CN105532767A - Insecticide, preparation method and application thereof - Google Patents
Insecticide, preparation method and application thereof Download PDFInfo
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- CN105532767A CN105532767A CN201510937673.4A CN201510937673A CN105532767A CN 105532767 A CN105532767 A CN 105532767A CN 201510937673 A CN201510937673 A CN 201510937673A CN 105532767 A CN105532767 A CN 105532767A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/38—Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses an insecticide, a preparation method and an application thereof, and belongs to the field of preparation technology of insecticide. The insecticide comprises the following raw materials in parts by weight: arborvitae leaves, mints, lettuces, Anabasis aphylla, paulownia leaves, Sophora alopecuroides, wormwood, ginger dioscorea, aloes, Azadirachta Indica, ash barks, flavescent sophora roots, Euphorbia soongarica, tea tree leaves, datura, pyrethrum, capsicum, sabadilla, tobacco, Chinese ash leaves, and water; the insecticide is prepared by the following steps: extraction, condensation, drying, crushing, sieving, disinfection, etc. The insecticide does not have toxic components, residuals, and pollution, and is green and environmentally friendly; the insecticide has the advantages of simple production method, low cost and good application effects; the insecticide can be used for effectively controlling blister mite, Parlatoria pergandii, long-horned beetles, chitinozoans and other plant insects, one-time killing rate reaches above 96.14%, and the insects do not have drug resistance.
Description
Technical field
The invention belongs to insecticide preparing technical field, be specifically related to a kind of insecticide, preparation method and application thereof.
Background technology
Current control pest all use chemical insecticide mostly, along with the raising of living standards of the people, require high, not only will eat, and will eat health agricultural product quality.The Pesticide Residue that high malicious chemical pesticide causes more and more becomes the focus of social concerns.High-toxic pesticide is the core and the key that affect agricultural product quality and safety, not only affects agricultural product quality, directly endangers the healthy of the people, also affects increasing peasant income.Because the toxicity of high-toxic pesticide is large, the event of person poultry poisoning was caused to happen occasionally in the past.Very big on the impact of women and children, the children that teratogenesis is disabled are a lot.In addition, along with the protective awareness of countries in the world to environment for human survival and natural, ecological strengthens day by day, high malicious high residue insecticide will be restricted further.The quality safety of unreasonable use to agricultural product of agricultural chemicals constitutes a threat to, therefore, reduce Pesticide use particularly high-toxic pesticide use, to raising agricultural product quality and the market competitiveness, promote China's agricultural sustainable development, ensure the life security of broad masses of the people and very great meaning of building a harmonious society.
Because chemical pesticide is easy to the pesticide resistance causing insect; dosage is made in order to control efficiency well constantly increases; a lot of natural enemy and beneficial organism are murdered; and pollute us and to depend on for existence living environment; the more and more attention of Environmental protection; will be further strict to the Detecting Pesticide in agricultural product, therefore, greatly develop the direction that non-toxic and non-pollution high-efficiency plant source pesticide is Agrochemicals from now on.
Summary of the invention
The invention provides a kind of insecticide, preparation method and application thereof, use chemical pesticide control insect to cause the problem such as pest resistance to insecticide and contaminated environment to solve, insecticide ingredient of the present invention is nontoxic, and noresidue is nuisanceless, environmental protection; Insecticide production method of the present invention is simple, and cost is low, and effect is good; Insecticide of the present invention effectively can prevent and treat the plant insects such as blister mite, chaff sheet a red-spotted lizard, longicorn, several Tintinnids, and one time killing rate all reaches more than 96.14%, and does not have drug resistance.
