CN1183902A - Plant protecting agent - Google Patents
Plant protecting agent Download PDFInfo
- Publication number
- CN1183902A CN1183902A CN96120784A CN96120784A CN1183902A CN 1183902 A CN1183902 A CN 1183902A CN 96120784 A CN96120784 A CN 96120784A CN 96120784 A CN96120784 A CN 96120784A CN 1183902 A CN1183902 A CN 1183902A
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- mother liquor
- nicotine
- kuh
- seng
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The plant protecting agent is pesticide containing plant material. It is preparey by mixing the acid or alcohol extracted mother liquor of nicotine, chinaberry, orange seed, derris trifoliata, Radix Sophorae Flavescentis, orange peel, etc. with the supplementary material including emulsifier, assistant, penetrant antioxidant, resistance eliminating liquid and turpentine oil and emulsification under heating and stirring condition. It has pesticidal and bacteriostasis effect and is suitable for vegetable, fruits, medicinal plant, tobacco and flower.
Description
The present invention relates to a kind of plant protection product, belong to the insecticide that contains vegetable material.
Current, the agricultural of countries in the world all exists the infringement of chemical highly toxic pesticide, and the remaining toxicity of agricultural chemicals and the pesticide resistance of insect pest have been brought serious vicious circle again.Human for overcoming existing highly toxic pesticide " substantivity " " property indirectly " " accumulative total property " " permeability " " potentiality " disaster, continually developing efficiently, the novel pesticide of low toxicity, noresidue, particularly utilize the novel plant insecticide of Chinese herbal medicine extracting.
" the kushenin vegetable insecticide " that Chinese patent 1064389 is introduced is to be main propose immersion liquid and be equipped with preservative etc. and form by kuh-seng, the tuber of stemona, Rhododendron molle, Chinese honey locust, Dalmatian chrysanthemum.
Chinese patent 1076082 disclosed " vegetable insecticide " is formulated with trifoliate jewelvine, crotons, Rhododendron molle, acetone, antioxidant etc.
Chinese patent 1109708 disclosed " a kind of plant pesticide composition and method of making the same " is leaching liquor of kuh-seng, tobacco, monkshood, radix aconiti agrestis, Snakegourd Fruit, Li Lu, the root of langdu and thunder godvine and emulsifier etc. to be mixed form.
Chinese patent 1107654 disclosed " preparation of margosine vegetable insecticide and make usage " then is based on China tree, kuh-seng, Chinese honey locust, tobacco leaf, tarragon, monomer decoct gained medicinal extract with the alcohol deposition method decontamination after adding emulsifier etc. mix.
Chinese patent 1116050 disclosed " agricultural synergist of high effect nontoxic no medicine damage pure plant " is that the effective ingredient of alcohol extracting river white silk, capsicum, kuh-seng, Chinese wingnut leaf forms.
Purpose of the present invention is exactly to be the low toxicity of raw material, little residual, nuisanceless, safe and reliable novel plant insecticide with the natural Chinese medicinal herb in order to provide a kind of.
Plant protection product is made up of the medicinal material of following weight parts proportioning.Mother liquor part: nicotine 22-27 China tree 13-17, oranges and tangerines seed 2-6, trifoliate jewelvine 4-8, kuh-seng 3-8, dried orange peel 2-5, gelsemium elegan 1-4, tarragon 1-4; The auxiliary material part; Emulsifier 6-10, auxiliary agent 5-10, bleeding agent 4-8, turpentine oil 12-18, xiaokangye 2-6, antioxidant 2-5.
