CN105519613A - Novel botanical insecticide, preparation method and application thereof - Google Patents
Novel botanical insecticide, preparation method and application thereof Download PDFInfo
- Publication number
- CN105519613A CN105519613A CN201510937590.5A CN201510937590A CN105519613A CN 105519613 A CN105519613 A CN 105519613A CN 201510937590 A CN201510937590 A CN 201510937590A CN 105519613 A CN105519613 A CN 105519613A
- Authority
- CN
- China
- Prior art keywords
- parts
- novel botanical
- botanical pesticide
- tree
- ash
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- Biotechnology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a novel botanical insecticide and its preparation method and application and belongs to the field of insecticide preparation technology. The novel botanical insecticide comprises the following raw materials: ailanthus altissima, castor-oil plant, Chinese prickly ash, sabah veratrum nigrum, tubatoxin, garlic, tarragon, melia azadarach, onion, leaves of cinnamomum burm anii, ash bark, radix sophorae flavescentis, euphorbia soongarica, sophora alopecuroide, pyrethrum, dioscorea zingiberensis, lettuce, mint, wasabi, patrinia herb and water. The novel botanical insecticide is prepared by steps of medical liquid extraction, concentration, drying, crushing, sieving, sterilization and the like. The novel botanical insecticide has advantages of nontoxic component and no residue, is pollution-free, green and environmentally friendly, and will not cause environmental pollution. The novel botanical insecticide can effectively control plant insects such as inchworm, red spider, lopholeucaspis japonica, leaf miner and the like. One-time killing rate reaches 96.42% and above, and the plant insects have no drug resistance.
Description
Technical field
The invention belongs to insecticide preparing technical field, be specifically related to a kind of Novel botanical pesticide, preparation method and application thereof.
Background technology
Current control pest all use chemical insecticide mostly, along with the raising of living standards of the people, require high, not only will eat, and will eat health agricultural product quality.The Pesticide Residue that high malicious chemical pesticide causes more and more becomes the focus of social concerns.High-toxic pesticide is the core and the key that affect agricultural product quality and safety, not only affects agricultural product quality, directly endangers the healthy of the people, also affects increasing peasant income.Because the toxicity of high-toxic pesticide is large, the event of person poultry poisoning was caused to happen occasionally in the past.Very big on the impact of women and children, the children that teratogenesis is disabled are a lot.In addition, along with the protective awareness of countries in the world to environment for human survival and natural, ecological strengthens day by day, high malicious high residue insecticide will be restricted further.The quality safety of unreasonable use to agricultural product of agricultural chemicals constitutes a threat to, therefore, reduce Pesticide use particularly high-toxic pesticide use, to raising agricultural product quality and the market competitiveness, promote China's agricultural sustainable development, ensure the life security of broad masses of the people and very great meaning of building a harmonious society.
Because chemical pesticide is easy to the pesticide resistance causing insect; dosage is made in order to control efficiency well constantly increases; a lot of natural enemy and beneficial organism are murdered; and pollute us and to depend on for existence living environment; the more and more attention of Environmental protection; will be further strict to the Detecting Pesticide in agricultural product, therefore, greatly develop the direction that non-toxic and non-pollution high-efficiency plant source pesticide is Agrochemicals from now on.
Summary of the invention
The invention provides a kind of Novel botanical pesticide, preparation method and application thereof, chemical pesticide control insect is used to cause the problem such as pest resistance to insecticide and contaminated environment to solve, Novel botanical pesticide composition of the present invention is nontoxic, noresidue, nuisanceless, environmental protection, can not bring environmental pollution; Novel botanical pesticide of the present invention effectively can prevent and treat the plant insect such as looper, two spotted spider mite, long white a red-spotted lizard, leaf miner, and one time killing rate all reaches more than 96.42%, and does not have drug resistance.
For solving above technical problem, the present invention by the following technical solutions:
A kind of Novel botanical pesticide, in units of weight portion, comprise following raw material: tree-of-heaven 30-50 part, castor-oil plant 30-50 part, Chinese prickly ash 30-50 part, sabadilla 30-40 part, malicious trifoliate jewelvine 30-40 part, garlic 30-40 part, tarragon 20-30 part, China tree 20-30 part, onion 20-30 part, burmann cinnamon leaf 20-25 part, bark of ash 20-25 part, kuh-seng 20-25 part, Roots of Euphorbia soongarica 20-25 part, Sophora alopecuroide 15-20 part, Dalmatian chrysanthemum 15-20 part, yellow ginger 15-20 part, lettuce 15-20 part, peppermint 10-15 part, horseradish 10-15 part, field pennycress 10-15 part, water 1500-6000 part.
