CN106342911A - Botanical insecticide - Google Patents
Botanical insecticide Download PDFInfo
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- CN106342911A CN106342911A CN201610618497.2A CN201610618497A CN106342911A CN 106342911 A CN106342911 A CN 106342911A CN 201610618497 A CN201610618497 A CN 201610618497A CN 106342911 A CN106342911 A CN 106342911A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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Abstract
The invention discloses a botanical insecticide. The botanical insecticide is prepared by euphorbia soongarica, sowthistle, sabah hellebore, tripterygium wilfordii, salix babylonica, neem, angled bittersweet, ailanthus, asparagus lettuce, mint, castor nitrogen, sylvite, phosphorus salt, nitrogen salt, calcium salt, magnesium salt, iodized salt, boron, molybdenum salt, zinc salt, manganese salt, copper salt, ferric salt, vitamins, amino acids, indolebutyric acid, gibberellin, 6-benzyl gland purine, rootone, agar, kinetin, polyvinylpyrrolidone, methylene binaphthalene sodium, America Dupont EEA2112AC compatilizer, earthworm powder, potassium alkyl sulphate, acrylate, chloropropyl-trimethoxysilane, xanthan gum and ethanol. The one-time kill rate of the botanical insecticide for inchworm, yellow spider, pearlong white scale and other plant insects is over 97.18%, which is higher than the kill rate of regular botanical insecticide; moreover, the botanical insecticide is free from the drug tolerance, and can last for 5-8 years; meanwhile, the botanical insecticide can be used for improving yield and sugar content.
Description
Technical field
The invention belongs to insecticide preparing technical field is and in particular to a kind of multi-functional plant insecticide.
Background technology
Prevent and treat agricultural pests at present mostly all using chemical insecticide, with the raising of living standards of the people, to agricultural product
Prescription is high, not only will eat, and health to be eaten.The Pesticide Residue that high poison chemical pesticide is caused is increasingly
Become the focus of social concerns.High-toxic pesticide is core and the key of impact agricultural product quality and safety, not only affects agricultural production quality
Amount, directly the harm people's is healthy, has an effect on increasing peasant income.Because the toxicity of high-toxic pesticide is big, caused people in the past
The event of poultry poisoning happens occasionally.Greatly, the child that teratogenesis is disabled is a lot of for impact to women and child.Additionally, with the world
Various countries increasingly strengthen to the protective awareness of environment for human survival and natural, ecological, and high poison high residue insecticide will be limited further
System.The unreasonable of pesticide uses the quality safety to agricultural product to constitute a threat to, and therefore, reduces Pesticide use particularly high-toxic pesticide
Use, to improving agricultural product quality and the market competitiveness, promote China's agricultural sustainable development, ensure the life of broad masses of the people
Safety suffers from very great meaning with building a harmonious society.
Because chemical pesticide is easy to cause the Drug resistance of insect, use dose in order to prevention effect is continuously increased well, kill
Done harm to a lot of natural enemies and beneficial organism, and polluted us and depend on for existence living environment, Environmental protection more next
More pay attention to, will be further strict to the Detecting Pesticide in agricultural product, therefore, greatly develop non-toxic and non-pollution high-efficiency plant
Source pesticide is the direction of Agrochemicals from now on.Additionally, the insecticide feature of routine single it is impossible to meet demand.
Content of the invention
The present invention provide a kind of plant insecticide, with solve using chemical pesticide control insect cause pest resistance to insecticide and
Pollution environment, the insecticide feature of rule single it is impossible to the problems such as meet demand, the plant insecticide of the present invention to looper,
Yellow spider, long white a red-spotted lizard plant insect a killing rate all more than 97.24%, higher than conventional plant insecticide killing rate, and
And there is no resistance to medical, can be with 5-8；Simultaneously using this plant insecticide, yield and sugar content also can be improved.
