CN102334518B - Szechwan chinaberry fruit mosquito coil and preparation method thereof - Google Patents
Szechwan chinaberry fruit mosquito coil and preparation method thereof Download PDFInfo
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- CN102334518B CN102334518B CN2011103090025A CN201110309002A CN102334518B CN 102334518 B CN102334518 B CN 102334518B CN 2011103090025 A CN2011103090025 A CN 2011103090025A CN 201110309002 A CN201110309002 A CN 201110309002A CN 102334518 B CN102334518 B CN 102334518B
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Classifications
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a Szechwan chinaberry fruit mosquito coil and a preparation method thereof. The Szechwan chinaberry fruit mosquito coil comprises the following components in parts by weight: 50-60 parts of Szechwan chinaberry fruit, 20-25 parts of bee hive, 3-6 parts of lilac daphne, 1-3 parts of Angelica dahurica, 15-25 parts of elm bark, 1-3 parts of sandalwood, 35-40 parts of camphor wood, 1-3 parts of mint, 1-3 parts of honeysuckle and 0.5-1.5 parts of musk. The Szechwan chinaberry fruit mosquito coil has strong expelling and killing functions on mosquitoes and no harmful effect to the human body.
Description
Technical field
The present invention relates to a kind of mosquito-repellent incense and preparation method thereof, relate in particular to a kind of Fructus meliae toosendan mosquito-repellent incense and preparation method thereof.
Background technology
Mosquito-repellent incense is a kind of mosquito repellent thing, and medicine is wherein lighted the cigarette that is sent the back can drive mosquito or smoked dead mosquito away.China's very long history that kindles mosquito repellent incense, traditional mosquito-repellent incense are divided two kinds of line spices and incense coils.
Yet the effective ingredient of most of mosquito-repellent incenses is pyrethrin insecticides, and organic filler, binder, dyestuff and other additives etc., therefore contains many harmful materials in the cigarette of mosquito incense burning, might bring out diseases such as asthma.
Summary of the invention
At above shortcomings in the prior art, one of technical problem to be solved by this invention provides a kind of Fructus meliae toosendan mosquito-repellent incense, and mosquito is had the stronger effect of killing, and can not produce harmful effect to human body.
Two of technical problem to be solved by this invention provides a kind of preparation method of Fructus meliae toosendan mosquito-repellent incense.
The present invention seeks to be achieved through the following technical solutions:
A kind of Fructus meliae toosendan mosquito-repellent incense is made of by weight following component: Fructus meliae toosendan 50-60 part, honeycomb 20-25 part, lilac daphne 3-6 part, root of Dahurain angelica 1-3 part, elm bark 15-25 part, santal 1-3 part, camphorwood 35-40 part, peppermint 1-3 part, honeysuckle 1-3 part, Moschus 0.5-1.5 part.
Preferably, a kind of Fructus meliae toosendan mosquito-repellent incense is made of by weight following component: Fructus meliae toosendan 50-60 part, honeycomb 20-25 part, lilac daphne 3-6 part, root of Dahurain angelica 1-3 part, elm bark 15-25 part, santal 1-3 part, camphorwood 35-40 part, peppermint 1-3 part, honeysuckle 1-3 part, Moschus 0.5-1.5 part, black false hellebore 2-4 part, Radix Codonopsis 0.5-1.5 part.
Fructus meliae toosendan mosquito-repellent incense of the present invention can adopt industry conventional method to be prepared from.
Further, the present invention also provides the preparation method of above-mentioned Fructus meliae toosendan mosquito-repellent incense, is made up of following step:
Above-mentioned each component is dried and crushed into 80-120 purpose powder respectively, takes by weighing each component according to proportioning, add water and fully be mixed into mud, dry after mud is put into the joss sticks manufacturing machine extrusion molding, can make Fructus meliae toosendan mosquito-repellent incense of the present invention.
Concrete, in the present invention:
Fructus meliae toosendan is the dry mature fruit of Meliaceae plant melia toosendan.Function with cure mainly: the liver promoting qi circulation and relieving pain of relaxing, expelling parasite.Be recorded in an one-29 of Pharmacopoeia of the People's Republic of China version in 2005.
Honeycomb is the nest of Vespidae insect fruit hornet, the long pin wasp of Japan or different abdomen wasp.Function with cure mainly: dispel the wind merit poison, desinsection, pain relieving.Be recorded in an one-249 of Pharmacopoeia of the People's Republic of China version in 2005.