Preferably, described Novel botanical pesticide, in units of weight portion, comprise following raw material: tree-of-heaven 35-45 part, castor-oil plant 35-45 part, Chinese prickly ash 35-45 part, sabadilla 32-38 part, poison trifoliate jewelvine 32-38 part, garlic 32-38 part, tarragon 22-28 part, China tree 22-28 part, onion 22-28 part, burmann cinnamon leaf 22-24 part, bark of ash 22-24 part, kuh-seng 22-24 part, Roots of Euphorbia soongarica 22-24 part, Sophora alopecuroide 16-18 part, Dalmatian chrysanthemum 16-18 part, yellow ginger 16-18 part, lettuce 16-18 part, peppermint 12-14 part, horseradish 12-14 part, field pennycress 12-14 part, water 2500-4000 part.
Preferably, described Novel botanical pesticide, in units of weight portion, comprise following raw material: tree-of-heaven 40 parts, castor-oil plant 40 parts, 40 parts, Chinese prickly ash, sabadilla 35 parts, malicious trifoliate jewelvine 35 parts, 35 parts, garlic, tarragon 25 parts, China tree 25 parts, onion 25 parts, burmann cinnamon leaf 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 22 parts, Sophora alopecuroide 17 parts, Dalmatian chrysanthemum 17 parts, yellow ginger 17 parts, 17 parts, lettuce, peppermint 12 parts, horseradish 12 parts, field pennycress 12 parts, 3700 parts, water.
The present invention also provides a kind of preparation method of Novel botanical pesticide, it is characterized in that, comprises the following steps:
S1: by tree-of-heaven, castor-oil plant, Chinese prickly ash, sabadilla, malicious trifoliate jewelvine, garlic, tarragon, China tree, onion, burmann cinnamon leaf, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Sophora alopecuroide, Dalmatian chrysanthemum, yellow ginger, lettuce, peppermint, horseradish, field pennycress co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140-180W, concentration of alcohol is 55%-75%, Extracting temperature is 55-65 DEG C, and extraction time is 30-50min;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained Novel botanical pesticide.
Preferably, step S2 herb liquid filters, and is concentrated into water content≤25%.
Preferably, in step S2, mixture B is dry at 90-100 DEG C.
More preferably, described mixture B is dried to water content≤6% at 90-100 DEG C.
Preferably, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
Preferably, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
The application of described Novel botanical pesticide in one or more plant insects of control looper, two spotted spider mite, long white a red-spotted lizard, leaf miner.
Pharmacology of the present invention is as follows:
The effects such as tree-of-heaven has heat-clearing and damp-drying drug, inducing astrigency stops band, antidiarrheal, hemostasis removing toxic substances desinsection.
Castor-oil plant can be swollen and be drawn out pus by applying a plaster to the affected part, antipruritic, and control sore swollen toxin, fresh goods mashes external application, controls eczema itch, (drugs) to be decocted and used as a lotion, and maggot of can going out, infanticide Jue.
Chinese prickly ash can alleviate chest abdomen crymodynia, prevents dysentery, kills and presses down stomach abdomen entozoa, controls cardiopathy and coronary sclerosis, the function such as have sterilization, anticorrosion, seasoning, nutrition, dispel cold.
Sabadilla is Melanthiaceae perennial plant, and extract has insecticidal properties, may be used for that jumping is disturbed, fall army worm, louse, thrips, fleahopper and cockroach etc.
Poison trifoliate jewelvine dicotyledon medicine leguminous plant, extract bitter, very toxic, there is killing parasites to relieve itshing, by effects such as arthritis with fixed pain caused by dampness.
In garlic, sulfur-containing compound has strong antibacterial and anti-inflammation functions, all has suppression and killing action to multiple coccus, bacillus, fungi and virus etc., is the one that in the natural plants found at present, antibacterial action is the strongest.
Tarragon has strong antibacterial and anti-inflammation functions, all has suppression and killing action to multiple coccus, bacillus, fungi and virus etc., is the one that in the natural plants found at present, antibacterial action is extremely strong.
China tree famous paradise tree, it contains toxin, can as insecticide, pest repellant and growth inhibitor.
Onion is warm in nature, acrid-sweet flavor, eliminate the phlegm, diuresis, stomach-invigorating intestine-moisturizing, the function such as removing toxic substances desinsection, staphylococcus aureus, diphtheria bacillus can be killed.
Burmann cinnamon leaf has antibacterial, anti-inflammatory, desinsection and antitumor activity composition, and extract has obvious antibacterial action to watermelon Fusarium oxysporum, mango anthrax-bacilus, banana Fusarium oxysporum and musae etc.
The bark of ash has antibacterial insecticidal action, has obvious inhibitory action, be usually used in controlling bacillary dysentery clinically to staphylococcus aureus, bacillus subtilis, Escherichia coli, brewer's yeast, bacterium wine yeast etc., enteritis, leukorrhea, chronic bronchitis, red eye, swell pain etc.