For solving above technical problem, the present invention by the following technical solutions:
A kind of insecticide, in units of weight portion, comprise following raw material: cacumen biotae 30-60 part, peppermint 30-60 part, lettuce 30-60 part, Herba Anabasis aphyllae 30-40 part, paulownia leaves 30-40 part, Sophora alopecuroide 30-40 part, absinth 20-30 part, yellow ginger 20-30 part, aloe 20-30 part, print chinaberry 20-25 part, bark of ash 20-25 part, kuh-seng 20-25 part, Roots of Euphorbia soongarica 20-25 part, tea free 10-20 part, datura 10-20 part, Dalmatian chrysanthemum 10-20 part, capsicum 10-20 part, sabadilla 10-20 part, tobacco 6-16 part, leaf of Pterocarya Stenoptera 6-16 part, water 1500-6500 part.
Preferably, described insecticide, in units of weight portion, comprise following raw material: cacumen biotae 40-50 part, peppermint 40-50 part, lettuce 40-50 part, Herba Anabasis aphyllae 32-38 part, paulownia leaves 32-38 part, Sophora alopecuroide 32-38 part, absinth 22-28 part, yellow ginger 22-28 part, aloe 22-28 part, print chinaberry 22-24 part, bark of ash 22-24 part, kuh-seng 22-24 part, Roots of Euphorbia soongarica 22-24 part, tea free 12-18 part, datura 12-18 part, Dalmatian chrysanthemum 12-18 part, capsicum 12-18 part, sabadilla 12-18 part, tobacco 8-14 part, leaf of Pterocarya Stenoptera 8-14 part, water 2500-5500 part.
Preferably, described insecticide, in units of weight portion, comprise following raw material: cacumen biotae 45 parts, peppermint 45 parts, 45 parts, lettuce, Herba Anabasis aphyllae 35 parts, paulownia leaves 35 parts, Sophora alopecuroide 35 parts, absinth 25 parts, yellow ginger 25 parts, aloe 25 parts, print chinaberry 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 22 parts, tea free 15 parts, datura 15 parts, Dalmatian chrysanthemum 15 parts, 15 parts, capsicum, sabadilla 15 parts, tobacco 10 parts, leaf of Pterocarya Stenoptera 10 parts, 4000 parts, water.
The present invention also provides a kind of method for producing insecticide, comprises the following steps:
S1: by cacumen biotae, peppermint, lettuce, Herba Anabasis aphyllae, paulownia leaves, Sophora alopecuroide, absinth, yellow ginger, aloe, print chinaberry, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, tea free, datura, Dalmatian chrysanthemum, capsicum, sabadilla, tobacco, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140-180W, concentration of alcohol is 55%-75%, Extracting temperature is 55-65 DEG C, and extraction time is 30-50min;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained insecticide.
Preferably, step S2 herb liquid filters, and is concentrated into water content≤25%.
Preferably, in step S2, mixture B is dry at 90-100 DEG C.
More preferably, described mixture B is dried to water content≤6% at 90-100 DEG C.
Preferably, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
Preferably, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
The application of described insecticide in one or more plant insects of control blister mite, chaff sheet a red-spotted lizard, longicorn, a few Tintinnid.
Pharmacology of the present invention is as follows:
Containing volatile oil, flavones, tannic acid and tannin class phenolic constituent in cacumen biotae, there is the effects such as anti-inflammatory, anti-oxidant, hemostasis, antibacterial desinsection.
Peppermint has the effects such as desinsection, antibacterial, sterilization, anti-inflammatory, has stronger inhibitory action to shigella dysenteriae, typhoid bacillus and Escherichia coli.
Lettuce profit the five internal organs, qualcomm meridian, diuresis, improving eyesight sharps teeth, promoting lactation, hard muscles and bones, has the effect of antibacterial desinsection.
Herba Anabasis aphyllae belongs to chenopod, is dicotyledon, has the effects such as clearing heat and detoxicating, anti-inflammation, pain relieving desinsection, can be used for rural area preparation agricultural chemicals of eliminating the four pests--rats, bedbugs, flies and mosquitoes, the use of disinfestation and deratization.