Lilac daphne is the dry flower of Thymelaeceae plant lilac daphne.Be recorded in an one-109 of Pharmacopoeia of the People's Republic of China version in 2005.
The root of Dahurain angelica is the dry root of the umbellate form section plant root of Dahurain angelica or Radix angelicae dahuricae.Be recorded in one one-69-70 of Pharmacopoeia of the People's Republic of China version in 2005.
Elm bark is dry bark or the root skin of Ulmaceae plant elm.Be recorded in " the colored atlas of practical Chinese herbal medicine " the 4th, Nationalities Press's " hiding Chinese voluminous dictionary " version in 1985.
Santal is the heartwood of Santalaceae plant santal trunk.Be recorded in an one-264 of Pharmacopoeia of the People's Republic of China version in 2005.
Camphorwood, aiphyllium, the bark yellowish-brown has irregular longitudinal crack, on the south the main product the Changjiang river and southwestern various places.Cut down trees winter and split broken or be sawn into bulk, dry or air-dry.The timber bulk is not of uniform size, and surface red is brown to burgundy, the visible annual ring in cross section.Matter is heavy and hard.Strong camphor fragrance is arranged, and it is refrigerant to distinguish the flavor of, and pungent sense is arranged.
Peppermint, this product are the dry aerial parts of labiate peppermint.Be recorded in an one-261 of Pharmacopoeia of the People's Republic of China version in 2005.
Honeysuckle is caprifoliaceae plant dry flower or the first flower of opening of band of honeysuckle.Function with cure mainly: clearing heat and detoxicating, wind-heat dissipating.Be recorded in one one-152-153 of Pharmacopoeia of the People's Republic of China version in 2005.
Moschus is the dry secretion in the ripe male body note capsule of animal in deer family woods musk deer, horse musk deer or former musk deer.Be recorded in an one-266 of Pharmacopoeia of the People's Republic of China version in 2005.
Black false hellebore (formal name used at school: the plant of Liliaceae Veratrum Veratrum nigrum L.), perennial herb.Effect: clearing heat and detoxicating, desinsection.Also many places are on the books in one one of Pharmacopoeia of the People's Republic of China version in 2005.
Radix Codonopsis is the dry root of Campanulaceae plant Radix Codonopsis, plain flower Radix Codonopsis or radix codonpsis tangshen.Be recorded in an one-199 of Pharmacopoeia of the People's Republic of China version in 2005.
The present invention is made by natural wild Chinese herbal medicine fully, and Fructus meliae toosendan, honeycomb, lilac daphne and the root of Dahurain angelica are composite, and the smell that distributes in combustion process can suppress, the kill virus germ, and the prevention respiratory disease strengthens immune function of human body, mosquito killer; The powder that elm bark, santal and camphorwood are made makes mosquito-repellent incense moulding and the double burning matrix of doing, and santal, camphorwood, peppermint, honeysuckle and Moschus are in combustion process, fresh air not only, and can be antibacterial except poison, especially effective mosquito killer, more crucial is to use the present invention to produce harmful effect to human body for a long time.
Especially, in one one of Pharmacopoeia of the People's Republic of China version in 2005, particularly point out: Radix Codonopsis should not with black false hellebore with using.Discovery after yet the process inventor tests is in a large number added Radix Codonopsis simultaneously in mosquito-repellent incense and black false hellebore not only can increase repelling effect, and can't produce harmful effect to human body.
Experimental results show that, the present invention has certain inhibition, killing action to multiple germs such as gold look staphylococcus, shigella dysenteriae, tubercle bacillus, Pseudomonas aeruginosa, bacillus anthracis, hepatitis bacillus, particularly the virus and bacteria for the epidemic infection disease has very strong insect killing effect, and mosquito is had the stronger effect of killing.
Embodiment
Embodiment 1:
Take by weighing: 50 kilograms of Fructus meliae toosendans, 25 kilograms in honeycomb, 3 kilograms of lilac daphnes, 3 kilograms of the roots of Dahurain angelica, 15 kilograms of elm barks, 3 kilograms in santal, 35 kilograms of camphorwoods, 3 kilograms of peppermints, 3 kilograms of honeysuckles, 0.5 kilogram in Moschus.
Above-mentioned each component is dried and crushed into 80-120 purpose powder respectively, adds water and fully be mixed into mud, dry after mud is put into the joss sticks manufacturing machine extrusion molding, can make Fructus meliae toosendan mosquito-repellent incense of the present invention.
