CN106511142A - Centella asiatica floral water and preparation method and application thereof - Google Patents

Centella asiatica floral water and preparation method and application thereof Download PDF

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Publication number
CN106511142A
CN106511142A CN201710037023.3A CN201710037023A CN106511142A CN 106511142 A CN106511142 A CN 106511142A CN 201710037023 A CN201710037023 A CN 201710037023A CN 106511142 A CN106511142 A CN 106511142A
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CN
China
Prior art keywords
preparation
herba centellae
distillate
skin
centella asiatica
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710037023.3A
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Chinese (zh)
Inventor
邹录惠
杨明珠
黄丽凤
蒋红光
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Guangxi Nanning's Biotechnology Co Ltd
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Guangxi Nanning's Biotechnology Co Ltd
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Publication date
Application filed by Guangxi Nanning's Biotechnology Co Ltd filed Critical Guangxi Nanning's Biotechnology Co Ltd
Priority to CN201710037023.3A priority Critical patent/CN106511142A/en
Publication of CN106511142A publication Critical patent/CN106511142A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/004Aftersun preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses centella asiatica floral water and a preparation method and application thereof. Fresh centella asiatica is picked, washed, subjected to impurity removal, cut and placed in a distiller, hot deionized water is added for soaking, then the temperature is increased and distillation is conducted, circulating cooling liquid is introduced, condenser distillate is collected, distillation stops when the volume of the collected distillate is 0.8-1.2 times of the mass of fed centella asiatica, the distillate is filtered and sterilized through a microporous filter membrane with the aperture of 0.22 micrometer, and the centella asiatica floral water is obtained. The obtained floral waster is clear and transparent, has the special fragrance of centella asiatica floral water, is stable in quality, and can be stored for one year in a sealed mode at low temperature. Inedible chemical components are not added in the extraction process, and it is guaranteed that the floral water is natural and free of toxin, has a repair function on scarred and wounded skin, has anti-inflammation and antibacterial functions on acne skin, can accelerate skin regeneration, relieves sensitive skin, reduces irritation and meanwhile provides sufficient moisture for skin.

