CN110179727A - A kind of skin care compound hydrosol and its preparation method and application - Google Patents
A kind of skin care compound hydrosol and its preparation method and application Download PDFInfo
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- CN110179727A CN110179727A CN201910399665.7A CN201910399665A CN110179727A CN 110179727 A CN110179727 A CN 110179727A CN 201910399665 A CN201910399665 A CN 201910399665A CN 110179727 A CN110179727 A CN 110179727A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9767—Pinaceae [Pine family], e.g. pine or cedar
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a kind of skin care compound hydrosols and its preparation method and application.The compound hydrosol is made of the component of following volume ratio: 15~25% masson pine hydrosols, 15~25% moso bamboo hydrosols, 30~60% armeniaca mume hydrosols, 1~10% olibanum hydrosol.The present invention passes through synergistic function between each component, there is very effective moisturizing to moisten, Sage Extract, moistening effect by selecting the hydrosol of particular types and specific proportion to carry out coordination compounding；It being moistened with moisturizing for major function, there is good biocompatibility to human body, active constituent is easy to be absorbed by the skin, and fragrant, and it is no added, it does not stimulate mildly naturally.Moreover, this compound hydrosol also has a variety of skin-care effects, having improves microgroove, anti-aging, anti-inflammatory, Red blood streak dispelling, anti-acne, lightens the stain, bright color, the comprehensive skin effect such as whitening.The compound hydrosol can be used directly, and also can be used for preparing various skin-protection products, has a good application prospect.
Description
Technical field
The invention belongs to cosmetic technical fields.More particularly, to a kind of skin care compound hydrosol and its application.
Background technique
Hydrosol, also known as crystal oil (Hydrolat), refer to the one kind separated during distillation extraction essential oil
The distillation stoste of 100% saturation, is a kind of byproduct of essential oil, and composition is naturally pure, the light pleasant (Modern Marketing (warp of fragrance
Seek version) 01 phase in 2017).Grease can separate during distillation extraction, and because of density difference, essential oil can be swum in above, moisture
It is then deposited in the following, these moisture are just hydrosol.In hydrosol other than containing a small amount of derived essential oil, also containing abundant vegetation water
Soluble substance, contained mineral nutrients (such as tannic acid and flavonoids) are that essential oil is lacked.In addition, consumer is for naturally planting
The product receiving of raw material concept is higher and higher at spending, and more and more receives the concern of people in recent years, there is good market
Prospect.
But individually hydrosol ingredient is more single, effect is also barely satisfactory, it is difficult to meet the needs of comprehensive skin care.With two kinds
Or two or more natural aromatic plants are the compound compound plant hydrosol of raw material, borrow Chinese Traditional Medicine prescription theory, are merged various
Plant essence function, interaction, property is more balanced, and by distilling obtained condensation aqueous solution, fragrance is also richer
Variability is better able to adapt to a variety of demands.
Summary of the invention
The technical problem to be solved by the present invention is to overcome the deficiencies of existing hydrosol Related product, pass through masson pine hydrosol, hair
The coordination compounding of bamboo hydrosol, four kinds of armeniaca mume hydrosol, olibanum hydrosol hydrosols, be made it is a kind of moistened with moisturizing for major function and
It is aided with the compound hydrosol product of more skin-care effects,
The object of the present invention is to provide a kind of skin care compound hydrosols.
Another object of the present invention is to provide the application of the skin care compound hydrosol.
Above-mentioned purpose of the present invention is achieved through the following technical solutions:
A kind of skin care compound hydrosol, is made of the component of following volume ratio: 15~25% masson pine hydrosols, 15~25% maos
Bamboo hydrosol, 30~60% armeniaca mume hydrosols, 1~10% olibanum hydrosol.
Preferably, the compound hydrosol is made of the component of following volume ratio: 20~24% masson pine hydrosols, 20~24%
Moso bamboo hydrosol, 40~50% armeniaca mume hydrosols, 2~6% olibanum hydrosols.
It is highly preferred that the compound hydrosol is made of the component of following volume ratio: 24% masson pine hydrosol, 24% moso bamboo are pure
Dew, 49% armeniaca mume hydrosol, 3% olibanum hydrosol.
In addition to preferably the preparation process of hydrosol is also optimized in the quality and effect of control product, the present invention
Research.
Preferably, the preparation process of hydrosol are as follows:
(1) pre-treatment of raw material: acquiring fresh raw material, distilled at the first time, guarantees the freshness of distillating material；
Fresh raw material, which need to pick before entering pot, removes branch sundries etc.；
(2) filler: raw material, mountain spring water are put into distillation still by the solid-liquid ratio of 1:3~10；
(3) it distills, condense, gained oil water mixture imports oil water separator, and the water phase after water-oil separating is up to hydrosol；
Wherein, control distillation condition: before beginning heat to boiling, access coil pipe steam pressure be 0.35~
0.45MPa；After boiling in 1h, steam pressure is 0.07~0.09MPa；4h after boiling, steam pressure are 0.09~0.11MPa；
6h after boiling, steam pressure are 0.11~0.14MPa；For 8h to terminating, steam pressure is 0.16~0.22MPa after boiling；
The control of condensed water: when heating distillation still to temperature in the kettle is 50~80 DEG C, opening condenser, connect cooling water,
By cooling water control condenser efflux temperature after cooling, after boiling in 1h, efflux temperature is controlled at 30~45 DEG C；When
Stop heating when the amount of efflux reaches suitable with the amount ratio of raw material, during which efflux temperature control is collected at 30~45 DEG C
Efflux obtains oil water mixture.