Embodiment 2:
Take by weighing: 60 kilograms of Fructus meliae toosendans, 20 kilograms in honeycomb, 6 kilograms of lilac daphnes, 1 kilogram of the root of Dahurain angelica, 25 kilograms of elm barks, 1 kilogram in santal, 40 kilograms of camphorwoods, 1 kilogram of peppermint, 1 kilogram of honeysuckle, 1.5 kilograms in Moschus.
Above-mentioned each component is dried and crushed into 80-120 purpose powder respectively, adds water and fully be mixed into mud, dry after mud is put into the joss sticks manufacturing machine extrusion molding, can make Fructus meliae toosendan mosquito-repellent incense of the present invention.
Embodiment 3:
Take by weighing: 55 kilograms of Fructus meliae toosendans, 23 kilograms in honeycomb, 5 kilograms of lilac daphnes, 2 kilograms of the roots of Dahurain angelica, 20 kilograms of elm barks, 2 kilograms in santal, 38 kilograms of camphorwoods, 2 kilograms of peppermints, 2 kilograms of honeysuckles, 1 kilogram in Moschus, 3 kilograms of black false hellebores, 1 kilogram of Radix Codonopsis.
Above-mentioned each component is dried and crushed into 80-120 purpose powder respectively, adds water and fully be mixed into mud, dry after mud is put into the joss sticks manufacturing machine extrusion molding, can make Fructus meliae toosendan mosquito-repellent incense of the present invention.
Embodiment 4:
Take by weighing: 55 kilograms of Fructus meliae toosendans, 23 kilograms in honeycomb, 5 kilograms of lilac daphnes, 2 kilograms of the roots of Dahurain angelica, 20 kilograms of elm barks, 2 kilograms in santal, 38 kilograms of camphorwoods, 2 kilograms of peppermints, 2 kilograms of honeysuckles, 1 kilogram in Moschus.
Above-mentioned each component is dried and crushed into 80-120 purpose powder respectively, adds water and fully be mixed into mud, dry after mud is put into the joss sticks manufacturing machine extrusion molding, can make Fructus meliae toosendan mosquito-repellent incense of the present invention.
Test case 1: indoor harmacological effect
Adopt mosquito-repellent incense indoor harmacological effect assay method and the evaluation criterion of GB/T 13917.4-2009 regulation, test.Concrete grammar is as follows:
1, for the examination material
Adopt the sensitive strain standard examination worm of laboratory rearing.
Culex pipiens pallens (Culex pipiens pallens), the 3rd day～the 5th day female insect for sucking blood in back of sprouting wings.
2, instrument and equipment
Cylinder unit
Water white transparency cylinder frame is on support, and cylinder respectively has a water white transparency garden plate up and down.There is a circular hole in last plectane central authorities, clog with plug; There is a circular hole in following plectane central authorities, clog with plug, and the plug mosquito coil frame of having put on the shelf is used for placing tested mosquito-repellent incense; Reveal with protection from fumes with the rubber washer pad respectively cylinder and upper and lower plectane joint.
Mosquito sucking tube, stopwatch, counter
3, test method
Experiment condition: temperature: (26 ± 1) ℃; Relative moisture: 60% ± 10%
4, experimental procedure
Adopt cylinder unit.Draw 30 of examination mosquitos, put into the jam-pack plug from the central circular hole place of tube below plectane.After waiting to try worm recovery normal activity, get one section of mosquito-repellent incense to be measured at random, horizontal on mosquito coil frame; after lighting 5min in advance elsewhere, move to and smoke cigarette 1min in the cylinder, immediately mosquito-repellent incense is removed; plug, and timing beyond the Great Wall records down and out examination borer population at regular intervals.Be limited to 20min during observation.Test should be established three times and above repetition, and repeated test should be coiled mosquito-repellent incense in difference with mosquito-repellent incense and taked at random.After each off-test, answer the washing test device.
5, calculate
The retest data are pressed linear weighted function Return Law calculating K T50 value and virulence regression equation.
6, evaluation index
Carry out evaluating drug effect according to KT50.
Drug effect result is divided into A, B two-stage, does not reach B grade standard person and belongs to substandard product.
A level: KT50≤4.0 minute; B level: KT50≤8.0 minute.
Table 1: mosquito-repellent incense indoor harmacological effect table
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | |
| The KT50 value | 2 minutes 36 seconds | 2 minutes 30 seconds | 1 minute 57 seconds | 2 minutes 41 seconds |
Test case 2: toxotest
With reference to health ministry " toxicity disease in the blood system diagnostic criteria in the management of occupational acute chemicals " and " technological guidance's principle of Chinese medicine, the research of natural drug immunotoxicity " standard, formulate test case of the present invention.
