CN108056120A - A kind of curara insecticide and preparation method thereof - Google Patents

A kind of curara insecticide and preparation method thereof Download PDF

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Publication number
CN108056120A
CN108056120A CN201711340301.9A CN201711340301A CN108056120A CN 108056120 A CN108056120 A CN 108056120A CN 201711340301 A CN201711340301 A CN 201711340301A CN 108056120 A CN108056120 A CN 108056120A
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Prior art keywords
parts
insecticide
curara
weight
raw material
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CN201711340301.9A
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Chinese (zh)
Inventor
李恪言
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Liuzhou Han Elephant Education Consulting Co Ltd
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Liuzhou Han Elephant Education Consulting Co Ltd
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Priority to CN201711340301.9A priority Critical patent/CN108056120A/en
Publication of CN108056120A publication Critical patent/CN108056120A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/36Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/44Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Mycology (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention belongs to technical field of insecticide, and in particular to a kind of curara insecticide and preparation method thereof.The curara insecticide is made of the raw material of following parts by weight:50~60 parts of vomiting nut, 30~50 parts of strophanthus divaricatus, 15~20 parts of grass-leaved sweetflag, 8~10 parts of rhizoma typhonii, 5~7 parts of rhizoma imperatae, 3~6 parts of the root bark of shaggy-fruited dittany.The vegetable insecticide simple production process of the present invention, material source is extensive, can gather materials on the spot, of low cost, safe to use to people, animal, crop;It is sprayed on crop and easily decomposes, avoid retaining residual hazard, reduce environmental pollution, there is unique control effect to rice-stem borer.

Description

A kind of curara insecticide and preparation method thereof
【Technical field】
The present invention relates to technical field of insecticide, and in particular to a kind of curara insecticide and preparation method thereof.
【Background technology】
With Pests with Botanical Pesticides pest and disease damage, have the history of 1500 in China,《Compendium of Materia Medica》In just have use The record of herbal medicine desinsection.It studies according to investigations, has 200 various plants that can be processed into natural plant medicament, for preventing agricultural fruits and vegetables Crop disease and insect.How the world today mitigates chemical pesticide pollution, ensures food security, production organic food, nuisanceless green Food increasingly gets more and more people's extensive concerning.
Vegetable insecticide can meet the environment protection requirement of the mankind, and plant insecticide, can be rapid by extracted form natural plant Degradation, no environmental problem, have it is highly selective, to safety of human and livestock, and also have do not generate resistance, without poisoning, have fertilizer efficiency, to crop Growth have stimulation, simultaneous can cure the disease insect pest the advantages that.
It can be said that appliable plant insecticide, in terms of ecological protection, has special not replaceable advantage.
【The content of the invention】
The goal of the invention of the present invention is:In view of the above problems, provide a kind of curara insecticide and its Preparation method, the vegetable insecticide simple production process, material source is extensive, can gather materials on the spot, of low cost, to people, Poultry, crop are safe to use;It is sprayed on crop and easily decomposes, avoid retaining residual hazard, reduce environmental pollution, have to rice-stem borer There is unique control effect.
To achieve these goals, the technical solution adopted by the present invention is as follows:
A kind of curara insecticide, is made of the raw material of following parts by weight:50~60 parts of vomiting nut, strophanthus divaricatus 30~ 50 parts, 15~20 parts of grass-leaved sweetflag, 8~10 parts of rhizoma typhonii, 5~7 parts of rhizoma imperatae, 3~6 parts of the root bark of shaggy-fruited dittany.
Preferably, it is made of the raw material of following parts by weight:55 parts of vomiting nut, 40 parts of strophanthus divaricatus, 17 parts of grass-leaved sweetflag, rhizoma typhonii 9 parts, 6 parts of rhizoma imperatae, 4 parts of the root bark of shaggy-fruited dittany.
Preferably, it is made of the raw material of following parts by weight:It is 50 parts of vomiting nut, 50 parts of strophanthus divaricatus, 15 parts of grass-leaved sweetflag, white attached 10 parts of son, 5 parts of rhizoma imperatae, 6 parts of the root bark of shaggy-fruited dittany.
It is highly preferred that it is made of the raw material of following parts by weight:It is 60 parts of vomiting nut, 30 parts of strophanthus divaricatus, 20 parts of grass-leaved sweetflag, white attached 8 parts of son, 7 parts of rhizoma imperatae, 3 parts of the root bark of shaggy-fruited dittany.
Further, the vegetable insecticide further includes the auxiliary agent of 5~15% mass percents.
Further, the auxiliary agent is lauric monoglyceride.
A kind of method for preparing curara insecticide of the present invention, comprises the following steps:
(1) raw material is weighed according to the parts by weight, mix and is ground into powder, it is spare;
(2) mixed-powder of step (1) is taken, adds in the volume fraction of its 10 times of weight as 60% ethyl alcohol, 20~35 DEG C Under the conditions of Soakage extraction 30 days, 200 mesh filter to take filtrate, and filtrate recycling ethanol, relative density is when being then concentrated into 60 DEG C 1.10~1.20 to get to concentrated medicament;
(3) auxiliary agent is added in concentrated medicament obtained by step (2) and obtains mixed solution, the auxiliary agent is in mixed solution Mass percent concentration reaches 5~15%, be sufficiently stirred to get.
In the present invention, the curara insecticide is for the prevention to rice-stem borer.
In conclusion by adopting the above-described technical solution, the beneficial effects of the invention are as follows:
The vegetable insecticide simple production process of the present invention, material source is extensive, can gather materials on the spot, of low cost, right People, animal, crop are safe to use;It is sprayed on crop and easily decomposes, avoid retaining residual hazard, reduce environmental pollution, rice two is changed Snout moth's larva has unique control effect.
【Specific embodiment】
Embodiment 1
A kind of curara insecticide, is made of the raw material of following parts by weight:55 parts of vomiting nut, 40 parts of strophanthus divaricatus, stone 17 parts of calamus, 9 parts of rhizoma typhonii, 6 parts of rhizoma imperatae, 4 parts of the root bark of shaggy-fruited dittany.
Wherein, the vegetable insecticide further includes the lauric monoglyceride of 10% mass percent.
A kind of method for preparing curara insecticide described in the present embodiment, comprises the following steps:
(1) raw material is weighed according to the parts by weight, mix and is ground into powder, it is spare;
(2) mixed-powder of step (1) is taken, adds in the volume fraction of its 10 times of weight as 60% ethyl alcohol, 20~35 DEG C Under the conditions of Soakage extraction 30 days, 200 mesh filter to take filtrate, and filtrate recycling ethanol, relative density is when being then concentrated into 60 DEG C 1.15 to get to concentrated medicament;
(3) lauric monoglyceride is added in concentrated medicament obtained by step (2) and obtains mixed solution, wherein lauric acid list Mass percent concentration of the glyceride in mixed solution reaches 10%, be sufficiently stirred to get.
Embodiment 2
A kind of curara insecticide, is made of the raw material of following parts by weight:50 parts of vomiting nut, 50 parts of strophanthus divaricatus, stone 15 parts of calamus, 10 parts of rhizoma typhonii, 5 parts of rhizoma imperatae, 6 parts of the root bark of shaggy-fruited dittany.
Wherein, the vegetable insecticide further includes the lauric monoglyceride of 5% mass percent.
A kind of method for preparing curara insecticide described in the present embodiment, comprises the following steps:
(1) raw material is weighed according to the parts by weight, mix and is ground into powder, it is spare;
(2) mixed-powder of step (1) is taken, adds in the volume fraction of its 10 times of weight as 60% ethyl alcohol, 20~35 DEG C Under the conditions of Soakage extraction 30 days, 200 mesh filter to take filtrate, and filtrate recycling ethanol, relative density is when being then concentrated into 60 DEG C 1.10 to get to concentrated medicament;
(3) lauric monoglyceride is added in concentrated medicament obtained by step (2) and obtains mixed solution, make lauric acid list sweet Mass percent concentration of the grease in mixed solution reaches 5%, be sufficiently stirred to get.
Embodiment 3
A kind of curara insecticide, is made of the raw material of following parts by weight:60 parts of vomiting nut, 30 parts of strophanthus divaricatus, stone 20 parts of calamus, 8 parts of rhizoma typhonii, 7 parts of rhizoma imperatae, 3 parts of the root bark of shaggy-fruited dittany.
Wherein, the vegetable insecticide further includes the lauric monoglyceride of 15% mass percent.
A kind of method for preparing curara insecticide described in the present embodiment, comprises the following steps:
(1) raw material is weighed according to the parts by weight, mix and is ground into powder, it is spare;
(2) mixed-powder of step (1) is taken, adds in the volume fraction of its 10 times of weight as 60% ethyl alcohol, 20~35 DEG C Under the conditions of Soakage extraction 30 days, 200 mesh filter to take filtrate, and filtrate recycling ethanol, relative density is when being then concentrated into 60 DEG C 1.20 to get to concentrated medicament;
(3) lauric monoglyceride is added in concentrated medicament obtained by step (2) and obtains mixed solution, make lauric acid list sweet Mass percent concentration of the grease in mixed solution reaches 15%, be sufficiently stirred to get.
Experimental example Examples 1 to 3 field control effectiveness test
1. reagent agent:Examples 1 to 3
2. controlling object:Rice-stem borer
3. place:Liuzhou suburbs
4. test period:On August 10th, 2016
5. application method:Application method is sprayed after being diluted with water and is prevented, per acre 30 kilograms of water consumption.
Plot area and repetition:Plot area:Plot area 20m2;Number of repetition:4 repetitions.
Investigation method:In August investigation insect population on the 10th before medication, residual worm is investigated respectively at August within 12,24 after medication Amount is investigated 3 times altogether.Investigation method investigates 20 plants per cell, the work borer population amount of every plant of investigation.
Control effect (%)=(chemicals treatment district Revision insect recluced rate-blank district Revision insect recluced rate)/(100- blank pair According to area's Revision insect recluced rate) × 100.
The results are shown in table below:
Examples 1 to 3 various concentration is to the control effect of rice-stem borer
1~3 pair of rice-stem borer of the embodiment of the present invention has preferable control effect as can be seen from the above table.
Above description is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair Bright patent claim, the equal variation or modification change completed under the technical spirit suggested by all present invention, should all belong to Cover the scope of the claims in the present invention.

Claims (8)

1. a kind of curara insecticide, which is characterized in that be made of the raw material of following parts by weight:50~60 parts of vomiting nut, 30~50 parts of strophanthus divaricatus, 15~20 parts of grass-leaved sweetflag, 8~10 parts of rhizoma typhonii, 5~7 parts of rhizoma imperatae, 3~6 parts of the root bark of shaggy-fruited dittany.
2. curara insecticide according to claim 1, it is characterised in that be made of the raw material of following parts by weight:Horse 55 parts of money, 40 parts of strophanthus divaricatus, 17 parts of grass-leaved sweetflag, 9 parts of rhizoma typhonii, 6 parts of rhizoma imperatae, 4 parts of the root bark of shaggy-fruited dittany.
3. curara insecticide according to claim 1, it is characterised in that be made of the raw material of following parts by weight:Horse 50 parts of money, 50 parts of strophanthus divaricatus, 15 parts of grass-leaved sweetflag, 10 parts of rhizoma typhonii, 5 parts of rhizoma imperatae, 6 parts of the root bark of shaggy-fruited dittany.
4. curara insecticide according to claim 1, it is characterised in that be made of the raw material of following parts by weight:Horse 60 parts of money, 30 parts of strophanthus divaricatus, 20 parts of grass-leaved sweetflag, 8 parts of rhizoma typhonii, 7 parts of rhizoma imperatae, 3 parts of the root bark of shaggy-fruited dittany.
5. according to Claims 1 to 4 any one of them curara insecticide, which is characterized in that the vegetable insecticide Further include the auxiliary agent of 5~15% mass percents.
6. curara insecticide according to claim 5, which is characterized in that the auxiliary agent is lauric monoglyceride Ester.
A kind of 7. method for preparing any one of Claims 1 to 4 curara insecticide, which is characterized in that including with Lower step:
(1) raw material is weighed according to the parts by weight, mix and is ground into powder, it is spare;
(2) mixed-powder of step (1) is taken, adds in the volume fraction of its 10 times of weight as 60% ethyl alcohol, 20~35 DEG C of conditions Lower Soakage extraction 30 days, 200 mesh filter to take filtrate, filtrate recycling ethanol, when being then concentrated into 60 DEG C relative density for 1.10~ 1.20 to get to concentrated medicament;
(3) auxiliary agent is added in concentrated medicament obtained by step (2) and obtains mixed solution, quality of the auxiliary agent in mixed solution Percent concentration reaches 5~15%, be sufficiently stirred to get.
8. according to Claims 1 to 4 any one of them curara insecticide, which is characterized in that the curara Insecticide is for the prevention to rice-stem borer.
CN201711340301.9A 2017-12-14 2017-12-14 A kind of curara insecticide and preparation method thereof Pending CN108056120A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108703164A (en) * 2018-06-28 2018-10-26 武汉中智德远科技开发有限公司 A kind of plant sapling insecticide and preparation method thereof

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