CN104430568B - A kind of botanical pesticide for preventing and treating matrimony vine thrips - Google Patents
A kind of botanical pesticide for preventing and treating matrimony vine thrips Download PDFInfo
- Publication number
- CN104430568B CN104430568B CN201410598813.5A CN201410598813A CN104430568B CN 104430568 B CN104430568 B CN 104430568B CN 201410598813 A CN201410598813 A CN 201410598813A CN 104430568 B CN104430568 B CN 104430568B
- Authority
- CN
- China
- Prior art keywords
- nicotine
- solution
- matrine
- emulsifying agent
- matrimony vine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of botanical pesticide, more particularly, to a kind of botanical pesticide for preventing and treating matrimony vine thrips, it is characterised in that：The preparation method of the pesticidal preparations is that active compound solubilizer first is dissolved into solution, then solution is mixed into compounding medicine company, turn into mother liquor after compounding medicine company is added into emulsifier for mixing again, finally mother liquor is stirred by the way that water, high shear is added dropwise, preparation is filtered to obtain, above-mentioned active compound is any one mixture in nicotine and matrine, Celastrus angulatus, margosine, stemonine, jervine, pyrethrin, nimbin or frutus cnidii；The present invention provides a kind of compounding scope that can improve botanical pesticide, is conducive to further improving the high efficiency of botanical pesticide, the problems such as to solve serious matrimony vine thrips harm and exceeded matrimony vine residues of pesticides.
Description
Technical field
The present invention relates to a kind of botanical pesticide, more particularly, to a kind of botanical pesticide for preventing and treating matrimony vine thrips.
Background technology
At present, the thrip fuana about more than 7400 that the whole world has been described is planted, point section of 2 suborder 8, the thrips about 400 of China's record
Remaining kind.Thrips is global important omnivorous insect, and based on phytophagous, host plant is extremely extensive, various grains of mainly causing harm
The plants such as food, fruits and vegetables flowers and gardening.The class pest is taken food or laid eggs with rasping-sucking mouthparts and caused in plant You Nen epidermal tissues
Directly cause harm, cause plant organ to damage, influence photosynthesis, so as to influence the exterior quality and yield of product, reduce economical
Value；Some thrips can also propagate various plants virus and cause to cause harm indirectly, make the viroses of plant a large amount of popular between crop.Ji
Horse is to the direct harm of host plant less than the indirect hazard caused by its transmitted virus.Thrips class insect build is small, often
Conceal in plant bud, cause harm and be difficult to find, and reproductive capacity is extremely strong, can largely break out cause harm in a short time, it is main in agricultural production
To use chemical prevention.For a long time, because the not scientific and reasonable of chemical pesticide uses, cause the agricultural chemicals of agricultural economy crop residual
Stay exceeded, safety in production is faced huge challenge.
And botanical pesticide typically has and influence less advantage on person poultry safety and on environmental quality, exactly compensate for
Learn to farm the defect of medicine.But botanical pesticide use cost is high, effect is slow, the lasting period is relatively short, and insecticidal spectrum is narrower, therefore
It is promoted, popularization also has certain difficulty.
In recent years, matrimony vine thrips turn into one of insect that harm is the most serious, preventing and treating is the most difficult, in matrimony vine produces with
The naked thrips of India is Main Populations, also with flower thrips, rice thripses, China letter pipe thrips and rice letter pipe thrips, has a strong impact on and makes
About the sound development of wolfberry industry.Therefore thatch agriculture blindly passive use chemical agent, does not obtain good anti-not only
Control effect and triggered the residual severe overweight problem of agriculture again so that matrimony vine Product Safety declines, large quantities of products outlet is limited.
Method there is presently no drawbacks described above is overcome.
The content of the invention
The purpose of the present invention is the defect for overcoming prior art, there is provided a kind of compounding model that can improve botanical pesticide
Enclose, be conducive to further improving the high efficiency of botanical pesticide, matrimony vine thrips harm is serious and matrimony vine residues of pesticides are super to solve
A kind of botanical pesticide of the preventing and treating matrimony vine thrips of the problems such as mark.