Preferably, in step (2), masson pine and mountain spring water solid-liquid ratio are 1:2~5, moso bamboo and mountain spring water material in step (2)
Liquor ratio is 1:2~5, and armeniaca mume and mountain spring water solid-liquid ratio are 1:2~5, and olibanum and mountain spring water solid-liquid ratio are 1:2~5.
It is highly preferred that masson pine and mountain spring water solid-liquid ratio are 1:3, and moso bamboo and mountain spring water solid-liquid ratio are 1:5 in step (2),
Armeniaca mume and mountain spring water solid-liquid ratio are 1:4, and olibanum and mountain spring water solid-liquid ratio are 1:5.
Preferably, in order to effectively retain its effective component, so that the saturation degree of hydrosol is high, while making fragrance matter
Can completely retain, masson pine controls according to following ratio in step (3): 1 kilogram of raw material distills out 1~3 kilogram of hydrosol, hair
Bamboo distills out 1~3 kilogram of hydrosol according to 1 kilogram of raw material, and armeniaca mume distills out 1~3 kilogram of hydrosol, olibanum according to 1 kilogram of raw material
2~4 kilograms of hydrosols are distilled out according to 1 kilogram of raw material.
It is highly preferred that masson pine according to 1 kilogram of raw material distills out 1 kilogram of hydrosol in step (3), moso bamboo is according to 1 kilogram of original
Material distills out 1 kilogram of hydrosol, and armeniaca mume distills out 1 kilogram of hydrosol according to 1 kilogram of raw material, and olibanum distills out 3 according to 1 kilogram of raw material
Kilogram hydrosol.
It is highly preferred that the distillation of various hydrosols and condensing condition need difference control as follows:
A. the distillation and condensing condition of masson pine
Control distillation condition: before beginning heat to boiling, the steam pressure for accessing coil pipe is 0.34MPa；1h after boiling
It is interior, steam pressure 0.08MPa；4h after boiling, steam pressure 0.1MPa；6h after boiling, steam pressure 0.12MPa；Boiling
Rear 8h is risen to terminating, steam pressure 0.18MPa；
The control of condensed water: when heating distillation still to temperature in the kettle is 70 DEG C, condenser is opened, cooling water is connected, passes through
Cooling water control condenser efflux temperature after cooling, after boiling in 1h, efflux temperature is controlled at 30~35 DEG C；Work as outflow
Stop heating when the amount of liquid reaches suitable with the amount ratio of raw material, during which efflux temperature control collects outflow at 35~45 DEG C
Liquid obtains oil water mixture；
B. the distillation and condensing condition of moso bamboo
Control distillation condition: before beginning heat to boiling, the steam pressure for accessing coil pipe is 0.4MPa；1h after boiling
It is interior, steam pressure 0.07MPa；4h after boiling, steam pressure 0.1MPa；6h after boiling, steam pressure 0.12MPa；Boiling
Rear 8h is risen to terminating, steam pressure 0.2MPa；
The control of condensed water: when heating distillation still to temperature in the kettle is 80 DEG C, condenser is opened, cooling water is connected, passes through
Cooling water control condenser efflux temperature after cooling, after boiling in 1h, efflux temperature is controlled at 35~45 DEG C；Work as outflow
Stop heating when the amount of liquid reaches suitable with the amount ratio of raw material, during which efflux temperature control collects outflow at 40~45 DEG C
Liquid obtains oil water mixture；
C. the distillation and condensing condition of armeniaca mume
Control distillation condition: before beginning heat to boiling, the steam pressure for accessing coil pipe is 0.45MPa；1h after boiling
It is interior, steam pressure 0.08MPa；4h after boiling, steam pressure 0.09MPa；6h after boiling, steam pressure be 0.11~
0.14MPa；For 8h to terminating, steam pressure is 0.16~0.22MPa after boiling；
The control of condensed water: when heating distillation still to temperature in the kettle is 60 DEG C, condenser is opened, cooling water is connected, passes through
Cooling water control condenser efflux temperature after cooling, after boiling in 1h, efflux temperature is controlled at 25~35 DEG C；Work as outflow
Stop heating when the amount of liquid reaches suitable with the amount ratio of raw material, during which efflux temperature control collects outflow at 35~45 DEG C
Liquid obtains oil water mixture；
D. the distillation and condensing condition of olibanum
Control distillation condition: before beginning heat to boiling, the steam pressure for accessing coil pipe is 0.35MPa；1h after boiling
It is interior, steam pressure 0.09MPa；4h after boiling, steam pressure 0.11MPa；6h after boiling, steam pressure 0.14MPa；Boiling
Rear 8h is risen to terminating, steam pressure 0.22MPa；
The control of condensed water: when heating distillation still to temperature in the kettle is 50 DEG C, condenser is opened, cooling water is connected, passes through
Cooling water control condenser efflux temperature after cooling, after boiling in 1h, efflux temperature is controlled at 20~30 DEG C；Work as outflow
Stop heating when the amount of liquid reaches suitable with the amount ratio of raw material, during which efflux temperature control collects outflow at 30~40 DEG C
Liquid obtains oil water mixture.