Paulownia leaves extract has antibacterial and antivirus action, propyl alcohol extract all has antibacterial activity, In vitro Bactericidal Experiments proves, paulownia leaves extract is stronger to staphylococcus aureus, hay bacillus effect, extract panlownin and sesamin, kill insect (fly, the mosquito etc.) effect of this binary to pyrethrins and allyl cinerin has synergistic effect.
The total alkaloid of sophora alopecuroide extracted in Sophora alopecuroide has anti-inflammatory, anticancer, antiallergic action, anti-arrhythmia cordis, antiulcer, increasing leukocyte, relievings asthma, antipyretic, desinsection, calmness, analgesia, the effect such as antiviral; The external application of Sophora alopecuroide powder has suppression or killing action to staphylococcus, Escherichia coli, streptococcus, fungi, bacterium protein of Gardnerella vaginalis and trichomonad; The killing ability of Sophora alopecuroide plant is between anabasine (Anadasine) and lupinine (Lupinine), and sparteine is Biocidal agriculture the effective elements of the medicine.
Absinth bitter, cold in nature, poisonous, there is heat-clearing and damp-drying drug, drive ascarid, stomach invigorating, the effect such as antibacterial desinsection, all have suppression and killing action to multiple coccus, bacillus, fungi and virus etc.
Turmeric extractive shows certain repellent to multiple grain storage pest, desert locusts and mythimna separata etc., fumigates, tags, stomach toxicity, growth inhibition or oviposition deterrence isoreactivity; Meanwhile, to some agriculture germs, there is very strong bactericidal action.
Aloe contains the multiple nutritional components such as lignin, aloietic acid, saponin, anthraquinone, aloin, vitamin, oxidase, lipase, amylase, lysine, leucine, threonine, isoleucine, phenyl alanine, valine.Extract component tinctura aloes in aloe is the material that antibiotic property is very strong, the germs such as energy killing fungus, mould, bacterium, virus, the growth breeding of suppression and eliminating pathogen, the germ class of aloe antibiotic sterilization has: the germ of the diseases such as diphtheria bacterium, tetanolysin, pulmonitis strain, lactic acid bacteria, dysentery bacillus, colon bacillus, plague bacterium, cholera bacteria and initiation tympanitis, cystitis, pyesis, measles, rabies, polio, epidemic encephalitis.
Print Melia, in Meliaceae, comes from Southeast Asia, and containing print chinaberry, solannin etc., have good disinsection efficiency, insect is once contact, and growth will be suppressed.
The bark of ash has antibacterial insecticidal action, has obvious inhibitory action, be usually used in controlling bacillary dysentery clinically to staphylococcus aureus, bacillus subtilis, Escherichia coli, brewer's yeast, bacterium wine yeast etc., enteritis, leukorrhea, chronic bronchitis, red eye, swell pain etc.
Kuh-seng belongs to herbaceos perennial; Be taken as the substitute of monkshood and radix aconiti agrestis at the Northwest's kuh-seng and use, simultaneously the traditional medicine of the ethnic group such as Ye Shi Kazak, the Hui ethnic group, is mainly used in pain relieving, dehumidifying, cold-dispelling.
Roots of Euphorbia soongarica is herbaceos perennial, main product in Gansu, the ground such as Xinjiang and Russia, the substitute in new thick area as the root of Beijing euphorbia uses, and has effect of removing water retention by purgation, dispersing swelling and dissipating binds.
The extract of tea free has potent bactericidal action, and tea tree can effectively tackle for various mycotic infection, can kill staphylococcus aureus, diphtheria bacillus.
Datura is botanical pesticide, has extremely strong sterilization, insecticidal action.
Dalmatian chrysanthemum containing 4 kinds of insecticidal constituents, pyrethrin (pyrethrin) I, II and cinerin (cinerin) I, II, Dalmatian chrysanthemum to various insects as mosquito, fly, bedbug and cockroach etc. have toxic action.
Capsicum can alleviate chest abdomen crymodynia, prevents dysentery, kills and presses down stomach abdomen entozoa, controls cardiopathy and coronary sclerosis, the function such as have sterilization, anticorrosion, seasoning, nutrition, dispel cold.