The present invention is realized in the following way：
A kind of botanical pesticide preparation for preventing and treating matrimony vine thrips, it is characterised in that：The preparation method of the pesticidal preparations is for first
Active compound solubilizer is dissolved into solution, solution is then mixed into compound solution, then by compound solution add after emulsifier for mixing into
It is mother liquor, finally mother liquor is stirred by the way that water, high shear is added dropwise, preparation is filtered to obtain, above-mentioned active compound is nicotine and matrine, bitter skin
Rattan element, margosine, stemonine, jervine, pyrethrin, nimbin or any one mixture in frutus cnidii；
The mass concentration of the active compound is followed successively by matrine 15%, Celastrus angulatus 6%, margosine 1%, stemonine 2%, lamb's-quarters
Reed alkali 5%, pyrethrin 25%, nimbin 5%, nicotine 95%, frutus cnidii 30%, obtain to be mixed molten after the active compound dilution
The concentration of liquid is followed successively by print chinaberry 0.01g/L, matrine 0.01g/L, nicotine 0.03g/L, Dalmatian chrysanthemum 0.08g/L, frutus cnidii concentration
0.05g/L, Celastrus angulatus 3g/L, China tree 0.05g/L, jervine 0.35g/L, stemonine 20g/L；
The volume ratio of solution mixing is：Nicotine：Print chinaberry=1:5~5:1, nicotine：Matrine=1:5~5:1, cigarette
Alkali：Frutus cnidii=1:5~5:1, nicotine：China tree=1:5~5:1, nicotine：Celastrus angulatus=1:5~5:1；
The pharmaceutical formulation it is following any one：
Volume ratio is：Nicotine：Print chinaberry=1:5~5:The emulsifying agent of 1+20% solvents+8%, pure water complements to 100%；
Volume ratio is：Nicotine：Matrine=1:5~5:The emulsifying agent of 1+20% solvents+8%, pure water complements to 100%；
Volume ratio is：Nicotine：Frutus cnidii=1:5~5:The emulsifying agent of 1+25% solvents+8%, pure water complements to 100%；
Volume ratio is：Nicotine：China tree=1:5~5:The emulsifying agent of 1+18% solvents+8%, pure water complements to 100%；
Volume ratio is：Nicotine：Celastrus angulatus=1:5~5:The emulsifying agent of 1+35% solvents+8%, pure water complements to 100%；
Above-mentioned content is volumn concentration；
The solvent is acetone, alcohol or water, and the emulsifying agent is dense newborn 500, OP-10 or Tween 80.
The present invention has following effect：
Experimental technique used in following embodiments is conventional method unless otherwise specified.
Material used, reagent etc. in following embodiments, unless otherwise specified, commercially obtain.
Embodiment 1, the agent of 9 kind of plant source Cupric sulfate are to the Toxicity Determination of thrips
Test worm：Matrimony vine thrips pick up from Yinchuan of Ningxia Province city gardens, are identified as compound population.Continue band indoors to raise, take
Matrimony vine thrips two ages nymph is for examination.
Reagent agent：15% matrine, 6% Celastrus angulatus, 1% margosine, 2% stemonine, 5% jervine, 25% are removed
Worm chrysanthemum element, 5% nimbin, 95% nicotine, 30% frutus cnidii, the source of the raw material is the bright biological limited public affairs of exploitation in Baoji side
Department；
Solvent acetone, emulsifying agent Tween-80, is made through stirring.
Assay method：Using medicine film leaf dipping method, comprise the following steps that：
(1) first above-mentioned 9 kinds of medicine based on herbs solvent is dissolved, then some gradients is diluted to water-emulsifying agent, it is ensured that
Liquid is prepared for transparent, finely dispersed concentration of participating in the experiment.After liquid is prepared, insect box medicine film is made first：By plant source
After medicament adds acetone solution, some concentration are diluted to water-emulsifying agent, to even spraying in insect box, the Indoor Natural system of drying
Into medicine film.
(2) matrimony vine blade is impregnated with identical liquor strength again, until after medicine film and leaching medicine blade dry, will be with medicine blade
It is put into medicine film insect box, constitutes medicine film leaf dipping method.Finally, test worm 30 or so of participating in the experiment is accessed, and cultivates observation, calculate dead
Rate.
With the matrimony vine blade of water box and leaching clear water as a control group, 4 repetitions are processed per concentration.Control group death rate ＜
10% is efficiency test.