Kuh-seng belongs to herbaceos perennial; Be taken as the substitute of monkshood and radix aconiti agrestis at the Northwest's kuh-seng and use, simultaneously the traditional medicine of the ethnic group such as Ye Shi Kazak, the Hui ethnic group, is mainly used in pain relieving, dehumidifying, cold-dispelling.
Roots of Euphorbia soongarica is herbaceos perennial, main product in Gansu, the ground such as Xinjiang and Russia, the substitute in new thick area as the root of Beijing euphorbia uses, and has effect of removing water retention by purgation, dispersing swelling and dissipating binds.
The total alkaloid of sophora alopecuroide extracted in Sophora alopecuroide has anti-inflammatory, anticancer, antiallergic action, anti-arrhythmia cordis, antiulcer, increasing leukocyte, relievings asthma, antipyretic, desinsection, calmness, analgesia, the effect such as antiviral; The external application of Sophora alopecuroide powder has suppression or killing action to staphylococcus, Escherichia coli, streptococcus, fungi, bacterium protein of Gardnerella vaginalis and trichomonad; The killing ability of Sophora alopecuroide plant is between anabasine (Anadasine) and lupinine (Lupinine), and sparteine is Biocidal agriculture the effective elements of the medicine.
Dalmatian chrysanthemum containing 4 kinds of insecticidal constituents, pyrethrin (pyrethrin) I, II and cinerin (cinerin) I, II, Dalmatian chrysanthemum to various insects as mosquito, fly, bedbug and cockroach etc. have toxic action.
Turmeric extractive shows certain repellent to multiple grain storage pest, desert locusts and mythimna separata etc., fumigates, tags, stomach toxicity, growth inhibition or oviposition deterrence isoreactivity; Meanwhile, to some agriculture germs, there is very strong bactericidal action.
Lettuce profit the five internal organs, qualcomm meridian, diuresis, improving eyesight sharps teeth, promoting lactation, hard muscles and bones, has the effect of antibacterial desinsection.
Peppermint has the effects such as desinsection, antibacterial, sterilization, anti-inflammatory, has stronger inhibitory action to shigella dysenteriae, typhoid bacillus and Escherichia coli.
Pungent thing in horseradish has strong antibacterial killing ability, particularly has obvious effect to cholera bacteria, typhoid fever bacterium, colon bacillus, diphtheria bacterium, staphylococcus aureus etc.
Field pennycress, with root-like stock and root, all herbal medicine, belongs to antipyretic and antidotal type medicine in Chinese medicine, cool in nature, taste is pungent, bitter.Return liver, stomach, large intestine channel, have effect that is clearing heat and detoxicating, removing blood stasis and expelling pus.Modern pharmacy is thought, it is containing volatile oil, Patrinia scaniosaefolia saponin and β-sterol glucose formula, have anti-inflammatory, antibacterial, calm, protect the liver the effect with cardiac stimulant diuresis.Field pennycress has suppression or killing action to staphylococcus aureus, shigella dysenteriae, typhoid bacillus, Pseudomonas aeruginosa.
The present invention has following beneficial effect:
(1) Novel botanical pesticide composition of the present invention is nontoxic, and noresidue is nuisanceless, environmental protection, can not bring environmental pollution;
(2) Novel botanical pesticide of the present invention effectively can prevent and treat the plant insect such as looper, two spotted spider mite, long white a red-spotted lizard, leaf miner, and one time killing rate all reaches more than 96.42%, and does not have resistance to medical, can use by 4-6;
(3) Novel botanical pesticide production method of the present invention is simple, and cost is low, easy to use, and effect is good, is conducive to applying.
Embodiment
Be specifically described below in conjunction with specific embodiment.
Embodiment 1
A kind of Novel botanical pesticide, in units of weight portion, comprise following raw material: tree-of-heaven 30 parts, castor-oil plant 30 parts, 30 parts, Chinese prickly ash, sabadilla 30 parts, malicious trifoliate jewelvine 30 parts, 30 parts, garlic, tarragon 20 parts, China tree 20 parts, onion 20 parts, burmann cinnamon leaf 20 parts, the bark of ash 20 parts, kuh-seng 20 parts, Roots of Euphorbia soongarica 20 parts, Sophora alopecuroide 15 parts, Dalmatian chrysanthemum 15 parts, yellow ginger 15 parts, 15 parts, lettuce, peppermint 10 parts, horseradish 10 parts, field pennycress 10 parts, 1500 parts, water.
The preparation method of described Novel botanical pesticide, comprises the following steps:
S1: by tree-of-heaven, castor-oil plant, Chinese prickly ash, sabadilla, malicious trifoliate jewelvine, garlic, tarragon, China tree, onion, burmann cinnamon leaf, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Sophora alopecuroide, Dalmatian chrysanthemum, yellow ginger, lettuce, peppermint, horseradish, field pennycress co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140W, concentration of alcohol is 55%, and Extracting temperature is 55 DEG C, and extraction time is 50min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 25%, obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, and pressure is sterilizing 5min under 210KPa, obtained Novel botanical pesticide.
