CN1123087A - Composition of traditional Chinese medicine and preparation method thereof - Google Patents
Composition of traditional Chinese medicine and preparation method thereof Download PDFInfo
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- CN1123087A CN1123087A CN 94114165 CN94114165A CN1123087A CN 1123087 A CN1123087 A CN 1123087A CN 94114165 CN94114165 CN 94114165 CN 94114165 A CN94114165 A CN 94114165A CN 1123087 A CN1123087 A CN 1123087A
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Abstract
This traditional Chinese medicinal composition is prepared by using tobacco, oil-tea camellia dregs, vomiting nut, croton, trifoliate jewelvine, chinaberry, the tuber of stemona, kuh-seng and semen armeniacae as raw material. Extracting nicotine from tobacco; extracting saponin from oil-tea camellia dregs; vomiting nut, croton, trifoliate jewelvine, chinaberry, the tuber of stemona, kuh-sen and semen armeniacae are mixed after being pulverized, then decocted and filtered. The filtrate is mixed with the nicotine and saponin, then added with inorganic acid. Said product is mainly used for crops to kill pests and their eggs. Safety production and application, without pollution.
Description
The present invention relates to Chinese medicine composition of a kind of desinsection and preparation method thereof:
China's cultural control crop pests mainly adopts chemicals, comprise organic phosphates as: parathion-methyl, phoxim, acephatemet etc. and chrysanthemum ester class as: come good fortune spirit, decis, go out and sweep profit etc.The chemicals insecticidal effect is better, but has the pest resistance height, and the person poultry toxicity is big, contaminated environment, price height, defective such as cost is big.Past, the employing vegetable insecticide desinsection that also has, as utilize crop pests such as the tobacco leaf soak anti-eliminates aphis, plant hopper, leafhopper, and what also have controls insect with tobacco leaf and limewash soak or tobacco leaf powder with lime, and southern rice district usefulness withered powder of tea or the withered limewash of tea are prevented and treated rice pests such as rice borer.But above-mentioned vegetable insecticide general independent use or two to three kinds be mixed and use, the desinsection scope is little, effect is low, and is poor than the chemicals drug effect, and is difficult to promote and uses.
The object of the invention provides Chinese medicine composition of a kind of efficient insecticide and preparation method thereof, utilizes the multiple desinsection composition of said composition, prevents and treats insects such as cotton sandfly worm, thereby replaces current widely used chemical pesticide.
The present invention is on the basis of accumulation traditional Chinese medicine insecticidal technology for many years, forms through comparative trial, screening.
Dominant mechanism of the present invention is the effective ingredient of utilizing in the Chinese medicine composition, the insect body surface is corroded and penetrates in the body, poison the insect central nervous system, after insect poisons, excited earlier, systems such as the breathing of back inhibition central nervous system control, digestion, motion make the insect whole body, especially mouthpart, anus dewater and shrink, thereby reach the purpose that kills off the insect pests.
Technical essential of the present invention is:
1. invention Chinese medicine composition proportioning (percentage by weight) is:
Tobacco powder 10-30%
The withered powder 8-16% of tea
Prepared nux vomica 5-20%
Crotons powder 5-15%
Perian insect powder 10-18%
Derris dust 5-12%
Chinaberry powder 5-12%
Tuber of stemona powder 1-3%
Kuh-seng powder 2-4%
Semen armeniacae amarae 0.5-1%
Inorganic acid 1-2%
It is acid that composition is, and pH value is 2.5-3.
2. Chinese medicine composition of the present invention is preferably selected following prescription (percentage by weight) for use:
Tobacco powder 15%-20%
The withered powder 9%-15% of tea
Prepared nux vomica 10%-15%
Crotons powder 8%-12%
Perian insect powder 10%-15%
Derris dust 6%-10%
Chinaberry powder 6%-10%
Tuber of stemona powder 1.5%-2.5%
Kuh-seng powder 3%-4%
Semen armeniacae amarae 0.8%-1%
Inorganic acid 1.5%-2%
3. Chinese medicine composition preparation method of the present invention
The preparation method divided for five steps:
A. the tobacco of 10-30% (weight) is pulverized, add solvent extraction nicotine, nicotine is yellow liquid.
B. will squeeze its oily liquids tea oil with filtering after the withered powder 8-16% of the tea of seed (weight) cold press, extract saponin adding reagent in the tea oil.