Study on Fungicide Toxicity：Carry out data processing using DPS analysis softwares, obtain medicament virulence regression equation,
LC50 values and its 95% confidence limit etc..
The common poison factor>20, representing that two single doses are mixed has synergistic effect；≤ -20 indicate antagonism, and -20~20 represent
Summation action.
19 kinds of Toxicity Determinations of medicine based on herbs of table
Can be learnt by the data of table 1, print chinaberry, matrine and nicotine are relatively low to the LC50 of thrips, the lower Contact toxicities of LC50
It is stronger, therefore select 6 kinds of medicine based on herbs of this 3 kinds of medicaments and other to be compounded, and investigate the Contact toxicity to thrips.
The Toxicity Determination of embodiment 2, print chinaberry and other 8 kinds of medicine based on herbs to thrips
The botanical pesticide print chinaberry that will be screened in embodiment 1 is 5 according to volume ratio with other 8 kinds of active compounds:1、2:1、
1:1、1:2、1:5 carry out binary mixture obtain Mixed Pharmacy (each drug concentration is LC50 values, print chinaberry：0.01g/L；Matrine：
0.01g/L；Nicotine：0.03g/L；Dalmatian chrysanthemum：0.08g/L；Frutus cnidii：0.05g/L；Celastrus angulatus：3g/L；China tree：0.05g/L；
Jervine：0.35g/L；Stemonine：20g/L).Toxicity Determination of 8 kinds of Mixed Pharmacies to thrips is investigated, leaf is soaked using medicine film
Method is measured, and specific steps are with embodiment 1.
The joint toxicity measuring result of above-mentioned 8 kinds of Mixed Pharmacies is as shown in table 2.
Table 2 prints the binary mixture toxicity test of chinaberry and other 8 kinds of medicine based on herbs
Print chinaberry is can be seen that from the data in table 2：Matrine=1：5 mixtures, the poison factor is 31.08 ＞ 20 altogether, with increasing
Effect is acted on, and the poison factor is bigger altogether, and synergistic effect is more obvious, shows that its synergistic effect is the most obvious, therefore print chinaberry and matrine two
Plant medicament mixing ratio single dose high to the insecticidal activity of thrips；Print chinaberry：Nicotine=1:5~2:1 mixture, the common poison factor is all higher than 20,
Show that its mixture is respectively provided with synergistic effect, print chinaberry and two kinds of medicament mixing ratio single doses of nicotine are high to the insecticidal activity of thrips；Wherein
Print chinaberry：Nicotine=1:2, the poison factor is maximum altogether, reaches 54.77, shows that this Mixed Pharmacy is tagged synergy work to the interior of thrips
With the most substantially, two kinds of medicaments of print chinaberry and nicotine mix, and ratio is 1:2 pairs of contact toxicity highests of thrips.
Embodiment 3, according to volume ratio it is 5 by botanical pesticide matrine and other 7 kinds of active compounds:1、2:1、1:1、1:2、1:
5 carry out binary mixture obtains Mixed Pharmacy.Toxicity Determination of 7 kinds of Mixed Pharmacies to thrips is investigated, using medicine film leaf dipping method
It is measured, specific steps are with embodiment 1.
The joint toxicity measuring result of above-mentioned 7 kinds of Mixed Pharmacies is as shown in table 3.
The binary mixture toxicity test of the matrine of table 3 and other 7 kinds of medicine based on herbs
Matrine is can be seen that from the data in table 3：Nicotine=1:5~5:1 mixture, the common poison factor is all higher than 20, shows
Its mixture has synergistic effect, therefore after matrine and nicotine are compounded according to the ratio, effect of the effect is significant higher than each single dose
Really.Particularly matrine：Nicotine=5:When 1, the poison factor is 48.03 to the maximum altogether, shows that its mixed synergies is the most notable, right
Thrips activity is the most notable.
Consolidated statement 2 and table 3, by a large amount of compound screenings, can obtain nicotine prevent and treat matrimony vine thrips in synergistic effect significantly, because
This is compounded to 8 kinds of medicine based on herbs of nicotine and other.