It is highly preferred that the compound hydrosol the preparation method comprises the following steps: above-mentioned 200~400 mesh filter screens of various hydrosols are filtered
Afterwards, it is pumped into emulsion pot in proportion, is stirred 5~10 minutes by the revolving speed of 10~30 turns/min, take pattern detection physicochemical data, closed
With 200~400 mesh filter screen filtering and dischargings after lattice.Emulsion pot is clean using preceding cleaning and sterilizing.
Compound hydrosol of the invention can be used directly, be can also be used as raw material use, be used for various cosmetic products, skin care
The preparation of product, daily chemical product.
Therefore, the compound pure is exposed at the application prepared in the products such as skin care item, cosmetics, daily chemical product, also Ying Ben
Within the protection scope of invention.Including toner, toner, makeup remover, stoste, lotion, facial mask, eye cream, face cream, mildy wash,
Sun screen, BB frost, CC frost, suncream, eau de toilette, hair products, bath product etc..
The invention has the following advantages:
The present invention passes through collaboration by selecting the hydrosol of particular types and specific proportion to carry out coordination compounding between each component
Synergistic effect, gained compound hydrosol moist, Sage Extract, moistening effect with very effective moisturizing；With moisturizing moisten based on
Function is wanted, there is good biocompatibility to human body, active constituent is easy to be absorbed by the skin, and fragrant, with day
Right fragrant plant formula constitutes natural anticorrosion system, and preservative free, without essence, the addition of prosthetic pigment do not stimulate mildly naturally,
Quality is uniform, reliable and stable.
And this compound pure is exposed at while having ensured product basic moisturizing effect, is made by the adjustment of technique and formula multiple
Fang Chunlu has a variety of skin-care effects, can improve microgroove, anti-aging, anti-inflammatory, Red blood streak dispelling, anti-acne, lighten the stain, highlights skin
The compound skin care such as color, whitening；The richer variation of fragrance and intelligence of compound hydrosol simultaneously, meets the happiness of most of female consumers
It is good.
The compound hydrosol is from the angle of traditional culture, the angle of Chinese Traditional Medicine, the angle multi-angle of conventional fragrant plant
Incision has effects that a as material base, chooses the raw material having good quality, ground by scientific formula using fragrant plant itself
Study carefully, standardized extraction processing technology, obtains the compound plant hydrosol product of fragrance pleasure.In use, spray can be chosen
Dosage form of the mist as its carrying more emphasizes daily moisturizing and convenient and practical, at home, handles official business, standing product of travelling.
In addition, the compound hydrosol either directly uses, or various cosmetic products, skin care production are used to prepare as raw material
Product, daily chemical product etc., all have a good application prospect.
Specific embodiment
Further illustrate the present invention below in conjunction with specific embodiment, but embodiment the present invention is not done it is any type of
It limits.Unless stated otherwise, the present invention uses reagent, method and apparatus is the art conventional reagents, method and apparatus.
Unless stated otherwise, agents useful for same and material of the present invention are commercially available.
The preparation process of 1 hydrosol of embodiment
The preparation process of each hydrosol is as follows:
(1) pre-treatment of raw material: acquiring fresh raw material, distilled at the first time, guarantees the freshness of distillating material；
Fresh raw material, which need to pick before entering pot, removes branch sundries etc..
(2) filler: raw material, mountain spring water are put into distillation still in the ratio of 1:3~5；Specifically, masson pine and mountain spring water
Solid-liquid ratio is 1:3, and moso bamboo and mountain spring water solid-liquid ratio are 1:5, and armeniaca mume and mountain spring water solid-liquid ratio are 1:4, olibanum and mountain spring water material
Liquor ratio is 1:5.
(3) it distills, condense, gained oil water mixture imports oil water separator, and the water phase after water-oil separating is up to hydrosol.
Masson pine distills out 1 kilogram of hydrosol according to 1 kilogram of raw material, and moso bamboo distills out 1 kilogram of hydrosol according to 1 kilogram of raw material, and armeniaca mume is pressed
1 kilogram of hydrosol is distilled out according to 1 kilogram of raw material, olibanum distills out 3 kilograms of hydrosols according to 1 kilogram of raw material.