Sabadilla is Melanthiaceae perennial plant, and extract has insecticidal properties, may be used for that jumping is disturbed, fall army worm, louse, thrips, fleahopper and cockroach etc.
Tobacco has the effects such as promoting qi circulation and relieving pain, eliminating dampness, detumescence, removing toxic substances desinsection.
Chinese ash has the effects such as antibacterial, desinsection, removing toxic substances, and leaf is poisonous, can used as pesticides insecticide.
The present invention has following beneficial effect:
(1) insecticide ingredient of the present invention is nontoxic, and noresidue is nuisanceless, environmental protection, can not bring environmental pollution;
(2) insecticide of the present invention effectively can prevent and treat the plant insects such as blister mite, chaff sheet a red-spotted lizard, longicorn, several Tintinnids, and one time killing rate all reaches more than 96.14%, and does not have resistance to medical, can use by 4-6;
(3) insecticide production method of the present invention is simple, and cost is low, easy to use, and effect is good, is conducive to applying.
Embodiment
Be specifically described below in conjunction with specific embodiment.
Embodiment 1
A kind of insecticide, in units of weight portion, comprise following raw material: cacumen biotae 30 parts, peppermint 30 parts, 30 parts, lettuce, Herba Anabasis aphyllae 30 parts, paulownia leaves 30 parts, Sophora alopecuroide 30 parts, absinth 20 parts, yellow ginger 20 parts, aloe 20 parts, print chinaberry 20 parts, the bark of ash 20 parts, kuh-seng 20 parts, Roots of Euphorbia soongarica 20 parts, tea free 10 parts, datura 10 parts, Dalmatian chrysanthemum 10 parts, 10 parts, capsicum, sabadilla 10 parts, tobacco 6 parts, leaf of Pterocarya Stenoptera 6 parts, 1500 parts, water.
Described method for producing insecticide, comprises the following steps:
S1: by cacumen biotae, peppermint, lettuce, Herba Anabasis aphyllae, paulownia leaves, Sophora alopecuroide, absinth, yellow ginger, aloe, print chinaberry, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, tea free, datura, Dalmatian chrysanthemum, capsicum, sabadilla, tobacco, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140W, concentration of alcohol is 55%, and Extracting temperature is 55 DEG C, and extraction time is 50min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 25%, and obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, pressure is sterilizing 5min under 210KPa, obtained insecticide.
Embodiment 2
A kind of insecticide, in units of weight portion, comprise following raw material: cacumen biotae 60 parts, peppermint 60 parts, 60 parts, lettuce, Herba Anabasis aphyllae 40 parts, paulownia leaves 40 parts, Sophora alopecuroide 40 parts, absinth 30 parts, yellow ginger 30 parts, aloe 30 parts, print chinaberry 25 parts, the bark of ash 25 parts, kuh-seng 25 parts, Roots of Euphorbia soongarica 25 parts, tea free 20 parts, datura 20 parts, Dalmatian chrysanthemum 20 parts, 20 parts, capsicum, sabadilla 20 parts, tobacco 16 parts, leaf of Pterocarya Stenoptera 16 parts, 6500 parts, water.
Described method for producing insecticide, comprises the following steps:
S1: by cacumen biotae, peppermint, lettuce, Herba Anabasis aphyllae, paulownia leaves, Sophora alopecuroide, absinth, yellow ginger, aloe, print chinaberry, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, tea free, datura, Dalmatian chrysanthemum, capsicum, sabadilla, tobacco, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 180W, concentration of alcohol is 75%, and Extracting temperature is 65 DEG C, and extraction time is 30min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 18%, and obtain mixture B, it is 4% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained insecticide.
Embodiment 3
A kind of insecticide, in units of weight portion, comprise following raw material: cacumen biotae 45 parts, peppermint 45 parts, 45 parts, lettuce, Herba Anabasis aphyllae 35 parts, paulownia leaves 35 parts, Sophora alopecuroide 35 parts, absinth 25 parts, yellow ginger 25 parts, aloe 25 parts, print chinaberry 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 22 parts, tea free 15 parts, datura 15 parts, Dalmatian chrysanthemum 15 parts, 15 parts, capsicum, sabadilla 15 parts, tobacco 10 parts, leaf of Pterocarya Stenoptera 10 parts, 4000 parts, water.
Described method for producing insecticide, comprises the following steps:
S1: by cacumen biotae, peppermint, lettuce, Herba Anabasis aphyllae, paulownia leaves, Sophora alopecuroide, absinth, yellow ginger, aloe, print chinaberry, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, tea free, datura, Dalmatian chrysanthemum, capsicum, sabadilla, tobacco, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 65%, and Extracting temperature is 60 DEG C, and extraction time is 40min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 135 DEG C in temperature, pressure is sterilizing 4min under 220KPa, obtained insecticide.
Embodiment 4
A kind of insecticide, in units of weight portion, comprise following raw material: cacumen biotae 40 parts, peppermint 40 parts, 40 parts, lettuce, Herba Anabasis aphyllae 32 parts, paulownia leaves 32 parts, Sophora alopecuroide 32 parts, absinth 22 parts, yellow ginger 22 parts, aloe 22 parts, print chinaberry 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 22 parts, tea free 12 parts, datura 12 parts, Dalmatian chrysanthemum 12 parts, 12 parts, capsicum, sabadilla 12 parts, tobacco 8 parts, leaf of Pterocarya Stenoptera 8 parts, 2500 parts, water.
Described method for producing insecticide, comprises the following steps:
S1: by cacumen biotae, peppermint, lettuce, Herba Anabasis aphyllae, paulownia leaves, Sophora alopecuroide, absinth, yellow ginger, aloe, print chinaberry, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, tea free, datura, Dalmatian chrysanthemum, capsicum, sabadilla, tobacco, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 150W, concentration of alcohol is 60%, and Extracting temperature is 55 DEG C, and extraction time is 45min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 22%, and obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, pressure is sterilizing 5min under 210KPa, obtained insecticide.
Embodiment 5
A kind of insecticide, in units of weight portion, comprise following raw material: cacumen biotae 50 parts, peppermint 50 parts, 50 parts, lettuce, Herba Anabasis aphyllae 38 parts, paulownia leaves 38 parts, Sophora alopecuroide 38 parts, absinth 28 parts, yellow ginger 28 parts, aloe 28 parts, print chinaberry 24 parts, the bark of ash 24 parts, kuh-seng 24 parts, Roots of Euphorbia soongarica 24 parts, tea free 18 parts, datura 18 parts, Dalmatian chrysanthemum 18 parts, 18 parts, capsicum, sabadilla 18 parts, tobacco 14 parts, leaf of Pterocarya Stenoptera 14 parts, 5500 parts, water.
Described method for producing insecticide, comprises the following steps:
S1: by cacumen biotae, peppermint, lettuce, Herba Anabasis aphyllae, paulownia leaves, Sophora alopecuroide, absinth, yellow ginger, aloe, print chinaberry, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, tea free, datura, Dalmatian chrysanthemum, capsicum, sabadilla, tobacco, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 170W, concentration of alcohol is 70%, and Extracting temperature is 65 DEG C, and extraction time is 35min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained insecticide.
Embodiment 6
A kind of insecticide, in units of weight portion, comprise following raw material: cacumen biotae 55 parts, peppermint 55 parts, 55 parts, lettuce, Herba Anabasis aphyllae 35 parts, paulownia leaves 35 parts, Sophora alopecuroide 35 parts, absinth 25 parts, yellow ginger 25 parts, aloe 25 parts, print chinaberry 24 parts, the bark of ash 24 parts, kuh-seng 24 parts, Roots of Euphorbia soongarica 24 parts, tea free 18 parts, datura 18 parts, Dalmatian chrysanthemum 18 parts, 18 parts, capsicum, sabadilla 18 parts, tobacco 15 parts, leaf of Pterocarya Stenoptera 15 parts, 6000 parts, water.
Described method for producing insecticide, comprises the following steps:
S1: by cacumen biotae, peppermint, lettuce, Herba Anabasis aphyllae, paulownia leaves, Sophora alopecuroide, absinth, yellow ginger, aloe, print chinaberry, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, tea free, datura, Dalmatian chrysanthemum, capsicum, sabadilla, tobacco, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 70%, and Extracting temperature is 60 DEG C, and extraction time is 45min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 23%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained insecticide.
For verifying the effect of insecticide of the present invention, by following experimental verification.
Adopt the insecticide of embodiment 1-6, the ratio of joining 40g water in 1g insecticide uses, and once prevents and treats the test of the plant insects such as blister mite, chaff sheet a red-spotted lizard, longicorn, several Tintinnids, the results are shown in following table.
From upper table, the insecticide of embodiment of the present invention 1-6 is to a killing rate of the plant insects such as blister mite, chaff sheet a red-spotted lizard, longicorn, several Tintinnids all more than 96.14%, and result of use is good.Due to insecticide nonhazardous of the present invention, do not pollute, do not remain, it is efficient to add control efficiency, therefore, can widely popularize application.
Above content can not assert that the present invention specifically implements to be confined to these explanations; for general technical staff of the technical field of the invention; do not departing under concept thereof of the present invention; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted to claims.
Claims (10)
1. an insecticide, it is characterized in that, in units of weight portion, comprise following raw material: cacumen biotae 30-60 part, peppermint 30-60 part, lettuce 30-60 part, Herba Anabasis aphyllae 30-40 part, paulownia leaves 30-40 part, Sophora alopecuroide 30-40 part, absinth 20-30 part, yellow ginger 20-30 part, aloe 20-30 part, print chinaberry 20-25 part, bark of ash 20-25 part, kuh-seng 20-25 part, Roots of Euphorbia soongarica 20-25 part, tea free 10-20 part, datura 10-20 part, Dalmatian chrysanthemum 10-20 part, capsicum 10-20 part, sabadilla 10-20 part, tobacco 6-16 part, leaf of Pterocarya Stenoptera 6-16 part, water 1500-6500 part.
2. insecticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: cacumen biotae 40-50 part, peppermint 40-50 part, lettuce 40-50 part, Herba Anabasis aphyllae 32-38 part, paulownia leaves 32-38 part, Sophora alopecuroide 32-38 part, absinth 22-28 part, yellow ginger 22-28 part, aloe 22-28 part, print chinaberry 22-24 part, bark of ash 22-24 part, kuh-seng 22-24 part, Roots of Euphorbia soongarica 22-24 part, tea free 12-18 part, datura 12-18 part, Dalmatian chrysanthemum 12-18 part, capsicum 12-18 part, sabadilla 12-18 part, tobacco 8-14 part, leaf of Pterocarya Stenoptera 8-14 part, water 2500-5500 part.
3. insecticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: cacumen biotae 45 parts, peppermint 45 parts, 45 parts, lettuce, Herba Anabasis aphyllae 35 parts, paulownia leaves 35 parts, Sophora alopecuroide 35 parts, absinth 25 parts, yellow ginger 25 parts, aloe 25 parts, print chinaberry 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 22 parts, tea free 15 parts, datura 15 parts, Dalmatian chrysanthemum 15 parts, 15 parts, capsicum, sabadilla 15 parts, tobacco 10 parts, leaf of Pterocarya Stenoptera 10 parts, 4000 parts, water.
