CN105248469A - Plant source pesticide, preparation method and application thereof - Google Patents
Plant source pesticide, preparation method and application thereof Download PDFInfo
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- CN105248469A CN105248469A CN201510701739.XA CN201510701739A CN105248469A CN 105248469 A CN105248469 A CN 105248469A CN 201510701739 A CN201510701739 A CN 201510701739A CN 105248469 A CN105248469 A CN 105248469A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a plant source pesticide, a preparation method and application thereof and belongs to the technical field of pesticide preparation. The plant source pesticide is prepared from, by weight, 20-50 parts of tobaccos, 20-50 parts of tripterygium wilfordii, 20-50 parts of hot peppers, 30-40 parts of aconitum, 30-40 parts of pyrethrums, 30-40 parts of neem, 20-30 parts of tea tree leaves, 20-30 parts of dahurian patrinia herb, 20-30 parts of bitter herb and 800-3500 parts of water. The plant source pesticide is prepared through medicine liquid extraction, concentration, drying, smashing, sieving, sterilization and other steps. The plant source pesticide contains non-toxic components, is free of residues, pollution-free and green, is environmentally friendly and does not bring environmental pollution. The plant source pesticide can effectively prevent and control inchworms, red spiders, pearlong white scale insects, leaf miners and other plant pests, the one-time killing rate is above 90.43%, and no pesticide resistance is produced.
Description
[technical field]
The invention belongs to insecticide preparing technical field, be specifically related to a kind of plant insecticide, preparation method and application thereof.
[background technology]
Current control pest all use chemical insecticide mostly, along with the raising of living standards of the people, require high, not only will eat, and will eat health agricultural product quality.The Pesticide Residue that high malicious chemical pesticide causes more and more becomes the focus of social concerns.High-toxic pesticide is the core and the key that affect agricultural product quality and safety, not only affects agricultural product quality, directly endangers the healthy of the people, also affects increasing peasant income.Because the toxicity of high-toxic pesticide is large, the event of person poultry poisoning was caused to happen occasionally in the past.Very big on the impact of women and children, the children that teratogenesis is disabled are a lot.In addition, along with the protective awareness of countries in the world to environment for human survival and natural, ecological strengthens day by day, high malicious high residue insecticide will be restricted further.The quality safety of unreasonable use to agricultural product of agricultural chemicals constitutes a threat to, therefore, reduce Pesticide use particularly high-toxic pesticide use, to raising agricultural product quality and the market competitiveness, promote China's agricultural sustainable development, ensure the life security of broad masses of the people and very great meaning of building a harmonious society.
Because chemical pesticide is easy to the pesticide resistance causing insect; dosage is made in order to control efficiency well constantly increases; a lot of natural enemy and beneficial organism are murdered; and pollute us and to depend on for existence living environment; the more and more attention of Environmental protection; will be further strict to the Detecting Pesticide in agricultural product, therefore, greatly develop the direction that non-toxic and non-pollution high-efficiency plant source pesticide is Agrochemicals from now on.
[summary of the invention]
The invention provides a kind of plant insecticide, preparation method and application thereof, use chemical pesticide control insect to cause the problem such as pest resistance to insecticide and contaminated environment to solve, plant insecticide composition of the present invention is nontoxic, noresidue, nuisanceless, environmental protection, can not bring environmental pollution; Plant insecticide of the present invention effectively can prevent and treat the plant insect such as looper, two spotted spider mite, long white a red-spotted lizard, leaf miner, and one time killing rate all reaches more than 90.43%, and does not have drug resistance.
For solving above technical problem, the present invention by the following technical solutions:
A kind of plant insecticide, in units of weight portion, comprise following raw material: tobacco 20-50 part, thunder godvine 20-50 part, capsicum 20-50 part, rhizome of Chinese monkshood 30-40 part, Dalmatian chrysanthemum 30-40 part, print chinaberry 30-40 part, tea free 20-30 part, field pennycress 20-30 part, bitter dish 20-30 part, water 800-3500 part.
Preferably, described plant insecticide, in units of weight portion, comprise following raw material: tobacco 30-40 part, thunder godvine 30-40 part, capsicum 30-40 part, rhizome of Chinese monkshood 32-38 part, Dalmatian chrysanthemum 32-38 part, print chinaberry 32-38 part, tea free 22-28 part, field pennycress 22-28 part, bitter dish 22-28 part, water 1000-3000 part.