The preparation method who carries the plant protection product that soaks mother liquor with hydrochloric acid is made up of the medicinal material of following weight parts proportioning, nicotine 22-27, the China tree 13-17 that screening is cleaned, oranges and tangerines seed 2-6, trifoliate jewelvine 4-8, kuh-seng 3-8, dried orange peel 2-5, gelsemium elegan 1-4, tarragon 1-4 soak more than 12 hours through 0.5-0.8% hydrochloric acid 100 weight portions, heating to 60-70 ℃ fully leaches soup, behind water clock method water clock, dry or drain, filter behind its impurity in concentration tank negative pressure and carry and heat up in a steamer the method low-temperature reduced-pressure and concentrate and form; Heating is 8-15 ℃ in the mother liquid obtained input synthesis tank, add auxiliary material emulsifier (4107) 6-10 weight portion, bleeding agent dimethyl sulfoxide (DMSO) 4-8, antioxidant sodium benzoate 2-5, be heated to 30-50 ℃ again, stir it, treat to add again when temperature is reduced to 15-25 ℃ auxiliary agent (in) 5-10 xiaokangye 2-6, turpentine oil 12-18, multiple row stirred 50-60 minute, made its complete emulsification, left standstill that not occur layering in 24 hours can packing standby.
The preparation method who carries the plant protection product that soaks mother liquor with ethanol is made up of the medicinal material of following weight parts proportioning, nicotine 22-27, China tree 13-17, oranges and tangerines seed 2-6, trifoliate jewelvine 4-8, kuh-seng 3-8, dried orange peel 2-5, gelsemium elegan 1-4, tarragon 1-4 that screening is cleaned, get the absolute alcohol of 4 times of above traditional Chinese medicine weight portion summations, with the airtight immersion of above-mentioned medicinal material after 7-10 days with rustless steel container through seepage method seepage it, filter, the alcohol extracting soup is put the reflow of alcohol device and is added hot reflux thereupon; Heating is 8-15 ℃ in the mother liquid obtained input synthesis tank, add auxiliary material emulsifier (4107) 6-10 weight portion, bleeding agent dimethyl sulfoxide (DMSO) 4-8, antioxidant sodium benzoate 2-5, be heated to 30-50 ℃ again, stir it, treat to add again when temperature is reduced to 15-25 ℃ auxiliary agent (in) 5-10, xiaokangye 2-6, turpentine oil 12-18, multiple row stirred 50-60 minute, made its complete emulsification, left standstill that not occur layering in 24 hours can packing standby.
Zhi Bei vegetable insecticide is dark brown like this, and aromatic odor is arranged, and not only has stronger insecticidal effect, the effect of antibacterial in addition, sterilization.Be applicable to greengrocery, fruit tree kind, medicinal material, tobacco, flowers and other crops desinsection.Nontoxic to people, animal and bird, have no side effect.Because said preparation contains multiple crude fat, nitrogen, phosphorus, potassium, calcium nutrition, so the effect of growth promotion, volume increase is also very remarkable.
Below in conjunction with embodiment it is described in the present invention.
Carry the plant protection product that soaks the mother liquor preparation with hydrochloric acid: carry earlier and soak mother liquor; will be through screening, remove clean sandy soil foreign material and put into 20 ℃ 0.5% hydrochloric acid 100kg immersion 12 hours through traditional Chinese medicine nicotine 25kg, China tree 15kg, kuh-seng 5kg, oranges and tangerines seed 3kg trifoliate jewelvine 5kg, gelsemium elegan 2kg, tarragon 2kg, the dried orange peel 3kg of flushing with clean water 2-3 time; soup is kept H5.5; then immersion liquid is heated to 60-70 ℃; continue 6 hours; soup fully leach the back use water clock method water clock it; the drying that continues or drain; and, remove impurity through the flame filter press filtration.Immersion liquid suction concentration tank uses negative pressure to carry and heats up in a steamer method low temperature (10-20 ℃) concentrating under reduced pressure, reaches required Baume degrees 10-12.In mother liquor and 6: 4 ratio of auxiliary material, the 60kg mother liquor is dropped into synthesis tank, drop into emulsifier (4107) 8kg, bleeding agent dimethyl sulfoxide (DMSO) 5kg, antioxidant sodium benzoate 2k9 after heating 10 ℃, further being heated to 50 ℃ stirs, treat to drop into again when temperature is reduced to 15 ℃ auxiliary agent (in) 8kg, xiaokangye 3kg, turpentine oil 14kg, continue fully to stir 60 minutes, make its complete emulsification, leave standstill that not occur layering in 24 hours can packing standby.
