CN104116681B - A kind of hair washing bath shampoo and preparation method thereof - Google Patents

A kind of hair washing bath shampoo and preparation method thereof Download PDF

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Publication number
CN104116681B
CN104116681B CN201410376357.XA CN201410376357A CN104116681B CN 104116681 B CN104116681 B CN 104116681B CN 201410376357 A CN201410376357 A CN 201410376357A CN 104116681 B CN104116681 B CN 104116681B
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extract
hair washing
washing bath
bath shampoo
radix
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CN201410376357.XA
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CN104116681A (en
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陈锐
舒士君
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LIUZHOU NUOXIN MEIDA SCIENCE & TECHNOLOGY Co Ltd
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LIUZHOU NUOXIN MEIDA SCIENCE & TECHNOLOGY Co Ltd
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Abstract

The invention discloses a kind of hair washing bath shampoo, the present invention uses these damp eliminatings of wormwood extract, Cortex Dictamni extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract, heat clearing away, the compounding gentle surfactant of antipruritic botanical herbs composition to make described hair washing bath shampoo, described hair washing bath shampoo is safer, zest and toxic and side effects are less, it is difficult to cause skin allergy, inflammation, safe and reliable and simple for production, it is particularly well-suited to skin sensitivity crowd and infant.Can help to eliminate baby's skin because antiperspirant or urine leaching cause the anaphylaxis of diaper rash and eczema, additionally aid simultaneously and alleviate mosquito bite and sufferings symptom that skin allergy brings.