Wherein, specific condition is as follows:
A. the distillation and condensing condition of masson pine
Control distillation condition: before beginning heat to boiling, the steam pressure for accessing coil pipe is 0.34MPa；1h after boiling
It is interior, steam pressure 0.08MPa；4h after boiling, steam pressure 0.1MPa；6h after boiling, steam pressure 0.12MPa；Boiling
Rear 8h is risen to terminating, steam pressure 0.18MPa；
The control of condensed water: when heating distillation still to temperature in the kettle is 70 DEG C, condenser is opened, cooling water is connected, passes through
Cooling water control condenser efflux temperature after cooling, after boiling in 1h, efflux temperature is controlled at 30 DEG C；When efflux
Stop heating when amount reaches suitable with the amount ratio of raw material, during which efflux temperature control collects efflux and obtain oil at 35 DEG C
Aqueous mixtures；
B. the distillation and condensing condition of moso bamboo
Control distillation condition: before beginning heat to boiling, the steam pressure for accessing coil pipe is 0.4MPa；1h after boiling
It is interior, steam pressure 0.07MPa；4h after boiling, steam pressure 0.1MPa；6h after boiling, steam pressure 0.12MPa；Boiling
Rear 8h is risen to terminating, steam pressure 0.2MPa；
The control of condensed water: when heating distillation still to temperature in the kettle is 80 DEG C, condenser is opened, cooling water is connected, passes through
Cooling water control condenser efflux temperature after cooling, after boiling in 1h, efflux temperature is controlled at 35 DEG C；When efflux
Stop heating when amount reaches suitable with the amount ratio of raw material, during which efflux temperature control collects efflux and obtain oil at 45 DEG C
Aqueous mixtures；
C. the distillation and condensing condition of armeniaca mume
Control distillation condition: before beginning heat to boiling, the steam pressure for accessing coil pipe is 0.45MPa；1h after boiling
It is interior, steam pressure 0.08MPa；4h after boiling, steam pressure 0.09MPa；6h after boiling, steam pressure 0.13MPa；Boiling
Rear 8h is risen to terminating, steam pressure 0.16MPa；
The control of condensed water: when heating distillation still to temperature in the kettle is 60 DEG C, condenser is opened, cooling water is connected, passes through
Cooling water control condenser efflux temperature after cooling, after boiling in 1h, efflux temperature is controlled at 30 DEG C；When efflux
Stop heating when amount reaches suitable with the amount ratio of raw material, during which efflux temperature control collects efflux and obtain oil at 40 DEG C
Aqueous mixtures；
D. the distillation and condensing condition of olibanum
Control distillation condition: before beginning heat to boiling, the steam pressure for accessing coil pipe is 0.35MPa；1h after boiling
It is interior, steam pressure 0.09MPa；4h after boiling, steam pressure 0.11MPa；6h after boiling, steam pressure 0.14MPa；Boiling
Rear 8h is risen to terminating, steam pressure 0.22MPa；
The control of condensed water: when heating distillation still to temperature in the kettle is 50 DEG C, condenser is opened, cooling water is connected, passes through
Cooling water control condenser efflux temperature after cooling, after boiling in 1h, efflux temperature is controlled at 25 DEG C；When efflux
Stop heating when amount reaches suitable with the amount ratio of raw material, during which efflux temperature control collects efflux and obtain oil at 35 DEG C
Aqueous mixtures.
The preparation process of 2 hydrosol of embodiment
The preparation process of each hydrosol with embodiment 1, the difference is that:
In step (2), masson pine and mountain spring water solid-liquid ratio are 1:5, and moso bamboo and mountain spring water solid-liquid ratio are 1:2, armeniaca mume with
Mountain spring water solid-liquid ratio is 1:2, and olibanum and mountain spring water solid-liquid ratio are 1:2.
Masson pine distills out 2 kilograms of hydrosols according to 1 kilogram of raw material in step (3), and moso bamboo distills out 2 according to 1 kilogram of raw material
Kilogram hydrosol, armeniaca mume distill out 2 kilograms of hydrosols according to 1 kilogram of raw material, and olibanum distills out 4 kilograms of hydrosols according to 1 kilogram of raw material.
The preparation process of 3 hydrosol of embodiment
The preparation process of each hydrosol with embodiment 1, the difference is that:
In step (2), masson pine and mountain spring water solid-liquid ratio are 1:2, and moso bamboo and mountain spring water solid-liquid ratio are 1:5, armeniaca mume with
Mountain spring water solid-liquid ratio is 1:5, and olibanum and mountain spring water solid-liquid ratio are 1:5.
Masson pine distills out 3 kilograms of hydrosols according to 1 kilogram of raw material in step (3), and moso bamboo distills out 3 according to 1 kilogram of raw material
Kilogram hydrosol, armeniaca mume distill out 3 kilograms of hydrosols according to 1 kilogram of raw material, and olibanum distills out 2 kilograms of hydrosols according to 1 kilogram of raw material.
The preparation of 4 skin care compound hydrosol of embodiment
1, skin care compound pure reveals volume proportion: 24% masson pine hydrosol, 24% moso bamboo hydrosol, 49% armeniaca mume hydrosol, 3%
Olibanum hydrosol.
2, compound hydrosol is prepared:
After the various hydrosols of above-mentioned preparation are filtered with 300 mesh filter screens, it is pumped into emulsion pot in proportion, by 20 turns/min's
Revolving speed stirs 5 minutes, takes pattern detection physicochemical data, it is qualified after with 300 mesh filter screen filtering and dischargings.Emulsion pot is using preceding cleaning
Disinfection is clean.
The preparation of 5 skin care compound hydrosol of embodiment
1, skin care compound pure reveals volume proportion: 20% masson pine hydrosol, 24% moso bamboo hydrosol, 50% armeniaca mume hydrosol, 6%
Olibanum hydrosol.
2, compound hydrosol is prepared:
After above-mentioned various hydrosols are filtered with 200 mesh filter screens, it is pumped into emulsion pot, is stirred by the revolving speed of 30 turns/min in proportion
Mix 5 minutes, take pattern detection physicochemical data, it is qualified after with 200 mesh filter screen filtering and dischargings.Emulsion pot is dry using preceding cleaning and sterilizing
Only.
The preparation of 6 skin care compound hydrosol of embodiment
1, skin care compound pure reveals volume proportion: 24% masson pine hydrosol, 24% moso bamboo hydrosol, 50% armeniaca mume hydrosol, 2%
Olibanum hydrosol.
2, compound hydrosol is prepared:
After above-mentioned various hydrosols are filtered with 400 mesh filter screens, it is pumped into emulsion pot, is stirred by the revolving speed of 10 turns/min in proportion
Mix 10 minutes, take pattern detection physicochemical data, it is qualified after with 400 mesh filter screen filtering and dischargings.Emulsion pot is using preceding cleaning and sterilizing
Completely.
The preparation of 7 skin care compound hydrosol of embodiment
Skin care compound pure reveals volume proportion: 15% masson pine hydrosol, 15% moso bamboo hydrosol, 60% armeniaca mume hydrosol, 10%
Olibanum hydrosol.Compound hydrosol is prepared with embodiment 4.
The preparation of 8 skin care compound hydrosol of embodiment
Skin care compound pure reveals volume proportion: 20% masson pine hydrosol, 20% moso bamboo hydrosol, 50% armeniaca mume hydrosol, 10%
Olibanum hydrosol.Compound hydrosol is prepared with embodiment 4.
The preparation of 9 skin care compound hydrosol of embodiment
Skin care compound pure reveals volume proportion: 25% masson pine hydrosol, 25% moso bamboo hydrosol, 49% armeniaca mume hydrosol, 1% cream
Fragrant hydrosol.Compound hydrosol is prepared with embodiment 4.
Comparative example 1~7
Comparative example is set according to such as the following table 1 different compounding, is prepared with embodiment 4.
Table 1
| Group | Composition |
| Comparative example 1 | 25% masson pine hydrosol, 25% moso bamboo hydrosol, 50% armeniaca mume hydrosol |
| Comparative example 2 | 48% masson pine hydrosol, 49% armeniaca mume hydrosol, 3% olibanum hydrosol |
| Comparative example 3 | 48% moso bamboo hydrosol, 49% armeniaca mume hydrosol, 3% olibanum hydrosol |
| Comparative example 4 | 45% masson pine hydrosol, 45% moso bamboo hydrosol, 10% olibanum hydrosol |
| Comparative example 5 | 30% masson pine hydrosol, 30% moso bamboo hydrosol, 25% armeniaca mume hydrosol, 15% olibanum hydrosol |
| Comparative example 6 | 10% masson pine hydrosol, 10% moso bamboo hydrosol, 70% armeniaca mume hydrosol, 10% olibanum hydrosol |
| Comparative example 7 | 30% masson pine hydrosol, 30% moso bamboo hydrosol, 25% armeniaca mume hydrosol, 15% olibanum hydrosol |
The skin irritation test of 10 skin care compound hydrosol of embodiment
1, with the compound hydrosol external application of embodiment 4~9, its irritation and allergic reaction to skin is observed.
(1) rabbit skin irritation test is used, divides intact skin group and damage skin group, continues after smearing external application respectively
Observing skin, whether there is or not the stimulate the reactions such as erythema, oedema.
(2) guinea pig skin allergic experiment is used, is smeared daily external application 2 times, continuous 3 weeks, whether there is or not erythema, oedema for observation skin
Equal allergic reactions.
2, result:
The intact skin and damaged skin of rabbit, remove after being intended for single use or be used for multiple times for 24 hours, respectively at 1,24,48,
72h observation, is showed no erythema and oedema, and stimulate the reaction mean scores are < 0.5, nonirritant.
In guinea pig skin allergic experiment, does not occur the cutaneous anaphylaxises such as the obvious erythema of skin, oedema and other are systemic
Allergic reaction.
Therefore, compound hydrosol of the invention will not cause irritative response to rabbit intact skin and damage skin, to globefish
Mouse skin has good cutaneous safety without allergic reaction.
The moisturizing of 11 skin care compound hydrosol of embodiment is tested
1, arm is directly smeared with the compound hydrosol of embodiment 4~9 and comparative example 1~7 to be tested.Utilize multifunctional leather
Skin tester (there is skin moisture content test probe and the lost TEWL test probe of moisture of skin) test skin moisture content
It scatters and disappears with moisture of skin.Testing environment temperature is 25 ± 1 DEG C, and humidity is 60 ± 5%, and carries out Real-time and Dynamic Detection.
It does not use any product within 2~3 days before tested arm position, cleans recipient site before testing.First measure each test section
The blank value in domain, then by the tested part of compound hydrosol even spread.It is right behind 30min, 1 hour, 2 hours, 4 hours
The skin in tested region and blank control region is tested, and the test of the same volunteer is completed by the same survey crew.
Each region is according to parallel determination 15 times.
(1) calculation formula of each period MMV value are as follows:
W%=(W1-W0)/W0 × 100%
In formula, W%=skin moisture content increased percentage (MMV), W0=skin uses moisture content before sample, W1=
Skin uses moisture content after sample.