Carry the plant protection product that soaks the mother liquor preparation with ethanol: carry earlier and soak mother liquor; will be through screening, remove clean sandy soil foreign material and put in the 240kg absolute alcohol (being 4 times of traditional Chinese medicine gross weights) sealing immersion 10 days through traditional Chinese medicine nicotine 25kg, the China tree 15kg of flushing with clean water 2-3 time, kuh-seng 5kg, oranges and tangerines seed 3kg, trifoliate jewelvine 5kg, gelsemium elegan 2kg, tarragon 2kg, old 3kg; the pure soup seepage that will leach with rustless steel container seepage method it; filter through 160 keevil frame filters thereupon, in the reflow of alcohol device, add hot reflux at last.6: 4 ratio of gained alcohol extracting mother liquor and auxiliary material drops into synthesis tank with the 60kg mother liquor, mixes with auxiliary material, all to carry the mother liquor that soaks identical with hydrochloric acid for heating, the process that stirs, condition, proportioning, does not give unnecessary details again.
Its extension rate is with 1 when using this preparation: 500-800 is advisable, and scientifically uses agricultural chemicals to reach, and brings into play bigger effectiveness.Should avoid mixing, prevent that drug effect from reducing with alkaline matter.Also should not dilute,, influence drug effect in order to avoid calcium, magnesium combine the generation precipitation in the well water with agricultural chemicals with well water.
This preparation carries out the liriomyza bryoniae test in Shengli Oil Field Dongying District rural area, Shandong Province to the muskmelon of outdoor cropping flower in full bloom, implements twice sprinkling with 500 times of liquid in spawning period, receives remarkable result.And being evaluated as the initiative of control liriomyza bryoniae domestic plant pesticide by this area's new agricultural technology developmental research, its effect is that other plant pesticide hardly matches.
Claims (3)
1. plant protection product is characterized in that said preparation mainly is made up of the medicinal material of following weight parts proportioning; Mother liquor part: nicotine 22-27 China tree 13-17 oranges and tangerines seed 2-6 trifoliate jewelvine 4-8
Kuh-seng 3-8 dried orange peel 2-5 gelsemium elegan 1-4 tarragon 1-4
Auxiliary material part: emulsifier 6-10 auxiliary agent 5-10 bleeding agent 4-8
Turpentine oil 12-18 xiaokangye 2-6 antioxidant 2-5
2. the preparation method of a plant protection product, it is characterized in that said preparation hydrochloric acid carries the mother liquor that soaks and be made up of the medicinal material of following weight parts proportioning: screening is cleaned
Nicotine 22-27 China tree 13-17 oranges and tangerines seed 2-6 trifoliate jewelvine 4-8
Kuh-seng 3-8 dried orange peel 2-5 gelsemium elegan 1-4 tarragon 1-4 soaks more than 12 hours through 0.5-0.8% hydrochloric acid 100 weight portions, heating to 60-70 ℃ fully leaches soup, behind water clock method water clock, dry or drain, filter behind its impurity in concentration tank negative pressure and carry and heat up in a steamer the method low-temperature reduced-pressure and concentrate and form; Heating is 8-15 ℃ in the mother liquid obtained input synthesis tank, add auxiliary material emulsifier (4107) 6-10 weight portion, bleeding agent dimethyl sulfoxide (DMSO) 4-8, antioxidant sodium benzoate 2-5, be heated to 30-50 ℃ again, stir it, treat to add when temperature is reduced to 15-25 ℃ auxiliary agent (in) 5-10 xiaokangye 2-6, turpentine oil 12-18, multiple row stirred 50-60 minute, made its complete emulsification again, leave standstill and do not occur layering in 24 hours, can packing standby.