1. the mosquito-repellent incense of experiment material: embodiment 3
2. experiment kind: two young age small white mouse.
3. experimental technique:
(1) experiment condition: laboratory temperature (27 ± 2) ℃
(2) experimental provision: in the laboratory of two 25 square metres of uniform temps, each places fine and closely woven ventilative netted the shrouding of 80 * 80 * 80cm of a big or small same size.
(3) experimental procedure: with two young age small white mouse separately respectively be put in netted the shrouding in two laboratories, and be divided into control group and smoke mosquito-repellent incense group of the present invention, give not smoke mosquito-repellent incense of the present invention respectively and smoke mosquito-repellent incense of the present invention, measure children's small white mouse body weight in age, the recovery situation after observing the biochemical index of hematology, histopathology changes and stopping to smoke mosquito-repellent incense of the present invention etc.To be installed in when placing mosquito-repellent incense of the present invention netted shroud interior the end of from 30 centimeters.Dosage: an early late dish mosquito-repellent incense in shrouding keeps 24 hours mosquito-repellent incense Chang Ran.Time: used continuously one month, and observed control group and smoke the small white mouse in young age of mosquito-repellent incense group of the present invention, use mosquito-repellent incense of the present invention to toxicity and the side effect of children small white mouse in age for a long time.Cleaning: shroud interior two days cleanings once.
Table 2: children's small white mouse mosquito-repellent incense toxicity test statistical form in age
Above children's small white mouse mosquito-repellent incense toxicity test statistical form in age is taken from the sampling combination table that obvious situation record was arranged in five days that add up every day in month, tests altogether 30 days, adds a week of stopping using and observing, totally 37 days.After two young small white mouse blood drawing chemical examinations in age, every biochemical indicator is normally, shows that mosquito-repellent incense of the present invention has no side effect to children small white mouse in age, has only to surpass when indoor mosquito-repellent incense smog was too dense in 24 hours, need window and take a breath 10-15 minute, draw blood and gave two children small white mouses in age feeds in preceding 8 hours.
The result: after each main organs heart, liver, spleen, lung, kidney, suprarenal gland, brain etc. were dissected, naked eyes are no abnormal variation all.Smoke mosquito-repellent incense group organ coefficient of the present invention and do not smoke mosquito-repellent incense group of the present invention relatively there are no significant difference, the organs and tissues pathological examination is not seen significantly pathological change such as atrophy, sex change, necrosis, and does not smoke relatively there was no significant difference of mosquito-repellent incense group of the present invention.
Conclusion: use mosquito-repellent incense of the present invention that children small white mouse in age is not had any toxicity for a long time.
Test case 3: acute oral toxicity test
The mosquito-repellent incense of experiment material: embodiment 3.The back 5 minutes activities in rats of contaminating increase, and continue about 2 minutes, and activity transfers to normally, and diet is normal, and the observation period does not have death, and LD50 belongs to actual nontoxic greater than 5000 milligrams/kilogram.
Test case 4: acute toxicity on inhalation test
The mosquito-repellent incense of experiment material: embodiment 3.Contamination back rat diet activity no abnormality seen, the observation period does not have death, and LD50 belongs to actual nontoxic greater than 10 grams/cubic meter.
Test case 5: skin patch test
The mosquito-repellent incense of experiment material: embodiment 3.It is 0 that experimental group erythema and oedema form the scoring sum, illustrates skin is had no stimulation.
Test case 6: eye irritant test
It is 0 that the acute eye of experimental group stimulates the integration number, illustrates mucous membrane is had no stimulation.
Test case 7: treatment tinea pedis test
Especially, the inventor is surprised to find that the residue behind the mosquito incense burning of the present invention, and namely the mosquito-repellent incense ash also has the effect for the treatment of tinea pedis.20 routine tinea pedis patients are tested, adopt the disclosed method of testing of Chinese invention patent Granted publication CN100448443C, residue behind the mosquito incense burning of the embodiment of the invention 3 is added in the rice vinegar, the amount of used rice vinegar is 10 times of residue weight behind the mosquito incense burning, mix, be coated on the skin of suffering from tinea pedis, each medication sooner or later once, 14 days is a course for the treatment of.Treat and efficiently reach 94%.
Claims (3)
1. a Fructus meliae toosendan mosquito-repellent incense is characterized in that, is prepared by following components by part by weight: Fructus meliae toosendan 50-60 part, honeycomb 20-25 part, lilac daphne 3-6 part, root of Dahurain angelica 1-3 part, elm bark 15-25 part, santal 1-3 part, camphorwood 35-40 part, peppermint 1-3 part, honeysuckle 1-3 part, Moschus 0.5-1.5 part.