Preferably, described plant insecticide, in units of weight portion, comprise following raw material: tobacco 35 parts, thunder godvine 35 parts, 35 parts, capsicum, the rhizome of Chinese monkshood 35 parts, Dalmatian chrysanthemum 35 parts, print chinaberry 35 parts, tea free 25 parts, field pennycress 25 parts, bitter dish 25 parts, 2000 parts, water.
The present invention also provides a kind of preparation method of plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish co-grinding, obtain mixture A, mixture A is added to the water, extract liquid under ultrasonic assistant extraction method;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained plant insecticide.
Preferably, the condition of the extraction method of ultrasonic assistant described in step S1 extraction liquid is: ultrasonic power is 140-180W, and concentration of alcohol is 55%-75%, and Extracting temperature is 55-65 DEG C, and extraction time is 90-120min.
Preferably, step S2 herb liquid filters, and is concentrated into water content≤25%.
Preferably, in step S2, mixture B is dried to water content≤6% at 90-100 DEG C.
Preferably, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
Preferably, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
The application of described plant insecticide in one or more plant insects of control looper, two spotted spider mite, long white a red-spotted lizard, leaf miner.
Pharmacology of the present invention is as follows:
Tobacco has the effects such as promoting qi circulation and relieving pain, eliminating dampness, detumescence, removing toxic substances desinsection.
Thunder godvine can be dispeled the wind, removing toxic substances, desinsection.External application treating rheumatic arthritis, skin is itched, and kills maggot, wriggler, water-snail eradication, malicious mouse.
Capsicum can alleviate chest abdomen crymodynia, prevents dysentery, kills and presses down stomach abdomen entozoa, controls cardiopathy and coronary sclerosis, the function such as have sterilization, anticorrosion, seasoning, nutrition, dispel cold.
The aconitine of aconite extract has suppression or killing action to staphylococcus aureus, shigella dysenteriae, typhoid bacillus, Pseudomonas aeruginosa.
Dalmatian chrysanthemum containing 4 kinds of insecticidal constituents, pyrethrin (pyrethrin) I, II and cinerin (cinerin) I, II, Dalmatian chrysanthemum to various insects as mosquito, fly, bedbug and cockroach etc. have toxic action.
Print Melia, in Meliaceae, comes from Southeast Asia, and containing print chinaberry, solannin etc., have good disinsection efficiency, insect is once contact, and growth will be suppressed.
The extract of tea free has potent bactericidal action, and tea tree can effectively tackle for various mycotic infection, can kill staphylococcus aureus, diphtheria bacillus.
Field pennycress, with root-like stock and root, all herbal medicine, belongs to antipyretic and antidotal type medicine in Chinese medicine, cool in nature, taste is pungent, bitter.Return liver, stomach, large intestine channel, have effect that is clearing heat and detoxicating, removing blood stasis and expelling pus.Modern pharmacy is thought, it is containing volatile oil, Patrinia scaniosaefolia saponin and β-sterol glucose formula, have anti-inflammatory, antibacterial, calm, protect the liver the effect with cardiac stimulant diuresis.Field pennycress has suppression or killing action to staphylococcus aureus, shigella dysenteriae, typhoid bacillus, Pseudomonas aeruginosa.
Containing the composition such as taraxasterol, choline in bitter dish, stronger bactericidal action is had to staphylococcus aureus resistance bacterial strain, hemolytic streptococcus, also there is certain lethal effect to Diplococcus pneumopniae, meningococcus, diphtheria bacillus, Pseudomonas aeruginosa, shigella dysenteriae etc., therefore all have certain curative effect to icterepatitis, sphagitis, bacillary dysentery, cold, fever and chronic bronchitis, tonsillitis etc.
The present invention has following beneficial effect:
(1) plant insecticide composition of the present invention is nontoxic, and noresidue is nuisanceless, environmental protection, can not bring environmental pollution;
(2) plant insecticide of the present invention effectively can prevent and treat the plant insect such as looper, two spotted spider mite, long white a red-spotted lizard, leaf miner, and one time killing rate all reaches more than 90.43%, and does not have resistance to medical, can use by 3-5;
(3) vegetable source pesticide agent and process for producing same of the present invention is simple, and cost is low, easy to use, and effect is good, is conducive to applying.
[embodiment]
Be specifically described below in conjunction with specific embodiment.
Embodiment 1
A kind of plant insecticide, in units of weight portion, comprises following raw material: tobacco 20 parts, thunder godvine 20 parts, 20 parts, capsicum, the rhizome of Chinese monkshood 30 parts, Dalmatian chrysanthemum 30 parts, print chinaberry 30 parts, tea free 20 parts, field pennycress 20 parts, bitter dish 20 parts, 800 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140W, concentration of alcohol is 55%, and Extracting temperature is 55 DEG C, and extraction time is 120min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 25%, and obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, pressure is sterilizing 5min under 210KPa, obtained plant insecticide.
Embodiment 2
A kind of plant insecticide, in units of weight portion, comprises following raw material: tobacco 50 parts, thunder godvine 50 parts, 50 parts, capsicum, the rhizome of Chinese monkshood 40 parts, Dalmatian chrysanthemum 40 parts, print chinaberry 40 parts, tea free 30 parts, field pennycress 30 parts, bitter dish 30 parts, 3500 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 180W, concentration of alcohol is 75%, and Extracting temperature is 65 DEG C, and extraction time is 90min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 18%, and obtain mixture B, it is 4% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained plant insecticide.
Embodiment 3
A kind of plant insecticide, in units of weight portion, comprises following raw material: tobacco 35 parts, thunder godvine 35 parts, 35 parts, capsicum, the rhizome of Chinese monkshood 35 parts, Dalmatian chrysanthemum 35 parts, print chinaberry 35 parts, tea free 25 parts, field pennycress 25 parts, bitter dish 25 parts, 2000 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 65%, and Extracting temperature is 60 DEG C, and extraction time is 105min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 135 DEG C in temperature, pressure is sterilizing 4min under 220KPa, obtained plant insecticide.
Embodiment 4
A kind of plant insecticide, in units of weight portion, comprises following raw material: tobacco 30 parts, thunder godvine 30 parts, 30 parts, capsicum, the rhizome of Chinese monkshood 32 parts, Dalmatian chrysanthemum 32 parts, print chinaberry 32 parts, tea free 22 parts, field pennycress 22 parts, bitter dish 22 parts, 1000 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 150W, concentration of alcohol is 60%, and Extracting temperature is 55 DEG C, and extraction time is 110min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 22%, and obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, pressure is sterilizing 5min under 210KPa, obtained plant insecticide.
Embodiment 5
A kind of plant insecticide, in units of weight portion, comprises following raw material: tobacco 40 parts, thunder godvine 40 parts, 40 parts, capsicum, the rhizome of Chinese monkshood 38 parts, Dalmatian chrysanthemum 38 parts, print chinaberry 38 parts, tea free 28 parts, field pennycress 28 parts, bitter dish 28 parts, 3000 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 170W, concentration of alcohol is 70%, and Extracting temperature is 65 DEG C, and extraction time is 100min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained plant insecticide.
Embodiment 6
A kind of plant insecticide, in units of weight portion, comprises following raw material: tobacco 45 parts, thunder godvine 45 parts, 45 parts, capsicum, the rhizome of Chinese monkshood 35 parts, Dalmatian chrysanthemum 35 parts, print chinaberry 35 parts, tea free 25 parts, field pennycress 25 parts, bitter dish 25 parts, 2500 parts, water.
The preparation method of described plant insecticide, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 70%, and Extracting temperature is 60 DEG C, and extraction time is 110min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 23%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained plant insecticide.
For verifying the effect of plant insecticide of the present invention, by following experimental verification.
Adopt the plant insecticide of embodiment 1-6, the ratio of joining 40g water in 1g plant insecticide uses, and once prevents and treats the test of the plant insect such as looper, two spotted spider mite, long white a red-spotted lizard, leaf miner, the results are shown in following table.
From upper table, the plant insecticide of embodiment of the present invention 1-6 is to a killing rate of the plant insect such as looper, two spotted spider mite, long white a red-spotted lizard, leaf miner all more than 90.43%, and result of use is good.Due to plant insecticide nonhazardous of the present invention, do not pollute, do not remain, it is efficient to add control efficiency, therefore, can widely popularize application.
Above content can not assert that the present invention specifically implements to be confined to these explanations; for general technical staff of the technical field of the invention; do not departing under concept thereof of the present invention; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted to claims.
Claims (10)
1. a plant insecticide, it is characterized in that, in units of weight portion, comprise following raw material: tobacco 20-50 part, thunder godvine 20-50 part, capsicum 20-50 part, rhizome of Chinese monkshood 30-40 part, Dalmatian chrysanthemum 30-40 part, print chinaberry 30-40 part, tea free 20-30 part, field pennycress 20-30 part, bitter dish 20-30 part, water 800-3500 part.
2. plant insecticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: tobacco 30-40 part, thunder godvine 30-40 part, capsicum 30-40 part, rhizome of Chinese monkshood 32-38 part, Dalmatian chrysanthemum 32-38 part, print chinaberry 32-38 part, tea free 22-28 part, field pennycress 22-28 part, bitter dish 22-28 part, water 1000-3000 part.
3. plant insecticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: tobacco 35 parts, thunder godvine 35 parts, 35 parts, capsicum, the rhizome of Chinese monkshood 35 parts, Dalmatian chrysanthemum 35 parts, print chinaberry 35 parts, tea free 25 parts, field pennycress 25 parts, bitter dish 25 parts, 2000 parts, water.
4. a preparation method for the plant insecticide according to any one of claim 1-3, is characterized in that, comprises the following steps:
S1: by tobacco, thunder godvine, capsicum, the rhizome of Chinese monkshood, Dalmatian chrysanthemum, print chinaberry, tea free, field pennycress, bitter dish co-grinding, obtain mixture A, mixture A is added to the water, extract liquid under ultrasonic assistant extraction method;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained plant insecticide.
5. the preparation method of plant insecticide according to claim 4, it is characterized in that, the condition that the extraction method of ultrasonic assistant described in step S1 extracts liquid is: ultrasonic power is 140-180W, concentration of alcohol is 55%-75%, Extracting temperature is 55-65 DEG C, and extraction time is 90-120min.
6. the preparation method of plant insecticide according to claim 4, is characterized in that, step S2 herb liquid filters, and is concentrated into water content≤25%.
7. the preparation method of plant insecticide according to claim 4, is characterized in that, in step S2, mixture B is dried to water content≤6% at 90-100 DEG C.
8. the preparation method of plant insecticide according to claim 4, is characterized in that, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
9. the preparation method of plant insecticide according to claim 4, is characterized in that, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
10. the application of the plant insecticide according to any one of claim 1-3 in one or more plant insects of control looper, two spotted spider mite, long white a red-spotted lizard, leaf miner.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107691506A (en) * | 2016-08-08 | 2018-02-16 | 庞锦霞 | A kind of aconite root vegetable insecticide and preparation method thereof |
CN108477235A (en) * | 2018-04-28 | 2018-09-04 | 芜湖扬展新材料科技服务有限公司 | A kind of plant pesticide |
CN108684736A (en) * | 2018-04-28 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | Plant pesticide |
CN110250228A (en) * | 2019-05-13 | 2019-09-20 | 台州煜农生物科技有限公司 | A kind of plant insecticide and preparation method |
CN110786348A (en) * | 2019-07-24 | 2020-02-14 | 邓必南 | Nontoxic sterile pollution-free insect-resist agent beneficial to growth of plants and vegetables |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107691506A (en) * | 2016-08-08 | 2018-02-16 | 庞锦霞 | A kind of aconite root vegetable insecticide and preparation method thereof |
CN108477235A (en) * | 2018-04-28 | 2018-09-04 | 芜湖扬展新材料科技服务有限公司 | A kind of plant pesticide |
CN108684736A (en) * | 2018-04-28 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | Plant pesticide |
CN110250228A (en) * | 2019-05-13 | 2019-09-20 | 台州煜农生物科技有限公司 | A kind of plant insecticide and preparation method |
CN110786348A (en) * | 2019-07-24 | 2020-02-14 | 邓必南 | Nontoxic sterile pollution-free insect-resist agent beneficial to growth of plants and vegetables |
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