3. the preparation method of a plant protection product, it is characterized in that said preparation ethanol carries the mother liquor that soaks and be made up of the medicinal material of following weight parts proportioning: nicotine 22-27, China tree 13-17, oranges and tangerines seed 2-6, trifoliate jewelvine 4-8, kuh-seng 3-8, dried orange peel 2-5, gelsemium elegan 1-4, tarragon 1-4 that screening is cleaned, get the absolute alcohol of 4 times of above traditional Chinese medicine weight portion summations, with the airtight immersion of above-mentioned medicinal material after 7-10 days with rustless steel container through seepage method seepage it, filter, the alcohol extracting soup is put the reflow of alcohol device and is added hot reflux thereupon; Heating is 8-15 ℃ in the mother liquid obtained input synthesis tank, add auxiliary material emulsifier (4107) 6-10 weight portion, bleeding agent dimethyl sulfoxide (DMSO) 4-8, antioxidant sodium benzoate 2-5, be heated to 30-50 ℃ again, stir it, treat to add when temperature is reduced to 15-25 ℃ auxiliary agent (in) 5-10, xiaokangye 2-6, turpentine oil 12-18, multiple row stirred 50-60 minute, made its complete emulsification again, leave standstill and do not occur layering in 24 hours, can packing standby.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN96120784A CN1057194C (en) | 1996-11-28 | 1996-11-28 | Plant protecting agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN96120784A CN1057194C (en) | 1996-11-28 | 1996-11-28 | Plant protecting agent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1183902A true CN1183902A (en) | 1998-06-10 |
| CN1057194C CN1057194C (en) | 2000-10-11 |
Family
ID=5126583
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN96120784A Expired - Fee Related CN1057194C (en) | 1996-11-28 | 1996-11-28 | Plant protecting agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1057194C (en) |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100429977C (en) * | 2007-01-15 | 2008-11-05 | 柳厚先 | Environmental protection and public nuisance free type insecticide, and its preparing method |
| CN102659484A (en) * | 2012-04-13 | 2012-09-12 | 常熟市滨江农业科技有限公司 | Traditional Chinese medicinal herb protective granule |
| CN103340219A (en) * | 2013-07-18 | 2013-10-09 | 奉节县瑞康中药材种植有限公司 | Chinese herbal medicine pesticide and preparation method thereof |
| CN103449934A (en) * | 2013-01-05 | 2013-12-18 | 胡素芳 | Vegetable insecticide |
| CN103609611A (en) * | 2013-11-11 | 2014-03-05 | 李文斌 | Green and environment-friendly insecticide synergist |
| CN104273184A (en) * | 2014-10-30 | 2015-01-14 | 张金诚 | Insect-resistant pesticide for vegetables and preparation method of insect-resistant pesticide |
| CN105248479A (en) * | 2015-10-23 | 2016-01-20 | 广西农垦国有立新农场 | Pesticide special for tangerine tree and preparation method of pesticide |
| CN105393762A (en) * | 2015-11-17 | 2016-03-16 | 蚌埠龙达农业专业合作社 | Method for planting Gelsemium elegan |
| CN105475393A (en) * | 2015-11-27 | 2016-04-13 | 广德经济开发区绿源生态家庭农场 | Special residual-free insect prevention bactericide for trees and flowers |
| CN105660727A (en) * | 2015-12-18 | 2016-06-15 | 信宜市四海永丰现代种养场 | Preparation method of biological disease and pest prevention medicine used for melon and fruit vegetables |
| CN106561750A (en) * | 2016-10-30 | 2017-04-19 | 贵州省蕙安农业科技发展有限公司 | Special vegetable insecticide for honeysuckle planting and preparation method thereof |
| CN106665678A (en) * | 2016-11-24 | 2017-05-17 | 蚌埠市宗洼草鸡养殖农民专业合作社 | Traditional Chinese medicine agent for preventing and treating carrot soft rot |