Description

A kind of hair washing bath shampoo and preparation method thereof
Technical field
The present invention relates to a kind of hair washing bath shampoo, be specifically related to the hair washing of a kind of nontoxic, non-stimulated and easy flushing Bath shampoo.
Background technology
The safety of articles for children is always when each head of a family selects article for child concern the most.Right In the cleaning supplies of child, nontoxic, non-stimulated and easy flushing is the first-selection of most of family.Currently on the market Hair washing for child bath product the most still use fatty alcohol polyoxyethylene ether sulfate, alkanolamide, Radix Betae Alkali and amine oxide etc. have bigger irritating surfactant to hair and skin, additionally as fatty alcohol polyoxy Containing carcinogen dioxanes in vinyl Ether sulfate, child is allowed to use the hair washing of these preparation of raw material for a long time Bath product, can become its healthy big hidden danger of harm.
The fatty alcohol polyoxyethylene ether sulfate of most hair washing for child bath product uses, alkanolamide, Radix Betae The surfactant zest such as alkali and amine oxide is big and defat is too strong, easy injured skin.And these tables Containing poisonous and harmful substance inside the activating agent of face, in use may make in entering child's body through skin Health is become seriously to damage.
The function of existing hair washing for child bath product is less, simply has cleaning action.
Cause reason: the materials safety of use is the highest and does not produces for the skin problem that child is common Product design.
Summary of the invention
The weak point that it is an object of the invention to overcome prior art to exist and provide a kind of nontoxic, stingless The hair washing bath shampoo swashed and easily rinse, present invention also offers the preparation method of described hair washing bath shampoo.
For achieving the above object, the technical scheme taked: a kind of hair washing bath shampoo, described hair washing bath shampoo Including following components in percentage by weight: Chinese medicine extract: 1-10%, cod-liver oil: 0.1-3%, ethoxy sulphur Acid sodium: 10-30%, lanoline: 0.1-1%, glycerol: 20-50%, preservative: appropriate, surplus is water;
Described Chinese medicine extract includes that wormwood extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae carry Take thing and Radix et Caulis Opuntiae Dillenii extract.
In hair washing bath shampoo of the present invention, the consumption 1-10% of Chinese medicine extract is preferred amount ranges, its effect Best;When in described hair washing bath shampoo, the consumption of Chinese medicine extract is less than 1%, its effect can substantially reduce; When the consumption of Chinese medicine extract is higher than 10% in described hair washing bath shampoo, cost can be greatly increased.
Folium Artemisiae Argyi of the present invention is perennial herb or slightly becomes suffruticose plant.All herbal medicine has damp eliminating, dissipates The effects such as cold, antiinflammatory, antiallergic.
Cortex Dictamni of the present invention is the root bark of Rutaceae herbaceos perennial shaggy-fruited dittany.There is antipyretic and itching-stopping, Dispel the wind removing toxic substances effect.
Flos Chrysanthemi Indici of the present invention is Compositae herbaceos perennial.There is subduing swelling and detoxicating, dispelling wind and heat pathogens, resist Effect of virus.
Radix Scutellariae of the present invention is the root of Radix Scutellariae, is a kind of medical herbs, it is possible to heat clearing and damp drying, antibacterial and detoxicating.
Radix et Caulis Opuntiae Dillenii of the present invention is Cactaeous plants, have relaxing muscles and tendons and activating QI and blood in the collateral, dissipating blood stasis for subsidence of swelling, mosquito bite and The effect of healing of wound.
Sodium isethionate of the present invention, CAS NO.1562-00-1, for nontoxic non-stimulated surface activity Agent, may be used for cleaning hair and skin.
Cod-liver oil of the present invention is the fat extracting from the liver such as shark, morrhua, containing enrich Nutritional labeling can nourish hair and skin care.
Lanoline of the present invention is by smegma natural materials out, is good moistness material, Hair and skin can be allowed to keep point water and repair the skin histology impaired because of hydropenia.
Glycerol of the present invention, formal name used at school glycerol, there is the effect of moisturizing and increase-volume, increase system stability.
As the preferred implementation of hair washing bath shampoo of the present invention, described hair washing bath shampoo includes following heavy The component of amount percentage ratio: Chinese medicine extract: 8-10%, cod-liver oil: 2-3%, sodium isethionate: 25-30%, Lanoline: 0.8-1%, glycerol: 40-50%, surplus is water.
As the preferred implementation of hair washing bath shampoo of the present invention, described hair washing bath shampoo includes following heavy The component of amount percentage ratio: Chinese medicine extract: 10%, cod-liver oil: 3%, sodium isethionate: 30%, sheep Hair fat: 1%, glycerol: 50%, surplus is water.
As the preferred implementation of hair washing bath shampoo of the present invention, described hair washing bath shampoo also includes anticorrosion Agent.Described preservative plays antisepsis in hair washing bath shampoo of the present invention, makes described hair washing bath shampoo deposit Putting more long, the kind of described preservative and consumption can be with selector combination cosmetic hygienic practice (2007) requirements Kind and consumption.
As the preferred implementation of hair washing bath shampoo of the present invention, in described Chinese medicine extract, Folium Artemisiae Argyi is extracted The weight ratio of thing, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract is Chinese mugwort Grass extract: Cortex Dictamni extract: Flos Chrysanthemi Indici extract: Radix Scutellariae extract: Radix et Caulis Opuntiae Dillenii extract=1:2:2:1:2. Above-mentioned damp eliminating, heat clearing away, itching-relieving efficacies composition: wormwood extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, The percentage by weight of Radix et Caulis Opuntiae Dillenii extract is: wormwood extract 12.5%, Cortex Dictamni extract 25%, Flos Chrysanthemi Indici Extract 25%, Radix Scutellariae extract 12.5%, Radix et Caulis Opuntiae Dillenii extract 25%.These damp eliminatings, heat clearing away, antipruritic As long as functional component accounts for bath shampoo total composition more than 1% of having one's hair wash, just may conform to wormwood extract and wash one's hair in hair washing Percentage by weight >=0.125% of bath agent total composition, Cortex Dictamni extract is at hair washing bath shampoo total composition Percentage by weight >=0.25%, Flos Chrysanthemi Indici extract hair washing bath shampoo total composition percentage by weight >= 0.25%;Radix Scutellariae extract is at percentage by weight >=0.125% of hair washing bath shampoo total composition;Radix et Caulis Opuntiae Dillenii extracts Thing is at percentage by weight >=0.25% of hair washing bath shampoo total composition, to guarantee that described Chinese medicine ingredients is washed described Send out the consumption in bath shampoo, it is ensured that its effect.
