CN102428972B - Liquidd mosquito-repellent incense made of folium artemisiae argyi and preparation method thereof - Google Patents
Liquidd mosquito-repellent incense made of folium artemisiae argyi and preparation method thereof Download PDFInfo
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- CN102428972B CN102428972B CN2011103103294A CN201110310329A CN102428972B CN 102428972 B CN102428972 B CN 102428972B CN 2011103103294 A CN2011103103294 A CN 2011103103294A CN 201110310329 A CN201110310329 A CN 201110310329A CN 102428972 B CN102428972 B CN 102428972B
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
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- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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Abstract
The invention discloses liquid mosquito-repellent incense made of folium artemisiae argyi and a preparation method thereof. The liquid mosquito-repellent incense made of the folium artemisiae argyi is formed by mixing the following components by weight in parts: 100 parts of n-tetracosane, 1-3 parts of concentrated liquid of traditional Chinese medicine compound and 0.03-0.06 parts of piperomyl butoxide. The method for preparing the concentrated liquid of the traditional Chinese medicine compound comprises the following steps: weighting the following traditional Chinese medicine components by weight in parts: 70-80 parts of the folium artemisiae argyi, 20-25 parts of artemisiacapillaris thunb, 3-6 parts of daphne genkwa, 1-3 parts of ferulae, 15-25 parts of ulmus pumila skins, 1-3 parts of santalum album, 4-6 parts of aquilaria agallocha, 1-3 parts of crocus sativus, 2-4 parts of veratrum nigrum and 0.5-1.5 parts of codonopsis pilosula; crushing and uniformly mixing these materials to obtain the traditional Chinese medicine compound; adding water to the traditional Chinese medicine compound; decocting the traditional Chinese medicine compound at 70-90 DEG C for 0.5-2.5 hours; filtering and concentrating the traditional Chinese medicine compound to obtain the concentrated liquid of the traditional Chinese medicine compound. The liquid mosquito-repellent incense made of folium artemisiae argyi provided by the invention has strong expelling and killing actions for mosquitoes and has no adverse effects for human bodies.
Description
Technical field
The present invention relates to a kind of vaporizer mosquito liquid and preparation method thereof, relate in particular to a kind of Liquidd mosquito and preparation method thereof.
Background technology
Mosquito-repellent incense is a kind of mosquito repellent thing, and medicine is wherein lighted the rear cigarette that sends can drive mosquito or smoked dead mosquito away.China's very long history that kindles mosquito repellent incense, traditional mosquito-repellent incense divides line spices, incense coil and vaporizer mosquito liquid.
Vaporizer mosquito liquid be mainly a kind of chemical composition that is called pyrethroid, cinerins can pass through digestive tract, respiratory tract and absorb, and certain toxicity is arranged, if long-term excessive contact has carcinogenic, teratogenesis.
Summary of the invention
For above shortcomings in prior art, one of technical problem to be solved by this invention provides a kind of Liquidd mosquito, and mosquito is had the stronger effect of killing, and can not produce harmful effect to human body.
Two of technical problem to be solved by this invention is to provide above-mentioned Liquidd mosquito and preparation method thereof.
The present invention seeks to be achieved through the following technical solutions:
A kind of Liquidd mosquito is mixed by weight by following component: 100 parts of positive structure tetradecane hydrocarbon, and Chinese medicine composition concentrate 1-3 part, piperonyl butoxide 0.03-0.06 part,
Wherein, described Chinese medicine composition concentrate is prepared from by following method:
(1) take each traditional Chinese medicinal components of following weight parts: tarragon 70-80 part, oriental wormwood 20-25 part, lilac daphne 3-6 part, asafoetide 1-3 part, elm bark 15-25 part, santal 1-3 part, agalloch eaglewood 4-6 part, west safflower 1-3 part, black false hellebore 2-4 part and Radix Codonopsis 0.5-1.5 part, pulverize, mix, obtain Chinese medicine composition;
(2) water is added in above-mentioned Chinese medicine composition, the addition of water is 6-8 times of Chinese medicine composition gross weight, decocts 0.5-2.5 hour in 70-90 ℃, filter, concentrated, obtain the Chinese medicine composition concentrate, the weight of described Chinese medicine composition concentrate is 1-3 times of Chinese medicine composition gross weight.
