CN105248479A - Pesticide special for tangerine tree and preparation method of pesticide - Google Patents
Pesticide special for tangerine tree and preparation method of pesticide Download PDFInfo
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- CN105248479A CN105248479A CN201510696247.6A CN201510696247A CN105248479A CN 105248479 A CN105248479 A CN 105248479A CN 201510696247 A CN201510696247 A CN 201510696247A CN 105248479 A CN105248479 A CN 105248479A
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- tangerine
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- allicin
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses pesticide special for a tangerine tree and a preparation method of the pesticide. The pesticide is prepared from, by weight, 10-20 parts of black false hellebore, 10-20 parts of melia azedarach, 10-20 parts of derris and 20-40 parts of allicin. The pesticide is prepared through the steps of drying, smashing, solvent extracting, filtering, concentrating, mixing, grinding and the like. Pest killing functions of black false hellebore, melia azedarach, derris and allicin are fused; if the pesticide is added to fertilizer for the tangerine tree, invasion of pests can be effectively prevented, the capacity of the tangerine tree for resisting diseases and pests is improved, and therefore the yield and quality of the tangerine tree are improved. The pesticide is free of pollution and residues, green and environmentally friendly.
Description
[technical field]
The invention belongs to application technical field, be specifically related to a kind of tangerine special-purpose insecticide and preparation method thereof.
[background technology]
China is one of main cradle of tangerine, and Chinese ancients eat orange, and wild tangerine is carried out artificial cultivation, has had long history.Orange is the fruit of rutaceae, has several kind, and fruit rinds is plump, is made up of juice bubble and seed.Orange belongs to tropical crop, mainly plants in southern china, and orange is bright in luster but also sweet and sour taste not only, is common delicious food.The sweet acid of Orange flavor, warm in nature, enter lung.Mainly control very thirsty in septum pectorale knot gas, vomit inverse few food, deficiency of stomach-Yin, mouth, cough with lung heat and insobriety.There is appetizing, the effect of moistening lung of quenching the thirst.Orange nutrition is also very abundant, and an orange just almost meets human body Vitamin C content required in a day, and plants flavonoids containing more than 170 Plants compounds and more than 60 in orange, and most of materials are wherein all naturals.Nutrient component abundant in orange has the effect such as reducing blood lipid, antiatherosclerosis, benefiting for angiocardiopathy preventing.Material containing a kind of " Nomilin " by name in orange juice, has the ability suppressing and kill cancer cell, has prevention effect to cancer of the stomach.
Damage by disease and insect is come to the biggest threat of orange yield and quality.Peasant households adopt pharmaceutical treatment when tangerine generation damage by disease and insect.Damage by disease and insect, once generation, even if adopt chemical control, produces effects also undesirable.Most of agricultural chemical insecticide not only can cause environmental pollution, and cannot play a role at tangerine organization internal, and tangerine disease can not be controlled to greatest extent.
[summary of the invention]
In order to solve in prior art pesticide pollution residual large, can not the problem such as prevention and control tangerine damage by disease and insect to greatest extent, the invention provides a kind of tangerine special-purpose insecticide and preparation method thereof, give full play to the disinsection efficiency of black false hellebore, China tree, trifoliate jewelvine and allicin, join in tangerine fertilizer, effectively can resist insect invasion, improve the ability of tangerine disease and insect resistance, thus improve the seed output and quality of orange.
Technical scheme of the present invention is as follows:
A kind of tangerine special-purpose insecticide, comprises the raw material of following weight portion: black false hellebore 10-20 part, China tree 10-20 part, trifoliate jewelvine 10-20 part, allicin 20-40 part.
Preferably, described tangerine special-purpose insecticide comprises the raw material of following weight portion: black false hellebore 12-18 part, China tree 13-17 part, trifoliate jewelvine 12-18 part, allicin 25-35 part.
Preferably, described tangerine special-purpose insecticide comprises the raw material of following weight portion: black false hellebore 15 parts, China tree 14 parts, trifoliate jewelvine 14 parts, allicin 30 parts.
In described tangerine special pesticide agent prescription, the function of each raw material is as follows:
Black false hellebore, containing alkaloids such as jervine, false jervine, Rubijevine, colchicin, germerine and veratroylzygadenines, is effective insecticidal constituent, insect is had to the effects such as poisoning, food refusal and Developing restraint growth.
China tree, has insecticidal activity, has stomach toxicity, food refusal and the inhibit activities that grows to insect.