4. the method for producing insecticide according to any one of claim 1-3, is characterized in that, comprises the following steps:
S1: by cacumen biotae, peppermint, lettuce, Herba Anabasis aphyllae, paulownia leaves, Sophora alopecuroide, absinth, yellow ginger, aloe, print chinaberry, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, tea free, datura, Dalmatian chrysanthemum, capsicum, sabadilla, tobacco, leaf of Pterocarya Stenoptera co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140-180W, concentration of alcohol is 55%-75%, Extracting temperature is 55-65 DEG C, and extraction time is 30-50min;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained insecticide.
5. method for producing insecticide according to claim 4, is characterized in that, step S2 herb liquid filters, and is concentrated into water content≤25%.
6. method for producing insecticide according to claim 4, is characterized in that, in step S2, mixture B is dry at 90-100 DEG C.
7. method for producing insecticide according to claim 6, is characterized in that, described mixture B is dried to water content≤6% at 90-100 DEG C.
8. method for producing insecticide according to claim 4, is characterized in that, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
9. method for producing insecticide according to claim 4, is characterized in that, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
10. the application of the insecticide according to any one of claim 1-3 in one or more plant insects of control blister mite, chaff sheet a red-spotted lizard, longicorn, a few Tintinnid.
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| CN106212578A (en) * | 2016-07-29 | 2016-12-14 | 广西素安生态农业有限公司 | A kind of herbal control agent of Flos Jasmini Sambac ash curculionid and preparation method thereof |
| CN106234481A (en) * | 2016-07-29 | 2016-12-21 | 广西素安生态农业有限公司 | A kind of Chinese herbal medicine pesticide of Flos Jasmini Sambac and preparation method thereof |
| CN106417401A (en) * | 2016-10-31 | 2017-02-22 | 郑州思辩科技有限公司 | Botanical pesticide for preventing and treating diseases and insect pests of tea trees |
| CN106508987A (en) * | 2016-10-21 | 2017-03-22 | 赖丰光 | Pesticide fertilizer for controlling diamondback moth |
| CN107624810A (en) * | 2017-09-02 | 2018-01-26 | 赖丰光 | A kind of Pesticidal combination |
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| CN107873360A (en) * | 2017-11-16 | 2018-04-06 | 广西壮族自治区畜牧研究所 | A kind of interplanting method of purple napier grass and mulberry tree |
| CN108703160A (en) * | 2018-07-11 | 2018-10-26 | 合肥雪立歆农业科技有限公司 | The preparation method of one vegetative insecticide |
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| CN106212578A (en) * | 2016-07-29 | 2016-12-14 | 广西素安生态农业有限公司 | A kind of herbal control agent of Flos Jasmini Sambac ash curculionid and preparation method thereof |
| CN106234481A (en) * | 2016-07-29 | 2016-12-21 | 广西素安生态农业有限公司 | A kind of Chinese herbal medicine pesticide of Flos Jasmini Sambac and preparation method thereof |
| CN106508987A (en) * | 2016-10-21 | 2017-03-22 | 赖丰光 | Pesticide fertilizer for controlling diamondback moth |
| CN106417401A (en) * | 2016-10-31 | 2017-02-22 | 郑州思辩科技有限公司 | Botanical pesticide for preventing and treating diseases and insect pests of tea trees |
| CN107624810A (en) * | 2017-09-02 | 2018-01-26 | 赖丰光 | A kind of Pesticidal combination |
| CN107711317A (en) * | 2017-11-16 | 2018-02-23 | 广西壮族自治区畜牧研究所 | A kind of interplanting method of purple napier grass and eucalyptus |
| CN107873360A (en) * | 2017-11-16 | 2018-04-06 | 广西壮族自治区畜牧研究所 | A kind of interplanting method of purple napier grass and mulberry tree |
| CN108703160A (en) * | 2018-07-11 | 2018-10-26 | 合肥雪立歆农业科技有限公司 | The preparation method of one vegetative insecticide |
| WO2020180280A1 (en) * | 2019-03-01 | 2020-09-10 | Hi-Ag Group, Ltd. | Plant and soil amendment composition and method |
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