(2) TEWL value is an important symbol of skin barrier quality, and the TEWL value of skin is lower, illustrates the barrier of skin
Function is better, otherwise poorer.
The TEWL value calculation formula of each period are as follows:
T%=(T1-T0)/T0 × 100%
In formula: T%=moisture of skin, which percutaneously scatters and disappears, reduces percentage (TEWL)；T0=skin uses moisture before sample percutaneous
It scatters and disappears and is worth；T1=skin is percutaneously scattered and disappeared using moisture after sample to be worth.
2, test result is respectively as shown in table 2, table 3
The MMV value of each period of table 2
The TEWL value of each period of table 3
| 0min | 30min | 1 hour | 2 hours | 4 hours | |
| Embodiment 4 | 0 | 3.1% | 3.9% | 7.9% | 11.5% |
| Embodiment 5 | 0 | 3.2% | 4.1% | 8.6% | 16.1% |
| Embodiment 6 | 0 | 3.5% | 4.7% | 8.3% | 15.2% |
| Embodiment 7 | 0 | 3.7% | 4.8% | 8.9% | 19.3% |
| Embodiment 8 | 0 | 3.9% | 4.6% | 9.3% | 18.5% |
| Embodiment 9 | 0 | 3.6% | 4.9% | 9.6% | 15.9% |
| Comparative example 1 | 0 | 9.4% | 15.8% | 19.3% | 29.6% |
| Comparative example 2 | 0 | 6.5% | 11.4% | 17.6% | 25.4% |
| Comparative example 3 | 0 | 7.1% | 12.6% | 19.4% | 22.3% |
| Comparative example 4 | 0 | 6.1% | 15.7% | 17.7% | 24.5% |
| Comparative example 5 | 0 | 9.3% | 13.8% | 16.8% | 23.8% |
| Comparative example 6 | 0 | 8.9% | 14.4% | 16.2% | 21.2% |
| Comparative example 7 | 0 | 7.4% | 9.6% | 11.4% | 23.7% |
The results show that compound hydrosol provided by the invention, compounding and proportion science, can make moisture of skin in 30min
Content is improved to 99.5%, the timely moisturizing significant effect of skin；The growth of 80% or more skin moisture content is also able to maintain after 2h,
The growth of 65% or more skin moisture content is also able to maintain after 4h.Its ability for reducing the lost TEWL of moisture of skin also obtains significantly
It is promoted, is conducive to the abundant moisturizing of skin.Compared with comparative example 1~7, the compound pure that embodiment 4~9 provides is exposed at raising moisture
Content, the effect aspect for inhibiting moisture loss, show conspicuousness and improve (p < 0.05), and it is aobvious to show that each component compounding plays
The synergistic function of work.
The whitening spot-removing of 12 skin care compound hydrosol of embodiment is tested
Face is directly smeared with the compound hydrosol of embodiment 4~9 and comparative example 1~7 to be tested, while commercially available beauty is set
White product is control.The random screening age was 20~35 one full year of life, has color spot, acne print crowd as experimental subjects, and test uses
Subjects skin's data after compound hydrosol the 1st week, the 4th week, the 6th week.
The measurement result of dermal melanin content MI value and content of hemachrome EI value shows that experimental group compound hydrosol can be shown
Writing reduces dermal melanin content, has the effect of desalinating dermal melanin, reduces skin content of hemachrome, embodiment group effect
Significantly better than control group, and difference on effect is in rising trend at any time.Simultaneously to the analysis of skin splash area accounting and skin-color
Spot optical density the results of analysis of variance shows that experimental group compound hydrosol desalinates skin pigment spot, reduces skin splash optical density variance
Significant effect, hence it is evident that be better than control group.Compound hydrosol of the invention has the effect of bright color, whitening spot-removing, anti-acne.
The Antisenility Experiment of 13 skin care compound hydrosol of embodiment
1, experimental method
Test specimen: to be tested for the compound hydrosol of embodiment 4 and comparative example 1,6.
Experimental animal: healthy mice, 12 week old, 40~45g of weight, half male and half female.
Test method: the depilation of each group back of mice, exposure test section.Clearing skin before testing, it is each daily morning and evening to smear one
Secondary compound hydrosol, it is continuous to smear 60 days, the mouse hair newly grown is during which shaved off in time.After 30th day and the 60th day last smearing 12h,
Clip mouse test section skin histology, prepares skin histology homogenate, with kit measurement superoxide dismutase (SOD) vigor
And malonaldehyde (MDA), Kong proline (HYP) content.
2, experimental result is shown in Table 4
Influence of the 4 compound hydrosol of table to MDA, SOD, HYP content in skin histology homogenate
Known to test result: the SOD vigor in mice skin tissue homogenate rises, and the content of HYP obviously increases, and MDA
Content be then substantially reduced, and there were significant differences with comparative example, shows between compound hydrosol each component of the present invention there is collaboration to increase
Imitate facilitation.In addition compound hydrosol is also tested for the scavenging capacity of DPPH, and clearance rate can reach 95% or more.The present invention
Compound hydrosol has significant antioxidant and anti-aging effect.