Trifoliate jewelvine, containing multiple insecticidal active compounds such as rotenone, tephrosin, bastard indigo phenol.Insecticidal rotenone spectrum is wide, can cause insect antifeedant, movable sluggish and paralysis, can prevent and treat 800 various pests.
Allicin, has strong expelling parasite antibacterial action, all has suppression and killing action to multiple coccus, bacillus, fungi and virus etc., is the one that in the natural plants found at present, antibacterial action is the strongest, without toxicity, side effect, and drug residue free.
The present invention also provides a kind of preparation method of tangerine special-purpose insecticide, comprises the following steps:
S1: black false hellebore, China tree and trifoliate jewelvine are cleaned, and dry under being put in the temperature of 70-80 DEG C;
S2: black false hellebore dried in step S1, China tree and trifoliate jewelvine are carried out mixing, pulverizing, crosses 40-50 object sieve, obtains mixture A;
S3: the mixture A that step S2 is obtained pours in solvent, filters, can obtain mixed liquor at the temperature of 93-97 DEG C after heating 10-12h;
S4: the mixed liquor obtained by step S3 is concentrated at the temperature of 70-80 DEG C, obtains mixture B;
S5: by after mixture B obtained for step S4 and allicin combination drying, grind to form 100-120 object powder, namely obtain tangerine special-purpose insecticide.
Preferably, solvent described in step S3 comprises ethanol, acetone or ethyl acetate.
Preferably, weight of solvent described in step S3 is 5 times of the weight of the mixture A that step S2 obtains.
Preferably, in step S4, described mixed liquor is concentrated into water content≤20%.
The invention has the beneficial effects as follows:
1, tangerine special-purpose insecticide of the present invention can be uniformly distributed in fertilizer, play a role at tangerine organization internal, give full play to the insecticidal power of black false hellebore, China tree, trifoliate jewelvine and allicin, effective opposing insect invasion, improve the ability of tangerine disease and insect resistance, thus improve the output of tangerine and the quality of orange.
2, tangerine special-purpose insecticide of the present invention environmental protection, not contaminated soil and water source, and to orange drug residue free, ensure that the edible safety of orange.
[embodiment]
Be described below in conjunction with specific embodiment.
Embodiment 1
A kind of tangerine special-purpose insecticide, comprises the raw material of following weight portion: black false hellebore 10 parts, China tree 10 parts, trifoliate jewelvine 20 parts, allicin 20 parts.
The present invention also provides a kind of preparation method of tangerine special-purpose insecticide, comprises the following steps:
S1: black false hellebore, China tree and trifoliate jewelvine are cleaned, and dry under being put in the temperature of 70 DEG C;
S2: black false hellebore dried in step S1, China tree and trifoliate jewelvine are carried out mixing, pulverizing, crosses 40 object sieves, obtains mixture A;
S3: the mixture A that step S2 is obtained pours in ethanol, and the weight of ethanol is 5 times of the weight of described mixture A, filters, can obtain mixed liquor at the temperature of 93 DEG C after heating 12h;
S4: the mixed liquor obtained by step S3 is concentrated into water content≤20% at the temperature of 70 DEG C, obtains mixture B;
S5: by after mixture B obtained for step S4 and allicin combination drying, grind to form 100 object powder, namely obtain tangerine special-purpose insecticide.
Embodiment 2
A kind of tangerine special-purpose insecticide, comprises the raw material of following weight portion: black false hellebore 20 parts, China tree 20 parts, trifoliate jewelvine 10 parts, allicin 40 parts.
The present invention also provides a kind of preparation method of tangerine special-purpose insecticide, comprises the following steps:
S1: black false hellebore, China tree and trifoliate jewelvine are cleaned, and dry under being put in the temperature of 80 DEG C;
S2: black false hellebore dried in step S1, China tree and trifoliate jewelvine are carried out mixing, pulverizing, crosses 50 object sieves, obtains mixture A;
S3: the mixture A that step S2 is obtained pours in ethyl acetate, and the weight of ethyl acetate is 5 times of the weight of described mixture A, filters, can obtain mixed liquor at the temperature of 97 DEG C after heating 10h;
S4: the mixed liquor obtained by step S3 is concentrated into water content≤20% at the temperature of 80 DEG C, obtains mixture B;
S5: by after mixture B obtained for step S4 and allicin combination drying, grind to form 120 object powder, namely obtain tangerine special-purpose insecticide.
Embodiment 3
A kind of tangerine special-purpose insecticide, comprises the raw material of following weight portion: black false hellebore 12 parts, China tree 17 parts, trifoliate jewelvine 12 parts, allicin 25 parts.
The present invention also provides a kind of preparation method of tangerine special-purpose insecticide, comprises the following steps:
S1: black false hellebore, China tree and trifoliate jewelvine are cleaned, and dry under being put in the temperature of 70 DEG C;
S2: black false hellebore dried in step S1, China tree and trifoliate jewelvine are carried out mixing, pulverizing, crosses 50 object sieves, obtains mixture A;
S3: the mixture A that step S2 is obtained pours in acetone, and acetone weight is 5 times of the weight of described mixture A, filters, can obtain mixed liquor at the temperature of 97 DEG C after heating 12h;
S4: the mixed liquor obtained by step S3 is concentrated into water content≤20% at the temperature of 70 DEG C, obtains mixture B;
S5: by after mixture B obtained for step S4 and allicin combination drying, grind to form 100 object powder, namely obtain tangerine special-purpose insecticide.
Embodiment 4
A kind of tangerine special-purpose insecticide, comprises the raw material of following weight portion: black false hellebore 18 parts, China tree 13 parts, trifoliate jewelvine 18 parts, allicin 35 parts.
The present invention also provides a kind of preparation method of tangerine special-purpose insecticide, comprises the following steps:
S1: black false hellebore, China tree and trifoliate jewelvine are cleaned, and dry under being put in the temperature of 80 DEG C;
S2: black false hellebore dried in step S1, China tree and trifoliate jewelvine are carried out mixing, pulverizing, crosses 40 object sieves, obtains mixture A;
S3: the mixture A that step S2 is obtained pours in ethanol, and ethanol weight is 5 times of the weight of described mixture A, filters, can obtain mixed liquor at the temperature of 93 DEG C after heating 10h;
S4: the mixed liquor obtained by step S3 is concentrated into water content≤20% at the temperature of 80 DEG C, obtains mixture B;
S5: by after mixture B obtained for step S4 and allicin combination drying, grind to form 120 object powder, namely obtain tangerine special-purpose insecticide.
Embodiment 5
A kind of tangerine special-purpose insecticide, comprises the raw material of following weight portion: black false hellebore 15 parts, China tree 14 parts, trifoliate jewelvine 14 parts, allicin 30 parts.
The present invention also provides a kind of preparation method of tangerine special-purpose insecticide, comprises the following steps:
S1: black false hellebore, China tree and trifoliate jewelvine are cleaned, and dry under being put in the temperature of 75 DEG C;
S2: black false hellebore dried in step S1, China tree and trifoliate jewelvine are carried out mixing, pulverizing, crosses 45 object sieves, obtains mixture A;
S3: the mixture A that step S2 is obtained pours in acetone, and acetone weight is 5 times of the weight of described mixture A, filters, can obtain mixed liquor at the temperature of 96 DEG C after heating 10h;
S4: the mixed liquor obtained by step S3 is concentrated into water content≤20% at the temperature of 76 DEG C, obtains mixture B;
S5: by after mixture B obtained for step S4 and allicin combination drying, grind to form 110 object powder, namely obtain tangerine special-purpose insecticide.
For verifying the effect of tangerine special-purpose insecticide of the present invention, be described by following experiment.
The sample of embodiments of the invention 1-5 is added in tangerine fertilizer, be applied to respectively on the tangerine seedling of identical sturdy degree with commercially available fertilizer.Following table is the effectiveness comparison of fertilizer after adding embodiment sample and commercially available fertilizer:
Can be drawn the following conclusions by upper table: after adding embodiment of the present invention sample, the tangerine incidence of disease reduces greatly, illustrates that product of the present invention can effectively strengthen tangerine diseases and insect pests resistance, improves orange output.
Above content can not assert that specific embodiment of the invention is confined to these explanations; for general technical staff of the technical field of the invention; without departing from the inventive concept of the premise; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted to claims.
Claims (7)
1. a tangerine special-purpose insecticide, is characterized in that, comprises the raw material of following weight portion: black false hellebore 10-20 part, China tree 10-20 part, trifoliate jewelvine 10-20 part, allicin 20-40 part.
2. tangerine special-purpose insecticide according to claim 1, is characterized in that, comprises the raw material of following weight portion: black false hellebore 12-18 part, China tree 13-17 part, trifoliate jewelvine 12-18 part, allicin 25-35 part.
3. tangerine special-purpose insecticide according to claim 1, is characterized in that, comprises the raw material of following weight portion: black false hellebore 15 parts, China tree 14 parts, trifoliate jewelvine 14 parts, allicin 30 parts.