For solving above technical problem, the present invention employs the following technical solutions:
A kind of plant insecticide, in units of weight portion, including following raw material: Roots of Euphorbia soongarica 82-98 part, Herba Sonchi Oleracei 82-98
Part, sabadilla 62-88 part, Radix Tripterygii Wilfordii 60-90 part, Salix babylonica L. leaf 50-80 part, Melia azedarach L. 50-80 part, Celastrus angulatus 40-70 part, ailanthus altissima (mill.) swingle
40-70 part, Caulis et Folium Lactucae sativae 35-60 part, Herba Menthae 35-60 part, Semen Ricini 30-50 part, potassium salt 2-3 part, microcosmic salt 1-3 part, nitrogen salt 1-2 part, calcium
Salt 0.6-0.9 part, magnesium salt 0.6-0.9 part, iodine salt 0.2-0.4 part, boron salt 0.2-0.4 part, molybdenum salt 0.2-0.4 part, zinc salt 0.2-
0.4 part, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 part, iron salt 0.2-0.4 part, vitamin 0.2-0.4 part, aminoacid 0.2-0.3
Part, 09 part of indolebutyric acid 0.06-0., gibberellins 0.06-0.09 part, 6- benzyl gland fat purine 0.06-0.08 part, naphthalene acetic acid 0.04-
0.06 part, agar 0.1-0.3 part, kinetins 0.04-0.06 part, Polyvinylpyrrolidone 0.8-2.4 part, di-2-ethylhexylphosphine oxide LOMAR PWA EINECS 246-676-2
Sodium 0.6-1.8 part, Dupont eea2112ac compatilizer 1-1.5 part, Lumbricus powder 0.6-1.5 part, alkyl sulfate potassium 0.4-
1.4 parts, acrylate 0.5-0.8 part, glycidoxy-propyltrimethoxy silane 0.6-1.6 part, xanthan gum 0.5-1.5 part, second
Alcohol 2000-6000 part；
Described potassium salt is composed of the following components: potassium chloride 0.6-0.8 part, potassium sulfate 0.5-0.6 part, potassium nitrate 0.4-0.6 part, carbon
Sour potassium 0.3-0.5 part, potassium bicarbonate 0.2-0.5 part；
Described microcosmic salt is composed of the following components: calcium phosphate 0.3-0.8 part, magnesium phosphate 0.3-0.8 part, iron phosphate 0.2-0.7 part, phosphorus
Sour zinc 0.2-0.7 part；
Described nitrogen salt is composed of the following components: ammonium hydrogen carbonate 0.4-0.8 part, ammonium carbonate 0.3-0.6 part, ammonium chloride 0.3-0.6 part；
Described calcium salt is composed of the following components: calcium glycine 0.3-0.4 part, calcium chloride 0.2-0.3 part, sulphuric acid Asia calcium 0.1-0.2
Part；
Described magnesium salt is composed of the following components: magnesium glycinate 0.3-0.4 part, magnesium chloride 0.2-0.3 part, sulphuric acid Asia magnesium 0.1-0.2
Part；
Described iodine salt is composed of the following components: sodium iodide 0.1-0.2 part, potassium iodate 0.1-0.2 part；
Described vitamin is composed of the following components: raw element a0.08-0.14 part, vitamin b10.08-0.12 part, vitamin
b20.02-0.08 part, vitamin d0.02-0.06 part；
Described aminoacid is composed of the following components: glycine 0.08-0.1 part, cystine 0.06-0.08 part, proline 0.04-
0.07 part, serine 0.02-0.05 part；
Described Polyvinylpyrrolidone is cosolvent；
Described sodium methylene bis-naphthalene sulfonate is dispersant；
Described Lumbricuss are powder conditioner；
Described alkyl sulfate potassium is penetrating agent；
Described acrylate is regulator；
Described glycidoxy-propyltrimethoxy silane is viscosifier；
Described xanthan gum is stabilizer；
The preparation method of described plant insecticide, comprises the following steps:
S1: by Roots of Euphorbia soongarica, Herba Sonchi Oleracei, sabadilla, Radix Tripterygii Wilfordii, Salix babylonica L. leaf, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, castor
Numb co-grinding, obtains mixture, adds mixture in ethanol, is 1:14-16 in solid-liquid ratio, and ultrasonic power is
200-300w, concentration of alcohol is 65%-80%, and Extracting temperature extracts medicinal liquid 18-24min, prepared medicinal liquid at being 66-72 DEG C；
S2: the medicinal liquid that step s1 is obtained crosses 3000-5000 mesh sieve, prepared filtrate；
S3: the filtrate that step s2 is obtained adds potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc salt, manganese
Salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purine, naphthalene acetic acid, agar, kinetins, poly-
Vinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont eea2112ac compatilizer, Lumbricus powder, alkyl sulfate potassium, third
Olefin(e) acid ester, glycidoxy-propyltrimethoxy silane, xanthan gum, are 42-50 DEG C in temperature, and rotating speed is to stir under 100-300r/min
Mix dissolving 20-30min, prepared mixed liquor；
S4: the mixed liquor that step s3 is obtained is concentrated into water content≤22% at temperature is for 60-80 DEG C, prepared mixture；
S5: the mixture that step s4 is obtained is dried to water content≤6% at temperature is for 84-88 DEG C, then pulverizes, mistake
120-260 mesh sieve, gained powder is 134-136 DEG C using pulse vacuum pressure steam sterilizer in temperature, and pressure is 210-
Sterilize under 230kpa 3-4min, prepared plant insecticide.
Further, described boron salt is potassium borate.
Further, described molybdenum salt is potassium molybdate.
Further, described zinc salt is zinc chloride.
Further, described manganese salt is Mn-Gly.
Further, described mantoquita is cupric glycinate.
Further, described iron salt is ferrous sulfate.