Further, the present invention also provides a kind of preparation method of Liquidd mosquito, is comprised of following step:
(1) take each traditional Chinese medicinal components of following weight parts: tarragon 70-80 part, oriental wormwood 20-25 part, lilac daphne 3-6 part, asafoetide 1-3 part, elm bark 15-25 part, santal 1-3 part, agalloch eaglewood 4-6 part, west safflower 1-3 part, black false hellebore 2-4 part and Radix Codonopsis 0.5-1.5 part, pulverize, mix, obtain Chinese medicine composition;
(2) water is added in above-mentioned Chinese medicine composition, the addition of water is 6-8 times of Chinese medicine composition gross weight, decocts 0.5-2.5 hour in 70-90 ℃, filter, concentrated, obtain the Chinese medicine composition concentrate, the weight of described Chinese medicine composition concentrate is 1-3 times of Chinese medicine composition gross weight;
(3) the positive structure tetradecane hydrocarbon of 100 weight portions, the above-mentioned Chinese medicine composition concentrate of 1-3 weight portion and the piperonyl butoxide of 0.03-0.06 weight portion are mixed, can make Liquidd mosquito of the present invention.
Concrete, in the present invention,
Tarragon is the dried leaves of feverfew Chinese mugwort.Be recorded in an one-61 of Pharmacopoeia of the People's Republic of China version in 2005.
Oriental wormwood, this product are the dry aerial parts of feverfew shore wormwood artemisia or Artemisia capillaris.Be recorded in an one-166 of Pharmacopoeia of the People's Republic of China version in 2005.
Lilac daphne is the dry flower of Isolated From Thymelaeaceae Species lilac daphne.Be recorded in an one-109 of Pharmacopoeia of the People's Republic of China version in 2005.
Asafoetide is the resin of samphire Ferula sinkiangensis or Ferula fukanensis K.M.Shen.Be recorded in an one-131 of Pharmacopoeia of the People's Republic of China version in 2005.
Elm bark is dry bark or the root skin of Ulmaceae elm.Be recorded in " the colored atlas of practical Chinese herbal medicine " the 4th, Nationalities Press's " hiding Chinese voluminous dictionary " version in 1985.
Santal is the heartwood of Santalaceae plant santal trunk.Be recorded in an one-264 of Pharmacopoeia of the People's Republic of China version in 2005.
Agalloch eaglewood contains the timber of resin for the Isolated From Thymelaeaceae Species suspension culture of Aquilaria sinensis.Be recorded in an one-128 of Pharmacopoeia of the People's Republic of China version in 2005.
West safflower is the dry column cap of irides Crocus sativus.Be recorded in an one-86 of Pharmacopoeia of the People's Republic of China version in 2005.
Black false hellebore (formal name used at school: the Veratrum nigrum L.) plant of Liliaceae Veratrum, perennial herb.Effect: clearing heat and detoxicating, desinsection.Also many places are on the books in one one of Pharmacopoeia of the People's Republic of China version in 2005.
Radix Codonopsis is the dry root of Campanulaceae Radix Codonopsis, element flower Radix Codonopsis or radix codonpsis tangshen.Be recorded in an one-199 of Pharmacopoeia of the People's Republic of China version in 2005.
Mosquito repellent component of the present invention is made by the wild Chinese herbal medicine fully, the smell that distributes in vaporizer mosquito liquid heating process can suppress, the kill virus germ, the prevention respiratory disease, strengthen immune function of human body, mosquito killer, fresh air, more crucial is to use for a long time the present invention to produce harmful effect to human body.
Especially, particularly point out in one one of Pharmacopoeia of the People's Republic of China version in 2005: Radix Codonopsis should not be with black false hellebore with using.Yet find through after the inventor great many of experiments, add simultaneously Radix Codonopsis and black false hellebore not only can increase repelling effect in vaporizer mosquito liquid, and can't produce harmful effect to human body.
Experimental results show that, the present invention has certain inhibition, killing action to multiple germs such as gold look staphylococcus, shigella dysenteriae, tubercle bacillus, Pseudomonas aeruginosa, bacillus anthracis, hepatitis bacillus, particularly the virus and bacteria for the epidemic infection disease has very strong insect killing effect, and mosquito is had the stronger effect of killing.
Embodiment
Embodiment 1:
(1) take following each traditional Chinese medicinal components: tarragon 70 grams, oriental wormwood 25 grams, lilac daphne 3 grams, asafoetide 3 grams, elm bark 15 grams, santal 3 grams, agalloch eaglewood 4 grams, west safflower 3 grams, black false hellebore 2 grams and Radix Codonopsis 1.5 grams, pulverize, mix, obtain Chinese medicine composition;
(2) 780 gram water are added in above-mentioned Chinese medicine composition in 90 ℃ and decocted 0.5 hour, filter, concentrated, obtain 388 gram Chinese medicine composition concentrates;
(3) the positive structure tetradecane hydrocarbon of 100 grams, the above-mentioned Chinese medicine composition concentrate of 1 gram and the piperonyl butoxide of 0.06 gram are mixed, can make Liquidd mosquito of the present invention.
Embodiment 2:
(1) take each traditional Chinese medicinal components of following gram: tarragon 80 grams, oriental wormwood 20 grams, lilac daphne 6 grams, asafoetide 1 gram, elm bark 25 grams, santal 1 gram, agalloch eaglewood 6 grams, west safflower 1 gram, black false hellebore 4 grams and Radix Codonopsis 0.5 gram, pulverize, mix, obtain Chinese medicine composition;
(2) 1150 gram water are added in above-mentioned Chinese medicine composition, in 70 ℃ of decoctions 2.5 hours, filter, concentrated, obtain 145 gram Chinese medicine composition concentrates;
(3) the positive structure tetradecane hydrocarbon of 100 grams, the above-mentioned Chinese medicine composition concentrate of 3 grams and the piperonyl butoxide of 0.03 gram are mixed, can make Liquidd mosquito of the present invention.
Embodiment 3:
(1) take each traditional Chinese medicinal components of following gram: tarragon 75 grams, oriental wormwood 23 grams, lilac daphne 4 grams, asafoetide 2 grams, elm bark 20 grams, santal 2 grams, agalloch eaglewood 5 grams, west safflower 2 grams, black false hellebore 3 grams and Radix Codonopsis 1 gram, pulverize, mix, obtain Chinese medicine composition;
(2) 960 gram water are added in above-mentioned Chinese medicine composition, in 80 ℃ of decoctions 1.5 hours, filter, concentrated, obtain 270 gram Chinese medicine composition concentrates;
(3) the positive structure tetradecane hydrocarbon of 100 grams, the above-mentioned Chinese medicine composition concentrate of 2 grams and the piperonyl butoxide of 0.05 gram are mixed, can make Liquidd mosquito of the present invention.
Test case 1: indoor harmacological effect
Adopt GB 18418-2001 domestic sanitary desinsection articles for use electric liquid device standard, test.In this standard, it is qualified that KT50 value (boxing method)≤10 minute can be judged to.
Table 1: vaporizer mosquito liquid indoor harmacological effect table (boxing method)
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| The KT50 value | 8 minutes 11 seconds | 6 minutes 45 seconds | 7 minutes 50 seconds |
Test case 2: acute oral toxicity test
The vaporizer mosquito liquid of experiment material: embodiment 2.The rear 5 minutes activities in rats of contaminating increase, and continue about 2 minutes, and activity transfers to normally, and diet is normal, and the observation period, LD50 belonged to actual nontoxic greater than 5000 mg/kgs without death.
Test case 3: acute inhalation toxicity test
The vaporizer mosquito liquid of experiment material: embodiment 2.Rat diet activity no abnormality seen after contamination, the observation period, LD50 belonged to actual nontoxic greater than 10 gram/cubic meters without death.
Test case 4: skin patch test
The vaporizer mosquito liquid of experiment material: embodiment 2.It is 0 that experimental group erythema and oedema form the scoring sum, illustrates skin is had no stimulation.
Test case 5: eye irritant test
The acute eye irritation score index of the vaporizer mosquito liquid of embodiment 2 is 0, illustrates mucous membrane is had no stimulation.
Claims (2)
1. a Liquidd mosquito, is characterized in that, mixed by weight by following component: 100 parts of positive structure tetradecane hydrocarbon, and Chinese medicine composition concentrate 1-3 part, piperonyl butoxide 0.03-0.06 part,
Wherein, described Chinese medicine composition concentrate is prepared from by following method:
(1) take each traditional Chinese medicinal components of following weight parts: tarragon 70-80 part, oriental wormwood 20-25 part, lilac daphne 3-6 part, asafoetide 1-3 part, elm bark 15-25 part, santal 1-3 part, agalloch eaglewood 4-6 part, west safflower 1-3 part, black false hellebore 2-4 part and Radix Codonopsis 0.5-1.5 part, pulverize, mix, obtain Chinese medicine composition;
(2) water is added in above-mentioned Chinese medicine composition, the addition of water is 6-8 times of Chinese medicine composition gross weight, decocts 0.5-2.5 hour in 70-90 ℃, filter, concentrated, obtain the Chinese medicine composition concentrate, the weight of described Chinese medicine composition concentrate is 1-3 times of Chinese medicine composition gross weight.