4. a preparation method for the tangerine special-purpose insecticide according to any one of claim 1-3, is characterized in that, comprise the following steps:
S1: black false hellebore, China tree and trifoliate jewelvine are cleaned, and dry under being put in the temperature of 70-80 DEG C;
S2: black false hellebore dried in step S1, China tree and trifoliate jewelvine are carried out mixing, pulverizing, crosses 40-50 object sieve, obtains mixture A;
S3: the mixture A that step S2 is obtained pours in solvent, filters, can obtain mixed liquor at the temperature of 93-97 DEG C after heating 10-12h;
S4: the mixed liquor obtained by step S3 is concentrated at the temperature of 70-80 DEG C, obtains mixture B;
S5: by after mixture B obtained for step S4 and allicin combination drying, grind to form 100-120 object powder, namely obtain tangerine special-purpose insecticide.
5. the preparation method of tangerine special-purpose insecticide according to claim 4, is characterized in that, solvent described in step S3 comprises ethanol, acetone or ethyl acetate.
6. the preparation method of tangerine special-purpose insecticide according to claim 4, is characterized in that, weight of solvent described in step S3 is 5 times of the weight of the mixture A that step S2 obtains.
7. the preparation method of tangerine special-purpose insecticide according to claim 4, is characterized in that, in step S4, described mixed liquor is concentrated into water content≤20%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510696247.6A CN105248479A (en) | 2015-10-23 | 2015-10-23 | Pesticide special for tangerine tree and preparation method of pesticide |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510696247.6A CN105248479A (en) | 2015-10-23 | 2015-10-23 | Pesticide special for tangerine tree and preparation method of pesticide |
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| CN105248479A true CN105248479A (en) | 2016-01-20 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510696247.6A Pending CN105248479A (en) | 2015-10-23 | 2015-10-23 | Pesticide special for tangerine tree and preparation method of pesticide |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106538641A (en) * | 2016-11-14 | 2017-03-29 | 李媛源 | A kind of plant protecting liquid, preparation method and application |
| CN107244962A (en) * | 2017-05-27 | 2017-10-13 | 兰溪市酉泽饲料技术服务有限公司 | Chinese herbal medicine reinforcing agent for preventing and treating wheat insect pest |
| CN107668105A (en) * | 2017-08-28 | 2018-02-09 | 广西柳城县绿之缘生态农业科技有限公司 | A kind of citrus plantation special-purpose insecticide, its preparation method and application method |
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| CN1108474A (en) * | 1994-03-16 | 1995-09-20 | 詹桂边 | "Shamieling"-an agrichemical without enviromental pollution for plant |
| CN1183902A (en) * | 1996-11-28 | 1998-06-10 | 阎福永 | Plant protecting agent |
| CN102659484A (en) * | 2012-04-13 | 2012-09-12 | 常熟市滨江农业科技有限公司 | Traditional Chinese medicinal herb protective granule |
| CN104855433A (en) * | 2015-04-20 | 2015-08-26 | 唐兴龙 | Grape special-purposed botanical pesticide |
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2015
- 2015-10-23 CN CN201510696247.6A patent/CN105248479A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1108474A (en) * | 1994-03-16 | 1995-09-20 | 詹桂边 | "Shamieling"-an agrichemical without enviromental pollution for plant |
| CN1183902A (en) * | 1996-11-28 | 1998-06-10 | 阎福永 | Plant protecting agent |
| CN102659484A (en) * | 2012-04-13 | 2012-09-12 | 常熟市滨江农业科技有限公司 | Traditional Chinese medicinal herb protective granule |
| CN104855433A (en) * | 2015-04-20 | 2015-08-26 | 唐兴龙 | Grape special-purposed botanical pesticide |
Non-Patent Citations (4)
| Title |
|---|
| 徐建国: "《柑橘优良品种及无公害栽培技术》", 31 January 2003, 中国农业出版社 * |
| 李会平等: "《果树栽培与病虫害防治》", 31 March 2013, 北京理工大学出版社 * |
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| 陈三斌: "《农用化工产品手册》", 30 April 2008, 金盾出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106538641A (en) * | 2016-11-14 | 2017-03-29 | 李媛源 | A kind of plant protecting liquid, preparation method and application |
| CN107244962A (en) * | 2017-05-27 | 2017-10-13 | 兰溪市酉泽饲料技术服务有限公司 | Chinese herbal medicine reinforcing agent for preventing and treating wheat insect pest |
| CN107668105A (en) * | 2017-08-28 | 2018-02-09 | 广西柳城县绿之缘生态农业科技有限公司 | A kind of citrus plantation special-purpose insecticide, its preparation method and application method |
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| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160120 |
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| RJ01 | Rejection of invention patent application after publication |