Embodiment 2
A kind of Novel botanical pesticide, in units of weight portion, comprise following raw material: tree-of-heaven 50 parts, castor-oil plant 50 parts, 50 parts, Chinese prickly ash, sabadilla 40 parts, malicious trifoliate jewelvine 40 parts, 40 parts, garlic, tarragon 30 parts, China tree 30 parts, onion 30 parts, burmann cinnamon leaf 25 parts, the bark of ash 25 parts, kuh-seng 25 parts, Roots of Euphorbia soongarica 25 parts, Sophora alopecuroide 20 parts, Dalmatian chrysanthemum 20 parts, yellow ginger 20 parts, 20 parts, lettuce, peppermint 15 parts, horseradish 15 parts, field pennycress 15 parts, 6000 parts, water.
The preparation method of described Novel botanical pesticide, comprises the following steps:
S1: by tree-of-heaven, castor-oil plant, Chinese prickly ash, sabadilla, malicious trifoliate jewelvine, garlic, tarragon, China tree, onion, burmann cinnamon leaf, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Sophora alopecuroide, Dalmatian chrysanthemum, yellow ginger, lettuce, peppermint, horseradish, field pennycress co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 180W, concentration of alcohol is 75%, and Extracting temperature is 65 DEG C, and extraction time is 30min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 18%, obtain mixture B, it is 4% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, and pressure is sterilizing 3min under 230KPa, obtained Novel botanical pesticide.
Embodiment 3
A kind of Novel botanical pesticide, in units of weight portion, comprise following raw material: tree-of-heaven 40 parts, castor-oil plant 40 parts, 40 parts, Chinese prickly ash, sabadilla 35 parts, malicious trifoliate jewelvine 35 parts, 35 parts, garlic, tarragon 25 parts, China tree 25 parts, onion 25 parts, burmann cinnamon leaf 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 22 parts, Sophora alopecuroide 17 parts, Dalmatian chrysanthemum 17 parts, yellow ginger 17 parts, 17 parts, lettuce, peppermint 12 parts, horseradish 12 parts, field pennycress 12 parts, 3700 parts, water.
The preparation method of described Novel botanical pesticide, comprises the following steps:
S1: by tree-of-heaven, castor-oil plant, Chinese prickly ash, sabadilla, malicious trifoliate jewelvine, garlic, tarragon, China tree, onion, burmann cinnamon leaf, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Sophora alopecuroide, Dalmatian chrysanthemum, yellow ginger, lettuce, peppermint, horseradish, field pennycress co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 65%, and Extracting temperature is 60 DEG C, and extraction time is 40min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 135 DEG C in temperature, and pressure is sterilizing 4min under 220KPa, obtained Novel botanical pesticide.
Embodiment 4
A kind of Novel botanical pesticide, in units of weight portion, comprise following raw material: tree-of-heaven 35 parts, castor-oil plant 35 parts, 35 parts, Chinese prickly ash, sabadilla 32 parts, malicious trifoliate jewelvine 32 parts, 32 parts, garlic, tarragon 22 parts, China tree 22 parts, onion 22 parts, burmann cinnamon leaf 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 22 parts, Sophora alopecuroide 16 parts, Dalmatian chrysanthemum 16 parts, yellow ginger 16 parts, 16 parts, lettuce, peppermint 12 parts, horseradish 12 parts, field pennycress 12 parts, 2500 parts, water.
The preparation method of described Novel botanical pesticide, comprises the following steps:
S1: by tree-of-heaven, castor-oil plant, Chinese prickly ash, sabadilla, malicious trifoliate jewelvine, garlic, tarragon, China tree, onion, burmann cinnamon leaf, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Sophora alopecuroide, Dalmatian chrysanthemum, yellow ginger, lettuce, peppermint, horseradish, field pennycress co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 150W, concentration of alcohol is 60%, and Extracting temperature is 55 DEG C, and extraction time is 45min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 22%, obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, and pressure is sterilizing 5min under 210KPa, obtained Novel botanical pesticide.
Embodiment 5
A kind of Novel botanical pesticide, in units of weight portion, comprise following raw material: tree-of-heaven 45 parts, castor-oil plant 45 parts, 45 parts, Chinese prickly ash, sabadilla 38 parts, malicious trifoliate jewelvine 38 parts, 38 parts, garlic, tarragon 28 parts, China tree 28 parts, onion 28 parts, burmann cinnamon leaf 24 parts, the bark of ash 24 parts, kuh-seng 24 parts, Roots of Euphorbia soongarica 24 parts, Sophora alopecuroide 18 parts, Dalmatian chrysanthemum 18 parts, yellow ginger 18 parts, 18 parts, lettuce, peppermint 14 parts, horseradish 14 parts, field pennycress 14 parts, 4000 parts, water.
The preparation method of described Novel botanical pesticide, comprises the following steps:
S1: by tree-of-heaven, castor-oil plant, Chinese prickly ash, sabadilla, malicious trifoliate jewelvine, garlic, tarragon, China tree, onion, burmann cinnamon leaf, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Sophora alopecuroide, Dalmatian chrysanthemum, yellow ginger, lettuce, peppermint, horseradish, field pennycress co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 170W, concentration of alcohol is 70%, and Extracting temperature is 65 DEG C, and extraction time is 35min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, obtain mixture B, it is 5% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, and pressure is sterilizing 3min under 230KPa, obtained Novel botanical pesticide.
Embodiment 6
A kind of Novel botanical pesticide, in units of weight portion, comprise following raw material: tree-of-heaven 48 parts, castor-oil plant 48 parts, 48 parts, Chinese prickly ash, sabadilla 35 parts, malicious trifoliate jewelvine 35 parts, 35 parts, garlic, tarragon 25 parts, China tree 25 parts, onion 25 parts, burmann cinnamon leaf 23 parts, the bark of ash 23 parts, kuh-seng 23 parts, Roots of Euphorbia soongarica 23 parts, Sophora alopecuroide 18 parts, Dalmatian chrysanthemum 18 parts, yellow ginger 18 parts, 18 parts, lettuce, peppermint 14 parts, horseradish 14 parts, field pennycress 14 parts, 5000 parts, water.
The preparation method of described Novel botanical pesticide, comprises the following steps:
S1: by tree-of-heaven, castor-oil plant, Chinese prickly ash, sabadilla, malicious trifoliate jewelvine, garlic, tarragon, China tree, onion, burmann cinnamon leaf, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Sophora alopecuroide, Dalmatian chrysanthemum, yellow ginger, lettuce, peppermint, horseradish, field pennycress co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 70%, and Extracting temperature is 60 DEG C, and extraction time is 45min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 23%, obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 136 DEG C in temperature, and pressure is sterilizing 3min under 230KPa, obtained Novel botanical pesticide.
For verifying the effect of Novel botanical pesticide of the present invention, by following experimental verification.
Adopt the Novel botanical pesticide of embodiment 1-6, the ratio of joining 40g water in 1g Novel botanical pesticide uses, and once prevents and treats the test of the plant insect such as looper, two spotted spider mite, long white a red-spotted lizard, leaf miner, the results are shown in following table.
From upper table, the Novel botanical pesticide of embodiment of the present invention 1-6 is to a killing rate of the plant insect such as looper, two spotted spider mite, long white a red-spotted lizard, leaf miner all more than 96.42%, and result of use is good.Due to Novel botanical pesticide nonhazardous of the present invention, do not pollute, do not remain, it is efficient to add control efficiency, therefore, can widely popularize application.
Above content can not assert that the present invention specifically implements to be confined to these explanations; for general technical staff of the technical field of the invention; do not departing under concept thereof of the present invention; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted to claims.
Claims (10)
1. a Novel botanical pesticide, it is characterized in that, in units of weight portion, comprise following raw material: tree-of-heaven 30-50 part, castor-oil plant 30-50 part, Chinese prickly ash 30-50 part, sabadilla 30-40 part, poison trifoliate jewelvine 30-40 part, garlic 30-40 part, tarragon 20-30 part, China tree 20-30 part, onion 20-30 part, burmann cinnamon leaf 20-25 part, bark of ash 20-25 part, kuh-seng 20-25 part, Roots of Euphorbia soongarica 20-25 part, Sophora alopecuroide 15-20 part, Dalmatian chrysanthemum 15-20 part, yellow ginger 15-20 part, lettuce 15-20 part, peppermint 10-15 part, horseradish 10-15 part, field pennycress 10-15 part, water 1500-6000 part.
2. Novel botanical pesticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: tree-of-heaven 35-45 part, castor-oil plant 35-45 part, Chinese prickly ash 35-45 part, sabadilla 32-38 part, poison trifoliate jewelvine 32-38 part, garlic 32-38 part, tarragon 22-28 part, China tree 22-28 part, onion 22-28 part, burmann cinnamon leaf 22-24 part, bark of ash 22-24 part, kuh-seng 22-24 part, Roots of Euphorbia soongarica 22-24 part, Sophora alopecuroide 16-18 part, Dalmatian chrysanthemum 16-18 part, yellow ginger 16-18 part, lettuce 16-18 part, peppermint 12-14 part, horseradish 12-14 part, field pennycress 12-14 part, water 2500-4000 part.
3. Novel botanical pesticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: tree-of-heaven 40 parts, castor-oil plant 40 parts, 40 parts, Chinese prickly ash, sabadilla 35 parts, malicious trifoliate jewelvine 35 parts, 35 parts, garlic, tarragon 25 parts, China tree 25 parts, onion 25 parts, burmann cinnamon leaf 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 22 parts, Sophora alopecuroide 17 parts, Dalmatian chrysanthemum 17 parts, yellow ginger 17 parts, 17 parts, lettuce, peppermint 12 parts, horseradish 12 parts, field pennycress 12 parts, 3700 parts, water.
4. a preparation method for the Novel botanical pesticide according to any one of claim 1-3, is characterized in that, comprises the following steps:
S1: by tree-of-heaven, castor-oil plant, Chinese prickly ash, sabadilla, malicious trifoliate jewelvine, garlic, tarragon, China tree, onion, burmann cinnamon leaf, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Sophora alopecuroide, Dalmatian chrysanthemum, yellow ginger, lettuce, peppermint, horseradish, field pennycress co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140-180W, concentration of alcohol is 55%-75%, and Extracting temperature is 55-65 DEG C, and extraction time is 30-50min;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained Novel botanical pesticide.
5. the preparation method of Novel botanical pesticide according to claim 4, is characterized in that, step S2 herb liquid filters, and is concentrated into water content≤25%.
6. the preparation method of Novel botanical pesticide according to claim 4, is characterized in that, in step S2, mixture B is dry at 90-100 DEG C.
7. the preparation method of Novel botanical pesticide according to claim 6, is characterized in that, described mixture B is dried to water content≤6% at 90-100 DEG C.
8. the preparation method of Novel botanical pesticide according to claim 4, is characterized in that, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
9. the preparation method of Novel botanical pesticide according to claim 4, is characterized in that, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
10. the application of the Novel botanical pesticide according to any one of claim 1-3 in one or more plant insects of control looper, two spotted spider mite, long white a red-spotted lizard, leaf miner.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510937590.5A CN105519613A (en) | 2015-12-16 | 2015-12-16 | Novel botanical insecticide, preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510937590.5A CN105519613A (en) | 2015-12-16 | 2015-12-16 | Novel botanical insecticide, preparation method and application thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105519613A true CN105519613A (en) | 2016-04-27 |
Family
ID=55762529
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510937590.5A Pending CN105519613A (en) | 2015-12-16 | 2015-12-16 | Novel botanical insecticide, preparation method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105519613A (en) |
Cited By (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106135323A (en) * | 2016-06-29 | 2016-11-23 | 固镇县华丰蔬菜专业合作社 | A kind of insecticide preventing and treating Fructus Benincasae liriomyza bryoniae insect pest |
| CN106242743A (en) * | 2016-08-01 | 2016-12-21 | 韦波 | A kind of plant source fruit tree insecticide |
| CN106242739A (en) * | 2016-08-01 | 2016-12-21 | 韦波 | A kind of Novel botanical pesticide |
| CN106234448A (en) * | 2016-08-01 | 2016-12-21 | 韦波 | A kind of novel plant source fruit tree insecticide |
| CN106259556A (en) * | 2016-08-15 | 2017-01-04 | 卞佳林 | A kind of preparation method of loquat insecticides |
| CN106259557A (en) * | 2016-08-15 | 2017-01-04 | 卞佳林 | A kind of preparation method of flowering plum microencapsulation insecticide |
| CN106342911A (en) * | 2016-08-01 | 2017-01-25 | 韦波 | Botanical insecticide |
| CN106561744A (en) * | 2016-09-22 | 2017-04-19 | 广西汇智生产力促进中心有限公司 | Pesticide for cucurbita moschata (duch. ex lam.) duch. ex poiret |
| CN107155764A (en) * | 2017-05-10 | 2017-09-15 | 王立存 | A kind of mandarin orange planting method |
| CN107333811A (en) * | 2017-08-21 | 2017-11-10 | 贞丰县顶罈椒业有限公司 | A kind of Chinese pricklyash insecticide and preparation method thereof |
| CN107593777A (en) * | 2017-08-31 | 2018-01-19 | 钟山佳园生态农业有限公司 | A kind of method for preventing and treating sugar orange leaf miner |