2. a Fructus meliae toosendan mosquito-repellent incense is characterized in that, is prepared by following components by part by weight: Fructus meliae toosendan 50-60 part, honeycomb 20-25 part, lilac daphne 3-6 part, root of Dahurain angelica 1-3 part, elm bark 15-25 part, santal 1-3 part, camphorwood 35-40 part, peppermint 1-3 part, honeysuckle 1-3 part, Moschus 0.5-1.5 part, black false hellebore 2-4 part, Radix Codonopsis 0.5-1.5 part.
3. the preparation method of Fructus meliae toosendan mosquito-repellent incense as claimed in claim 1 or 2, it is characterized in that, formed by following step: above-mentioned each component is dried and crushed into 80-120 purpose powder respectively, take by weighing each component according to proportioning, add water and fully be mixed into mud, dry after mud put into the joss sticks manufacturing machine extrusion molding, namely make described Fructus meliae toosendan mosquito-repellent incense.
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| CN103355361A (en) * | 2013-08-06 | 2013-10-23 | 谢安军 | Mosquito-repellent incense |
| CN103355364A (en) * | 2013-08-06 | 2013-10-23 | 谢安军 | Traditional-Chinese-medicine mosquito-repellent incense |
| CN104509555A (en) * | 2013-09-27 | 2015-04-15 | 青岛锦涟鑫商贸有限公司 | Improved traditional Chinese medicine insect-repelling joss-stick |
| CN104186576A (en) * | 2014-08-18 | 2014-12-10 | 中山市品汇创新专利技术开发有限公司 | Rhamnus crenata natural plant mosquito-repellent incense capable of calming mind and nerves and preparation method of rhamnus crenata natural plant mosquito-repellent incense |
| CN104186577A (en) * | 2014-08-18 | 2014-12-10 | 中山市品汇创新专利技术开发有限公司 | Slow-release electrothermal mosquito incense liquor containing ambergris extract and preparation method |
| CN104206445A (en) * | 2014-08-18 | 2014-12-17 | 中山市品汇创新专利技术开发有限公司 | Cortex-meliae plant mosquito-repellent incense and preparation method thereof |
| CN105594754A (en) * | 2016-02-17 | 2016-05-25 | 广西大学 | Fructus toosendan electrothermal liquid mosquito-repellent incense and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1199550A (en) * | 1997-05-21 | 1998-11-25 | 刘军 | Compound chinaberry-Radix Sophorae Flavescentis pesticide for animal and plant protection |
| CN1502243A (en) * | 2002-11-20 | 2004-06-09 | 邓志宏 | Broad-spectrum pesticide using plant composition as raw material and preparation process thereof |
| CN1843126A (en) * | 2006-05-19 | 2006-10-11 | 山东大学 | Traditional Chinese medicine composite biological pesticide using crusta as main material |
| CN1883277A (en) * | 2006-06-30 | 2006-12-27 | 刘景相 | A botanical pesticide |
| GB2477317A (en) * | 2010-01-29 | 2011-08-03 | Rosalyn Louise Simon | Environmentally safe and skin safe insecticide and repellant for human and other vertebrates |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1332963A (en) * | 2001-02-26 | 2002-01-30 | 西北农林科技大学无公害农药研究服务中心 | Toosendanin pesticide composition |
| CN1209028C (en) * | 2003-09-12 | 2005-07-06 | 李瑞金 | Insecticide, bactericide and its preparation and application method |
-
2011
- 2011-09-28 CN CN2011103090025A patent/CN102334518B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1199550A (en) * | 1997-05-21 | 1998-11-25 | 刘军 | Compound chinaberry-Radix Sophorae Flavescentis pesticide for animal and plant protection |
| CN1502243A (en) * | 2002-11-20 | 2004-06-09 | 邓志宏 | Broad-spectrum pesticide using plant composition as raw material and preparation process thereof |
| CN1843126A (en) * | 2006-05-19 | 2006-10-11 | 山东大学 | Traditional Chinese medicine composite biological pesticide using crusta as main material |
| CN1883277A (en) * | 2006-06-30 | 2006-12-27 | 刘景相 | A botanical pesticide |
| GB2477317A (en) * | 2010-01-29 | 2011-08-03 | Rosalyn Louise Simon | Environmentally safe and skin safe insecticide and repellant for human and other vertebrates |
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