mass ratio of the sum of the mass of the material powder and the sheared material pieces to water is 1: 10.

7. The method for preparing a mixed extract of a plant composition for cosmetics according to claim 4, wherein: in the step S5, the ultrafiltration apparatus is an ultrafiltration membrane device.