| CN109258635A (en) * | 2018-09-26 | 2019-01-25 | 大连百事农生物有机肥研究所 | Remaining biological agent of pesticide and preparation method thereof in a kind of degrading plant |
| CN114009429A (en) * | 2021-11-25 | 2022-02-08 | 张艳华 | Plant protective agent and preparation method and application thereof |
| CN115843836A (en) * | 2022-12-14 | 2023-03-28 | 新沂市永诚化工有限公司 | Green novel crop leaf protective agent and preparation method thereof |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1045684A (en) * | 1989-03-20 | 1990-10-03 | 曹先立 | A kind of insecticide that contains margosic toxin |
| CN1044075C (en) * | 1992-02-25 | 1999-07-14 | 李瑛� | Chinese herbal medicine plant insecticide and priparing method |
| CN1123087A (en) * | 1994-11-14 | 1996-05-29 | 李洪新 | Composition of traditional Chinese medicine and preparation method thereof |
| CN1079009C (en) * | 1994-12-19 | 2002-02-13 | 王德元 | Preparation of margosine as plant insecticide and its using method |
-
1996
- 1996-11-28 CN CN96120784A patent/CN1057194C/en not_active Expired - Fee Related
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100429977C (en) * | 2007-01-15 | 2008-11-05 | 柳厚先 | Environmental protection and public nuisance free type insecticide, and its preparing method |
| CN102659484A (en) * | 2012-04-13 | 2012-09-12 | 常熟市滨江农业科技有限公司 | Traditional Chinese medicinal herb protective granule |
| CN103449934A (en) * | 2013-01-05 | 2013-12-18 | 胡素芳 | Vegetable insecticide |
| CN103340219A (en) * | 2013-07-18 | 2013-10-09 | 奉节县瑞康中药材种植有限公司 | Chinese herbal medicine pesticide and preparation method thereof |
| CN103609611A (en) * | 2013-11-11 | 2014-03-05 | 李文斌 | Green and environment-friendly insecticide synergist |
| CN103609611B (en) * | 2013-11-11 | 2015-11-11 | 李文斌 | A kind of environment-friendlyinsecticide insecticide synergist |
| CN104273184B (en) * | 2014-10-30 | 2016-06-08 | 张金诚 | A kind of vegetable insecticide and preparation method thereof |
| CN104273184A (en) * | 2014-10-30 | 2015-01-14 | 张金诚 | Insect-resistant pesticide for vegetables and preparation method of insect-resistant pesticide |
| CN105248479A (en) * | 2015-10-23 | 2016-01-20 | 广西农垦国有立新农场 | Pesticide special for tangerine tree and preparation method of pesticide |
| CN105393762A (en) * | 2015-11-17 | 2016-03-16 | 蚌埠龙达农业专业合作社 | Method for planting Gelsemium elegan |
| CN105475393A (en) * | 2015-11-27 | 2016-04-13 | 广德经济开发区绿源生态家庭农场 | Special residual-free insect prevention bactericide for trees and flowers |
| CN105660727A (en) * | 2015-12-18 | 2016-06-15 | 信宜市四海永丰现代种养场 | Preparation method of biological disease and pest prevention medicine used for melon and fruit vegetables |
| CN106561750A (en) * | 2016-10-30 | 2017-04-19 | 贵州省蕙安农业科技发展有限公司 | Special vegetable insecticide for honeysuckle planting and preparation method thereof |
| CN106665678A (en) * | 2016-11-24 | 2017-05-17 | 蚌埠市宗洼草鸡养殖农民专业合作社 | Traditional Chinese medicine agent for preventing and treating carrot soft rot |
| CN109258635A (en) * | 2018-09-26 | 2019-01-25 | 大连百事农生物有机肥研究所 | Remaining biological agent of pesticide and preparation method thereof in a kind of degrading plant |
| CN114009429A (en) * | 2021-11-25 | 2022-02-08 | 张艳华 | Plant protective agent and preparation method and application thereof |
| CN115843836A (en) * | 2022-12-14 | 2023-03-28 | 新沂市永诚化工有限公司 | Green novel crop leaf protective agent and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1057194C (en) | 2000-10-11 |
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