The method have the advantages that
(1) the plant insecticide composition of the present invention is nontoxic, and noresidue will not bring environmental pollution；
(2) plant insecticide of the present invention to looper, yellow spider, long white a red-spotted lizard plant insect a killing rate all 97.18%
More than, higher than conventional plant insecticide killing rate, and there is no resistance to medical, can be with 5-8；Killed using this plant source simultaneously
Worm agent, also can improve yield and sugar content；
(3) the vegetable source pesticide agent and process for producing same of the present invention is simple, low cost, and easy to use, application effect is good, is conducive to promoting
Application.
Specific embodiment
For ease of more fully understanding the present invention, it is illustrated by following examples, these embodiments belong to the present invention's
Protection domain, but do not limit the scope of the invention.
In an embodiment, described plant insecticide, in units of weight portion, including following raw material: Roots of Euphorbia soongarica 82-
98 parts, Herba Sonchi Oleracei 82-98 part, sabadilla 62-88 part, Radix Tripterygii Wilfordii 60-90 part, Salix babylonica L. leaf 50-80 part, Melia azedarach L. 50-80 part, bitter skin
Rattan 40-70 part, ailanthus altissima (mill.) swingle 40-70 part, Caulis et Folium Lactucae sativae 35-60 part, Herba Menthae 35-60 part, Semen Ricini 30-50 part, potassium salt 2-3 part, microcosmic salt 1-3
Part, nitrogen salt 1-2 part, calcium salt 0.6-0.9 part, magnesium salt 0.6-0.9 part, iodine salt 0.2-0.4 part, boron salt 0.2-0.4 part, molybdenum salt 0.2-
0.4 part, zinc salt 0.2-0.4 part, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 part, iron salt 0.2-0.4 part, vitamin 0.2-0.4
Part, aminoacid 0.2-0.3 part, 09 part of indolebutyric acid 0.06-0., gibberellins 0.06-0.09 part, 6- benzyl gland fat purine 0.06-
0.08 part, naphthalene acetic acid 0.04-0.06 part, agar 0.1-0.3 part, kinetins 0.04-0.06 part, Polyvinylpyrrolidone 0.8-
2.4 parts, sodium methylene bis-naphthalene sulfonate 0.6-1.8 part, Dupont eea2112ac compatilizer 1-1.5 part, Lumbricus powder 0.6-1.5
Part, alkyl sulfate potassium 0.4-1.4 part, acrylate 0.5-0.8 part, glycidoxy-propyltrimethoxy silane 0.6-1.6 part,
Xanthan gum 0.5-1.5 part, ethanol 2000-6000 part；
Described potassium salt is composed of the following components: potassium chloride 0.6-0.8 part, potassium sulfate 0.5-0.6 part, potassium nitrate 0.4-0.6 part, carbon
Sour potassium 0.3-0.5 part, potassium bicarbonate 0.2-0.5 part；
Described microcosmic salt is composed of the following components: calcium phosphate 0.3-0.8 part, magnesium phosphate 0.3-0.8 part, iron phosphate 0.2-0.7 part, phosphorus
Sour zinc 0.2-0.7 part；
Described nitrogen salt is composed of the following components: ammonium hydrogen carbonate 0.4-0.8 part, ammonium carbonate 0.3-0.6 part, ammonium chloride 0.3-0.6 part；
Described calcium salt is composed of the following components: calcium glycine 0.3-0.4 part, calcium chloride 0.2-0.3 part, sulphuric acid Asia calcium 0.1-0.2
Part；
Described magnesium salt is composed of the following components: magnesium glycinate 0.3-0.4 part, magnesium chloride 0.2-0.3 part, sulphuric acid Asia magnesium 0.1-0.2
Part；
Described iodine salt is composed of the following components: sodium iodide 0.1-0.2 part, potassium iodate 0.1-0.2 part；
Described boron salt is potassium borate；
Described molybdenum salt is potassium molybdate；
Described zinc salt is zinc chloride；
Described manganese salt is Mn-Gly；
Described mantoquita is cupric glycinate；
Described iron salt is ferrous sulfate；
Described vitamin is composed of the following components: raw element a0.08-0.14 part, vitamin b10.08-0.12 part, vitamin
b20.02-0.08 part, vitamin d0.02-0.06 part；
Described aminoacid is composed of the following components: glycine 0.08-0.1 part, cystine 0.06-0.08 part, proline 0.04-
0.07 part, serine 0.02-0.05 part；
Described Polyvinylpyrrolidone is cosolvent；
Described sodium methylene bis-naphthalene sulfonate is dispersant；
Described Lumbricuss are powder conditioner；
Described alkyl sulfate potassium is penetrating agent；
Described acrylate is regulator；
Described glycidoxy-propyltrimethoxy silane is viscosifier；
Described xanthan gum is stabilizer；
The preparation method of described plant insecticide, comprises the following steps:
S1: by Roots of Euphorbia soongarica, Herba Sonchi Oleracei, sabadilla, Radix Tripterygii Wilfordii, Salix babylonica L. leaf, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, castor
Numb co-grinding, obtains mixture, adds mixture in ethanol, is 1:14-16 in solid-liquid ratio, and ultrasonic power is
200-300w, concentration of alcohol is 65%-80%, and Extracting temperature extracts medicinal liquid 18-24min, prepared medicinal liquid at being 66-72 DEG C；
S2: the medicinal liquid that step s1 is obtained crosses 3000-5000 mesh sieve, prepared filtrate；
S3: the filtrate that step s2 is obtained adds potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc salt, manganese
Salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purine, naphthalene acetic acid, agar, kinetins, poly-
Vinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont eea2112ac compatilizer, Lumbricus powder, alkyl sulfate potassium, third
Olefin(e) acid ester, glycidoxy-propyltrimethoxy silane, xanthan gum, are 42-50 DEG C in temperature, and rotating speed is to stir under 100-300r/min
Mix dissolving 20-30min, prepared mixed liquor；
S4: the mixed liquor that step s3 is obtained is concentrated into water content≤22% at temperature is for 60-80 DEG C, prepared mixture；
S5: the mixture that step s4 is obtained is dried to water content≤6% at temperature is for 84-88 DEG C, then pulverizes, mistake
120-260 mesh sieve, gained powder is 134-136 DEG C using pulse vacuum pressure steam sterilizer in temperature, and pressure is 210-
Sterilize under 230kpa 3-4min, prepared plant insecticide.
It is illustrated below by more specifically embodiment.
Embodiment 1
A kind of plant insecticide, in units of weight portion, including following raw material: 90 parts of Roots of Euphorbia soongarica, 90 parts of Herba Sonchi Oleracei, Sabah
75 parts of Rhizoma et radix veratri (Radix Rhizoma Veratri), 75 parts of Radix Tripterygii Wilfordii, 65 parts of Salix babylonica L. leaf, 65 parts of Melia azedarach L., 55 parts of Celastrus angulatus, 55 parts of ailanthus altissima (mill.) swingle, 50 parts of Caulis et Folium Lactucae sativae, Herba Menthae 50
Part, 40 parts of Semen Ricini, 2.5 parts of potassium salt, 2 parts of microcosmic salt, 1.5 parts of nitrogen salt, 0.8 part of calcium salt, 0.8 part of magnesium salt, 0.3 part of iodine salt, boron salt 0.3
Part, 0.3 part of molybdenum salt, 0.3 part of zinc salt, 0.3 part of manganese salt, 0.3 part of mantoquita, 0.3 part of iron salt, 0.3 part of vitamin, 0.2 part of aminoacid,
0.08 part of indolebutyric acid, 0.08 part of gibberellins, 0.07 part of 6- benzyl gland fat purine, 0.05 part of naphthalene acetic acid, 0.2 part of agar, kinetins
0.05 part, 1.6 parts of Polyvinylpyrrolidone, 1.2 parts of sodium methylene bis-naphthalene sulfonate, Dupont eea2112ac compatilizer 1.2
Part, 1 part of Lumbricus powder, 1 part of alkyl sulfate potassium, 0.7 part of acrylate, 1.2 parts of glycidoxy-propyltrimethoxy silane, xanthan
1 part of glue, 4000 parts of ethanol；
Described potassium salt is composed of the following components: 0.7 part of potassium chloride, 0.5 part of potassium sulfate, 0.4 part of potassium nitrate, 0.5 part of potassium carbonate, carbon
0.4 part of potassium hydrogen phthalate；
Described microcosmic salt is composed of the following components: 0.6 part of calcium phosphate, 0.6 part of magnesium phosphate, 0.5 part of iron phosphate, 0.3 part of zinc phosphate；
Described nitrogen salt is composed of the following components: 0.6 part of ammonium hydrogen carbonate, 0.5 part of ammonium carbonate, 0.4 part of ammonium chloride；
Described calcium salt is composed of the following components: 0.3 part of calcium glycine, 0.3 part of calcium chloride, 0.2 part of the calcium in sulphuric acid Asia；
Described magnesium salt is composed of the following components: 0.3 part of magnesium glycinate, 0.3 part of magnesium chloride, 0.2 part of the magnesium in sulphuric acid Asia；
Described iodine salt is composed of the following components: 0.2 part of sodium iodide, 0.1 part of potassium iodate；
Described boron salt is potassium borate；
Described molybdenum salt is potassium molybdate；
Described zinc salt is zinc chloride；
Described manganese salt is Mn-Gly；
Described mantoquita is cupric glycinate；
Described iron salt is ferrous sulfate；
Described vitamin is composed of the following components: raw element a0.1 part, vitamin b10.1 part, vitamin b20.05 part, vitamin
D0.05 part；