C. with the Dalmatian chrysanthemum of the crotons 10-18% (weight) of 5-20% (weight) vomiting nut 5-15% (weight), the trifoliate jewelvine of 5-12% (weight), the chinaberry of 5-12% (weight), the tuber of stemona of 1-3% (weight), the semen armeniacae amarae of the kuh-seng 0.5%-1% (weight) of 2-4% (weight) is pulverized the back and is mixed, under normal temperature, normal pressure, decoct, through 1.5-2 hour, cooled and filtered.
D. mix under the filtered fluid normal temperature and pressure of the nicotine that a, b step are extracted, saponin solution and c step.
E. in the mixed liquor that the d step is produced, add the inorganic acid of 1-2%, the modulation mixed liquor makes ph value of mixture between 2.5-3, is Chinese medicine composition of the present invention.
Chinese medicine composition of the present invention and preparation method's advantage:
1. the Chinese medicine composition insecticidal effect is obvious, because of it has stronger permeability and adhesivity, and energy rapid spread insect whole body, thorough killing, disposable killing rate 100%.Corn borer, stinkbug, thrips, cabbage caterpillar, cotton bollworm etc. are all had general killing effect, and especially to cotton sandfly moth, moth classes such as leaf miner have special efficacy.The existing high 3-5% of chemical pesticide of its insecticidal effect.Chronic administration continuously, pest resistance is poor.
2. present composition stable in properties, illumination is decomposed slow, is easy to storage, transportation, and is easy to use, has strong absorption and persistence, is difficult for being washed away by rainwater dew.
3. the preparation composition material is extensive, and technology is simple, and production cost is low.
Example 1: get 20 kilograms of tobacco powders, 10 kilograms in the withered powder of tea, 8 kilograms of prepared nux vomicas, 10 kilograms in crotons powder, 15 kilograms of perian insect powders, 8 kilograms of derris dusts, 8 kilograms in chinaberry powder, 2 kilograms in tuber of stemona powder, 4 kilograms in kuh-seng powder, 1 kilogram of semen armeniacae amarae, 1.5 kilograms of 65% dilute sulfuric acids.
According to the above ratio tobacco leaf powder is added alcohol (concentration 95%), produce nicotine; To filter after the withered cold press of tea, extracting tea seed oil adds alcohol (95%) and produces saponin in tea oil; After above-mentioned other several Chinese herbal medicines (except the acid) mixing, boiling at normal temperatures and pressures, cold filtration after two hours; Nicotine, saponin and other Chinese herbal medicine fluid are mixed the back modulate, make ph value of mixture 2.6 make Chinese medicine composition after the modulation with 65% sulfuric acid.
Above-mentioned Chinese medicine composition is the product that present optimum formula forms, and carries out indoor, field and large-scale demonstration test with it, and its result of the test is as follows:
Experiment one (laboratory test):
Agrotechnical station, Zhao Ge town, Anqiu City compares test indoor with said composition and 12 kinds of agricultural chemicals using always on August 8th, 94.
Test method: the above cotton sandfly worm of two orders is placed in the wide-mouth bottle.After all pressing 1000 times of concentration dilutions, be sprayed on the polypide with the equal quantities soup, 12 hours, 24 hours, observed cotton sandfly worm death toll respectively in 36 hours per 12 hours, death toll and the ratio of testing number deduct with clear water test 100%, are the killing effect of various agricultural chemicals.
Chinese medicine composition and chemical pesticide laboratory test effect commonly used
| Pesticide name | Working concentration (multiple) | 12 hours killing rates (%) | 24 hours killing rates (%) | 36 hours killing rates (%) |
| Eliminate completely | 1000 | 80 | 100 | |
| The little spirit of peach | 1000 | 40 | 80 | 95 |
| Exhausted sandfly No. one | 1000 | 82 | 100 | |
| Mianchongjing | 1000 | 60 | 85 | 97 |
| Parathion-methyl | 1000 | 58 | 83 | 92 |
| Phoxim | 1000 | 89 | 100 | |
| No. one, new light | 1000 | 91 | 100 | |
| Cotton sandfly treasured | 1000 | 95 | 98 | |
| Methomyl | 1000 | 81 | 92 | |
| Hot sulphur goes out and sweeps profit | 1000 | 90 | 98 | |
| The suffering prestige of going out | 1000 | 85 | 96 | |
| The sandfly emperor of going out | 1000 | 95 | 100 | |
| Chinese medicine composition | 1000 | 97 | 100 |
Experiment two (field trials)
One, test objective:
The organic phosphor that Chinese medicine composition of the present invention and local usage amount is maximum and the medicine parathion-methyl that is mixed thereof, cotton sandfly treasured carry out the test of pesticide effectiveness, and test factor is: same cotton field, same concentration, same amount of liquid medicine, same spray date; Every kind of prescription solely uses a knapsack sprayer, by test, differentiates the drug effect of Chinese medicine composition and common organophosphorous pesticide.