As the preferred implementation of hair washing bath shampoo of the present invention, described wormwood extract is by anhydrous Obtained by ethanol extraction;Described Cortex Dictamni extract is by obtained by dehydrated alcohol extraction;Described Flos Chrysanthemi Indici Extract is by obtained by dehydrated alcohol extraction;Described Radix Scutellariae extract is to be obtained by dehydrated alcohol extraction 's;Described Radix et Caulis Opuntiae Dillenii extract is by obtained by dehydrated alcohol extraction.
As the preferred implementation of hair washing bath shampoo of the present invention, described Folium Artemisiae Argyi passes through dehydrated alcohol extraction After, wormwood extract is concentrated into and described Folium Artemisiae Argyi identical weight;Described Cortex Dictamni passes through dehydrated alcohol extraction After, Cortex Dictamni extract is concentrated into and described Cortex Dictamni identical weight;Described Flos Chrysanthemi Indici passes through dehydrated alcohol After extraction, Flos Chrysanthemi Indici extract is concentrated into and described Flos Chrysanthemi Indici identical weight;Described Radix Scutellariae is by anhydrous second After alcohol extraction, Radix Scutellariae extract is concentrated into and described Radix Scutellariae identical weight;Described Radix et Caulis Opuntiae Dillenii is by anhydrous second After alcohol extraction, Radix et Caulis Opuntiae Dillenii extract is concentrated into and described Radix et Caulis Opuntiae Dillenii identical weight.
Present invention also offers the preparation method of hair washing bath shampoo described above, said method comprising the steps of:
(1) adding water and sodium isethionate in agitator, heat while stirring, homogenizing is to fully dissolving;
(2), when temperature is down to less than 50 DEG C, it is sequentially added into Chinese medicine extract, cod-liver oil, lanoline, glycerol.
The beneficial effects of the present invention is: the present invention uses wormwood extract, Cortex Dictamni extract, Radix Scutellariae to carry Take thing and live in these damp eliminatings of Radix et Caulis Opuntiae Dillenii extract, heat clearing away, the compounding gentle surface of antipruritic botanical herbs composition Hair washing bath shampoo is made in property agent, and described hair washing bath shampoo is safer, and zest and toxic and side effects are less, is difficult to Cause skin allergy, inflammation, safe and reliable and simple for production, be particularly well-suited to skin sensitivity crowd and Infant.Can help to eliminate baby's skin because antiperspirant or urine leaching cause the anaphylaxis of diaper rash and eczema, with Time additionally aid and alleviate the sufferings symptom that mosquito bite and skin allergy bring.
Detailed description of the invention
For better illustrating the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment pair The present invention is described further.
Embodiment 1
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo includes following weight percent The component of ratio: Chinese medicine extract: 1%, cod-liver oil: 0.1%, sodium isethionate: 10%, lanoline: 0.1%, glycerol: 20%, preservative: appropriate, surplus is water;
Described Chinese medicine extract includes that wormwood extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae carry Take thing and Radix et Caulis Opuntiae Dillenii extract, wormwood extract, Cortex Dictamni extract, Flos Chrysanthemi Indici in described Chinese medicine extract The weight ratio of extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract is wormwood extract: Cortex Dictamni extract: Flos Chrysanthemi Indici extract: Radix Scutellariae extract: Radix et Caulis Opuntiae Dillenii extract=1:2:2:1:2.
The kind of described preservative and consumption are to meet kind and the use that cosmetics health specification (2007) requires Amount.
The preparation method of hair washing bath shampoo of the present invention, said method comprising the steps of:
(1) adding water and sodium isethionate in agitator, heat while stirring, homogenizing is to fully dissolving;
(2) when temperature is down to less than 50 DEG C, be sequentially added into Chinese medicine extract, cod-liver oil, lanoline, glycerol, Preservative.
Embodiment 2
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo includes following weight percent The component of ratio: Chinese medicine extract: 4%, cod-liver oil: 1%, sodium isethionate: 15%, lanoline: 0.2%, Glycerol: 30%, preservative: appropriate, surplus is water;Other qualificationss and preparation process are with embodiment 1.
Embodiment 3
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo includes following weight percent The component of ratio: Chinese medicine extract: 6%, cod-liver oil: 1.5%, sodium isethionate: 20%, lanoline: 0.5%, glycerol: 30%, preservative: appropriate, surplus is water;Other qualificationss and preparation process are with implementing Example 1.
Embodiment 4
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo includes following weight percent The component of ratio: Chinese medicine extract: 8%, cod-liver oil: 2%, sodium isethionate: 25%, lanoline: 0.8%, Glycerol: 40%, preservative: appropriate, surplus is water;Other qualificationss and preparation process are with embodiment 1.
Embodiment 5
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo includes following weight percent The component of ratio: Chinese medicine extract: 10%, cod-liver oil: 3%, sodium isethionate: 30%, lanoline: 1%, glycerol: 50%, preservative: appropriate, surplus is water;Other qualificationss and preparation process are with implementing Example 1.
Embodiment 6
1, eye irritation test:
Requirement according to cosmetics health specification (2007) carries out acute ocular irritation test (DAVIS).Real Proved recipe method: select 3 healthy New Zealand to grow up rabbit, instills this sample of 0.1ml in rabbit one branch hole conjunctival sac In, another branch hole does not process makees own control, makes a rabbit eyes closed 1s time after painting.After being painted into tested material Eyes are not rinsed in 24h.Record tested rabbit cornea, iris or conjunctiva each comfortable 1,24,48,72h anti- Should and the 4th, the recovery situation of 7d, carry out eye infringement grade scale scoring and Eye irritation intensity evaluation.
The eye irritation result of the test of table 1 hair washing of the present invention bath shampoo
Due to horn film, iris integration=0;Conjunctival congestion or chemosis integration < 2, and integration is at < 0 it is down in 7 days, thus termination test, do not observe the recovery situation of 21d, result is as shown in table 1, thorn Sharp strength grading is: embodiment 1 nonirritant;Embodiment 2 is non-stimulated, embodiment 3 nonirritant;Real Execute example 4 non-stimulated, embodiment 5 microstimulation.
2, skin irritation test
Requirement according to cosmetics health specification (2007) carries out irritation test.Test method: choosing With healthy, adult, the white rabbit 4 of skin zero damage, 24h before experiment, every rabbit back spinal column both sides Each one piece of cropping, can not damage epidermis, is respectively 3.0cm × 3.0cm about unhairing scope.By this tested material 0.5ml Being applied on stripped region, side, area is 2.5cm × 2.5cm.Opposite side is coated with distilled water and compares.Every day is coated with skin Once, before being coated with, repair hair every time, remove residual tested material with warm water, be coated with skin 14d continuously.
The skin irritation test result of table 2 hair washing of the present invention bath shampoo
Result is as shown in table 2, according to " cosmetics health specification " skin irritation strength grading, and integration 0-0.5, Embodiment 1,2,3,4,5 broadly falls into without skin irritation.
3, acute toxicity testing
According to GB15193-2003 " foodsafety Toxicological Assessment program and method ", use maximum tolerance meter Amount test method(s), dosage is set to 10000mg/kg BW, selects 20 kunming mices, male and female half and half.Before test Animal fasting 16h, does not limit drinking-water.Use administration by gavage to give the sample solution of animal 500mg/ml concentration, fill Stomach amount is 0.4ml/20g body weight.Observe poisoning manifestations and the death condition of animal after gavage, weigh weekly 1 Secondary, observe 14 days.
The acute toxicity testing result of table 3 hair washing of the present invention bath shampoo
Result is as shown in table 3, according to the acute toxicity grading criteria evaluation of food, embodiment 1,2,3,4, 5 broadly fall into nontoxic level.
4, emollient experiment
Choosing experimenter 30 people to test, men and women half and half, the age from 30-50 year, 38 years old mean age, Testing first 2 months and do not used external preparation for skin medicine, skin is without wound.Experimenter is allowed to use respectively from the beginning Water, embodiment 1,2,3,4,5 sample, be divided into 4 days and test, and the most only surveys a sample.? Every time before test, experimenter cleans both hands with clear water, and towel, at 25 DEG C, the air-conditioned room of humidity 30rh Interior slow-witted upper 2 hour, and the circle of diameter 2cm is drawn random 4 positions of the back of the hand (each 2 of right-hand man) Region.Wash one's hands 3 minutes with 1g sample, be over after washing water on hand gently off with cotton balls and start timing.Use skin In skin Moisture Meter respectively test zone the 5th minute, the 10th minute, the moisture value of skin when the 30th minute, Skin moistening degree is passed judgment on according to moisture value size.(smear hand with the common moisturizer of 1g after washing with clear water to make For matched group).
The emollient experimental result of table 4 hair washing of the present invention bath shampoo
According to table 4 data it can be seen that use the guarantor of moisturizer after the sample of embodiment 1,2,3 and cleaning Wet effect is suitable;Along with the increase of Chinese medicine ingredients, good than with milky lotion of the moistening effect of embodiment 4 and 5.
5, inflammation-resisting itch-stopping test
Histamine phosphate is used to cause Cavia porcellus local pruritus model, the itching-relieving action of test sample.Choose body weight 250-400g healthy guinea pig 70, is divided into 7 groups at random, often group 10, male and female half and half.Blank group (is steamed Distilled water 0.1ml/100g), positive control drug antipruritic liquid medicine group (0.1ml/100g), embodiment 1-5 is large, medium and small Dosage group (0.2ml/100g, 0.1ml/100g, 0.05ml/100g).Test first 1 day and respectively organize instep behind the Cavia porcellus right side Portion's shaving, and at each treated animal shaving outside be coated with corresponding laboratory sample 1 time.Test the same day, abrade with coarse sandpaper At the shaving of instep, to damage epidermis, skin is slight, and oozing of blood is degree, area 1cm2, local repastes laboratory sample 1 Secondary, after last coating 10min, start at wound surface, only to drip 0.01% histamine phosphate solution 0.05ml/.Hereafter, Every 3min by 0.02%, 0.03%, 0.04% ... progressive concentration, only it is 0.05ml/, until occurring every time Cavia porcellus only later licks right metapedes, finally to there is the histamine phosphate total amount that Cavia porcellus is given when later licking right metapedes (ug) it is itch-threshold, records each group of data.
Table 5 inflammation-resisting itch-stopping result of the test
According to table 5 data it can be seen that embodiment 1-5 large, medium and small dosage group (0.2ml/100g, 0.1ml/100g, 0.05ml/100g) and itch stopping and diminish inflammation liquid medicine group (positive control) external all can significantly improve histamine phosphate to globefish The antipruritic threshold value of Mus, shows that embodiment 1-5 has obvious inflammation-resisting itch-stopping effect.
Last institute is it should be noted that, above example is only in order to illustrate technical scheme rather than to this The restriction of invention protection domain, although the present invention being explained in detail with reference to preferred embodiment, this area It is to be appreciated by one skilled in the art that technical scheme can be modified or equivalent, and Spirit and scope without departing from technical solution of the present invention.