Described aminoacid is composed of the following components: 0.08 part of glycine, 0.06 part of cystine, 0.04 part of proline, serine
0.02 part；
Described Polyvinylpyrrolidone is cosolvent；
Described sodium methylene bis-naphthalene sulfonate is dispersant；
Described Lumbricuss are powder conditioner；
Described alkyl sulfate potassium is penetrating agent；
Described acrylate is regulator；
Described glycidoxy-propyltrimethoxy silane is viscosifier；
Described xanthan gum is stabilizer；
The preparation method of described plant insecticide, comprises the following steps:
S1: by Roots of Euphorbia soongarica, Herba Sonchi Oleracei, sabadilla, Radix Tripterygii Wilfordii, Salix babylonica L. leaf, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, castor
Numb co-grinding, obtains mixture, adds mixture in ethanol, is 1:15 in solid-liquid ratio, and ultrasonic power is 250w,
Concentration of alcohol is 75%, and Extracting temperature extracts medicinal liquid 20min, prepared medicinal liquid at being 68 DEG C；
S2: the medicinal liquid that step s1 is obtained crosses 4000 mesh sieve, prepared filtrate；
S3: the filtrate that step s2 is obtained adds potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc salt, manganese
Salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purine, naphthalene acetic acid, agar, kinetins, poly-
Vinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont eea2112ac compatilizer, Lumbricus powder, alkyl sulfate potassium, third
Olefin(e) acid ester, glycidoxy-propyltrimethoxy silane, xanthan gum, are 46 DEG C in temperature, and rotating speed is stirring and dissolving under 200r/min
25min, prepared mixed liquor；
S4: it is 22% that the mixed liquor that step s3 is obtained is concentrated into water content at temperature is 70 DEG C, prepared mixture；
S5: it is 6% that the mixture that step s4 is obtained is dried to water content at temperature is 86 DEG C, then pulverizes, crosses 200 mesh
Sieve, gained powder adopts pulse vacuum pressure steam sterilizer to be 135 DEG C in temperature, and pressure is to sterilize under 220kpa
3.5min, prepared plant insecticide.
Embodiment 2
A kind of plant insecticide, in units of weight portion, including following raw material: 82 parts of Roots of Euphorbia soongarica, 82 parts of Herba Sonchi Oleracei, Sabah
62 parts of Rhizoma et radix veratri (Radix Rhizoma Veratri), 60 parts of Radix Tripterygii Wilfordii, 50 parts of Salix babylonica L. leaf, 50 parts of Melia azedarach L., 40 parts of Celastrus angulatus, 40 parts of ailanthus altissima (mill.) swingle, 35 parts of Caulis et Folium Lactucae sativae, Herba Menthae 35
Part, 30 parts of Semen Ricini, 2 parts of potassium salt, 1 part of microcosmic salt, 1 part of nitrogen salt, 0.6 part of calcium salt, 0.6 part of magnesium salt, 0.2 part of iodine salt, 0.2 part of boron salt,
0.2 part of molybdenum salt, 0.2 part of zinc salt, 0.2 part of manganese salt, 0.2 part of mantoquita, 0.2 part of iron salt, 0.2 part of vitamin, 0.2 part of aminoacid, Yin
0.06 part of diindyl butanoic acid, 0.06 part of gibberellins, 0.06 part of 6- benzyl gland fat purine, 0.04 part of naphthalene acetic acid, 0.1 part of agar, kinetins
0.04 part, 0.8 part of Polyvinylpyrrolidone, 0.6 part of sodium methylene bis-naphthalene sulfonate, 1 part of Dupont eea2112ac compatilizer,
0.6 part of Lumbricus powder, 0.4 part of alkyl sulfate potassium, 0.5 part of acrylate, 0.6 part of glycidoxy-propyltrimethoxy silane, Huang
0.5 part of virgin rubber, 2000 parts of ethanol；
Described potassium salt is composed of the following components: 0.6 part of potassium chloride, 0.5 part of potassium sulfate, 0.4 part of potassium nitrate, 0.3 part of potassium carbonate, carbon
0.2 part of potassium hydrogen phthalate；
Described microcosmic salt is composed of the following components: 0.3 part of calcium phosphate, 0.3 part of magnesium phosphate, 0.2 part of iron phosphate, 0.2 part of zinc phosphate；
Described nitrogen salt is composed of the following components: 0.4 part of ammonium hydrogen carbonate, 0.3 part of ammonium carbonate, 0.3 part of ammonium chloride；
Described calcium salt is composed of the following components: 0.3 part of calcium glycine, 0.2 part of calcium chloride, 0.1 part of the calcium in sulphuric acid Asia；
Described magnesium salt is composed of the following components: 0.3 part of magnesium glycinate, 0.2 part of magnesium chloride, 0.1 part of the magnesium in sulphuric acid Asia；
Described iodine salt is composed of the following components: 0.1 part of sodium iodide, 0.1 part of potassium iodate；
Described boron salt is potassium borate；
Described molybdenum salt is potassium molybdate；
Described zinc salt is zinc chloride；
Described manganese salt is Mn-Gly；
Described mantoquita is cupric glycinate；
Described iron salt is ferrous sulfate；
Described vitamin is composed of the following components: raw element a0.08 part, vitamin b10.08 part, vitamin b20.02 part, dimension life
Plain d0.02 part；
Described aminoacid is composed of the following components: 0.08 part of glycine, 0.06 part of cystine, 0.04 part of proline, serine
0.02 part；
Described Polyvinylpyrrolidone is cosolvent；
Described sodium methylene bis-naphthalene sulfonate is dispersant；
Described Lumbricuss are powder conditioner；
Described alkyl sulfate potassium is penetrating agent；
Described acrylate is regulator；
Described glycidoxy-propyltrimethoxy silane is viscosifier；
Described xanthan gum is stabilizer；
The preparation method of described plant insecticide, comprises the following steps:
S1: by Roots of Euphorbia soongarica, Herba Sonchi Oleracei, sabadilla, Radix Tripterygii Wilfordii, Salix babylonica L. leaf, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, castor
Numb co-grinding, obtains mixture, adds mixture in ethanol, is 1:14 in solid-liquid ratio, and ultrasonic power is 200w,
Concentration of alcohol is 65%, and Extracting temperature extracts medicinal liquid 24min, prepared medicinal liquid at being 66 DEG C；
S2: the medicinal liquid that step s1 is obtained crosses 3000 mesh sieve, prepared filtrate；
S3: the filtrate that step s2 is obtained adds potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc salt, manganese
Salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purine, naphthalene acetic acid, agar, kinetins, poly-
Vinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont eea2112ac compatilizer, Lumbricus powder, alkyl sulfate potassium, third
Olefin(e) acid ester, glycidoxy-propyltrimethoxy silane, xanthan gum, are 42 DEG C in temperature, and rotating speed is stirring and dissolving under 100r/min
30min, prepared mixed liquor；
S4: it is 20% that the mixed liquor that step s3 is obtained is concentrated into water content at temperature is 60 DEG C, prepared mixture；
S5: it is 5% that the mixture that step s4 is obtained is dried to water content at temperature is 84 DEG C, then pulverizes, crosses 120 mesh
Sieve, gained powder adopts pulse vacuum pressure steam sterilizer to be 134 DEG C in temperature, and pressure is the 4min that sterilizes under 210kpa,
Prepared plant insecticide.
Embodiment 3
A kind of plant insecticide, in units of weight portion, including following raw material: 98 parts of Roots of Euphorbia soongarica, 98 parts of Herba Sonchi Oleracei, Sabah
88 parts of Rhizoma et radix veratri (Radix Rhizoma Veratri), 90 parts of Radix Tripterygii Wilfordii, 80 parts of Salix babylonica L. leaf, 80 parts of Melia azedarach L., 70 parts of Celastrus angulatus, 70 parts of ailanthus altissima (mill.) swingle, 60 parts of Caulis et Folium Lactucae sativae, Herba Menthae 60
Part, 50 parts of Semen Ricini, 3 parts of potassium salt, 3 parts of microcosmic salt, 2 parts of nitrogen salt, 0.9 part of calcium salt, 0.9 part of magnesium salt, 0.4 part of iodine salt, 0.4 part of boron salt,
0.4 part of molybdenum salt, 0.4 part of zinc salt, 0.4 part of manganese salt, 0.4 part of mantoquita, 0.4 part of iron salt, 0.4 part of vitamin, 0.3 part of aminoacid, Yin
0. 09 parts of diindyl butanoic acid, 0.09 part of gibberellins, 0.08 part of 6- benzyl gland fat purine, 0.06 part of naphthalene acetic acid, 0.3 part of agar, kinetins
0.06 part, 2.4 parts of Polyvinylpyrrolidone, 1.8 parts of sodium methylene bis-naphthalene sulfonate, Dupont eea2112ac compatilizer 1.5
Part, 1.5 parts of Lumbricus powder, 1.4 parts of alkyl sulfate potassium, 0.8 part of acrylate, 1.6 parts of glycidoxy-propyltrimethoxy silane,
1.5 parts of xanthan gum, 6000 parts of ethanol；
Described potassium salt is composed of the following components: 0.8 part of potassium chloride, 0.6 part of potassium sulfate, 0.6 part of potassium nitrate, 0.5 part of potassium carbonate, carbon
0.5 part of potassium hydrogen phthalate；
Described microcosmic salt is composed of the following components: 0.8 part of calcium phosphate, 0.8 part of magnesium phosphate, 0.7 part of iron phosphate, 0.7 part of zinc phosphate；
Described nitrogen salt is composed of the following components: 0.8 part of ammonium hydrogen carbonate, 0.6 part of ammonium carbonate, 0.6 part of ammonium chloride；
Described calcium salt is composed of the following components: 0.4 part of calcium glycine, 0.3 part of calcium chloride, 0.2 part of the calcium in sulphuric acid Asia；
Described magnesium salt is composed of the following components: 0.4 part of magnesium glycinate, 0.3 part of magnesium chloride, 0.2 part of the magnesium in sulphuric acid Asia；
Described iodine salt is composed of the following components: 0.2 part of sodium iodide, 0.2 part of potassium iodate；
Described boron salt is potassium borate；
Described molybdenum salt is potassium molybdate；
Described zinc salt is zinc chloride；
Described manganese salt is Mn-Gly；
Described mantoquita is cupric glycinate；
Described iron salt is ferrous sulfate；
Described vitamin is composed of the following components: raw element a0.14 part, vitamin b10.12 part, vitamin b20.08 part, dimension life
Plain d0.06 part；
Described aminoacid is composed of the following components: 0.1 part of glycine, 0.08 part of cystine, 0.07 part of proline, serine 0.05
Part；
Described Polyvinylpyrrolidone is cosolvent；
Described sodium methylene bis-naphthalene sulfonate is dispersant；
Described Lumbricuss are powder conditioner；
Described alkyl sulfate potassium is penetrating agent；
Described acrylate is regulator；
Described glycidoxy-propyltrimethoxy silane is viscosifier；
Described xanthan gum is stabilizer；
The preparation method of described plant insecticide, comprises the following steps:
S1: by Roots of Euphorbia soongarica, Herba Sonchi Oleracei, sabadilla, Radix Tripterygii Wilfordii, Salix babylonica L. leaf, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, castor
Numb co-grinding, obtains mixture, adds mixture in ethanol, is 1:16 in solid-liquid ratio, and ultrasonic power is 300w,
Concentration of alcohol is 80%, and Extracting temperature extracts medicinal liquid 18min, prepared medicinal liquid at being 72 DEG C；
S2: the medicinal liquid that step s1 is obtained crosses 5000 mesh sieve, prepared filtrate；
S3: the filtrate that step s2 is obtained adds potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc salt, manganese
Salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purine, naphthalene acetic acid, agar, kinetins, poly-
Vinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont eea2112ac compatilizer, Lumbricus powder, alkyl sulfate potassium, third
Olefin(e) acid ester, glycidoxy-propyltrimethoxy silane, xanthan gum, are 50 DEG C in temperature, and rotating speed is stirring and dissolving under 300r/min
20min, prepared mixed liquor；
S4: it is 16% that the mixed liquor that step s3 is obtained is concentrated into water content at temperature is 80 DEG C, prepared mixture；
S5: it is 4% that the mixture that step s4 is obtained is dried to water content at temperature is for 84-88 DEG C, then pulverizes, crosses 260
Mesh sieve, gained powder adopts pulse vacuum pressure steam sterilizer to be 136 DEG C in temperature, and pressure is to sterilize under 230kpa
3min, prepared plant insecticide.
For verifying the effect of plant insecticide of the present invention, by following experimental verification.
Using plant insecticide and the conventional insecticide (matched group) of embodiment 1-3, join 45g water by 1g insecticide
Ratio uses, and carries out Citrus and once prevents and treats looper, yellow spider, the test of long white a red-spotted lizard plant insect, result see table.
From upper table, the plant insecticide of embodiment of the present invention 1-3 is to looper, yellow spider, long white a red-spotted lizard plant insect
A killing rate all more than 97.18%, higher than conventional plant insecticide killing rate, using effect is good；Simultaneously using this plant
Thing insecticide, also can improve yield and sugar content.
Above content is it cannot be assumed that the present invention is embodied as being confined to these explanations, for the technical field of the invention
Those of ordinary skill for, under the premise of without departing from present inventive concept, some simple deduction or replace can also be made, all answer
When being considered as belonging to the scope of patent protection that the present invention is determined by claims of being submitted to.
