CN113201421A - Graphene bacteriostatic skin-moistening perfumed soap and preparation method thereof - Google Patents
Graphene bacteriostatic skin-moistening perfumed soap and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/18—Water-insoluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/225—Polymers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Dermatology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Veterinary Medicine (AREA)
- Inorganic Chemistry (AREA)
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Abstract
The invention discloses a graphene bacteriostatic skin-moistening soap and a preparation method thereof, wherein the graphene bacteriostatic skin-moistening soap comprises the following components in parts by weight: 7-10 parts of biomass graphene, 2-4 parts of jasmine essential oil, 3-6 parts of folium artemisiae argyi extract, 1-3 parts of sodium hyaluronate, 15-19 parts of ginseng extract, 14-17 parts of olive oil, 12-16 parts of castor oil, 10-13 parts of glycerol, 4-7 parts of calendula extract, 8-11 parts of sodium stearate, 3-7 parts of EDTA tetrasodium, 0.05-0.1 part of sodium hydroxide, 2-6 parts of titanium dioxide and 19-28 parts of deionized water. The graphene antibacterial skin-moistening perfumed soap disclosed by the invention is strong in decontamination capability and obvious in skin cleaning effect, and is antibacterial and capable of softening and moistening skin.
Description
Technical Field
The invention relates to the technical field of daily necessities, in particular to graphene bacteriostatic skin-moistening perfumed soap and a preparation method thereof.
Background
The soap is an essential washing and nursing article in daily life, is a product prepared by taking sodium aliphatate and other surfactants as main raw materials, adding a quality modifier and an appearance modifier and processing and forming, and can be used for removing soil dirt, skin secretion, excrement, chemical substances or bacteria and the like, and also can be used for caring skin, sterilizing and deodorizing. In China washing products, the perfumed soap still has certain market demands, especially in vast rural areas and remote areas, people are still used to the perfumed soap for face washing and bathing, and in China with a large number of people, the perfumed soap still needs to be developed and improved correspondingly under various conditions. Chinese synthetic detergents have increased at a rate of 8% per year over the last 10 years. Chinese laundry products, particularly various synthetic detergent products, are still considered desirable in the foreseeable future.
The essential oil soap is mainly formed by combining aromatic plant essential oil with soap; the essential oil has short molecular chain, and can easily permeate into skin and enter into body from capillary. The essential oil soap has the functions of preventing infectious diseases, resisting bacteria, viruses and molds, preventing inflammation and spasm, and promoting cell metabolism and cell regeneration.
The prior publications also relate to the related technology of jasmine soap, and the following patent documents are searched for:
chinese patent document CN106281794A discloses a jasmine soap formula. The jasmine perfumed soap is prepared by blending soap base, jasmine essential oil, olive oil, angelica dahurica and edible ethanol, wherein the jasmine essential oil is used for treating conjunctival congestion and swelling pain, has the effects of relieving cough and reducing sputum, has the functions of pungent taste, sweet taste, cooling, clearing heat and toxic materials and promoting diuresis, and is reasonable in formula, good in skin cleaning effect, obvious in sterilization effect and beneficial to skin health.
Chinese patent document CN104306205A discloses a jasmine soap, which comprises the following components: 10-15 parts of bamboo charcoal powder, 18-20 parts of glycerol, 20-25 parts of olive oil, 10-15 parts of sweet almond oil, 7-11 parts of palm oil, 10-15 parts of aloe extract and 15-19 parts of jasmine essential oil. The advantages are that: has good cleaning effect, no irritation to skin and aromatic flavor.
Chinese patent document CN106906083A discloses a natural non-irritating aloe-jasmine essential oil handmade soap and a preparation method thereof, wherein the natural non-irritating aloe-jasmine essential oil handmade soap is prepared from the following components in parts by weight: 2-10 parts of sodium hydroxide, 1-5 parts of aloe juice, 0.5-3 parts of jasmine essential oil, 1-5 parts of vegetable white oil, 2-6 parts of refined cocoa butter, 2-6 parts of avocado oil, 3-6 parts of white beeswax, 10-15 parts of cocoyl glucoside, 2-10 parts of taurine, 8-25 parts of hyaluronic acid, 10-20 parts of grape seed oil, 1-5 parts of vegetable glycerin, 4-10 parts of triethanolamine, 10-15 parts of vitamin E, 1-5 parts of 1, 2-propylene glycol, 3-5 parts of hydroxyethyl urea and 1-5 parts of sodium lactate, and the preparation method comprises the following steps: obtaining a mixture A and weighing; obtaining sodium hydroxide solution; and slowly adding a sodium hydroxide solution into the stirrer to prepare the product. The invention has the advantages of no toxic or side effect, good effect on skin and the like.
Chinese patent document CN107603779A discloses a jasmine essential oil soap which is prepared from the following raw materials in parts by weight: 2-4% of jasmine essential oil, 3-5% of soapberry extract, 3-5% of aloe juice, 2-4% of cactus juice, 4-8% of glycerin, 3-5% of olive oil, 18-20% of sodium hydroxide, 25-30% of sodium fatty acid and the balance of deionized water. The jasmine essential oil soap disclosed by the invention has the unique fragrance of jasmine, and is pleasant to the mind.
At present, a plurality of toilet soaps on the market are added with a plurality of chemical components which have stimulation effect on skin, and the decontamination effect and the skin mildness are difficult to achieve. Therefore, the inventor develops a new toilet soap by creative work.
Disclosure of Invention
In view of the above, the invention aims to provide the graphene antibacterial moisturizing soap and the preparation method thereof, and the graphene antibacterial moisturizing soap has the advantages of strong decontamination capability, obvious skin cleaning effect, antibacterial property and skin softening.
The adopted technical scheme is as follows:
the invention relates to a graphene bacteriostatic skin-moistening perfumed soap which is prepared from the following components in parts by weight:
further, the ginseng extract is prepared by the following method: pulverizing Ginseng radix, and subjecting to supercritical CO2Extracting to obtain Ginseng radix extractive solution, and sequentially coarse filtering and fine filtering to obtain Ginseng radix extract.
The preparation method of the graphene bacteriostatic skin-moistening soap comprises the following steps:
s1, adding deionized water, sodium hyaluronate, sodium aliphatate, EDTA tetrasodium, sodium hydroxide, titanium dioxide and hydroxybenzoate into a reaction kettle, heating to 60-70 ℃, and mixing uniformly under full stirring;
s2, adding the folium artemisiae argyi extract, the ginseng extract and the calendula extract into a reaction kettle, cooling to 40-50 ℃, and fully stirring for 30-40 minutes;
s3, adding jasmine essential oil, olive oil, castor oil and glycerin into a reaction kettle, and mixing uniformly under full stirring;
s4, adding the biomass graphene into the reaction kettle, and uniformly dispersing the biomass graphene under the high-speed stirring of 2500-;
and S5, filling the mixed soap liquid obtained in the step S4 into a soap mould, cooling to 25-30 ℃, and standing for 2-3 days.
Further, the preparation method of the graphene antibacterial skin-moistening soap further comprises the following steps:
and S6, demolding, packaging and warehousing after the inspection is qualified.
In the above-mentioned technical solution,
in the soap, the biomass graphene has multiple functions:
1. cleaning of
In the soap, the biomass graphene has a rich porous structure and strong adsorption force, and can adsorb dirt or makeup residues in skin.
2. Antibacterial
In the soap, the biomass graphene can reduce microorganisms attached to the skin epidermis, has antibacterial performance, can replace antiseptic antibacterial agents with potential safety hazards, and reduces the incidence rate of contact allergic dermatitis.
3. Moisture retention
In the soap, the biomass graphene can activate water molecules, so that the water-locking and moisture-preserving capability of the surface layer is improved. The biomass graphene can continuously generate negative ions, resist oxidation and aging, reduce free radicals, effectively care skin and bring brand new skin care experience.
The jasmine essential oil is extracted from flowers of jasmine plants (Jasminum officinale) by a solvent extraction method, has elegant fragrance, and can relieve depression, refresh mind and promote self-confidence; is suitable for caring dry, oily, irritant and sensitive skin, increasing skin elasticity, caring skin, relieving skin dryness, water deficiency, oil excess and sensitivity, and relieving striae gravidarum and scar.
The folium Artemisiae Argyi extract has broad-spectrum antibacterial property, and can be used as antibacterial agent in the soap.
Sodium hyaluronate belongs to a skin conditioner, is an acidic mucopolysaccharide, and can absorb 1000 times of water of the sodium hyaluronate by weight so as to retain the water of the skin, prevent the water from losing through epidermis and repair a barrier when the skin is damaged, so that the skin does not feel dry after being used and luster is increased.
The ginseng extract can delay skin aging, prevent skin from drying and dehydrating, and increase skin elasticity, thereby playing the roles of protecting skin luster and tenderness, and preventing and reducing skin wrinkles, and the active substance of the ginseng extract also has the function of inhibiting the reduction of melanin, so that the skin is white and smooth.
The olive oil has the effect of softening and moistening skin.
The castor oil is extracted from castor seeds and used as a lubricant to lock the moisture of the skin and keep the skin in a moist and tender state.
The glycerin has water absorption effect, and can adsorb water molecules in air to keep the covered skin stratum corneum moist.
The calendula extract has antibacterial, skin calming, and sensitive skin improving effects.
Sodium stearate has a strong cleaning effect.
The EDTA tetrasodium is a chelating agent and is used for stabilizing a formula system of the graphene bacteriostatic skin-moistening soap. Can also be used for synergistic anticorrosion with biomass graphene.
Sodium hydroxide is a pH regulator and is used to regulate the pH value of the soap.
Titanium dioxide can play a role in sun protection. The titanium dioxide protective wave band is between 290 nm and 400nm, and belongs to full wave band protection.
The invention has the beneficial effects that:
in the graphene antibacterial moisturizing soap, the biomass graphene has cleaning and moisturizing effects and also has antibacterial effects, the artemisia argyi extract also has antibacterial effects, the calendula officinalis extract can resist bacteria and the like, and all components are mutually promoted and mutually supplemented under respective effects, so that the graphene antibacterial moisturizing soap is strong in decontamination capability, obvious in skin cleaning effect, antibacterial and skin softening.
Detailed Description
The present invention is described in detail below with reference to specific examples, but the use and purpose of these exemplary embodiments are merely to exemplify the present invention, and do not set forth any limitation on the actual scope of the present invention in any form, and the scope of the present invention is not limited thereto.
Example 1
The graphene bacteriostatic skin-moistening toilet soap disclosed by the embodiment comprises the following components in parts by weight:
wherein the ginseng extract is prepared by the following method: pulverizing Ginseng radix, and mixingSubjecting Ginseng radix powder to supercritical CO2Extracting to obtain Ginseng radix extractive solution, and sequentially coarse filtering and fine filtering to obtain Ginseng radix extract.
The preparation method of the graphene bacteriostatic skin-moistening soap comprises the following steps:
s1, adding deionized water, sodium hyaluronate, sodium aliphatate, EDTA tetrasodium, sodium hydroxide, titanium dioxide and hydroxybenzoate into a reaction kettle, heating to 60-70 ℃, and mixing uniformly under full stirring;
s2, adding the folium artemisiae argyi extract, the ginseng extract and the calendula extract into a reaction kettle, cooling to 40-50 ℃, and fully stirring for 30-40 minutes;
s3, adding jasmine essential oil, olive oil, castor oil and glycerin into a reaction kettle, and mixing uniformly under full stirring;
s4, adding the biomass graphene into the reaction kettle, and uniformly dispersing the biomass graphene under the high-speed stirring of 2500-;
and S5, filling the mixed soap liquid obtained in the step S4 into a soap mould, cooling to 25-30 ℃, and standing for 2-3 days.
And S6, demolding, packaging and warehousing after the inspection is qualified.
Example 2
Referring to example 1, different from example 1, the graphene bacteriostatic skin-moistening soap of the embodiment is composed of the following components in parts by weight:
the preparation method is as in example 1.
Example 3
Referring to example 1, different from example 1, the graphene bacteriostatic skin-moistening soap of the embodiment is composed of the following components in parts by weight:
comparative example 1
Referring to example 2, the skin moisturizing soap of the present comparative example does not include graphene, and 33 parts of deionized water, unlike example 2.
Test and test:
test 1
The moisturizing effects of the graphene bacteriostatic moisturizing soap of examples 1-3 and the moisturizing soap of comparative example 1 were tested.
50 healthy female testers without skin diseases at the age of 20-40 years are randomly selected, the graphene bacteriostatic skin-moistening toilet soap of the examples 1-3 and the skin-moistening toilet soap of the comparative example 1 are used for smearing on the skin, the moisture content of the right forearm is measured in the environment with the test environment temperature of 25 ℃ and the relative humidity of 60%, and the testee is kept calm. And marking 2 square experimental areas of 4cm multiplied by 4cm on the right forearm as a test area of the graphene bacteriostatic skin-moistening soap, respectively measuring the skin moisture content 1 hour, 2 hours and 3 hours after bathing by using a skin moisture tester, and recording the result.
Specific results are shown in table 1.
Table 1 moisturizing effect test results of skin moisturizing soap
Test 2
The bacteriostatic effects of the graphene bacteriostatic skin-moistening toilet soaps of examples 1-3 and the skin-moistening toilet soap of comparative example 1 were tested.
The specific results are shown in Table 2.
Table 2 bacteriostatic effect test result table of skin-moistening toilet soap
| Total number of colonies, cfu/g | |
| Example 1 | 19 |
| Example 2 | 17 |
| Example 3 | 15 |
| Comparative example 1 | 56 |
The above-listed detailed description is only a specific description of a possible embodiment of the present invention, and they are not intended to limit the scope of the present invention, and equivalent embodiments or modifications made without departing from the technical spirit of the present invention should be included in the scope of the present invention.
Claims (4)
1. The graphene bacteriostatic skin-moistening perfumed soap is characterized by comprising the following components in parts by weight:
2. the graphene bacteriostatic skin-moistening soap according to claim 1, wherein the ginseng extract is prepared by the following method: pulverizing Ginseng radix, and subjecting to supercritical CO2Extracting to obtain Ginseng radix extractive solution, and sequentially coarse filtering and fine filtering to obtain Ginseng radix extract.
3. The preparation method of the graphene bacteriostatic skin-moistening soap according to claim 1 or 2, which is characterized by comprising the following steps of:
s1, adding deionized water, sodium hyaluronate, sodium aliphatate, EDTA tetrasodium, sodium hydroxide, titanium dioxide and hydroxybenzoate into a reaction kettle, heating to 60-70 ℃, and mixing uniformly under full stirring;
s2, adding the folium artemisiae argyi extract, the ginseng extract and the calendula extract into a reaction kettle, cooling to 40-50 ℃, and fully stirring for 30-40 minutes;
s3, adding jasmine essential oil, olive oil, castor oil and glycerin into a reaction kettle, and mixing uniformly under full stirring;
s4, adding the biomass graphene into the reaction kettle, and uniformly dispersing the biomass graphene under the high-speed stirring of 2500-;
and S5, filling the mixed soap liquid obtained in the step S4 into a soap mould, cooling to 25-30 ℃, and standing for 2-3 days.
4. The preparation method of the graphene bacteriostatic skin-moistening soap according to claim 3, characterized by further comprising the following steps:
and S6, demolding, packaging and warehousing after the inspection is qualified.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202110497406.5A CN113201421A (en) | 2021-05-07 | 2021-05-07 | Graphene bacteriostatic skin-moistening perfumed soap and preparation method thereof |
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| CN202110497406.5A CN113201421A (en) | 2021-05-07 | 2021-05-07 | Graphene bacteriostatic skin-moistening perfumed soap and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114455575A (en) * | 2022-01-28 | 2022-05-10 | 中安新材料(深圳)有限公司 | Graphene and preparation method and application thereof |
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|---|---|---|---|---|
| TW201629198A (en) * | 2015-02-12 | 2016-08-16 | yong-li Chen | Soap and production method thereof |
| KR20170009170A (en) * | 2015-07-16 | 2017-01-25 | 신명철 | Functional soap composition containing graphene and its maunufacruring method |
| CN107603779A (en) * | 2017-09-22 | 2018-01-19 | 广西巧恩茶业有限公司 | A kind of jasmine essential oil soap |
| CN111234963A (en) * | 2020-03-12 | 2020-06-05 | 象鼻山香(杭州)生物科技有限公司 | Miao soap and its making method |
| KR102153750B1 (en) * | 2020-04-06 | 2020-09-09 | 주식회사 모아 | Soap including grapheme and manufacturing method of the same |
| CN111904884A (en) * | 2020-08-14 | 2020-11-10 | 广东墨睿科技有限公司 | Graphene shower gel |
-
2021
- 2021-05-07 CN CN202110497406.5A patent/CN113201421A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW201629198A (en) * | 2015-02-12 | 2016-08-16 | yong-li Chen | Soap and production method thereof |
| KR20170009170A (en) * | 2015-07-16 | 2017-01-25 | 신명철 | Functional soap composition containing graphene and its maunufacruring method |
| CN107603779A (en) * | 2017-09-22 | 2018-01-19 | 广西巧恩茶业有限公司 | A kind of jasmine essential oil soap |
| CN111234963A (en) * | 2020-03-12 | 2020-06-05 | 象鼻山香(杭州)生物科技有限公司 | Miao soap and its making method |
| KR102153750B1 (en) * | 2020-04-06 | 2020-09-09 | 주식회사 모아 | Soap including grapheme and manufacturing method of the same |
| CN111904884A (en) * | 2020-08-14 | 2020-11-10 | 广东墨睿科技有限公司 | Graphene shower gel |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114455575A (en) * | 2022-01-28 | 2022-05-10 | 中安新材料(深圳)有限公司 | Graphene and preparation method and application thereof |
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