Description

A kind of Herba Centellae hydrosol and its production and use
Technical field
The invention belongs to technical field of skin care, is related to a kind of hydrosol and its production and use.
Background technology
Hydrosol, also known as crystal's oil, common are MEIGUI CHUNLU, Camellia sinensis hydrosol, lavandula angustifolia hydrosol, chamomile hydrosol, orange blossom Hydrosol etc., because which contains the water-soluble substanceses (such as tannic acid and flavonoid) and micro quintessence oil of plant origin, is easily inhaled by skin Receive, alcohol-free composition does not gently stimulate, and is in recent years emerging daily cosmetics and skincare product.
《Dictionary of medicinal plant》Record:" Herba sambuci chinensis (Herba Centellae), the property of medicine are bitter, cold, enter spleen channel, its effect for promoting blood circulation, detumescence, Pain relieving, and have the purposes such as heat-clearing and toxic substances removing, diuretic." Herba Centellae is commonly called as tiger grass, injured tiger can roll about on this meadow, rub Wiping touches leaf juice and can releive and healing of wound, for wound, sun-damaged skin have repair, for small pox skin has antiinflammatory The effect of antibacterial, can accelerate skin regeneration, for sensitive skin, with more stimulation of releiving, reduce, improve the obscure work(of the colour of skin Effect.
Skin-protection product majority containing Herba Centellae is adjusted by adding Herba Centellae extract or asiaticoside on the market at present System is formed, and 104107160 A of CN disclose a kind of wrinkle removal nutritional solution containing Herba Centellae hydrosol, but have no the system of Herba Centellae hydrosol Preparation Method, and commercially available Herba Centellae hydrosol is mostly the detached by-product of asiaticoside extraction, without the distinctive delicate fragrance of plant itself Gas, substance content are low, and Consumer's Experience sense is bad.
Compared with prior art, the Herba Centellae hydrosol that the present invention is provided has the distinctive faint scent of plant itself, and clarification is saturating Bright, easy to operate, steady quality, Nantural non-toxic, to no skin irritation, while also having moisturizing, anti-inflammation, promote skin The effects such as regeneration.
The content of the invention
The technical problem to be solved, is to provide a kind of preparation method of Herba Centellae hydrosol.
The technical scheme that the present invention solves above-mentioned technical problem is as follows:
A kind of preparation method of Herba Centellae hydrosol, comprises the steps:
(1) Herba Centellae of fresh harvesting is cleaned, removes impurity;
(2) the fresh Herba Centellae cleaned is cut into into segment;
(3) put in distillator, add the deionization hot-water soak of 2~4 times of Herba Centellae quality 30 minutes;
(4) distillator heat temperature raising is distilled, opens the condensation switch of distillator, connect circulating cooling liquid, steam Condensed by condenser, collect condenser distillate;
(5) stop distillation when 0.8~1.2 times that the distillate quality collected is Herba Centellae quality;
(6) distillate Jing filtering with microporous membranes are degerming, and fill is obtained final product.
Preferably, in step (2), the length of cutting is 0.5~2cm, most preferably 1cm.
Preferably, the hot water temperature for adding in step (3) is 50~60 DEG C.
Further, step (4) can pass through the temperature for adjusting coolant, make the temperature of distillate be less than 40 DEG C.
Preferably, the distillate quality that step (5) is collected is optimal when being 0.8~1.0 times of Herba Centellae quality.
Preferably, the aperture of step (6) microporous filter membrane is 0.22 micron.
Second aspect present invention provides a kind of purposes of Herba Centellae hydrosol obtained in preparation method by mentioned earlier, can use In astringent, or it is used to allocate emulsion, facial cream or facial film as substrate.
Compared with prior art, the technical scheme that the present invention is provided has the advantage that:
1st, the inventive method uses the way of distillation, is distilled using deionized water, and Jing filtering with microporous membranes are degerming, the hydrosol for obtaining Appearance transparent is clarified, steady quality, and sealing low temperature can preserve 1 year.
2nd, the temperature that distillate is controlled in still-process of the present invention is less than 40 DEG C, enables hydrosol to retain former plant itself peculiar Faint scent, give product more preferably using effect.
3rd, Herba Centellae hydrosol sanitary index obtained in the present invention is complied fully with《Cosmetics health specification》(2007 editions) will Ask, it is as shown in table 1 below.
1 Herba Centellae hydrosol Testing index of table
4th, obtained Herba Centellae does not add any non-edible chemical composition, and zest is little, has no toxic side effect, and is pure day Right skin protection skin care productss.
Specific embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
The preparation method of the Herba Centellae hydrosol of the present embodiment, comprises the following steps:
(1) the Herba Centellae 10kg of fresh harvesting is taken, silt is washed away, is removed impurity;
(2) the fresh Herba Centellae cleaned is cut into the segment of 1cm;
(3) put in distillator, add 55 DEG C of deionization hot water 25kg to soak 30 minutes;
(4) distillator heat temperature raising is distilled, is opened the condenser of distillating still, connected -10 DEG C of recirculated cooling water, Collect condenser distillate, 33 DEG C of exposure temperature;
(5) stop distilling when the distillate quality collected is 8kg;
(6) filtering with microporous membrane of 0.22 micron of distillate Jing is degerming, detects qualified, fill, obtains final product.
After testing, its sanitary index meets all standard above shown in table 1 to Herba Centellae hydrosol obtained in embodiment 1. Obtained hydrosol has the distinctive fragrant of Herba Centellae itself, and clear, steady quality, placement have no muddy for 2 years.
Embodiment 2
The preparation method of the Herba Centellae hydrosol of the present embodiment, comprises the following steps:
(1) the Herba Centellae 20kg of fresh harvesting is taken, silt is washed away, is removed impurity;
(2) the fresh Herba Centellae cleaned is cut into the segment of 1.5cm;
(3) put in distillator, add 60 DEG C of deionization hot water 60kg to soak 30 minutes;
(4) distillator heat temperature raising is distilled, is opened the condenser of distillating still, connected -15 DEG C of recirculated cooling water, Collect condenser distillate, 30 DEG C of exposure temperature;
(5) stop distilling when the distillate quality collected is 20kg;
(6) filtering with microporous membrane of 0.22 micron of distillate Jing is degerming, detects qualified, fill, obtains final product.
After testing, its sanitary index meets all standard above shown in table 1 to Herba Centellae hydrosol obtained in embodiment 2. Obtained hydrosol has the distinctive fragrant of Herba Centellae itself, and clear, steady quality, placement have no muddy for 2 years.
Embodiment 3
Experience on probation is carried out to the Herba Centellae hydrosol for preparing of the invention, number of trying out is 50 people (skin sore, small pox skin, solarization Hinder skin, sensitive skin).Using method:Full face is gently wiped with cotton pads after face cleaning, is used 2 times daily, using 4 weeks.Mainly Investigate humidity of skin, acne removing, after-sun and the remission effect to sensitive skin.After continuously trying out 30 days, reflection is used After there is obtained Herba Centellae hydrosol of the invention preferable replenishing water and preserving moisture, skin sore small pox to reduce, reparation is shone rapidly, skin, reduction are quick The zest of sense skin.After on probation, hydrosol prepared by the present invention does not find allergic phenomena.Data statisticss are shown in Table 2.
The experience result on probation of table 2

Claims (7)

1. a kind of preparation method of Herba Centellae hydrosol, it is characterised in that comprise the following steps:
(1) Herba Centellae of fresh harvesting is cleaned, removes impurity;
(2) the fresh Herba Centellae cleaned is cut into into segment;
(3) put in distillator, add the deionization hot-water soak of 2~4 times of Herba Centellae quality 30 minutes;
(4) distillator heat temperature raising is distilled, opens the condensation switch of distillator, connect circulating cooling liquid, steam is passed through Condenser is condensed, and collects condenser distillate;
(5) stop distillation when 0.8~1.2 times that the distillate quality collected is Herba Centellae quality;
(6) distillate Jing filtering with microporous membranes are degerming, and fill is obtained final product.
2. preparation method according to claim 1, it is characterised in that in the step (2) length of cutting be 0.5~ 2cm。
3. preparation method according to claim 1, it is characterised in that the temperature of step (3) hot water is 50~60 DEG C.
4. preparation method according to claim 1, it is characterised in that the step (4) is by adjusting circulating cooling liquid Temperature, makes the temperature of distillate be less than 40 DEG C.
5. preparation method according to claim 1, it is characterised in that the aperture of step (6) microporous filter membrane is 0.22 Micron.
6. Herba Centellae hydrosol obtained in a kind of preparation method as described in any one of Claims 1 to 5.
7. the purposes of Herba Centellae hydrosol obtained in a kind of preparation method as described in any one of Claims 1 to 5, its feature exist In, for astringent, or as substrate be used for allocate emulsion, facial cream or facial film.
CN201710037023.3A 2017-01-18 2017-01-18 Centella asiatica floral water and preparation method and application thereof Pending CN106511142A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107858205A (en) * 2017-11-05 2018-03-30 成重任 A kind of hydrosol liquid, processing method and the application of cordyceps sinensis ginseng
CN109576062A (en) * 2019-02-12 2019-04-05 无锡薇泰药物技术有限公司 A kind of Chinese yew hydrosol extraction process
CN110179727A (en) * 2019-05-14 2019-08-30 株洲千金药业股份有限公司 A kind of skin care compound hydrosol and its preparation method and application
CN112210441A (en) * 2020-10-20 2021-01-12 梵诗吉生物科技(东莞)有限公司 Preparation method of joss-stick-flavor hydrolat and in-vitro antioxidant activity evaluation method thereof
CN113768834A (en) * 2021-08-28 2021-12-10 海南黎草纪新生物科技有限公司 Preparation method of centella asiatica hydrolat
CN115340907A (en) * 2021-10-08 2022-11-15 广州摩亚方舟贸易有限公司 Preparation method of centella asiatica hydrosol and centella asiatica hydrosol
CN116261462A (en) * 2020-07-14 2023-06-13 科然药业有限公司 Composition and use thereof

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CN103462854A (en) * 2013-09-26 2013-12-25 南京俏客网络科技有限公司 Chrysanthemum bud hydrolat and preparation method thereof
CN104490678A (en) * 2014-12-09 2015-04-08 付大亮 Rosemary hydrosol lotion and preparation method thereof
CN104546622A (en) * 2015-02-04 2015-04-29 孙志平 Pure natural plant skin-care product, and extraction process and extraction equipment thereof

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CN103462854A (en) * 2013-09-26 2013-12-25 南京俏客网络科技有限公司 Chrysanthemum bud hydrolat and preparation method thereof
CN104490678A (en) * 2014-12-09 2015-04-08 付大亮 Rosemary hydrosol lotion and preparation method thereof
CN104546622A (en) * 2015-02-04 2015-04-29 孙志平 Pure natural plant skin-care product, and extraction process and extraction equipment thereof

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107858205A (en) * 2017-11-05 2018-03-30 成重任 A kind of hydrosol liquid, processing method and the application of cordyceps sinensis ginseng
CN109576062A (en) * 2019-02-12 2019-04-05 无锡薇泰药物技术有限公司 A kind of Chinese yew hydrosol extraction process
CN110179727A (en) * 2019-05-14 2019-08-30 株洲千金药业股份有限公司 A kind of skin care compound hydrosol and its preparation method and application
CN116261462A (en) * 2020-07-14 2023-06-13 科然药业有限公司 Composition and use thereof
CN112210441A (en) * 2020-10-20 2021-01-12 梵诗吉生物科技(东莞)有限公司 Preparation method of joss-stick-flavor hydrolat and in-vitro antioxidant activity evaluation method thereof
CN113768834A (en) * 2021-08-28 2021-12-10 海南黎草纪新生物科技有限公司 Preparation method of centella asiatica hydrolat
CN115340907A (en) * 2021-10-08 2022-11-15 广州摩亚方舟贸易有限公司 Preparation method of centella asiatica hydrosol and centella asiatica hydrosol

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