Claims (7)
1. a kind of plant insecticide is it is characterised in that in units of weight portion, including following raw material: Roots of Euphorbia soongarica 82-98
Part, Herba Sonchi Oleracei 82-98 part, sabadilla 62-88 part, Radix Tripterygii Wilfordii 60-90 part, Salix babylonica L. leaf 50-80 part, Melia azedarach L. 50-80 part, Celastrus angulatus
40-70 part, ailanthus altissima (mill.) swingle 40-70 part, Caulis et Folium Lactucae sativae 35-60 part, Herba Menthae 35-60 part, Semen Ricini 30-50 part, potassium salt 2-3 part, microcosmic salt 1-3 part,
Nitrogen salt 1-2 part, calcium salt 0.6-0.9 part, magnesium salt 0.6-0.9 part, iodine salt 0.2-0.4 part, boron salt 0.2-0.4 part, molybdenum salt 0.2-0.4
Part, zinc salt 0.2-0.4 part, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 part, iron salt 0.2-0.4 part, vitamin 0.2-0.4 part, ammonia
Base acid 0.2-0.3 part, 09 part of indolebutyric acid 0.06-0., gibberellins 0.06-0.09 part, 6- benzyl gland fat purine 0.06-0.08 part,
Naphthalene acetic acid 0.04-0.06 part, agar 0.1-0.3 part, kinetins 0.04-0.06 part, Polyvinylpyrrolidone 0.8-2.4 part, Asia
Methyl double sodium naphthalene sulfonate 0.6-1.8 part, Dupont eea2112ac compatilizer 1-1.5 part, Lumbricus powder 0.6-1.5 part, alkyl sulfide
Acid esters potassium 0.4-1.4 part, acrylate 0.5-0.8 part, glycidoxy-propyltrimethoxy silane 0.6-1.6 part, xanthan gum
0.5-1.5 part, ethanol 2000-6000 part；
Described potassium salt is composed of the following components: potassium chloride 0.6-0.8 part, potassium sulfate 0.5-0.6 part, potassium nitrate 0.4-0.6 part, carbon
Sour potassium 0.3-0.5 part, potassium bicarbonate 0.2-0.5 part；
Described microcosmic salt is composed of the following components: calcium phosphate 0.3-0.8 part, magnesium phosphate 0.3-0.8 part, iron phosphate 0.2-0.7 part, phosphorus
Sour zinc 0.2-0.7 part；
Described nitrogen salt is composed of the following components: ammonium hydrogen carbonate 0.4-0.8 part, ammonium carbonate 0.3-0.6 part, ammonium chloride 0.3-0.6 part；
Described calcium salt is composed of the following components: calcium glycine 0.3-0.4 part, calcium chloride 0.2-0.3 part, sulphuric acid Asia calcium 0.1-0.2
Part；
Described magnesium salt is composed of the following components: magnesium glycinate 0.3-0.4 part, magnesium chloride 0.2-0.3 part, sulphuric acid Asia magnesium 0.1-0.2
Part；
Described iodine salt is composed of the following components: sodium iodide 0.1-0.2 part, potassium iodate 0.1-0.2 part；
Described vitamin is composed of the following components: raw element a0.08-0.14 part, vitamin b10.08-0.12 part, vitamin
B20.02-0.08 part, vitamin d0.02-0.06 part；
Described aminoacid is composed of the following components: glycine 0.08-0.1 part, cystine 0.06-0.08 part, proline 0.04-
0.07 part, serine 0.02-0.05 part；
The preparation method of described plant insecticide, comprises the following steps:
S1: by Roots of Euphorbia soongarica, Herba Sonchi Oleracei, sabadilla, Radix Tripterygii Wilfordii, Salix babylonica L. leaf, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae, Herba Menthae, castor
Numb co-grinding, obtains mixture, adds mixture in ethanol, is 1:14-16 in solid-liquid ratio, and ultrasonic power is
200-300w, concentration of alcohol is 65%-80%, and Extracting temperature extracts medicinal liquid 18-24min, prepared medicinal liquid at being 66-72 DEG C；
S2: the medicinal liquid that step s1 is obtained crosses 3000-5000 mesh sieve, prepared filtrate；
S3: the filtrate that step s2 is obtained adds potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc salt, manganese
Salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purine, naphthalene acetic acid, agar, kinetins, poly-
Vinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont eea2112ac compatilizer, Lumbricus powder, alkyl sulfate potassium, third
Olefin(e) acid ester, glycidoxy-propyltrimethoxy silane, xanthan gum, are 42-50 DEG C in temperature, and rotating speed is to stir under 100-300r/min
Mix dissolving 20-30min, prepared mixed liquor；
S4: the mixed liquor that step s3 is obtained is concentrated into water content≤22% at temperature is for 60-80 DEG C, prepared mixture；
S5: the mixture that step s4 is obtained is dried to water content≤6% at temperature is for 84-88 DEG C, then pulverizes, mistake
120-260 mesh sieve, gained powder is 134-136 DEG C using pulse vacuum pressure steam sterilizer in temperature, and pressure is 210-
Sterilize under 230kpa 3-4min, prepared plant insecticide.
2. plant insecticide according to claim 1 is it is characterised in that described boron salt is potassium borate.
3. plant insecticide according to claim 1 is it is characterised in that described molybdenum salt is potassium molybdate.
4. plant insecticide according to claim 1 is it is characterised in that described zinc salt is zinc chloride.
5. plant insecticide according to claim 1 is it is characterised in that described manganese salt is Mn-Gly.
6. plant insecticide according to claim 1 is it is characterised in that described mantoquita is cupric glycinate.
7. plant insecticide according to claim 1 is it is characterised in that described iron salt is ferrous sulfate.
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