The Red blood streak dispelling of 14 skin care compound hydrosol of embodiment is tested
1, face is directly smeared with the compound hydrosol of embodiment 4~9 and comparative example 1~7 to be tested, while being arranged commercially available
Red blood streak dispelling product is control.The random screening age was 20~35 one full year of life, with the people for having red blood trace on face symptom to a certain degree
Group is used as experimental subjects.
30min before testing, subject clean face.Every group of subject smears test sample in right face, and left face is blank
It compares, hydrosol is used after daily morning and evening face cleaning, during test, subject cannot smear any other cosmetics.Experiment periods two
Month.Using skin ferroheme tester, measurement uses red pigment value preceding and using left face and right face after two months respectively.
Inhibit the calculation method of situation (inhibiting rate) using haematochrome before and after compound hydrosol:
Inhibiting rate=(using the preceding rear red pigment value of red pigment value-use) × 100%/uses preceding red pigment value
It is effective: inhibiting rate >=20%；It is effective: inhibiting rate=5%~20%；It is invalid: inhibiting rate < 5%.
2, the results are shown in Table 5
5 red capillary inhibiting rate of table
| Obvious effective rate | It is efficient | Inefficiency | |
| Embodiment 4 | 78.2% | 19.7% | 2.1% |
| Embodiment 5 | 65.3% | 38.4% | 2.3% |
| Embodiment 6 | 63.2% | 33.6% | 3.2% |
| Embodiment 7 | 61.5% | 34.4% | 4.1% |
| Embodiment 8 | 62.1% | 33.7% | 4.2% |
| Embodiment 9 | 60.3% | 34.8% | 4.9% |
| Comparative example 1 | 18.2% | 62.7% | 19.1% |
| Comparative example 2 | 17.6% | 67.0% | 15.4% |
| Comparative example 3 | 16.5% | 71.2% | 12.3% |
| Comparative example 4 | 18.4% | 63.4% | 18.2% |
| Comparative example 5 | 19.5% | 62.4% | 18.1% |
| Comparative example 6 | 20.3% | 64.5% | 15.2% |
| Comparative example 7 | 21.9% | 58.2% | 19.9% |
| Control group | 16.2% | 28.7% | 55.1% |
The effect that compound hydrosol of the present invention repairs red capillary is substantially better than commercial product, and obvious effective rate always has 70% or more
Efficiency is up to 95% or more.In addition the investigation of subject is shown after experiment periods, the drying of compound hydrosol of the present invention opposite portion,
Red blood trace on face, facial itch have significant improvement.
The experiment on probation of 15 skin care compound hydrosol of embodiment
1, face paper is moistened with the compound pure dew retting of embodiment 4~9, gained facial mask is experimental group material.Simultaneously with commercially available
Certain brand smoothing toner is control.
It has collected that skin of face is coarse, pore is coarse, has wrinkle, face obscure, has there is the volunteer of acne print, scar print or pigment
210, wherein male 49, women 161, the age was at 25~40 years old.According to age level in batches after be divided into 7 groups at random, point
Do not try out above-mentioned facial mask, experimental period 3 months.Then trier pressed at interval of face mask film 10 minutes behind 3 days at night conventional face cleaning
Rub face 1~3 minute, then smears face cream.
2, trier is asked to provide effect assessment after testing, to take statistics.
The results show that the skin of all triers relatively moistens, moistening effect is good.Meanwhile experimental group fits the colour of skin of user
Obviously become ruddy, naturally pale, have a good complexion, skin obviously becomes smooth exquisiteness, and whitening effect is significant, and acne print, which is substantially reduced, to be subtracted
It is weak.Significantly excellent control group.
In addition, there are about the skin fine lines of 81% trier, especially canthus microgroove for experimental group, hence it is evident that reduce, even
It disappears.
In addition, thering are 9 skins to belong to sensitive flesh in trier, often because skin care item improper use generates erythema, small pox all
Condition susceptible.And in the experimentation, never there is allergic symptom, and red blood trace on face phenomenon is obviously improved.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology all without departing from the spirit and scope of the present invention, carries out modifications and changes to above-described embodiment.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should be covered by the claims of the present invention.
Claims (10)
1. a kind of skin care compound hydrosol, which is characterized in that be grouped as by following volume ratio group: 15~25% masson pine hydrosols, 15
~25% moso bamboo hydrosol, 30~60% armeniaca mume hydrosols, 1~10% olibanum hydrosol.
2. compound hydrosol according to claim 1, which is characterized in that be grouped as by following volume ratio group: 20~24% horse hairs
Loose hydrosol, 20~24% moso bamboo hydrosols, 40~50% armeniaca mume hydrosols, 2~6% olibanum hydrosols.
3. compound hydrosol according to claim 1, which is characterized in that be grouped as by following volume ratio group: 24% masson pine is pure
Dew, 24% moso bamboo hydrosol, 49% armeniaca mume hydrosol, 3% olibanum hydrosol.
4. the preparation method of any compound hydrosol of claims 1 to 3, which comprises the steps of:
(1) masson pine, moso bamboo, armeniaca mume, olibanum raw material are taken respectively；
(2) filler: raw material and mountain spring water are distilled by the solid-liquid ratio of 1:3~10；
(3) it distills, condense, obtain oil water mixture, the water phase after water-oil separating is hydrosol；
Control distillation condition: before beginning heat to boiling, 0.35~0.45MPa of steam pressure；After boiling in 1h, steam pressure
0.07~0.09MPa；4h after boiling, 0.09~0.11MPa of steam pressure；6h after boiling, 0.11~0.14MPa of steam pressure；
8h is to terminating after boiling, 0.16~0.22MPa of steam pressure；
The control of condensed water: be heated to temperature be 50~80 DEG C when, connect condensed water, by condense water management efflux temperature,
After boiling in 1h, efflux temperature is controlled at 30~45 DEG C；When the amount of efflux reaches it is suitable with the amount ratio of raw material when stopping
Heating, during which efflux temperature control collect efflux and obtain oil water mixture at 30~45 DEG C.
5. preparation method according to claim 5, which is characterized in that masson pine and mountain spring water solid-liquid ratio are 1:2 in step (2)
~5, moso bamboo and mountain spring water solid-liquid ratio are 1:2~5, and armeniaca mume and mountain spring water solid-liquid ratio are 1:2~5, olibanum and mountain spring water feed liquid
Than for 1:2~5.
6. any preparation method according to claim 1~3, which is characterized in that masson pine is according to 1 kilogram of original in step (3)
Material distills out 1~3 kilogram of hydrosol, and moso bamboo distills out 1~3 kilogram of hydrosol according to 1 kilogram of raw material, and armeniaca mume is according to 1 kilogram of raw material
1~3 kilogram of hydrosol is distilled out, olibanum distills out 2~4 kilograms of hydrosols according to 1 kilogram of raw material.
7. any preparation method according to claim 1~3, which is characterized in that the condition control of step (3) is as follows:
A. the distillation and condensing condition of masson pine
Control distillation condition: before beginning heat to boiling, steam pressure 0.34MPa；After boiling in 1h, steam pressure is
0.08MPa；4h after boiling, steam pressure 0.1MPa；6h after boiling, steam pressure 0.12MPa；8h is to terminating after boiling,
Steam pressure is 0.18MPa；
The control of condensed water: be heated to temperature be 70 DEG C when, connect condensed water, pass through condensation water management efflux temperature, boiling
Afterwards in 1h, efflux temperature is controlled at 30~35 DEG C；When the amount of efflux reaches it is suitable with the amount ratio of raw material when stop heating,
Period efflux temperature is controlled at 35~45 DEG C, is collected efflux and is obtained oil water mixture；
B. the distillation and condensing condition of moso bamboo
Control distillation condition: before beginning heat to boiling, steam pressure 0.4MPa；After boiling in 1h, steam pressure is
0.07MPa；4h after boiling, steam pressure 0.1MPa；6h after boiling, steam pressure 0.12MPa；8h is to terminating after boiling,
Steam pressure is 0.2MPa；
The control of condensed water: be heated to temperature be 80 DEG C when, connect condensed water, pass through condensation water management efflux temperature, boiling
Afterwards in 1h, efflux temperature is controlled at 35~45 DEG C；When the amount of efflux reaches it is suitable with the amount ratio of raw material when stop heating,
Period efflux temperature is controlled at 40~45 DEG C, is collected efflux and is obtained oil water mixture；
C. the distillation and condensing condition of armeniaca mume
Control distillation condition: before beginning heat to boiling, steam pressure 0.45MPa；After boiling in 1h, steam pressure is
0.08MPa；4h after boiling, steam pressure 0.09MPa；6h after boiling, steam pressure are 0.11~0.14MPa；8h after boiling
To terminating, steam pressure is 0.16~0.22MPa；
The control of condensed water: be heated to temperature be 60 DEG C when, connect condensed water, pass through condensation water management efflux temperature, boiling
Afterwards in 1h, efflux temperature is controlled at 25~35 DEG C；When the amount of efflux reaches it is suitable with the amount ratio of raw material when stop heating,
Period efflux temperature is controlled at 35~45 DEG C, is collected efflux and is obtained oil water mixture；
D. the distillation and condensing condition of olibanum
Control distillation condition: before beginning heat to boiling, steam pressure 0.35MPa；After boiling in 1h, steam pressure is
0.09MPa；4h after boiling, steam pressure 0.11MPa；6h after boiling, steam pressure 0.14MPa；8h is to terminating after boiling,
Steam pressure is 0.22MPa；
The control of condensed water: be heated to temperature be 50 DEG C when, connect condensed water, pass through condensation water management efflux temperature, boiling
Afterwards in 1h, efflux temperature is controlled at 20~30 DEG C；When the amount of efflux reaches it is suitable with the amount ratio of raw material when stop heating,
Period efflux temperature is controlled at 30~40 DEG C, is collected efflux and is obtained oil water mixture.
8. any preparation method according to claim 1~3, which is characterized in that the compound hydrosol the preparation method comprises the following steps: will
It after various hydrosols are filtered with 200~400 mesh filter screens, mixes in proportion, 5~10 points of stirring of the revolving speed emulsification of 10~30 turns/min
Clock, with 200~400 mesh filter screen filtering and dischargings.
9. any compound pure of claims 1 to 3 is exposed at the application prepared in skin care item.
10. any compound pure of claims 1 to 3 is exposed at the application prepared in cosmetics or daily chemical product.
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