CN1134786A - Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same - Google Patents
Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same Download PDFInfo
- Publication number
- CN1134786A CN1134786A CN 95107415 CN95107415A CN1134786A CN 1134786 A CN1134786 A CN 1134786A CN 95107415 CN95107415 CN 95107415 CN 95107415 A CN95107415 A CN 95107415A CN 1134786 A CN1134786 A CN 1134786A
- Authority
- CN
- China
- Prior art keywords
- extract powder
- extract
- oil
- agricultural chemicals
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The characteristic of the invented pesticide lies in that it is composed of croton, Java bruces, Chinese honey locust, Chinese prickly ash, trifoliate jewelvine, etc. 16 traditional Chinese medicinal herbs and these medicinal herbs are divided into three groups, i.e. croton etc. five kinds, Chinese honey locust etc. 10 kinds, and trifoliate jewelvine one kind, to be prepared separately; at last, the final product is obtained by mixing and fusing them. When applying said pesticide, it is blended with water in accordance with 1:2000 to 1:350000 to spray the crop. The advantages of said pesticide are small dosage, capable of killing multikinds of insects, no harm to humanbeing and animals, beneficial to protect ecotope, intensive raw material source and convenient for making.
Description
The present invention relates to a kind of multi-purpose, no-polution composite agricultural chemicals for plants and manufacture method thereof, be a kind of be raw material with the Chinese herbal medicine, extract the blend mixture of its leaching that can kill polytype harmful insect oil part and medicinal extract part.
Traditional chemical pesticide is to agricultural produce; prevention and elimination of disease and pests is an otherwise effective technique measure; but the popularization and application of chemical pesticide nearly half a century; serious to comprehensive ecological environmental pollutions such as the water source in the whole world, air, soil; the harmful substance that residues in the agricultural product has been damaged health; polytype harmful insect pesticide resistance strengthens day by day; the effectiveness that is applied to multipurpose control harmful insect reduces; consumption increases; dispenser is very dangerous; cost is more and more high, becomes agricultural production and comprehensive ecological environmental protection problem anxious to be solved.
At present, also utilize individual event poisonous plant aqua and pulvis, the research of control harmful insect damage by disease and insect.But owing to utilize individual event poisonous plant aqua, pure agent and pulvis, it is low that harmful insect is knocked down ability, and lethal time is long, and consumption is big, and the polytype harmful insect effectiveness of integrated control is low, is difficult to popularization.And to the compound compatibility of multiple Chinese herbal medicine, it is carried out multiple process for extracting be composited, the multi-purpose, no-polution composite agricultural chemicals for plants development that is applied to prevent and treat the polytype harmful insect does not but have (retrieval confirms through literature centre of Patent Office of the People's Republic of China).
The objective of the invention is to utilize herbal plant resource; develop a kind of efficient, little residual, consumption is few and safer to people, animal; the multi-purpose, no-polution composite agricultural chemicals for plants and the manufacture method thereof that are of value to plant growing and comprehensive ecological environmental protection; be used for crops, economic crops are killed harmful insect; suppress the crop germ; anti-fabrication virus, increase crop yield and harmful insect had tag, stomach toxicity, stifling and in daily life to the poisoning of harmful insect such as mosquito, fly and muroid.
The present invention is raw material with the Chinese herbal medicine, and herbal plant resource is abundant, mostly is wild, but and artificial cultivation again, regeneration power is stronger, and its resource can be used for a long time continuously.The present invention is according to Chinese herbal medicine, as: the pharmacology of crotons, crow egg seed, China tree seed, castor bean seed, sesame, Chinese honey locust, Thorn-Apple, Chinese prickly ash, Rhododendron molle, wartwort, black false hellebore, balloonflower root, Verbena officinalis, the tuber of stemona, tobacco leaf, trifoliate jewelvine is formulated.
The crotons main component is a croton oil, crotin, crotonoside and alkaloid, therefrom the croton oil of Ti Quing has very strong surface-active and extended capability and burns excitant, form homogeneous film at the insect body surface, insect tags, burn the wax layer of harmful insect body surface, stifling harmful insect makes crotin contained in the extract powder that therefrom extracts and crotonoside, alkaloid kill harmful insect by quick stomach.To the harmful insect action principle be: tag, effect such as stomach toxicity.
Crow egg seed main component is an alkaloid, crow egg seed toxin, and crow egg seed oil, crow egg seed saponin class, therefrom crow egg seed oil of Ti Quing and crow egg-shaped thing saponin have very strong surface-active and extended capability and excitant, have the pest body table to form homogeneous film, and insect tags.The harmful insect bodies table wax layer of dissolving, repellent is fumigated harmful insect, the alkaloid that the extract powder that therefrom extracts is contained, after the combination of crow egg seed toxin, crow egg seed saponin class fast stomach kill harmful insect, to the harmful insect mechanism of action for tag, stomach toxicity, fumigate, effect such as repellent.
China tree seed main component is a margosine, and insect is had stronger stomach poison function, and effect is slow and lasting, and China tree have tangible antibacterial resistant effect simultaneously.
The castor bean seed main component is a ricin (WA), ricin, recinine, castor oil, therefrom the castor oil of Ti Quing has very strong surface-active and extended capability and stability, can produce polymerization with above-mentioned croton oil, the crow egg oil of other compositions, avoids the layering precipitating, form film at the insect body surface, the insect that tags, the harmful insect bodies table wax layer of dissolving makes that ricin (WA) contained in the extract powder that therefrom extracts, ricin, recinine can be tagged fast, the stomach toxicity harmful insect.To the insect insect mechanism of action for tag, effect such as stomach toxicity.
The sesame main component is sesamin, sesame wet goods, and therefrom sesame oil of Ti Quing and the sesamin that contains thereof have very strong surface-active and extended capability, forms homogeneous film at the insect body surface, the insect that tags, is dissolved with insect body surface wax layer.Make the sesamin that is contained in the extract powder that therefrom extracts can increase the toxic effect effect that other plant extracts composition, to the mechanism of action of insect for tag, effect such as food calling.
The Chinese honey locust main component is a gledinin, therefrom contained gledinin has very strong superficiality and extended capability and stability in the extract powder of Ti Quing, the described composition polymerization that can extract with other above-mentioned raw materials, form froth bed at the insect body surface, the cell that causes poisonous saponin component rapid osmotic harmful insect, make it dead fast, to the mechanism of action of insect for effect such as tagging.
The Thorn-Apple main component is an alkaloid, and contained alkaloid in the extract powder of Ti Quing therefrom can play the effect of the anesthesia of tagging fast to insect, with the mechanism of action of insect for effect such as tagging.
The Chinese prickly ash main component is a geraniol etc., and therefrom the ox alcohol that is contained in the extract powder of Ti Quing can cooperate the medicine of above-mentioned other compositions to form mixing, the activity of harmful insect is suppressed, anaesthetizes its nerve, makes it dead fast.To the mechanism of action of insect for effect such as tagging.
Rhododendron molle main component Wei andromedotoxin etc., therefrom the lignin that is contained in the extract powder of Ti Quing can cooperate the medicine of above-mentioned other compositions to form mixing, the activity of harmful insect is suppressed, anaesthetizes its nerve, make it dead fast, to the mechanism of action of insect for effect such as tagging.
The wartwort main component is heliosin, wartwort saponin etc.Therefrom heliosin, the wartwort saponin that is contained in the extract powder of Ti Quing can cooperate above-mentioned other drug composition to form and mix, and harmful insect played the effect of killing fast.And the toxic effect time is long, can reach about 20 days, to the mechanism of insect for effect such as tagging.
Black false hellebore main component veratridine alkali etc., the veratridine alkali that is contained in the extract powder of Ti Quing therefrom has the very strong ability of knocking down, shoot dead to insect, makes it dead immediately, is action of contace poison to the mechanism of action of insect.
The balloonflower root main component be platycodoside etc., therefrom the platycodoside that is contained in the extract powder of Ti Quing etc., have very strong surface-active and extended capability, the insect body surface is formed the film insect that tags, rapid osmotic harmful insect bodily form cell, making it dead fast, is action of contace poison to the mechanism of action of insect.
The Verbena officinalis main component is a venbenalin etc., therefrom venbenalin that is contained in the extract powder of Ti Quing etc.Can the germ of various crops, economic crops be suppressed.
Tuber of stemona main component is a Stemonidine etc., and Stemonidine that is contained in the extract powder of Ti Quing etc. therefrom can be to the germ of various crops, economic crops, suppressed, and harmful insect had the very strong ability of shooting dead of knocking down, and lasting medicine, to the mechanism of action of insect for effect such as tagging.
The tobacco leaf main component is a nicotine, the nicotine that is contained in the extract powder of Ti Quing therefrom, and acute poisoning death fast similar to cyanide is action of contace poison to the insect mechanism of action.
The trifoliate jewelvine main component is a rotenone etc., the pure crystallization pulvis of the rotenone of Ti Quing therefrom, with 350,000/ dosage can kill most of insect, harmful insect had knock down the ability of shooting dead immediately, and lasting medicine, fundamentally reduce dosage, to the mechanism of action of insect for tag, stomach poison function.
Multi-purpose, no-polution composite agricultural chemicals for plants of the present invention is formed (weight %) by crotons, crow egg seed, China tree seed, castor bean seed, sesame etc.:
(1) crotons 1-3%
Crow egg seed 5-10%
China tree seed 2-5%
Castor bean seed 1-3%
Sesame 1-2%
(2) Chinese honey locust 25-28%
Thorn-Apple 1-3%
Chinese prickly ash 6.5-15%
Rhododendron molle 1-2%
Wartwort 20-25%
Black false hellebore 25-40%
Balloonflower root 0.5-1%
Verbena officinalis 0.5-1%
Tuber of stemona 5-10%
Tobacco 5-21%
(3) trifoliate jewelvine 0.5-1%
(4) above-mentioned each material enters dynamically with static high shearing mixing emulsor, static mixer, super-high-pressure homogenization pump and carries out mixing, emulsification.
The manufacture method of multi-purpose, no-polution composite agricultural chemicals for plants of the present invention is: at first (one) being formed: crotons, crow egg seed, the China tree seed, castor bean seed, after the oil that is contained in the sesame soaks press for extracting juice by oil press successively item by item, obtain to soak again behind the product oil dregs of a decoction after the press for extracting juice, extract by Chinese medicine lixiviate still item by item successively, temperature is between 50 ℃-60 ℃, adopt 65% ethanol lixiviate, under 78.3 ℃ of temperature, the ethanol volatilization is reclaimed, obtain liquid extract, after the oven dry, promptly obtain dry extract, then pass through freezing crusher successively item by item, airslide disintegrating mill, be ground into 400-800 order micro mist, treat and the following substances mixing after fully mixing through three-dimensional asymmetric mixer again.Secondly (two), with the Chinese honey locust in (two) composition, Thorn-Apple, Chinese prickly ash, Rhododendron molle, wartwort, black false hellebore, balloonflower root, Verbena officinalis, the tuber of stemona, after tobacco leaf is pulverized by freezing crusher successively item by item, successively item by item by Chinese medicine lixiviate still, extract temperature between 50 ℃-60 ℃, adopt the lixiviate of 65% ethanol, under 78.5 ℃ of temperature, the ethanol volatilization is reclaimed, after obtaining the liquid extract oven dry, then pass through freezing crusher successively item by item, airslide disintegrating mill, be ground into 400-800 order micro mist, after fully mixing by three-dimensional asymmetric mixer again, treat and above-mentioned and following substances mixing.
After trifoliate jewelvine in then (three) being formed is pulverized through freezing crusher, by Chinese medicine lixiviate still, extract temperature between 30 ℃-40 ℃, adopt the acetone lixiviate, under 56.5 ℃ of temperature, acetone volatilization is reclaimed, obtain the oven dry of rotenone liquid extract after, then by freezing crusher and steam flow cracker, be ground into 400-800 order micro mist, treat and the above-mentioned substance mixing.
At last (four) at last the various extractions of (), (two), (three) above-mentioned composition are carried lixiviate oil, with through being ground into 400-800 purpose medicinal extract micro mist, through the centrifugal rotational speed high shear process of dynamic high speed shear Mixingemulsificationmachine in per minute 1400-3000 commentaries on classics, above-mentioned substance is carried out the emulsification mixing, it is integrated, then carry out mixing by static mixer again, pass through super-high-pressure homogenization pump emulsifying mixing at last again, make its fully emulsified back not stratified in one to two year, thereby guarantee efficacy stability.
The present invention is through preliminary assay, and its active ingredient has also increased a variety of active ingredients except that having the active ingredient that Chinese herbal medicine itself contains, and the main active ingredient of the present invention has:
Alkaloid (7 kinds): veratridine alkali, Stemonidine, nicotine, croton seed alkaloid, crow egg seed alkaloid, recinine, Thorn-Apple alkaloid.
Alcohols (a kind): Mang geraniol
Ketone (a kind): rotenone
Glucoside (6 kinds): crotonoside, gledinin, heliosin, wartwort saponin, horsewhip glucoside
Plain class (6 kinds): crotin, crow egg seed toxin, margosine, ricin (WA), sesamin, toxin
Other classes: (2 kinds) crow egg-shaped thing saponin thing, ricin
The present invention compared with prior art has the following advantages:
1, the present invention compares with pulvis with individual event poisonous plant aqua, pure agent, harmful insect is comprehensively knocked down shoot dead, anaesthetize, fumigate, stomach toxicity, tag, abilities such as food calling, repellent strengthen significantly, lethal time shortens, integrated control effect is more satisfactory.
2, the scope of application of the present invention is wide, has the broad spectrum activity effect, through test to wheat-crop peat insect as the red honeybee spider of wheat, wheat mythimna separata, wheat aphid, wheat stinkbug, wheat stem maggot, wheat ephydrid, wheat thrips, wheat wasp, wheat head noctuid; To the rice class pest as paddy rice paddy stem borer, striped rice borer, pink rice borer, rice leaf roller, brown planthopper, white-backed planthopper, rice leafhopper, rice thrips and oryza chinensis, rice leaf beetles, the rice bar fly of diving.To the cotton class pest as cotton bollworm, cotten aphid, pink bollworm, cotton tetranychid, fleahopper, thrips, cotton leafhopper, Asiatic corn borer, cotton leafroller; To the greengrocery insect as imported cabbageworm, diamond-back moth, Oeobia undalis, prodenia litura, tomato moth, three-spotted plusia, onion thrips; To the fruit tree kind insect as: peach post fruit moth, the full melon mite of apple.Tetranychus viennensis, maroon spider, chestnut knurl honeybee, white little food worry, citrus root-knot nematode, tea caterpillar, dish be earwig, long white a red-spotted lizard, tea aphid, the black poison moth of tea, tea olethreutid, cluster caterpillar to the greatest extent; To the daily life class pest as: fly, mosquito, brown muroid all have good control efficiency.The minimum rate 76% of insect lethality after 24 hours, be up to 91.5%, 48 hour after, can reach 91.3-100%.
3, through test, insecticidal effect surpasses chemical pesticide, for example with 1 milliliter of the multi-purpose, no-polution plyability plant pesticide of the present invention that contains trifoliate jewelvine 1%, rare 350,000 milliliters in water converted still has the very strong ability of shooting dead of knocking down to above-mentioned insect, the harmful insect lethality is 91.3% after 24 hours, and the contrast medicament with 1000 times of-2000 times of soups of phoxim the insect lethality to be arranged after 24 hours be 90%, total drug effect that medicament adds the rare amount of converting of water is counted difference and is differed and reach 15 times.
4, the present invention remove have stomach toxicity, tag, stifling, anesthesia suffocates, outside the mechanism of food calling desinsection, also have very strong systemic action, can make noxious material enter that the back keeps one period effective time in the plant corpus, makes the efficacy of a drug lasting.
5, desinsection is held concurrently antibacterial, the sterilization resistant effect is obvious, can increase chlorophyll and plant endotrophic, impel plant growth, especially to melon, really, dish has the special role that increases endotrophic and active principle, wheat leaf blade behind the spray medicine is generous, leaf is green dense, the corn leaf greening of spray behind the medicine is significantly better than spray plot not, to stripe rust of wheat, rice leaf rust, fruit tree putrefaction disease, pepper falling leaf disease, leaf curl etc. all have reasonable control efficiency.
6, do not add any chemical agent, safe in utilization harmless to people, animal, basic unharmful substance is residual, helps the comprehensive ecological environmental protection.
7, with the Chinese herbal medicine be raw material, aboundresources, manufacture method is simple, and cost is low, easily promotes.
Flow chart below by embodiment and preparation agricultural chemicals further is illustrated the present invention:
Embodiment 1: get (one), (two), the multi-purpose, no-polution composite agricultural chemicals for plants of (three) each part after (four) mixing, during use, in 1: 2000-1: 350000 ratio is converted water sprinkling crop and is got final product.
Embodiment 2: get (one), crotons 1%, crow egg seed 5%, China tree seed 2%, castor bean seed 1%, sesame 1% is successively item by item after oil press soaks expressed oil, the dregs of a decoction are extracted temperature between 50 ℃-60 ℃ by the traditional Chinese medicine extraction still successively item by item, adopt its liquid extract of 65% alcohol extract, pass through freezing crusher after the oven dry, air-flow machine cracker, it is ground into 400-800 order micro mist, in then (two) being formed: Chinese honey locust 25%, Thorn-Apple 1%, Chinese prickly ash 6.5%, Rhododendron molle 1%, wartwort 20%, black false hellebore 25%, balloonflower root 0.5%, Verbena officinalis 0.5%, the tuber of stemona 5%, after tobacco 5% is pulverized by freezing crusher successively item by item, again successively item by item by the traditional Chinese medicine extraction still, extract temperature between 50 ℃-60 ℃, after adopting 65% alcohol extract to be the liquid extract oven dry, through freezing crusher, airslide disintegrating mill is ground into 400-800 order micro mist, mix with following substances with above-mentioned substance, after trifoliate jewelvine during (three) formed is pulverized by freezing crusher, again by the traditional Chinese medicine extraction still, the extraction temperature adopts acetone extraction between 30 ℃-40 ℃ be the rotenone liquid extract, after the oven dry, through freezing crusher, airslide disintegrating mill is ground into 400-800 order micro mist and above-mentioned substance changes-3000 centrifugal rotational speed high shear process of changeing through (four) dynamic high shearing mixing emulsor at per minute 1400, above-mentioned substance is carried out the emulsification mixing, just it is integrated, then carry out mixing by static mixer, last again through the super-high-pressure homogenization pump emulsifying become the drug effect stable components and in one to two year not stratified multi-purpose, no-polution composite agricultural chemicals for plants.
Embodiment 3: the leaching oil that the raw material during (), (two), (three) are respectively formed forms through extraction, extract powder promptly is divided into seven types according to the purposes difference prescription.
(1) is used for killing of rice class pest
Crow egg seed oil is 7% with its extract powder
China tree seed oil is 1.0% with its extract powder
Castor bean seed oil is 10% with its extract powder
Sesame oil and extract powder are 5%
The Chinese honey locust extract powder is 25%
The Chinese prickly ash extract powder is 5%
The wartwort extract powder is 20%
The black false hellebore extract powder is 19%
The rotenone extract powder is 1%
(2) killing wheat-crop peat insect
Crow egg seed oil is 15% with its extract powder
Croton oil and its extract powder are 1.5%
Castor oil and its extract powder are 1.0%
Sesame oil and its extract powder are 5%
Tuber of stemona extract powder is 15%
The tobacco extract powder is 5%
The Rhododendron molle extract powder is 8%
The black false hellebore extract powder is 14.5%
The Chinese honey locust extract powder is 23%
The rotenone extract powder is 1%
(3) be used for killing of cotton class pest
Crow egg seed and extract powder thereof are 15%
Croton oil and extract powder thereof are 3%
Castor oil and extract powder thereof are 10%
Sesame oil and extract powder thereof are 5%
The Chinese honey locust extract powder is 25%
The black false hellebore extract powder is 10%
The Chinese prickly ash extract powder is 8.5%
The wartwort extract powder is 25%
The rotenone extract powder is 1%
(4) killing vegetables, fruit tree, tea, oil crop class pest
Crow egg seed oil is 15% with its extract powder
Castor bean seed oil is 10% with its extract powder
Sesame oil and its extract powder are 5%
The Chinese honey locust extract powder is 20%
The Chinese prickly ash extract powder is 6.5%
The black false hellebore extract powder is 23%
The tobacco extract powder is 1%
(5) killing various crops class pests
Croton oil and extract powder 1% thereof
Crow egg seed oil and extract powder 5% thereof
China tree seed extract powder 2%
Castor bean seed oil and extract powder 1% thereof
Sesame oil and extract powder 1% thereof
Chinese honey locust extract powder 25%
Thorn-Apple extract powder 1%
Chinese prickly ash extract powder 6.5%
Rhododendron molle extract powder 1%
Wartwort extract powder 20%
Black false hellebore extract powder 25%
Balloonflower root extract powder 0.5%
Verbena concrete powder 0.5%
Tuber of stemona extract powder 5%
Tobacco extract powder 5%
Rotenone extract powder 1%
(6) to the poisoning of various muroids
Sesame oil and extract powder 42% thereof
Croton oil and extract powder 1% thereof
Chinese prickly ash extract powder 45%
Castor oil and extract powder 15% thereof
Rotenone extract powder 1%
(7) killing mosquito, fly pest type in the daily life each
Black false hellebore extract powder 45%
Crow egg seed oil and extract powder 20% thereof
Chinese prickly ash extract powder 25%
Nicotine extract powder 9%
Rotenone extract powder 1%
Accompanying drawing given below be to multi-purpose, no-polution composite agricultural chemicals for plants from the Chinese herbal medicine raw material, and their each group categories to the preparation flow figure of manufacture method until last generation finished product:
Claims (6)
1, a kind of multi-purpose, no-polution composite agricultural chemicals for plants, it is characterized in that it is by following plant: the agricultural chemicals that crotons, crow egg seed, China tree seed, castor bean seed, sesame, Chinese honey locust, Thorn-Apple, Chinese prickly ash, Rhododendron molle, wartwort, black false hellebore, balloonflower root, Verbena officinalis, the tuber of stemona, tobacco leaf, trifoliate jewelvine are made.
2, agricultural chemicals according to claim 1 is characterized in that, they are respectively above-mentioned agricultural chemicals than (weight %) by three assembly:
First group:
Crow egg seed: 5-10%
China tree seed: 2-5%
Castor bean seed: 1-3%
Sesame: 1-2%
Crotons: 1-3%,
Second group:
Chinese honey locust: 25-28%
Thorn-Apple: 1-3%
Chinese prickly ash: 6.5-15%
Rhododendron molle: 1-2%
Wartwort: 20-25%
Black false hellebore: 25-40%
Balloonflower root: 0.5-1%
Verbena officinalis: 0.5-1%
The tuber of stemona: 5-21%
Tobacco leaf: 0.5-10%,
The 3rd group:
Fish Teng: 0.5-1%.
3, a kind of preparation method of multi-purpose, no-polution composite agricultural chemicals for plants, it is characterized in that: (1) is with crotons, crow egg seed, the China tree seed, castor bean seed, sesame soaks press for extracting juice through oil press one by one, and respectively to get product oil standby, get again slag charge separately one by one through Chinese medicine lixiviate still between 50 ℃-60 ℃ of the temperature time with 65% ethanol lixiviate, heat to 78.3 ℃ afterwards and under this temperature, ethanol is volatilized, promptly get above-mentioned plant liquid extract separately, oven dry afterwards promptly gets dry extract, successively above-mentioned plant dry extract separately is ground into 400-800 order micro mist through freezing crusher and airslide disintegrating mill one by one subsequently, after the asymmetric mixer of three-dimensional fully mixes, takes out all micro mists of above-mentioned plant standby then;
(2) with Chinese honey locust, Thorn-Apple, Chinese prickly ash, Rhododendron molle, wartwort, black false hellebore, balloonflower root, Verbena officinalis, the tuber of stemona, tobacco leaf one by one after freezing crusher is pulverized, successively one by one through Chinese medicine lixiviate still between 50 ℃-60 ℃ of the temperature time with 65% ethanol lixiviate, heat afterwards to 78.3 ℃, and under this temperature, ethanol is volatilized, promptly get above-mentioned plant liquid extract separately, dry afterwards dry extract, be ground into 400-800 order micro mist through freezing crusher, airslide disintegrating mill one by one successively then, at last all micro mists put into three-dimensional asymmetric mixer and fully mixed the back and take out standby;
(3) with trifoliate jewelvine after freezing crusher is pulverized, again through Chinese medicine lixiviate still between 30 ℃-40 ℃ of the temperature time with the acetone lixiviate, heat afterwards to 56.5 ℃, and under this temperature, acetone is volatilized, promptly get rotenone medicinal extract, oven dry afterwards promptly get dry extract, and is then that dry extract taking-up after freezing crusher and airslide disintegrating mill are ground into 400-800 order micro mist is standby;
(4) product oil, the medicinal extract micro mist that are obtained among above-mentioned (1), (2), (3) preparation method are put into dynamic high speed shear-mixed mulser and carried out the emulsification mixing with the speed that per minute 1400 changes-3000 commentaries on classics, afterwards incorporated finished product is sent into static mixer again and carry out mixing, send into high pressure homogeneous pump at last and carry out the emulsifying mixing, can obtain composite agricultural chemicals for plants subsequently.
4, the preparation method of multi-purpose, no-polution composite agricultural chemicals for plants according to claim 3, the powder granularity that it is characterized in that above-mentioned its dry extract of composite agricultural chemicals for plants is the 400-800 order.
5, the preparation method of multi-purpose, no-polution composite agricultural chemicals for plants according to claim 3 is characterized in that above-mentioned composite agricultural chemicals for plants, and the water ratio of converting when it uses is 1: 2000 to 1: 35000.
6,, it is characterized in that the proportioning of above-mentioned agricultural chemicals and finished product thereof can also be according to the preparation method of claim 1,3 described multi-purpose, no-polution composite agricultural chemicals for plants and multi-purpose, no-polution composite agricultural chemicals for plants:
(1)
Crow egg seed oil is 7% with its extract powder
China tree seed oil is 1.0% with its extract powder
Castor bean seed oil is 10% with its extract powder
Sesame oil and extract powder are 5%
The Chinese honey locust extract powder is 25%
The Chinese prickly ash extract powder is 3%
The wartwort extract powder is 20%
The black false hellebore extract powder is 19%
The rotenone extract powder is 1%
(2)
Crow egg seed oil is 15% with its extract powder
Croton oil and its extract powder are 1.5%
Castor oil and its extract powder are 1.0%
Sesame oil and its extract powder are 5%
Tuber of stemona extract powder is 15%
The tobacco extract powder is 5%
The Rhododendron molle extract powder is 8%
The black false hellebore extract powder is 14.5%
The Chinese honey locust extract powder is 23%
The rotenone extract powder is 1%
(3)
Crow egg seed and extract powder thereof are 15%
Croton oil and extract powder thereof are 3%
Castor oil and extract powder thereof are 10%
Sesame oil and extract powder thereof are 5%
The Chinese honey locust extract powder is 25%
The black false hellebore extract powder is 10%
The Chinese prickly ash extract powder is 8.5%
The wartwort extract powder is 25%
The rotenone extract powder is 1%
(4)
Crow egg seed oil is 15% with its extract powder
Castor bean seed oil is 10% with its extract powder
Sesame oil and its extract powder are 5%
The Chinese honey locust extract powder is 20%
The Chinese prickly ash extract powder is 6.5%
The black false hellebore extract powder is 23%
The tobacco extract powder is 1%
(5)
Croton oil and extract powder 1% thereof
Crow egg seed oil and extract powder 5% thereof
China tree seed extract powder 2%
Castor bean seed oil and extract powder 1% thereof
Sesame oil and extract powder 1% thereof
Chinese honey locust extract powder 25%
Thorn-Apple extract powder 1%
Chinese prickly ash extract powder 6.5%
Rhododendron molle extract powder 1%
Wartwort extract powder 20%
Black false hellebore extract powder 25%
Balloonflower root extract powder 0.5%
Verbena concrete powder 0.5%
Tuber of stemona extract powder 5%
Tobacco extract powder 5%
Rotenone extract powder 1%
(6)
Sesame oil and extract powder 42% thereof
Croton oil and extract powder 1% thereof
Chinese prickly ash extract powder 45%
Castor oil and extract powder 15% thereof
Rotenone extract powder 1%
(7)
Black false hellebore extract powder 45%
Crow egg seed oil and extract powder 20% thereof
Chinese prickly ash extract powder 25%
Nicotine extract powder 9%
Rotenone extract powder 1%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95107415 CN1134786A (en) | 1995-07-04 | 1995-07-04 | Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95107415 CN1134786A (en) | 1995-07-04 | 1995-07-04 | Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1134786A true CN1134786A (en) | 1996-11-06 |
Family
ID=5076276
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 95107415 Pending CN1134786A (en) | 1995-07-04 | 1995-07-04 | Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1134786A (en) |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101300986B (en) * | 2008-07-07 | 2010-06-02 | 石天文 | Biological insecticide |
| CN101209059B (en) * | 2006-12-26 | 2011-06-22 | 河南农业大学 | Novel biological preparation for killing root-knot nematode and application method thereof |
| CN101361494B (en) * | 2008-09-28 | 2011-10-26 | 宁波市北仑区白峰山防大可桃子研究所 | Green non-poisonous pesticides and preparation method thereof |
| CN102626114A (en) * | 2012-03-20 | 2012-08-08 | 杨俊奇 | Disease-curing insecticidal plant nutrient solution with pure traditional Chinese medicinal formula, and making method thereof |
| CN103229786A (en) * | 2012-04-18 | 2013-08-07 | 湖北省文东农业发展有限公司 | Complex organic plant pesticide and preparation method thereof |
| CN103918730A (en) * | 2013-01-16 | 2014-07-16 | 潘少波 | Preparation method of Mandrake biopesticide and application thereof |
| CN104770407A (en) * | 2014-01-13 | 2015-07-15 | 马图基 | Pollution-free organic pesticide and preparation method thereof |
| CN104782685A (en) * | 2015-03-24 | 2015-07-22 | 阜南县永兴工艺品有限公司 | Medicine for treating salix purpurea yellows |
| CN104798826A (en) * | 2015-04-06 | 2015-07-29 | 韩城市秦龙花椒科技有限责任公司 | Method for processing adhesive-killing type non-polluted pesticide preparation through compounding of Chinese herbal medicine plants |
| CN105123800A (en) * | 2015-08-21 | 2015-12-09 | 张立华 | Botanical agricultural bactericidal and insecticidal wettable powder and preparation method and application thereof |
| CN105284942A (en) * | 2015-10-26 | 2016-02-03 | 广西农垦国有立新农场 | Novel botanical insecticide, preparation method and application of novel botanical insecticide |
| CN105519613A (en) * | 2015-12-16 | 2016-04-27 | 罗永城 | Novel botanical insecticide, preparation method and application thereof |
| CN105941493A (en) * | 2016-06-02 | 2016-09-21 | 江苏丰年果品种植园有限公司 | Bactericide for preventing and treating blueberry stiff fruit disease and preparation method thereof |
| CN106259513A (en) * | 2016-08-10 | 2017-01-04 | 吴远宁 | A kind of insecticide and preparation method thereof |
| CN106508992A (en) * | 2016-10-21 | 2017-03-22 | 赖丰光 | Plant pesticide for controlling leaf beetles |
| CN106538641A (en) * | 2016-11-14 | 2017-03-29 | 李媛源 | A kind of plant protecting liquid, preparation method and application |
| CN110959637A (en) * | 2019-12-17 | 2020-04-07 | 罗友祥 | Composition containing lycoris radiata, pesticide, preparation method and application thereof |
-
1995
- 1995-07-04 CN CN 95107415 patent/CN1134786A/en active Pending
Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101209059B (en) * | 2006-12-26 | 2011-06-22 | 河南农业大学 | Novel biological preparation for killing root-knot nematode and application method thereof |
| CN101300986B (en) * | 2008-07-07 | 2010-06-02 | 石天文 | Biological insecticide |
| CN101361494B (en) * | 2008-09-28 | 2011-10-26 | 宁波市北仑区白峰山防大可桃子研究所 | Green non-poisonous pesticides and preparation method thereof |
| CN102626114A (en) * | 2012-03-20 | 2012-08-08 | 杨俊奇 | Disease-curing insecticidal plant nutrient solution with pure traditional Chinese medicinal formula, and making method thereof |
| CN103229786A (en) * | 2012-04-18 | 2013-08-07 | 湖北省文东农业发展有限公司 | Complex organic plant pesticide and preparation method thereof |
| CN103229786B (en) * | 2012-04-18 | 2014-07-09 | 湖北省文东农业发展有限公司 | Complex organic plant pesticide and preparation method thereof |
| CN103918730A (en) * | 2013-01-16 | 2014-07-16 | 潘少波 | Preparation method of Mandrake biopesticide and application thereof |
| CN104770407A (en) * | 2014-01-13 | 2015-07-15 | 马图基 | Pollution-free organic pesticide and preparation method thereof |
| CN104782685A (en) * | 2015-03-24 | 2015-07-22 | 阜南县永兴工艺品有限公司 | Medicine for treating salix purpurea yellows |
| CN104798826A (en) * | 2015-04-06 | 2015-07-29 | 韩城市秦龙花椒科技有限责任公司 | Method for processing adhesive-killing type non-polluted pesticide preparation through compounding of Chinese herbal medicine plants |
| CN105123800A (en) * | 2015-08-21 | 2015-12-09 | 张立华 | Botanical agricultural bactericidal and insecticidal wettable powder and preparation method and application thereof |
| CN105284942A (en) * | 2015-10-26 | 2016-02-03 | 广西农垦国有立新农场 | Novel botanical insecticide, preparation method and application of novel botanical insecticide |
| CN105519613A (en) * | 2015-12-16 | 2016-04-27 | 罗永城 | Novel botanical insecticide, preparation method and application thereof |
| CN105941493A (en) * | 2016-06-02 | 2016-09-21 | 江苏丰年果品种植园有限公司 | Bactericide for preventing and treating blueberry stiff fruit disease and preparation method thereof |
| CN106259513A (en) * | 2016-08-10 | 2017-01-04 | 吴远宁 | A kind of insecticide and preparation method thereof |
| CN106508992A (en) * | 2016-10-21 | 2017-03-22 | 赖丰光 | Plant pesticide for controlling leaf beetles |
| CN106538641A (en) * | 2016-11-14 | 2017-03-29 | 李媛源 | A kind of plant protecting liquid, preparation method and application |
| CN110959637A (en) * | 2019-12-17 | 2020-04-07 | 罗友祥 | Composition containing lycoris radiata, pesticide, preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1134786A (en) | Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same | |
| KR101623744B1 (en) | Feed composition for Protaetia brevitarsis seulensis | |
| CN1271934C (en) | Traditional Chinese medicine compound for horticultural disinsection and its preparation method | |
| CN104472527A (en) | Dinotefuran insecticide having insect inducing effect | |
| CN101331886A (en) | Traditional Chinese medicine insecticidal liquid for killing crops pest and preparation method thereof | |
| CN1233243C (en) | Broad-spectrum pesticide using plant composition as raw material and preparation process thereof | |
| CN1209027C (en) | Pesticide without toxin and public nuisance and its production process | |
| CN104996483A (en) | Camphor mosquito-repellent incense coil for animal houses | |
| CN1303885C (en) | Synergistic botanical orange terpene pesticide | |
| CN1537432A (en) | Environmental protection type insecticide | |
| CN1282522A (en) | Wettable insecticide powder for plant | |
| CN103355322A (en) | Compound biological insecticide and application thereof | |
| CN107347921B (en) | Fly repelling product, preparation method thereof and application thereof in fly repelling | |
| CN101396024B (en) | Dendrolimus punctatus cytoplasmic polyhedrosis virus(dpcpv) bacillus thuringiensis wettable powder and preparation method thereof | |
| CN109169736A (en) | It is a kind of using peppermint and balsam pear as the pest repellant of substrate and preparation method, application | |
| CN107360904A (en) | A kind of prevention and controls of Pomacea canaliculata | |
| CN102988462B (en) | Chinese medicinal preparation for controlling parasites of aquatic animal as well as preparation method and application thereof | |
| CN111066827A (en) | Agent for attracting and killing termites and preparation method thereof | |
| CN1158927C (en) | Prepn. of incense used as herbal mosquito repelling agent | |
| CN1644057A (en) | Plant toxin for killing rats | |
| CN1292998A (en) | 'Junchongjing' as natural agricultural chemical and its preparing process | |
| CN109258724A (en) | A kind of biological pesticide pest repellant | |
| CN110024803A (en) | A kind of Pesticidal combination and its preparation of spirotetramat | |
| CN109221233A (en) | A kind of aqua type kills horse botfly agent and preparation method thereof | |
| CN107467090A (en) | A kind of ivory scented rice insect attractant and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |