CN107853334A - A kind of radix ranunculi ternati vegetable insecticide and preparation method thereof - Google Patents

A kind of radix ranunculi ternati vegetable insecticide and preparation method thereof Download PDF

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Publication number
CN107853334A
CN107853334A CN201711342096.XA CN201711342096A CN107853334A CN 107853334 A CN107853334 A CN 107853334A CN 201711342096 A CN201711342096 A CN 201711342096A CN 107853334 A CN107853334 A CN 107853334A
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China
Prior art keywords
parts
radix ranunculi
ranunculi ternati
vegetable insecticide
weight
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CN201711342096.XA
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Chinese (zh)
Inventor
李恪言
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Liuzhou Han Elephant Education Consulting Co Ltd
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Liuzhou Han Elephant Education Consulting Co Ltd
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Priority to CN201711342096.XA priority Critical patent/CN107853334A/en
Publication of CN107853334A publication Critical patent/CN107853334A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/36Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Microbiology (AREA)
  • Agronomy & Crop Science (AREA)
  • Biotechnology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Mycology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention belongs to technical field of insecticide, and in particular to a kind of radix ranunculi ternati vegetable insecticide and preparation method thereof.The radix ranunculi ternati vegetable insecticide is made up of the raw material of following parts by weight:30~50 parts of radix ranunculi ternati, 10~20 parts of golden cypress, 15~20 parts of Phytolacca acinosa, 13~18 parts of chrysanthemum indicum, 5~10 parts of Gorgon fruit, 6~8 parts of Golden Larch Bark.The vegetable insecticide simple production process of the present invention, material source is extensive, can gather materials on the spot, and cost is cheap, safe to use to people, animal, crop;It is sprayed on crop and easily decomposes, avoids retaining residual hazard, reduce environmental pollution, there is unique prevention effect to rice-stem borer.

Description

A kind of radix ranunculi ternati vegetable insecticide and preparation method thereof
【Technical field】
The present invention relates to technical field of insecticide, and in particular to a kind of radix ranunculi ternati vegetable insecticide and preparation method thereof.
【Background technology】
With Pests with Botanical Pesticides pest and disease damage, have the history of 1500 in China,《Compendium of Materia Medica》In just have use The record of herbal medicine desinsection.Study according to investigations, there are 200 various plants to be processed into natural plant medicament, for preventing and treating agricultural fruits and vegetables Crop disease and insect.How the world today mitigates chemical pesticide pollution, ensures food security, production organic food, nuisanceless green Food, increasingly get more and more people's extensive concerning.
Vegetable insecticide can meet the environment protection requirement of the mankind, and plant insecticide, can be rapid by extracted form natural plant Degraded, no environmental problem, there is high selectivity, to person poultry safety, and also have do not produce resistance, without poisoning, have fertilizer efficiency, to crop Growth have stimulation, simultaneous can cure the disease insect pest the advantages that.
It can be said that appliable plant insecticide, in terms of ecological protection, has special not replaceable advantage.
【The content of the invention】
The goal of the invention of the present invention is:For above-mentioned problem, there is provided a kind of radix ranunculi ternati vegetable insecticide and its Preparation method, the vegetable insecticide simple production process, material source is extensive, can gather materials on the spot, and cost is cheap, to people, Poultry, crop are safe to use;It is sprayed on crop and easily decomposes, avoids retaining residual hazard, reduce environmental pollution, have to rice-stem borer There is the prevention effect of uniqueness.
To achieve these goals, the technical solution adopted by the present invention is as follows:
A kind of radix ranunculi ternati vegetable insecticide, is made up of the raw material of following parts by weight:30~50 parts of radix ranunculi ternati, golden cypress 10~20 Part, 15~20 parts of Phytolacca acinosa, 13~18 parts of chrysanthemum indicum, 5~10 parts of Gorgon fruit, 6~8 parts of Golden Larch Bark.
Preferably, it is made up of the raw material of following parts by weight:40 parts of radix ranunculi ternati, 15 parts of golden cypress, 18 parts of Phytolacca acinosa, chrysanthemum indicum 15 Part, 7 parts of Gorgon fruit, 7 parts of Golden Larch Bark.
Preferably, it is made up of the raw material of following parts by weight:30 parts of radix ranunculi ternati, 20 parts of golden cypress, 15 parts of Phytolacca acinosa, chrysanthemum indicum 18 Part, 5 parts of Gorgon fruit, 8 parts of Golden Larch Bark.
It is highly preferred that it is made up of the raw material of following parts by weight:50 parts of radix ranunculi ternati, 10 parts of golden cypress, 20 parts of Phytolacca acinosa, chrysanthemum indicum 13 Part, 10 parts of Gorgon fruit, 6 parts of Golden Larch Bark.
Further, the vegetable insecticide also includes the auxiliary agent of 5~15% mass percents.
Further, the auxiliary agent is lauric monoglyceride.
A kind of method for preparing radix ranunculi ternati vegetable insecticide of the present invention, comprises the following steps:
(1) raw material is weighed according to the parts by weight, mixes and be ground into powder, it is standby;
(2) take the mixed-powder of step (1), add its 10 times of weight volume fraction be 60% ethanol, 20~35 DEG C Under the conditions of Soakage extraction 30 days, 200 mesh filter to take filtrate, and filtrate recycling ethanol, relative density is when being then concentrated into 60 DEG C 1.10~1.20, that is, obtain concentrated medicament;
(3) auxiliary agent is added in concentrated medicament obtained by step (2) and obtains mixed solution, the auxiliary agent is in mixed solution Mass percent concentration reaches 5~15%, is sufficiently stirred, and produces.
In the present invention, the radix ranunculi ternati vegetable insecticide is used for the preventing and treating to rice-stem borer.
In summary, by adopting the above-described technical solution, the beneficial effects of the invention are as follows:
The vegetable insecticide simple production process of the present invention, material source is extensive, can gather materials on the spot, and cost is cheap, right People, animal, crop are safe to use;It is sprayed on crop and easily decomposes, avoids retaining residual hazard, reduce environmental pollution, rice two is changed Snout moth's larva has unique prevention effect.
【Embodiment】
Embodiment 1
A kind of radix ranunculi ternati vegetable insecticide, is made up of the raw material of following parts by weight:
40 parts of radix ranunculi ternati, 15 parts of golden cypress, 18 parts of Phytolacca acinosa, 15 parts of chrysanthemum indicum, 7 parts of Gorgon fruit, 7 parts of Golden Larch Bark.
Wherein, the vegetable insecticide also includes the lauric monoglyceride of 10% mass percent.
A kind of method for preparing radix ranunculi ternati vegetable insecticide described in the present embodiment, comprises the following steps:
(1) raw material is weighed according to the parts by weight, mixes and be ground into powder, it is standby;
(2) take the mixed-powder of step (1), add its 10 times of weight volume fraction be 60% ethanol, 20~35 DEG C Under the conditions of Soakage extraction 30 days, 200 mesh filter to take filtrate, and filtrate recycling ethanol, relative density is when being then concentrated into 60 DEG C 1.15, that is, obtain concentrated medicament;
(3) lauric monoglyceride is added in concentrated medicament obtained by step (2) and obtains mixed solution, wherein laurate list Mass percent concentration of the glyceride in mixed solution reaches 10%, is sufficiently stirred, produces.
Embodiment 2
A kind of radix ranunculi ternati vegetable insecticide, is made up of the raw material of following parts by weight:
30 parts of radix ranunculi ternati, 20 parts of golden cypress, 15 parts of Phytolacca acinosa, 18 parts of chrysanthemum indicum, 5 parts of Gorgon fruit, 8 parts of Golden Larch Bark.
Wherein, the vegetable insecticide also includes the lauric monoglyceride of 5% mass percent.
A kind of method for preparing radix ranunculi ternati vegetable insecticide described in the present embodiment, comprises the following steps:
(1) raw material is weighed according to the parts by weight, mixes and be ground into powder, it is standby;
(2) take the mixed-powder of step (1), add its 10 times of weight volume fraction be 60% ethanol, 20~35 DEG C Under the conditions of Soakage extraction 30 days, 200 mesh filter to take filtrate, and filtrate recycling ethanol, relative density is when being then concentrated into 60 DEG C 1.10, that is, obtain concentrated medicament;
(3) lauric monoglyceride is added in concentrated medicament obtained by step (2) and obtains mixed solution, make laurate list sweet Mass percent concentration of the grease in mixed solution reaches 5%, is sufficiently stirred, produces.
Embodiment 3
A kind of radix ranunculi ternati vegetable insecticide, is made up of the raw material of following parts by weight:
50 parts of radix ranunculi ternati, 10 parts of golden cypress, 20 parts of Phytolacca acinosa, 13 parts of chrysanthemum indicum, 10 parts of Gorgon fruit, 6 parts of Golden Larch Bark.
Wherein, the vegetable insecticide also includes the lauric monoglyceride of 15% mass percent.
A kind of method for preparing radix ranunculi ternati vegetable insecticide described in the present embodiment, comprises the following steps:
(1) raw material is weighed according to the parts by weight, mixes and be ground into powder, it is standby;
(2) take the mixed-powder of step (1), add its 10 times of weight volume fraction be 60% ethanol, 20~35 DEG C Under the conditions of Soakage extraction 30 days, 200 mesh filter to take filtrate, and filtrate recycling ethanol, relative density is when being then concentrated into 60 DEG C 1.20, that is, obtain concentrated medicament;
(3) lauric monoglyceride is added in concentrated medicament obtained by step (2) and obtains mixed solution, make laurate list sweet Mass percent concentration of the grease in mixed solution reaches 15%, is sufficiently stirred, produces.
The field control effectiveness test of experimental example embodiment 1~3
1. reagent agent:Embodiment 1~3
2. controlling object:Rice-stem borer
3. place:Liuzhou suburbs
4. test period:On August 10th, 2016
5. application method:Application method, preventing and treating of being sprayed after being diluted with water, every mu of 30 kilograms of water consumption.
Plot area and repetition:Plot area:Plot area 20m2;Number of repetition:4 repetitions.
Investigation method:In August investigation insect population on the 10th before medication, residual worm is investigated within 12,24 respectively at August after medication Amount, investigate 3 times altogether.Investigation method investigates 20 plants per cell, the work borer population amount of every plant of investigation.
Prevention effect (%)=(chemicals treatment district Revision insect recluced rate-blank district Revision insect recluced rate)/(100- blank pair According to area's Revision insect recluced rate) × 100.
As a result it is as shown in the table:
Prevention effect of the various concentrations of embodiment 1~3 to rice-stem borer
1~3 pair of rice-stem borer of the embodiment of the present invention has preferable prevention effect as can be seen from the above table.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair Bright patent claim, the equal change completed or modification change under the technical spirit suggested by all present invention, all should belong to Cover the scope of the claims in the present invention.

Claims (8)

1. a kind of radix ranunculi ternati vegetable insecticide, it is characterised in that be made up of the raw material of following parts by weight:30~50 parts of radix ranunculi ternati, 10~20 parts of golden cypress, 15~20 parts of Phytolacca acinosa, 13~18 parts of chrysanthemum indicum, 5~10 parts of Gorgon fruit, 6~8 parts of Golden Larch Bark.
2. radix ranunculi ternati vegetable insecticide according to claim 1, it is characterised in that be made up of the raw material of following parts by weight:Cat 40 parts of pawl grass, 15 parts of golden cypress, 18 parts of Phytolacca acinosa, 15 parts of chrysanthemum indicum, 7 parts of Gorgon fruit, 7 parts of Golden Larch Bark.
3. radix ranunculi ternati vegetable insecticide according to claim 1, it is characterised in that be made up of the raw material of following parts by weight:Cat 30 parts of pawl grass, 20 parts of golden cypress, 15 parts of Phytolacca acinosa, 18 parts of chrysanthemum indicum, 5 parts of Gorgon fruit, 8 parts of Golden Larch Bark.
4. radix ranunculi ternati vegetable insecticide according to claim 1, it is characterised in that be made up of the raw material of following parts by weight:Cat 50 parts of pawl grass, 10 parts of golden cypress, 20 parts of Phytolacca acinosa, 13 parts of chrysanthemum indicum, 10 parts of Gorgon fruit, 6 parts of Golden Larch Bark.
5. the radix ranunculi ternati vegetable insecticide according to any one of Claims 1 to 4, it is characterised in that the vegetable insecticide Also include the auxiliary agent of 5~15% mass percents.
6. radix ranunculi ternati vegetable insecticide according to claim 5, it is characterised in that the auxiliary agent is lauric monoglyceride Ester.
A kind of 7. method for preparing any one of Claims 1 to 4 radix ranunculi ternati vegetable insecticide, it is characterised in that including with Lower step:
(1) raw material is weighed according to the parts by weight, mixes and be ground into powder, it is standby;
(2) mixed-powder of step (1) is taken, the volume fraction for adding its 10 times of weight is 60% ethanol, 20~35 DEG C of conditions Lower Soakage extraction 30 days, 200 mesh filter to take filtrate, filtrate recycling ethanol, when being then concentrated into 60 DEG C relative density be 1.10~ 1.20, that is, obtain concentrated medicament;
(3) auxiliary agent is added in concentrated medicament obtained by step (2) and obtains mixed solution, quality of the auxiliary agent in mixed solution Percent concentration reaches 5~15%, is sufficiently stirred, and produces.
8. the radix ranunculi ternati vegetable insecticide according to any one of Claims 1 to 4, it is characterised in that the radix ranunculi ternati plant Insecticide is used for the preventing and treating to rice-stem borer.
CN201711342096.XA 2017-12-14 2017-12-14 A kind of radix ranunculi ternati vegetable insecticide and preparation method thereof Pending CN107853334A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102960373A (en) * 2012-12-04 2013-03-13 南通恒鼎重型机床有限公司 Cockroach killer
CN103828867A (en) * 2012-11-27 2014-06-04 李建国 Traditional Chinese medicine insecticide and preparation method thereof
CN104938538A (en) * 2015-06-04 2015-09-30 胡凡营 Plant-derived pesticide and production method thereof
CN106106566A (en) * 2016-08-15 2016-11-16 青岛悦邦农种业有限公司 A kind of Farm chemical of Chinese berbs and preparation method thereof
CN106472597A (en) * 2015-09-01 2017-03-08 开县朝国农业开发有限公司 Citrus insecticide

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103828867A (en) * 2012-11-27 2014-06-04 李建国 Traditional Chinese medicine insecticide and preparation method thereof
CN102960373A (en) * 2012-12-04 2013-03-13 南通恒鼎重型机床有限公司 Cockroach killer
CN104938538A (en) * 2015-06-04 2015-09-30 胡凡营 Plant-derived pesticide and production method thereof
CN106472597A (en) * 2015-09-01 2017-03-08 开县朝国农业开发有限公司 Citrus insecticide
CN106106566A (en) * 2016-08-15 2016-11-16 青岛悦邦农种业有限公司 A kind of Farm chemical of Chinese berbs and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
姚荣林等: "《中药鉴定技术》", 31 January 2017, 中国医药科技出版社 *
王国夫等: "商陆等3种植物提取物对菜粉蝶的拒食作用", 《安徽农业科学》 *
苗耀东等: "猫爪草的化学成分及药理作用研究进展", 《中草药》 *

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Application publication date: 20180330

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