Two, test unit and testing crew:
Agrotechnical station, Zhao Ge town, Anqiu City, testing crew agrotechnical station head of a station agronomist Han Zhuping, assistant agronomist Zhang Zhi liter.
Three, test period: on August 26th, 1994
Four, test site: cotton field, big Shuan Goutou village
Five, test method: the cotton sandfly treasured of (1) Chinese medicine composition (2) parathion-methyl (3), three kinds of agricultural chemicals respectively dilute 1000 times, are sprayed in each experimental plot with the soup of equivalent.300 square metres of each sub-district areas are established twice repetition, take the randomized arrangement test method(s), and testing program sees the following form.
10 strain cottons are extracted in every sub-district before the test; The cotton sandfly worm's ovum of detailed survey amount; Evenly spray each sub-district cotton plant by 1000 times of concentration then, after the sprinkling sample is isolated (in case the transfer of cotton sandfly worm or go out enemy and outside immigration), check the larva survival rate after 24 hours, inspection ovum hatching number after four days.
Six, result of the test
Chinese medicine composition and parathion-methyl, the precious comparative efficacy test's table of cotton sandfly
| Pesticide name | Borer population alive | Ovum number alive | Spray back borer population alive | Spray back ovum number alive | Killing rate | Ovicidal rate |
| Methyl 1065 | ?27 | ?12 | ?3 | ?5 | ?88.8 | ?58.3 |
| Cotton sandfly treasured | ?26 | ?24 | ?2 | ?6 | ?92.3 | ?75 |
| Chinese medicine composition | ?29 | ?22 | ?2 | ?1 | ?93.1 | ?95.5 |
Annotate: worm, ovum amount are 20 strain cotton plant sums
From test result analysis, Chinese medicine composition desinsection, ovum effect all are better than organophosphorus insecticide and the absorbent cotton sandfly treasured that is mixed, and insecticidal effect is high by 0.8-4.3%, kill the high 20.5-27.2% of ovum effect.
Experiment three (demonstration tests)
On August 16th, 1994, demonstration test was carried out in agrotechnical station, Zhao Ge town in 1000 mu of cotton fields on the occasion of the cotton sandfly worm of three generations spawning period.Promptly spray Chinese medicine composition than large tracts of land, result of the test is:
1000 times of spraying concentrations, spray medicine with power driven sprayer, 150 kilograms of every mu of soups, spray date point in afternoons 5 is after 24 hours, be to look at 5 in afternoon next day, 1---3 ages cotton sandfly worm lethality above cotton sandfly worm lethality 93% in 97.%, 3 age, the rate 98% that aphid is dead, second day early 8 look into per three square metres, 1 of dead cotton sandfly moth (666.7 square metres, 233 dead moths).Lure moth with light trap at 9 in afternoon, the moth amount reduces 89%.
Example 2: take 10 kilograms of tobacco powders, 12 kilograms in the withered powder of tea, 16 kilograms of prepared nux vomicas, 5 kilograms in crotons powder, 10 kilograms of perian insect powders, 12 kilograms of derris dusts, 12 kilograms in chinaberry powder, 1 kilogram in tuber of stemona powder, 2 kilograms in kuh-seng powder, 0.5 kilogram of semen armeniacae amarae, 1 kilogram in watery hydrochloric acid.According to example 1 step, make 100 kilograms of invention Chinese medicine compositions.
Above-mentioned Chinese medicine composition is carried out indoor, outdoor, field experiment, and effect is lower than example 1.
Example 3: take 25 kilograms of tobacco powders, 16 kilograms in the withered powder of tea, 12 kilograms of prepared nux vomicas, 8 kilograms in crotons powder, 13 kilograms of perian insect powders, 10 kilograms of derris dusts, 10 kilograms in chinaberry powder, 1.5 kilograms in tuber of stemona powder, 2 kilograms in kuh-seng powder, 0.5 kilogram of semen armeniacae amarae, 2 kilograms of 65% dilute sulfuric acids.According to example 1 step, make 100 kilograms of invention Chinese medicine compositions.
Above-mentioned Chinese medicine composition is carried out indoor, outdoor field experiment, and effect is better than example 2, but is lower than example 1.
Claims (4)
1. Chinese medicine composition is characterized in that its prescription (percentage by weight) is:
Tobacco powder 10-30% derris dust 5-12%
The withered powder 8-16% of tea chinaberry powder 5-12%
Prepared nux vomica 5-20% tuber of stemona powder 1-3%
Crotons powder 5-15% kuh-seng powder 2-4%
Perian insect powder 10-18% semen armeniacae amarae 0.5-1%
Inorganic acid 1-2%
2. Chinese medicine composition according to claim 1 is characterized in that its prescription (percentage by weight) is preferably selected for use:
Tobacco powder 15-20% derris dust 6-10%
The withered powder 9-15% of tea chinaberry powder 6-10%
Prepared nux vomica 5-15% tuber of stemona powder 1.5-2.5%
Crotons powder 8-12% kuh-seng powder 3-4%
Perian insect powder 10-15% semen armeniacae amarae 0,8-1%
Acid 1.5-2%
3. method for preparing claim 1 or 2 described Chinese medicine compositions is characterized in that carrying out as follows:
A. the tobacco of 10-30% (weight) is pulverized, add solvent extraction nicotine, nicotine is yellow liquid.
B. will squeeze its oily liquids tea oil with filtering after the withered 8-16% of the tea of seed (weight) cold press, extract saponin adding reagent in the tea oil.
C. with 5-20% (weight) vomiting nut, the Dalmatian chrysanthemum of the crotons 10-18% (weight) of 5-15% (weight), the trifoliate jewelvine of 5-12% (weight), the chinaberry of 5-12% (weight), the tuber of stemona of 1-3% (weight), the semen armeniacae amarae of the kuh-seng 0.5%-1% (weight) of 2-4% (weight) are pulverized the back and are mixed, and decoct under normal temperature, normal pressure, through 1.5-2 hour, cooled and filtered.
D. mix under the filtered fluid normal temperature and pressure of the nicotine that a, b step are extracted, saponin solution and c step.
E. in the mixed liquor that the d step is produced, add the inorganic acid of 1-2%, the modulation mixed liquor.
4. the method for preparing the invention Chinese medicine composition according to claim 3 is characterized in that (a) (b) (c) (d) ph value of mixture 2.5-3 of making of (e) five step.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 94114165 CN1123087A (en) | 1994-11-14 | 1994-11-14 | Composition of traditional Chinese medicine and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 94114165 CN1123087A (en) | 1994-11-14 | 1994-11-14 | Composition of traditional Chinese medicine and preparation method thereof |
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| CN1123087A true CN1123087A (en) | 1996-05-29 |
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| CN 94114165 Pending CN1123087A (en) | 1994-11-14 | 1994-11-14 | Composition of traditional Chinese medicine and preparation method thereof |
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Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1057194C (en) * | 1996-11-28 | 2000-10-11 | 阎福永 | Plant protecting agent |
| CN100382707C (en) * | 2006-06-30 | 2008-04-23 | 刘景相 | A botanical pesticide |
| CN100429977C (en) * | 2007-01-15 | 2008-11-05 | 柳厚先 | Environmental protection and public nuisance free type insecticide, and its preparing method |
| CN102224832A (en) * | 2011-04-18 | 2011-10-26 | 陈本富 | Broad-spectrum insecticide prepared by Chinese herbal medicine and production method thereof |
| CN101378726B (en) * | 2006-02-08 | 2012-04-18 | 荷兰联合利华有限公司 | Hair conditioning compositions |
| CN101611724B (en) * | 2008-06-23 | 2012-07-04 | 中国科学院华南植物园 | Environmentally-friendly phytochemical pasty biopesticide and preparation method thereof |
| CN102640765A (en) * | 2012-04-18 | 2012-08-22 | 王振伟 | Green and novel crop pest repellent |
| CN101898916B (en) * | 2009-06-01 | 2012-12-26 | 李毓芳 | Water soluble organic fertilizer |
| CN101390518B (en) * | 2007-09-21 | 2013-02-06 | 天津市慧珍科技有限公司 | Plant pesticide of micro-emulsion and its preparing method |
| CN104273179A (en) * | 2013-07-11 | 2015-01-14 | 青岛罗素生物技术有限公司 | Preparation method of oxymatrine aqueous solution |
| CN104892287A (en) * | 2014-03-05 | 2015-09-09 | 常德红花园肥业科技有限公司 | Nutrition glue organic fertilizer and applications of nutrition glue organic fertilizer in plant planting |
| CN105557779A (en) * | 2015-07-10 | 2016-05-11 | 罗友祥 | Compound Chinese herbal medicine insecticide preparation method |
| CN105638788A (en) * | 2016-02-19 | 2016-06-08 | 滨州禾丰高效生态产业技术开发有限公司 | Special pesticide for corn borers |
| CN105660727A (en) * | 2015-12-18 | 2016-06-15 | 信宜市四海永丰现代种养场 | Preparation method of biological disease and pest prevention medicine used for melon and fruit vegetables |
| CN106234460A (en) * | 2016-07-15 | 2016-12-21 | 广西顺帆投资有限公司 | A kind of insecticide and preparation method thereof |
| CN106490002A (en) * | 2016-10-31 | 2017-03-15 | 郑州思辩科技有限公司 | A kind of oil-suspending agent for preventing and treating Pentatomiddae class pest and preparation method thereof |
| CN106490030A (en) * | 2016-10-31 | 2017-03-15 | 郑州思辩科技有限公司 | A kind of botanical pesticide and preparation method thereof |
| CN107836301A (en) * | 2017-11-20 | 2018-03-27 | 广西垚宇贸易有限公司 | A kind of cultural method of noodles dish |
| CN110946153A (en) * | 2018-09-26 | 2020-04-03 | 贵州省烟草公司铜仁市公司 | Insecticide liquid for oil tea cake and application method thereof |
-
1994
- 1994-11-14 CN CN 94114165 patent/CN1123087A/en active Pending
Cited By (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1057194C (en) * | 1996-11-28 | 2000-10-11 | 阎福永 | Plant protecting agent |
| CN101378726B (en) * | 2006-02-08 | 2012-04-18 | 荷兰联合利华有限公司 | Hair conditioning compositions |
| CN100382707C (en) * | 2006-06-30 | 2008-04-23 | 刘景相 | A botanical pesticide |
| CN100429977C (en) * | 2007-01-15 | 2008-11-05 | 柳厚先 | Environmental protection and public nuisance free type insecticide, and its preparing method |
| CN101390518B (en) * | 2007-09-21 | 2013-02-06 | 天津市慧珍科技有限公司 | Plant pesticide of micro-emulsion and its preparing method |
| CN101611724B (en) * | 2008-06-23 | 2012-07-04 | 中国科学院华南植物园 | Environmentally-friendly phytochemical pasty biopesticide and preparation method thereof |
| CN101898916B (en) * | 2009-06-01 | 2012-12-26 | 李毓芳 | Water soluble organic fertilizer |
| CN102224832B (en) * | 2011-04-18 | 2013-07-31 | 陈本富 | Broad-spectrum insecticide prepared by Chinese herbal medicine and production method thereof |
| CN102224832A (en) * | 2011-04-18 | 2011-10-26 | 陈本富 | Broad-spectrum insecticide prepared by Chinese herbal medicine and production method thereof |
| CN102640765B (en) * | 2012-04-18 | 2014-11-19 | 王振伟 | Green and novel crop pest repellent |
| CN102640765A (en) * | 2012-04-18 | 2012-08-22 | 王振伟 | Green and novel crop pest repellent |
| CN104273179A (en) * | 2013-07-11 | 2015-01-14 | 青岛罗素生物技术有限公司 | Preparation method of oxymatrine aqueous solution |
| CN104892287A (en) * | 2014-03-05 | 2015-09-09 | 常德红花园肥业科技有限公司 | Nutrition glue organic fertilizer and applications of nutrition glue organic fertilizer in plant planting |
| CN105557779A (en) * | 2015-07-10 | 2016-05-11 | 罗友祥 | Compound Chinese herbal medicine insecticide preparation method |
| CN105660727A (en) * | 2015-12-18 | 2016-06-15 | 信宜市四海永丰现代种养场 | Preparation method of biological disease and pest prevention medicine used for melon and fruit vegetables |
| CN105638788A (en) * | 2016-02-19 | 2016-06-08 | 滨州禾丰高效生态产业技术开发有限公司 | Special pesticide for corn borers |
| CN106234460A (en) * | 2016-07-15 | 2016-12-21 | 广西顺帆投资有限公司 | A kind of insecticide and preparation method thereof |
| CN106490002A (en) * | 2016-10-31 | 2017-03-15 | 郑州思辩科技有限公司 | A kind of oil-suspending agent for preventing and treating Pentatomiddae class pest and preparation method thereof |
| CN106490030A (en) * | 2016-10-31 | 2017-03-15 | 郑州思辩科技有限公司 | A kind of botanical pesticide and preparation method thereof |
| CN107836301A (en) * | 2017-11-20 | 2018-03-27 | 广西垚宇贸易有限公司 | A kind of cultural method of noodles dish |
| CN110946153A (en) * | 2018-09-26 | 2020-04-03 | 贵州省烟草公司铜仁市公司 | Insecticide liquid for oil tea cake and application method thereof |
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