Embodiment 4, nicotine and remaining 8 kinds of Toxicity Determination of medicine based on herbs
The binary mixture toxicity test of the nicotine of table 4 and other 6 kinds of medicine based on herbs
Drawn a conclusion by the data in table 4, nicotine：Frutus cnidii=1:5~5:1, the common poison factor is all higher than 20, shows that it is mixed
With with synergistic effect；Nicotine：China tree=1:5~5:1, the common poison factor is all higher than 20, shows that its mixture has synergistic effect；Cigarette
Alkali：Dalmatian chrysanthemum=1:5~5:1, the common poison factor is all higher than 20, shows that its mixture has synergistic effect；Nicotine：Jervine=1:5
~5:1, the common poison factor is all higher than 20, shows that its mixture has synergistic effect；Nicotine：Celastrus angulatus=1:5~5:1, the common poison factor
20 are all higher than, show that its mixture has synergistic effect；Nicotine：Stemonine=1:5~5:1, the common poison factor is all higher than 20, shows it
Mixture has synergistic effect, therefore in whole compound process, nicotine plays synergistic effect, and other 8 kinds of composite reagent preventing and treatings
The effect of thrips is all higher than the using effect of each single dose.
Can be drawn the following conclusions with reference to table 2,3,4 and the composite factor such as reagent cost and plant resources amount：
The component volume percentage：Nicotine：Print chinaberry=2:1, remaining is solvent-water-emulsifying agent
The component volume percentage：Nicotine：Matrine=1:5, remaining is water-emulsifying agent
The component volume percentage：Nicotine：Frutus cnidii=5:1, remaining is solvent-water-emulsifying agent
The component volume percentage：Nicotine：China tree=5:1, remaining is water-emulsifying agent
The component volume percentage：Nicotine：Celastrus angulatus=5:1, remaining is solvent-water-emulsifying agent
Be can be seen that from above-mentioned experiment and endanger serious and matrimony vine residues of pesticides excessive problem for matrimony vine thrips, there is provided be a kind of
There is significant synergistic effect of tagging to matrimony vine thrips, new technical support is provided to prevent and treat matrimony vine thrips in production.Nicotine
There is significant synergistic effect with print chinaberry, matrine, frutus cnidii, China tree, Celastrus angulatus compounding respectively, this 5 kinds of complex preparations：10 kinds
95% is above with the matrimony vine thrips effect death rate is compared, wherein working as nicotine：Print chinaberry=2:1；Nicotine and frutus cnidii=5:1；Cigarette
Alkali：China tree=5:1,2:1,1:5；Nicotine：Print chinaberry=1:When 5, its death rate reaches 100%, and to sum up this 10 kinds of complex preparations are prevented
Control the using effect that thrips effect is above each single dose.The Toxicity Determination of comprehensive 10 kinds of plant source active compounds proportioning and field examination
Test, obtain effect as follows：Under conditions of 200 times of dilution, more than 95% is reached to matrimony vine thrips indoor virulence；And its medicine
The field efficacy of 1 day reaches 85% afterwards, reaches 90% within 3 days after medicine, and 5 days preventive effects persistently reach 90% after medicine, and preventive effect is still after 7 days
It is 90%, therefore this 10 kinds of plant source active compounds are notable with matrimony vine thrips preventive effect is compared.
Specific embodiment
Embodiment 1：A kind of botanical pesticide preparation for preventing and treating matrimony vine thrips, the preparation method of the pesticidal preparations is first by original
Medicine solubilizer is dissolved into solution, and solution then is mixed into compound solution, then turns into mother after compound solution is added into emulsifier for mixing
Liquid, mother liquor is finally stirred, filter to obtain preparation by the way that water, high shear is added dropwise, and above-mentioned active compound is nicotine and matrine, Celastrus angulatus
Any one mixture in element, margosine, stemonine, jervine, pyrethrin, nimbin or frutus cnidii；The matter of the active compound
Amount concentration is followed successively by matrine 15%, Celastrus angulatus 6%, margosine 1%, stemonine 2%, jervine 5%, pyrethrin
25%th, nimbin 5%, nicotine 95%, frutus cnidii 30%, the concentration that solution to be mixed is obtained after the active compound dilution are followed successively by print
Chinaberry 0.01g/L, matrine 0.01g/L, nicotine 0.03g/L, Dalmatian chrysanthemum 0.08g/L, frutus cnidii concentration 0.05g/L, Celastrus angulatus 3g/
L, China tree 0.05g/L, jervine 0.35g/L, stemonine 20g/L.
The volume ratio of the solution mixing is nicotine：Print chinaberry=1:5, the preparation is that mixed solution+20% is molten
The emulsifying agent of agent+8%, pure water complements to 100%；
Embodiment 2：Remaining is identical with embodiment 1
The volume ratio of the solution mixing is nicotine：Print chinaberry=5:1, the preparation is that mixed solution+20% is molten
The emulsifying agent of agent+8%, pure water complements to 100%；
Embodiment 3：Remaining is identical with embodiment 1
The volume ratio of the solution mixing is nicotine：Matrine=1:5, the preparation is by mixed solution+20%
The emulsifying agent of solvent+8%, pure water complements to 100%；
Embodiment 4：Remaining is identical with embodiment 1
The volume ratio of the solution mixing is nicotine：Matrine=5:1, the preparation is by mixed solution+20%
The emulsifying agent of solvent+8%, pure water complements to 100%；
Embodiment 5：Remaining is identical with embodiment 1
The volume ratio of the solution mixing is nicotine：Frutus cnidii=1:5, the preparation is by mixed solution+25%
The emulsifying agent of solvent+8%, pure water complements to 100%；
Embodiment 6：Remaining is identical with embodiment 1
The volume ratio of the solution mixing is nicotine：Frutus cnidii=5:1, the preparation is by mixed solution+25%
The emulsifying agent of solvent+8%, pure water complements to 100%；
Embodiment 7：Remaining is identical with embodiment 1
The volume ratio of the solution mixing is nicotine：China tree=1:5, the preparation is that mixed solution+18% is molten
The emulsifying agent of agent+8%, pure water complements to 100%；
Embodiment 8：Remaining is identical with embodiment 1
The volume ratio of the solution mixing is nicotine：China tree=5:1, the preparation is that mixed solution+18% is molten
The emulsifying agent of agent+8%, pure water complements to 100%；
Embodiment 9：Remaining is identical with embodiment 1
The volume ratio of the solution mixing is nicotine：Celastrus angulatus=1:5, the preparation is by mixed solution+35%
The emulsifying agent of solvent+8%, pure water complements to 100%；
Embodiment 10：Remaining is identical with embodiment 1
The volume ratio of the solution mixing is nicotine：Celastrus angulatus=5:1, the preparation is by mixed solution+35%
The emulsifying agent of solvent+8%, pure water complements to 100%.
Above-mentioned solvent is acetone, alcohol or water, and the emulsifying agent is dense newborn 500, OP-10 or Tween 80.
Claims (2)
1. it is a kind of prevent and treat matrimony vine thrips botanical pesticide preparation, it is characterised in that：The preparation method of the pesticidal preparations is first will
Active compound solubilizer is dissolved into solution, and solution then is mixed into compound solution, then turns into after compound solution is added into emulsifier for mixing
Mother liquor, mother liquor is finally stirred, filter to obtain preparation by the way that water, high shear is added dropwise, and above-mentioned active compound is nicotine and matrine, Celastrus angulatus
Element, margosine or any one mixture in frutus cnidii, the mass concentration of the active compound are followed successively by matrine 15%, Celastrus angulatus
6%th, margosine 1%, nimbin 5%, nicotine 95%, frutus cnidii 30%, obtain the concentration of solution to be mixed successively after the active compound dilution
It is print chinaberry 0.01g/L, matrine 0.01g/L, nicotine 0.03g/L, frutus cnidii concentration 0.05g/L, Celastrus angulatus 3g/L, China tree
0.05g/L, the volume ratio of solution mixing is：Nicotine：Print chinaberry=2:1, nicotine：Matrine=1:5, nicotine：Frutus cnidii=5:1,
Nicotine：China tree=1:5, nicotine：Celastrus angulatus=5:1, the pharmaceutical formulation it is following any one：
Volume ratio is：Nicotine：Print chinaberry=2:The emulsifying agent of 1+20% solvents+8%, pure water complements to 100%；
Volume ratio is：Nicotine：Matrine=1:The emulsifying agent of 5+20% solvents+8%, pure water complements to 100%；
Volume ratio is：Nicotine：Frutus cnidii=5:The emulsifying agent of 1+25% solvents+8%, pure water complements to 100%；
Volume ratio is：Nicotine：China tree=1:The emulsifying agent of 5+18% solvents+8%, pure water complements to 100%；
Volume ratio is：Nicotine：Celastrus angulatus=5:The emulsifying agent of 1+35% solvents+8%, pure water complements to 100%
Above-mentioned content is volumn concentration.