Claims (8)

1. a hair washing bath shampoo, it is characterised in that described hair washing bath shampoo includes following percentage by weight Component: Chinese medicine extract: 1-10%, cod-liver oil: 0.1-3%, sodium isethionate: 10-30%, lanoline: 0.1-1%, glycerol: 20-50%, surplus is water;
Described Chinese medicine extract includes that wormwood extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae carry Take thing and Radix et Caulis Opuntiae Dillenii extract.
Hair washing bath shampoo the most according to claim 1, it is characterised in that described hair washing bath shampoo includes Following components in percentage by weight: Chinese medicine extract: 8-10%, cod-liver oil: 2-3%, sodium isethionate: 25-30%, lanoline: 0.8-1%, glycerol: 40-50%, surplus is water.
Hair washing bath shampoo the most according to claim 2, it is characterised in that described hair washing bath shampoo includes Following components in percentage by weight: Chinese medicine extract: 10%, cod-liver oil: 3%, sodium isethionate: 30%, Lanoline: 1%, glycerol: 50%, surplus is water.
Hair washing bath shampoo the most according to claim 1, it is characterised in that described hair washing bath shampoo also wraps Include preservative.
Hair washing bath shampoo the most according to claim 1, it is characterised in that end in described Chinese medicine extract Grass extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae extract and the weight of Radix et Caulis Opuntiae Dillenii extract Ratio is for wormwood extract: Cortex Dictamni extract: Flos Chrysanthemi Indici extract: Radix Scutellariae extract: Radix et Caulis Opuntiae Dillenii extract =1:2:2:1:2.
Hair washing bath shampoo the most according to claim 1, it is characterised in that described wormwood extract is logical Cross obtained by dehydrated alcohol extraction;Described Cortex Dictamni extract is by obtained by dehydrated alcohol extraction;Described Flos Chrysanthemi Indici extract is by obtained by dehydrated alcohol extraction;Described Radix Scutellariae extract is to be carried by dehydrated alcohol Obtained by taking;Described Radix et Caulis Opuntiae Dillenii extract is by obtained by dehydrated alcohol extraction.
Hair washing bath shampoo the most according to claim 6, it is characterised in that described Folium Artemisiae Argyi is by anhydrous second After alcohol extraction, wormwood extract is concentrated into and described Folium Artemisiae Argyi identical weight;Described Cortex Dictamni is by anhydrous second After alcohol extraction, Cortex Dictamni extract is concentrated into and described Cortex Dictamni identical weight;Described Flos Chrysanthemi Indici passes through nothing After water-ethanol extracts, Flos Chrysanthemi Indici extract is concentrated into and described Flos Chrysanthemi Indici identical weight;Described Radix Scutellariae passes through After dehydrated alcohol extraction, Radix Scutellariae extract is concentrated into and described Radix Scutellariae identical weight;Described Radix et Caulis Opuntiae Dillenii passes through After dehydrated alcohol extraction, Radix et Caulis Opuntiae Dillenii extract is concentrated into and described Radix et Caulis Opuntiae Dillenii identical weight.
8. the preparation method of a hair washing bath shampoo as claimed in claim 1, it is characterised in that described side Method comprises the following steps:
(1) adding water and sodium isethionate in agitator, heat while stirring, homogenizing is to fully dissolving;
(2), when temperature is down to less than 50 DEG C, it is sequentially added into Chinese medicine extract, cod-liver oil, lanoline, glycerol.
CN201410376357.XA 2014-07-31 2014-07-31 A kind of hair washing bath shampoo and preparation method thereof Expired - Fee Related CN104116681B (en)

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CN107854415A (en) * 2017-12-29 2018-03-30 四川农业大学 A kind of Chinese gall shampoo and its preparation method and application of pet

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