2. the preparation method of a Liquidd mosquito, is characterized in that, is comprised of following step:
(1) take each traditional Chinese medicinal components of following weight parts: tarragon 70-80 part, oriental wormwood 20-25 part, lilac daphne 3-6 part, asafoetide 1-3 part, elm bark 15-25 part, santal 1-3 part, agalloch eaglewood 4-6 part, west safflower 1-3 part, black false hellebore 2-4 part and Radix Codonopsis 0.5-1.5 part, pulverize, mix, obtain Chinese medicine composition;
(2) water is added in above-mentioned Chinese medicine composition, the addition of water is 6-8 times of Chinese medicine composition gross weight, decocts 0.5-2.5 hour in 70-90 ℃, filter, concentrated, obtain the Chinese medicine composition concentrate, the weight of described Chinese medicine composition concentrate is 1-3 times of Chinese medicine composition gross weight;
(3) the positive structure tetradecane hydrocarbon of 100 weight portions, the above-mentioned Chinese medicine composition concentrate of 1-3 weight portion and the piperonyl butoxide of 0.03-0.06 weight portion are mixed, can make described Liquidd mosquito.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011103103294A CN102428972B (en) | 2011-09-28 | 2011-09-28 | Liquidd mosquito-repellent incense made of folium artemisiae argyi and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2011103103294A CN102428972B (en) | 2011-09-28 | 2011-09-28 | Liquidd mosquito-repellent incense made of folium artemisiae argyi and preparation method thereof |
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| CN102428972A CN102428972A (en) | 2012-05-02 |
| CN102428972B true CN102428972B (en) | 2013-05-08 |
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Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103392748B (en) * | 2013-06-29 | 2015-04-01 | 安徽榄菊日用制品有限公司 | Natural mosquito repellent incense and preparation method thereof |
| CN103931674B (en) * | 2014-04-08 | 2015-09-23 | 许银亚 | Lavender vaporizer mosquito liquid |
| CN104206446A (en) * | 2014-08-18 | 2014-12-17 | 中山市品汇创新专利技术开发有限公司 | Electric-heating liquid mosquito-repellent incense containing crocus sativus plant fragrance and preparation method thereof |
| CN104186565A (en) * | 2014-08-18 | 2014-12-10 | 中山市品汇创新专利技术开发有限公司 | Electric-heating liquid mosquito-repellent incense with natural plant fragrance of agilawood and preparation method of electric-heating liquid mosquito-repellent incense |
| CN104206445A (en) * | 2014-08-18 | 2014-12-17 | 中山市品汇创新专利技术开发有限公司 | Cortex-meliae plant mosquito-repellent incense and preparation method thereof |
| CN104206450A (en) * | 2014-08-18 | 2014-12-17 | 中山市品汇创新专利技术开发有限公司 | Electric-heating mosquito-repellent incense liquid formed by combination of traditional Chinese medicines and surfactant and preparation method |
| CN105457062A (en) * | 2015-11-30 | 2016-04-06 | 杨立志 | Traditional Chinese medicine liquid incense capable of soothing nerves and preparation method thereof |
| CN105532761A (en) * | 2016-02-17 | 2016-05-04 | 广西大学 | Folium artemisiae argyi mosquito-repellent incense and manufacturing method thereof |
| CN106954651A (en) * | 2017-03-28 | 2017-07-18 | 滁州朝昱农业科技有限公司 | A kind of pig house pest repellant containing Chinese herbal medicine and preparation method thereof |
| KR102255904B1 (en) * | 2017-11-17 | 2021-05-26 | 한국생명공학연구원 | Pest control composition comprising Codonopsis pilosula (Franch.) Nannf. extract as active ingredient |
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| CN1316185A (en) * | 2001-02-27 | 2001-10-10 | 中国科学院上海昆虫研究所 | Liquid mosquito-repellent incense soup |
| CN1356033A (en) * | 2001-12-14 | 2002-07-03 | 宋建祥 | Mosquito-repellent incense made of Chinese-medicinal herbs |
| CN1547917A (en) * | 2003-05-20 | 2004-11-24 | 王纪宪 | Mosquito-repellent incense with moxa |
| CN1593266A (en) * | 2004-07-12 | 2005-03-16 | 肖社生 | Vanilla health cigarette |
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2011
- 2011-09-28 CN CN2011103103294A patent/CN102428972B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1282514A (en) * | 1999-07-30 | 2001-02-07 | 杨兵生 | Mosquito-repellent incense |
| CN1316185A (en) * | 2001-02-27 | 2001-10-10 | 中国科学院上海昆虫研究所 | Liquid mosquito-repellent incense soup |
| CN1356033A (en) * | 2001-12-14 | 2002-07-03 | 宋建祥 | Mosquito-repellent incense made of Chinese-medicinal herbs |
| CN1547917A (en) * | 2003-05-20 | 2004-11-24 | 王纪宪 | Mosquito-repellent incense with moxa |
| CN1593266A (en) * | 2004-07-12 | 2005-03-16 | 肖社生 | Vanilla health cigarette |
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