| CN107691522A (en) * | 2016-08-08 | 2018-02-16 | 庞锦霞 | A kind of Lindley Butterflybush Herb vegetable insecticide and preparation method thereof |
| CN107865079A (en) * | 2017-10-27 | 2018-04-03 | 蚌埠市禹会区马城胡本号家庭农场 | A kind of method for extending rice storage phase |
| CN107873755A (en) * | 2017-12-11 | 2018-04-06 | 林厚海 | Vegetable source pesticide, bactericidal microemulsion and preparation method thereof and application method |
| CN107996632A (en) * | 2017-12-12 | 2018-05-08 | 张* | A kind of a variety of insect pest insecticides of agricultural trees and preparation method thereof |
| CN108703162A (en) * | 2018-08-09 | 2018-10-26 | 徐州万盛现代农业发展有限公司 | A kind of grape insecticide and preparation method thereof |
| CN109362809A (en) * | 2018-11-28 | 2019-02-22 | 冯占亭 | The insecticide of one planting fruit-trees disease prevention |
| CN109892350A (en) * | 2019-03-04 | 2019-06-18 | 宁波市奉化区水蜜桃研究所 | A kind of composition pesticide of plant source |
| CN111528239A (en) * | 2020-05-26 | 2020-08-14 | 中国热带农业科学院热带生物技术研究所 | Chemical for preventing and treating banana mosaic and heart rot and banana streak and preparation method thereof |
| CN113475537A (en) * | 2021-04-30 | 2021-10-08 | 张永福 | Traditional Chinese medicine insecticidal sterilizing agent and preparation method thereof |
| CN118000201A (en) * | 2024-04-10 | 2024-05-10 | 北京市农林科学院 | Plant source green pesticide for preventing and controlling crop aphids and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1111478A (en) * | 1994-11-01 | 1995-11-15 | 吴日章 | Insectiside composed of Chinese herbal medicines and preparing method thereof |
| CN1134786A (en) * | 1995-07-04 | 1996-11-06 | 殷振鹏 | Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same |
| CN104522088A (en) * | 2014-12-31 | 2015-04-22 | 吴中区金庭小美华家庭农场 | Botanical insecticide |
| CN104663743A (en) * | 2015-03-26 | 2015-06-03 | 徐伟明 | Organic spraying agent for leaf vegetables for killing homopteran insects |
| CN102775238B (en) * | 2012-08-22 | 2015-06-24 | 乌鲁木齐木易联华生物科技有限公司 | Organic plant pesticide fertilizer with pesticidal and bactericidal effects and production technique thereof |
| CN105010437A (en) * | 2015-06-29 | 2015-11-04 | 广西大学 | Lettuce aphid botanical pesticide |
-
2015
- 2015-12-16 CN CN201510937590.5A patent/CN105519613A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1111478A (en) * | 1994-11-01 | 1995-11-15 | 吴日章 | Insectiside composed of Chinese herbal medicines and preparing method thereof |
| CN1134786A (en) * | 1995-07-04 | 1996-11-06 | 殷振鹏 | Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same |
| CN102775238B (en) * | 2012-08-22 | 2015-06-24 | 乌鲁木齐木易联华生物科技有限公司 | Organic plant pesticide fertilizer with pesticidal and bactericidal effects and production technique thereof |
| CN104522088A (en) * | 2014-12-31 | 2015-04-22 | 吴中区金庭小美华家庭农场 | Botanical insecticide |
| CN104663743A (en) * | 2015-03-26 | 2015-06-03 | 徐伟明 | Organic spraying agent for leaf vegetables for killing homopteran insects |
| CN105010437A (en) * | 2015-06-29 | 2015-11-04 | 广西大学 | Lettuce aphid botanical pesticide |
Non-Patent Citations (5)
| Title |
|---|
| 伍有声等 编: "《实用新农药指南》", 31 August 1991 * |
| 刘强等 主编: "《中药新产品开发》", 31 March 2013 * |
| 杨洪强 编著: "《有机园艺》", 31 July 2005 * |
| 谭仁祥: "《植物成分功能》", 31 October 2003 * |
| 邱立新: "《林业药剂药械使用技术》", 31 January 2011 * |
Cited By (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106135323A (en) * | 2016-06-29 | 2016-11-23 | 固镇县华丰蔬菜专业合作社 | A kind of insecticide preventing and treating Fructus Benincasae liriomyza bryoniae insect pest |
| CN106242743A (en) * | 2016-08-01 | 2016-12-21 | 韦波 | A kind of plant source fruit tree insecticide |
| CN106242739A (en) * | 2016-08-01 | 2016-12-21 | 韦波 | A kind of Novel botanical pesticide |
| CN106234448A (en) * | 2016-08-01 | 2016-12-21 | 韦波 | A kind of novel plant source fruit tree insecticide |
| CN106342911A (en) * | 2016-08-01 | 2017-01-25 | 韦波 | Botanical insecticide |
| CN107691522A (en) * | 2016-08-08 | 2018-02-16 | 庞锦霞 | A kind of Lindley Butterflybush Herb vegetable insecticide and preparation method thereof |
| CN106259556A (en) * | 2016-08-15 | 2017-01-04 | 卞佳林 | A kind of preparation method of loquat insecticides |
| CN106259557A (en) * | 2016-08-15 | 2017-01-04 | 卞佳林 | A kind of preparation method of flowering plum microencapsulation insecticide |
| CN106561744A (en) * | 2016-09-22 | 2017-04-19 | 广西汇智生产力促进中心有限公司 | Pesticide for cucurbita moschata (duch. ex lam.) duch. ex poiret |
| CN107155764A (en) * | 2017-05-10 | 2017-09-15 | 王立存 | A kind of mandarin orange planting method |
| CN107333811A (en) * | 2017-08-21 | 2017-11-10 | 贞丰县顶罈椒业有限公司 | A kind of Chinese pricklyash insecticide and preparation method thereof |
| CN107593777A (en) * | 2017-08-31 | 2018-01-19 | 钟山佳园生态农业有限公司 | A kind of method for preventing and treating sugar orange leaf miner |
| CN107865079A (en) * | 2017-10-27 | 2018-04-03 | 蚌埠市禹会区马城胡本号家庭农场 | A kind of method for extending rice storage phase |
| CN107873755A (en) * | 2017-12-11 | 2018-04-06 | 林厚海 | Vegetable source pesticide, bactericidal microemulsion and preparation method thereof and application method |
| CN107996632A (en) * | 2017-12-12 | 2018-05-08 | 张* | A kind of a variety of insect pest insecticides of agricultural trees and preparation method thereof |
| CN108703162A (en) * | 2018-08-09 | 2018-10-26 | 徐州万盛现代农业发展有限公司 | A kind of grape insecticide and preparation method thereof |
| CN109362809A (en) * | 2018-11-28 | 2019-02-22 | 冯占亭 | The insecticide of one planting fruit-trees disease prevention |
| CN109892350A (en) * | 2019-03-04 | 2019-06-18 | 宁波市奉化区水蜜桃研究所 | A kind of composition pesticide of plant source |
| CN111528239A (en) * | 2020-05-26 | 2020-08-14 | 中国热带农业科学院热带生物技术研究所 | Chemical for preventing and treating banana mosaic and heart rot and banana streak and preparation method thereof |
| CN113475537A (en) * | 2021-04-30 | 2021-10-08 | 张永福 | Traditional Chinese medicine insecticidal sterilizing agent and preparation method thereof |
| CN118000201A (en) * | 2024-04-10 | 2024-05-10 | 北京市农林科学院 | Plant source green pesticide for preventing and controlling crop aphids and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105519613A (en) | Novel botanical insecticide, preparation method and application thereof | |
| CN105379771A (en) | Plant-derived pesticide and its preparation method and use | |
| CN105532755A (en) | Novel plant source insecticide for fruit trees, preparation method and application thereof | |
| CN105519612A (en) | Botanical insecticide for fruit trees, preparation method and application thereof | |
| Sharma et al. | Medicinal values of bael (Aegle marmelos)(L.) Corr.: A review | |
| Grosvenor et al. | Medicinal plants from riau province, sumatra, Indonesia. Part 1: uses | |
| CN105532767A (en) | Insecticide, preparation method and application thereof | |
| CN105432695A (en) | Novel pesticide, and preparation method and application thereof | |
| CN105284942A (en) | Novel botanical insecticide, preparation method and application of novel botanical insecticide | |
| CN105542777A (en) | Humic acid type water-retaining agent by using edible vinegar factory waste liquid and preparation method thereof | |
| CN105379780A (en) | Pesticide, as well as preparation method and application thereof | |
| CN105594765A (en) | Environment-friendly pesticide | |
| CN106135318A (en) | A kind of Chinese medicine composition and its preparation method and application | |
| CN105394111A (en) | Organic conditioner utilizing starch industrial production wastewater and preparation method thereof | |
| CN105284941A (en) | Novel insecticide, preparation method and application of novel insecticide | |
| Lalitha et al. | Review on Anti-inflammatory Properties of Mangrove plants | |
| CN105248469A (en) | Plant source pesticide, preparation method and application thereof | |
| CN102428972A (en) | Liquidd mosquito-repellent incense made of folium artemisiae argyi and preparation method thereof | |
| CN109892350A (en) | A kind of composition pesticide of plant source | |
| CN105542778A (en) | Humic acid type organic water-retaining agent and preparation method thereof | |
| CN105419813A (en) | Novel conditioning agent utilizing starch industry production wastewater and preparation method of novel conditioning agent | |
| Sumi et al. | Ethnomedicinal Plants of Sumi Nagas in Zunheboto District, Nagaland, Northeast India | |
| CN105248470A (en) | Plant source fruit tree pesticide, preparation method and application thereof | |
| CN111317000A (en) | Chinese herbal medicine disinfectant and preparation method and application thereof | |
| CN105567243A (en) | Humic acid-type inorganic-organic water-retaining agent utilizing waste liquid of vinegar factory and preparation method for humic acid-type inorganic-organic water-retaining agent |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160427 |
|
| RJ01 | Rejection of invention patent application after publication |