2. a kind of botanical pesticide for preventing and treating matrimony vine thrips as claimed in claim 1, it is characterised in that：The solvent is third
Ketone, alcohol or water, the emulsifying agent are dense newborn 500, OP-10 or Tween 80.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410598813.5A CN104430568B (en) | 2014-10-30 | 2014-10-30 | A kind of botanical pesticide for preventing and treating matrimony vine thrips |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410598813.5A CN104430568B (en) | 2014-10-30 | 2014-10-30 | A kind of botanical pesticide for preventing and treating matrimony vine thrips |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104430568A CN104430568A (en) | 2015-03-25 |
| CN104430568B true CN104430568B (en) | 2017-07-11 |
Family
ID=52877921
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410598813.5A Expired - Fee Related CN104430568B (en) | 2014-10-30 | 2014-10-30 | A kind of botanical pesticide for preventing and treating matrimony vine thrips |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104430568B (en) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104892204A (en) * | 2015-06-10 | 2015-09-09 | 南京九康壹可农业科技有限公司 | Dedicated medical fertilizer for Chinese wolfberry and preparation method of dedicated medical fertilizer |
| CN105557763A (en) * | 2016-01-25 | 2016-05-11 | 陶遥力 | Novel plant source insecticidal bactericide and preparation process thereof |
| CN105532682B (en) * | 2016-02-17 | 2018-03-23 | 陕西先农生物科技有限公司 | A kind of composition of plant insecticide containing jervine and preparation method |
| CN106359459B (en) * | 2016-08-30 | 2019-08-16 | 武汉轻工大学 | Pyrethrin and matrine compound agent and its application |
| CN106376584A (en) * | 2016-09-12 | 2017-02-08 | 广西南宁乐蕊生物科技有限责任公司 | Botanical insecticide used on tea leaves |
| CN107410334A (en) * | 2017-06-28 | 2017-12-01 | 芮城华农生物化学有限公司 | A kind of Pesticidal combination and its application containing jervine and sulfoxaflor |
| CN107494581A (en) * | 2017-09-15 | 2017-12-22 | 芮城华农生物化学有限公司 | The Pesticidal combination of a kind of clothianidin-containing and jervine and its application |
| CN107624813A (en) * | 2017-10-23 | 2018-01-26 | 罗铭炽 | A kind of ecological agricultural chemical |
| CN107683857A (en) * | 2017-10-24 | 2018-02-13 | 惠州市无龄康态健康科技有限公司 | A kind of composition pesticide containing jervine |
| CN107787992A (en) * | 2017-12-05 | 2018-03-13 | 徐州农丰生物化工有限公司 | A kind of natural azadirachtin insecticide and preparation method thereof |
| CN109452317A (en) * | 2018-10-30 | 2019-03-12 | 陕西康禾立丰生物科技药业有限公司 | A kind of pesticide finish |
| CN110326623A (en) * | 2019-08-19 | 2019-10-15 | 扬州工业职业技术学院 | A kind of plant pesticide composition and preparation method thereof |
| CN110859185A (en) * | 2019-12-03 | 2020-03-06 | 贵州省烟草科学研究院 | Nicotine and veratrine compound pesticide and application thereof in preventing and treating myzus persicae |
| CN110870479A (en) * | 2019-12-09 | 2020-03-10 | 贵州省烟草科学研究院 | Nicotine and azadirachtin compound pesticide and application thereof in prevention and treatment of myzus persicae |
| CN114711245A (en) * | 2022-04-22 | 2022-07-08 | 广西大学 | Biopesticide composition for preventing and treating sweet potato weevil |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1308871A (en) * | 2000-11-23 | 2001-08-22 | 刘茂萱 | Agricultural chemical prepared from avermectin and alkaloid extracted from plant and its preparing process |
| CN1830263A (en) * | 2006-04-17 | 2006-09-13 | 山东泽禾农用化学品有限公司 | Biological pesticide composition and its preparation method and use |
| CN101317572A (en) * | 2008-07-21 | 2008-12-10 | 郭建康 | Mixed plant source insecticide |
| CN102860313A (en) * | 2012-09-28 | 2013-01-09 | 江苏省绿盾植保农药实验有限公司 | Insecticide containing sophoridine and nicotine |
| CN103004854A (en) * | 2013-01-04 | 2013-04-03 | 句容市农业技术推广中心 | Allyl isothiocyanate and nicotine compound insecticide and application thereof |
-
2014
- 2014-10-30 CN CN201410598813.5A patent/CN104430568B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1308871A (en) * | 2000-11-23 | 2001-08-22 | 刘茂萱 | Agricultural chemical prepared from avermectin and alkaloid extracted from plant and its preparing process |
| CN1830263A (en) * | 2006-04-17 | 2006-09-13 | 山东泽禾农用化学品有限公司 | Biological pesticide composition and its preparation method and use |
| CN101317572A (en) * | 2008-07-21 | 2008-12-10 | 郭建康 | Mixed plant source insecticide |
| CN102860313A (en) * | 2012-09-28 | 2013-01-09 | 江苏省绿盾植保农药实验有限公司 | Insecticide containing sophoridine and nicotine |
| CN103004854A (en) * | 2013-01-04 | 2013-04-03 | 句容市农业技术推广中心 | Allyl isothiocyanate and nicotine compound insecticide and application thereof |
Non-Patent Citations (2)
| Title |
|---|
| 《12种药剂对枸杞裸蓟马的毒力及天敌敏感性测定与田间防效试验》;关晓庆;《湖北农业科学》;20090630;第48卷(第6期);第1380-1382页 * |
| 《植物源药剂混配防治西花蓟马的药效研究》;曾亮等;《植物保护》;20090630;第35卷(第6期);第164-166页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104430568A (en) | 2015-03-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104430568B (en) | A kind of botanical pesticide for preventing and treating matrimony vine thrips | |
| CN103689017B (en) | A kind of composite plant source pesticide and preparation method thereof | |
| CN104397058B (en) | A kind of Chinese herbal medicine green pesticide and preparation method thereof | |
| CN101589716B (en) | Compound insecticide of osthole and matrine and application thereof | |
| JPH10245312A (en) | Plant protecting agent and its production | |
| CN105272633A (en) | Method of preparing fertilizer with effects of prevention and control of underground pests of crops | |
| KR20110033691A (en) | Environment-friendly organic agricultural products for soil insect pest control | |
| CN104920487B (en) | A kind of Chinese medicinal material extract and preparation method thereof and the method using Chinese medicinal material extract preventing and treating wheat aphid | |
| CN101984828A (en) | Compound pesticide | |
| CN105010368B (en) | Composition pesticide and its application | |
| CN103355322A (en) | Compound biological insecticide and application thereof | |
| CN101480199B (en) | Pesticide composition containing bamboo vinegar as well as preparation method and use thereof | |
| CN105315075A (en) | Fertilizer capable of controlling underground crop pests | |
| CN103070186B (en) | Insecticidal composition containing thiamethoxam and application of insecticidal composition | |
| CN104855432A (en) | Complex insecticide and application thereof | |
| CN104351283A (en) | Pesticide for preventing and treating rice planthoppers | |
| CN107821413A (en) | A kind of cockroach bait formulation and preparation method thereof | |
| CN106359458A (en) | Flos Inulae-containing insecticidal composition | |
| CN105685110A (en) | Plant source composite for preventing cutworms and plant source insecticide and application thereof | |
| CN111357777A (en) | Deinsectization ovum-inhibiting agent extracted from plant containing sweet wormwood herb and preparation and application methods thereof | |
| CN103875675B (en) | The complex composition of Osthole and imazalil and application thereof | |
| CN103755471A (en) | Biogas slurry compound bactericide for preventing and treating leaf mold | |
| CN108056120A (en) | A kind of curara insecticide and preparation method thereof | |
| CN104273173B (en) | Containing the pesticide synergistic composition of humic acids | |
| CN103109846B (en) | Dichlorovos kadethrine compounded pesticide |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170711 Termination date: 20201030 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |