CN107646893A - A kind of plants and flowers plant source efficient pesticides and preparation method thereof - Google Patents
A kind of plants and flowers plant source efficient pesticides and preparation method thereof Download PDFInfo
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- CN107646893A CN107646893A CN201710894443.3A CN201710894443A CN107646893A CN 107646893 A CN107646893 A CN 107646893A CN 201710894443 A CN201710894443 A CN 201710894443A CN 107646893 A CN107646893 A CN 107646893A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/32—Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- General Health & Medical Sciences (AREA)
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- Wood Science & Technology (AREA)
- Dentistry (AREA)
- Plant Pathology (AREA)
- Agronomy & Crop Science (AREA)
- Environmental Sciences (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Pest Control & Pesticides (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Mycology (AREA)
- Virology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of plants and flowers plant source efficient pesticides and preparation method thereof, it is prepared by the raw material of following parts by weight：16 25 parts of wilfordine, 8 14 parts of pokeberry root, freeze it is green 6 11 parts, 7 11 parts of baeckea frutescen, 35 parts of fructus viticis, 47 parts of Eupatorium adenophorum, 26 parts of Eclipta prostrata, 15 21 parts of matrine, 7 12 parts of tallow-seed oil, 6 12 parts of root of Chinese clematis herb.The present invention uses wilfordine, pokeberry root, freezes green, baeckea frutescen, fructus viticis, Eupatorium adenophorum, Eclipta prostrata, matrine, tallow-seed oil, root of Chinese clematis herb, effective proportioning of raw material, insecticide is made, feedstock capture cost is low, make simple and convenient, there is good insecticidal effect to absolute ethyl alcohol rice, vegetables, fruit tree, tea tree etc., and it is environmentally safe, meet the requirement of green production；Seedling can be protected well, can effectively be killed off the insect pests, and small toxicity itself, nursery stock and human body will not be impacted.
Description
Technical field
The present invention relates to a kind of insecticide, and in particular to a kind of plants and flowers plant source efficient pesticides and its preparation side
Method.
Background technology
With the change of global climate, the phenomenon that various crops and forest meet with parasitosis disaster is increasingly severe.At present
The insecticide variety of in the market is various, but in general insecticide can only prevent and treat particular kind of insect, a kind of insecticide control
A kind of insect, but can also insect is developed immunity to drugs insecticide with same kind of insecticide for a long time.
Nursery stock is the sapling for having root system and seedling stem.According to the growth characteristic of nursery stock different times, by the growth of nursery stock
Journey is greatly classified into four periods, i.e. seeding stage, early growth period, Fast-growing stage and Later growth.Because nursery stock is the childhood of plant
Phase, therefore have the characteristics that the speed of growth is fast, is easily caused death by pest and disease damage infringement.
At present, in seedling growth, for prevent pest and disease damage it is usually used be chemical pesticide, used due to a large amount of
Chemical pesticide and caused by problem of environmental pollution be on the rise.Meanwhile chemical pesticide because its without selectivity, to beneficial life
Thing will also result in threat.Moreover, many chemical pesticides are non-degradables or are difficult to degrade, easily in animals and plants cylinder accumulation and
Pollute the enrichment of thing.
As the public is to the requirement more and more higher of " pollution-free food ", " pollution-free food ", market to it is pollution-free, can drop naturally
The ecological agricultural chemical demand of solution also gradually increases.From the point of view of the development of pesticide science, upper " back to nature " is used in pesticide manufacturing
And " Harmless " of agricultural chemicals, it is society and the inexorable trend of Development of Natural Science, therefore new bio broad spectrum pesticide has
Wide development prospect.
The content of the invention
To solve the above problems, the invention provides a kind of plants and flowers plant source efficient pesticides and its preparation side
Method.
To achieve the above object, the technical scheme taken of the present invention is：
A kind of plants and flowers plant source efficient pesticides, are prepared by the raw material of following parts by weight：
Wilfordine 16-25 parts, pokeberry root 8-14 parts, freeze green 6-11 parts, baeckea frutescen 7-11 parts, fructus viticis 3-5 parts, Eupatorium adenophorum 4-
7 parts, Eclipta prostrata 2-6 parts, matrine 15-21 parts, tallow-seed oil 7-12 parts, root of Chinese clematis herb 6-12 parts, azalea 1-4 parts, folder bamboo
Peach 3-8 parts, beggar-ticks 1-7 parts, perilla leaf 2-8 parts, eucalyptus oil 2-8 parts, synergist 5-10 parts, emulsifying agent 6-11 parts, remaining is nothing
Water-ethanol.
Further, a kind of plants and flowers plant source efficient pesticides, are prepared by the raw material of following parts by weight：
Wilfordine 17-24 parts, pokeberry root 9-13 parts, freeze green 7-10 parts, baeckea frutescen 8-10 parts, fructus viticis 4-5 parts, Eupatorium adenophorum 4-
6 parts, Eclipta prostrata 3-5 parts, matrine 16-20 parts, tallow-seed oil 8-11 parts, root of Chinese clematis herb 7-11 parts, azalea 2-4 parts, folder bamboo
Peach 4-7 parts, beggar-ticks 2-6 parts, perilla leaf 3-7 parts, eucalyptus oil 3-7 parts, synergist 6-9 parts, emulsifying agent 7-10 parts, remaining is anhydrous
Ethanol.
Further, a kind of plants and flowers plant source efficient pesticides, are prepared by the raw material of following parts by weight：
19 parts of wilfordine, 11 parts of pokeberry root, freeze green 8 parts, be 9 parts of baeckea frutescen, 4 parts of fructus viticis, 4 parts of Eupatorium adenophorum, 4 parts of Eclipta prostrata, bitter
Join 17 parts of alkali, 9 parts of tallow-seed oil, 8 parts of root of Chinese clematis herb, 3 parts of azalea, 5 parts of oleander, 5 parts of beggar-ticks, 6 parts of perilla leaf, eucalyptus
5 parts of oil, 9 parts of synergist, 8 parts of emulsifying agent, remaining is absolute ethyl alcohol.
Further, the preparation method of a kind of plants and flowers plant source efficient pesticides, it is characterised in that by following step
Suddenly it is made：
S1：Pokeberry root 9-13 parts, the green 7-10 parts of jelly, oleander 4-7 parts, root of Chinese clematis herb 7-11 parts are passed through into airslide disintegrating mill powder
After broken, the 3-5 times of absolute ethyl alcohol weighed is added, it is 7-9 to adjust pH value with sodium bicarbonate, is extracted for 0 .5 hours, filtering, decompression, concentration
After obtain extract solution A；
S2:By wilfordine 17-24 parts, baeckea frutescen 8-10 parts, fructus viticis 4-5 parts, Eupatorium adenophorum 4-6 parts, Eclipta prostrata 3-5 parts, kuh-seng
Alkali 16-20 parts, tallow-seed oil 8-11 parts, beggar-ticks 2-6 parts, perilla leaf 3-7 parts, the impurity elimination of eucalyptus oil 3-7 part selection of crude drugs, meter
Amount, mixing, load diafiltration kettle after crushing, add the organic solvent of 3-7 times of bulk drug weight, be heated to 66-88 DEG C, heating 2-5 is small
When after be percolated to obtain percolate B；
S3:After azalea mechanical crushing, the mass fraction for adding 2 times of weights carries out the .5 of refluxing extraction 0 for 20-30% glacial acetic acid
Hour, obtain extract solution C after filtering, decompression, concentration；
S4：The obtained extract solution C of extract solution A, step S2 that step S1 is obtained obtained percolate B and step S3 are added to steaming
Evaporate kettle concentration, circulation diafiltration extraction；Liquid phase is obtained just to expect；
S5：The material at the beginning of step S4 liquid phase, add emulsifying agent 7-10 parts and be sufficiently mixed stirring 15-30min, be then concentrated into no alcohol
Taste, heat same weight water dissolving；This product is made.
Further, the emulsifying agent is one or both of ethoxylated dodecyl alcohol and aliphatic amine polyoxyethylene ether
Nonionic emulsifier.
The present invention uses wilfordine, pokeberry root, freezes green, baeckea frutescen, fructus viticis, Eupatorium adenophorum, Eclipta prostrata, matrine, tung oil tree
Seed oil, root of Chinese clematis herb, azalea, oleander, beggar-ticks, perilla leaf, effective proportioning of eucalyptus oil raw material, insecticide is made, it is former
Expect that acquisition cost is low, making is simple and convenient, has good insecticidal effect to absolute ethyl alcohol rice, vegetables, fruit tree, tea tree etc., and
It is environmentally safe, meet the requirement of green production；Seedling can be protected well, can effectively be killed off the insect pests, and
And small toxicity itself, nursery stock and human body will not be impacted.
The present invention uses plant material, pure natural, nuisanceless, makees extractant using water or alcohol, simplifies production technology, reduces
Production cost, the agricultural insecticide that the plant component that this technology is extracted makes is free of or contains organic solvent less, residual after processing
Slag can do the carrier of this product, can also do organic fertilizer raw material, the discharge of three wastes material, clean manufacturing, green；User
Just, application method is directly pouring, and can be to be used simultaneously with fertilizer before transplanting, time saving province convenient and swift compared with fumigating insecticide
Power, reduce human cost.
The pokeberry root used in the present invention contains abundant saponin, there is strong inhibitory action for nervous centralis, freezes green
Dyestuff is usually used as, freezes the green effect for playing desinsection in the present invention by extraction, especially for killing acarid class and moth class
Deng insect significant effect, killed off the insect pests within 0 .5-1 hours, oleander contains the glucosides such as oleandrin, digitalin, kills
Locust, aphid significant effect, the other materials that azalea can be benumbed in the insect nerve cooperation present invention kill insect；The present invention kills
Worm agent is made up of plant, and storeroom cooperates, the efficient deinsectization of energy, to person poultry harmless, safe green environmental protection.
Embodiment
In order that objects and advantages of the present invention are more clearly understood, the present invention is carried out with reference to embodiments further detailed
Explanation.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not intended to limit the present invention.
A kind of plants and flowers plant source efficient pesticides, are prepared by the raw material of following parts by weight：
Wilfordine 16-25 parts, pokeberry root 8-14 parts, freeze green 6-11 parts, baeckea frutescen 7-11 parts, fructus viticis 3-5 parts, Eupatorium adenophorum 4-
7 parts, Eclipta prostrata 2-6 parts, matrine 15-21 parts, tallow-seed oil 7-12 parts, root of Chinese clematis herb 6-12 parts, azalea 1-4 parts, folder bamboo
Peach 3-8 parts, beggar-ticks 1-7 parts, perilla leaf 2-8 parts, eucalyptus oil 2-8 parts, synergist 5-10 parts, emulsifying agent 6-11 parts, remaining is nothing
Water-ethanol.
A kind of plants and flowers plant source efficient pesticides, are prepared by the raw material of following parts by weight：
Wilfordine 17-24 parts, pokeberry root 9-13 parts, freeze green 7-10 parts, baeckea frutescen 8-10 parts, fructus viticis 4-5 parts, Eupatorium adenophorum 4-
6 parts, Eclipta prostrata 3-5 parts, matrine 16-20 parts, tallow-seed oil 8-11 parts, root of Chinese clematis herb 7-11 parts, azalea 2-4 parts, folder bamboo
Peach 4-7 parts, beggar-ticks 2-6 parts, perilla leaf 3-7 parts, eucalyptus oil 3-7 parts, synergist 6-9 parts, emulsifying agent 7-10 parts, remaining is anhydrous
Ethanol.
A kind of plants and flowers plant source efficient pesticides, are prepared by the raw material of following parts by weight：
19 parts of wilfordine, 11 parts of pokeberry root, freeze green 8 parts, be 9 parts of baeckea frutescen, 4 parts of fructus viticis, 4 parts of Eupatorium adenophorum, 4 parts of Eclipta prostrata, bitter
Join 17 parts of alkali, 9 parts of tallow-seed oil, 8 parts of root of Chinese clematis herb, 3 parts of azalea, 5 parts of oleander, 5 parts of beggar-ticks, 6 parts of perilla leaf, eucalyptus
5 parts of oil, 9 parts of synergist, 8 parts of emulsifying agent, remaining is absolute ethyl alcohol.
A kind of plants and flowers preparation method of plant source efficient pesticides, is made up of following steps：
S1：Pokeberry root 9-13 parts, the green 7-10 parts of jelly, oleander 4-7 parts, root of Chinese clematis herb 7-11 parts are passed through into airslide disintegrating mill powder
After broken, the 3-5 times of absolute ethyl alcohol weighed is added, it is 7-9 to adjust pH value with sodium bicarbonate, is extracted for 0 .5 hours, filtering, decompression, concentration
After obtain extract solution A；
S2:By wilfordine 17-24 parts, baeckea frutescen 8-10 parts, fructus viticis 4-5 parts, Eupatorium adenophorum 4-6 parts, Eclipta prostrata 3-5 parts, kuh-seng
Alkali 16-20 parts, tallow-seed oil 8-11 parts, beggar-ticks 2-6 parts, perilla leaf 3-7 parts, the impurity elimination of eucalyptus oil 3-7 part selection of crude drugs, meter
Amount, mixing, load diafiltration kettle after crushing, add the organic solvent of 3-7 times of bulk drug weight, be heated to 66-88 DEG C, heating 2-5 is small
When after be percolated to obtain percolate B；
S3:After azalea mechanical crushing, the mass fraction for adding 2 times of weights carries out the .5 of refluxing extraction 0 for 20-30% glacial acetic acid
Hour, obtain extract solution C after filtering, decompression, concentration；
S4：The obtained extract solution C of extract solution A, step S2 that step S1 is obtained obtained percolate B and step S3 are added to steaming
Evaporate kettle concentration, circulation diafiltration extraction；Liquid phase is obtained just to expect；
S5：The material at the beginning of step S4 liquid phase, add emulsifying agent 7-10 parts and be sufficiently mixed stirring 15-30min, be then concentrated into no alcohol
Taste, heat same weight water dissolving；This product is made.
The emulsifying agent is one or both of ethoxylated dodecyl alcohol and aliphatic amine polyoxyethylene ether nonionic Emulsion
Agent.
Embodiment 1
A kind of plants and flowers preparation method of plant source efficient pesticides, is made up of following steps：
S1：By 11 parts of pokeberry root, freeze green 8 parts, after 5 parts of oleander, 9 parts of root of Chinese clematis herb crushed by airslide disintegrating mill, add 4
Heavy absolute ethyl alcohol again, it is 8 with sodium bicarbonate regulation pH value, extracted for 0 .5 hours, filter, depressurize, obtain extract solution A after concentration；
S2:By 19 parts of wilfordine, 9 parts of baeckea frutescen, 4 parts of fructus viticis, 5 parts of Eupatorium adenophorum, 4 parts of Eclipta prostrata, 19 parts of matrine, tung oil tree
Load diafiltration kettle after 9 parts of oil, 4 parts of beggar-ticks, 4 parts of perilla leaf, eucalyptus oil 4 parts of selection of crude drugs impurity eliminations, metering, mixing, crushing, add
The organic solvent of 4 times of bulk drug weight, 69 DEG C are heated to, heating is percolated to obtain percolate B after 4 hours；
S3:After azalea mechanical crushing, the mass fraction for adding 2 times of weights carries out the .5 of refluxing extraction 0 for 20-30% glacial acetic acid
Hour, obtain extract solution C after filtering, decompression, concentration；
S4：The obtained extract solution C of extract solution A, step S2 that step S1 is obtained obtained percolate B and step S3 are added to steaming
Evaporate kettle concentration, circulation diafiltration extraction；Liquid phase is obtained just to expect；
S5：The material at the beginning of step S4 liquid phase, add 9 parts of emulsifying agent and be sufficiently mixed stirring 19min, be then concentrated into no alcohol taste, add
Heat dissolves with weight water；This product is made.
Embodiment 2
A kind of plants and flowers preparation method of plant source efficient pesticides, is made up of following steps：
S1：By 13 parts of pokeberry root, freeze green 10 parts, after 7 parts of oleander, 11 parts of root of Chinese clematis herb crushed by airslide disintegrating mill, add
Enter 5 times of heavy absolute ethyl alcohols, be 9 with sodium bicarbonate regulation pH value, extracted for 0 .5 hours, extract solution is obtained after filtering, decompression, concentration
A；
S2:By 24 parts of wilfordine, 10 parts of baeckea frutescen, 5 parts of fructus viticis, 6 parts of Eupatorium adenophorum, 5 parts of Eclipta prostrata, 20 parts of matrine, tung oil tree
Load diafiltration after 11 parts of seed oil, 6 parts of beggar-ticks, 7 parts of perilla leaf, eucalyptus oil 7 parts of selection of crude drugs impurity eliminations, metering, mixing, crushing
Kettle, add the organic solvent of 7 times of bulk drug weight, be heated to 88 DEG C, heating is percolated to obtain percolate B after 5 hours；
S3:After azalea mechanical crushing, the mass fraction for adding 2 times of weights carries out the .5 of refluxing extraction 0 for 20-30% glacial acetic acid
Hour, obtain extract solution C after filtering, decompression, concentration；
S4：The obtained extract solution C of extract solution A, step S2 that step S1 is obtained obtained percolate B and step S3 are added to steaming
Evaporate kettle concentration, circulation diafiltration extraction；Liquid phase is obtained just to expect；
S5：The material at the beginning of step S4 liquid phase, add 10 parts of emulsifying agent and be sufficiently mixed stirring 30min, be then concentrated into no alcohol taste, add
Heat dissolves with weight water；This product is made.
Embodiment 3
A kind of plants and flowers preparation method of plant source efficient pesticides, is made up of following steps：
S1：By pokeberry root part, freeze green 7 parts, after 4 parts of oleander, 7 parts of root of Chinese clematis herb crushed by airslide disintegrating mill, add 3 times
The absolute ethyl alcohol of weight, it is 7 with sodium bicarbonate regulation pH value, extracted for 0 .5 hours, extract solution A is obtained after filtering, decompression, concentration；
S2:By 17 parts of wilfordine, 8 parts of baeckea frutescen, 4 parts of fructus viticis, 4 parts of Eupatorium adenophorum, 3 parts of Eclipta prostrata, 16 parts of matrine, tung oil tree
Load diafiltration kettle after 8 parts of oil, 2 parts of beggar-ticks, 3 parts of perilla leaf, eucalyptus oil 3 parts of selection of crude drugs impurity eliminations, metering, mixing, crushing, add
The organic solvent of 3 times of bulk drug weight, 66 DEG C are heated to, heating is percolated to obtain percolate B after 2 hours；
S3:After azalea mechanical crushing, the mass fraction for adding 2 times of weights is small for 20% glacial acetic acid progress refluxing extraction 0 .5
When, obtain extract solution C after filtering, decompression, concentration；
S4：The obtained extract solution C of extract solution A, step S2 that step S1 is obtained obtained percolate B and step S3 are added to steaming
Evaporate kettle concentration, circulation diafiltration extraction；Liquid phase is obtained just to expect；
S5：The material at the beginning of step S4 liquid phase, add 7 parts of emulsifying agent and be sufficiently mixed stirring 15min, be then concentrated into no alcohol taste, add
Heat dissolves with weight water；This product is made.
The present invention uses wilfordine, pokeberry root, freezes green, baeckea frutescen, fructus viticis, Eupatorium adenophorum, Eclipta prostrata, matrine, tung oil tree
Seed oil, root of Chinese clematis herb, azalea, oleander, beggar-ticks, perilla leaf, effective proportioning of eucalyptus oil raw material, insecticide is made, it is former
Expect that acquisition cost is low, making is simple and convenient, has good insecticidal effect to absolute ethyl alcohol rice, vegetables, fruit tree, tea tree etc., and
It is environmentally safe, meet the requirement of green production；Seedling can be protected well, can effectively be killed off the insect pests, and
And small toxicity itself, nursery stock and human body will not be impacted.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (5)
1. a kind of plants and flowers plant source efficient pesticides, it is characterised in that be prepared by the raw material of following parts by weight：
Wilfordine 16-25 parts, pokeberry root 8-14 parts, freeze green 6-11 parts, baeckea frutescen 7-11 parts, fructus viticis 3-5 parts, Eupatorium adenophorum 4-
7 parts, Eclipta prostrata 2-6 parts, matrine 15-21 parts, tallow-seed oil 7-12 parts, root of Chinese clematis herb 6-12 parts, azalea 1-4 parts, folder bamboo
Peach 3-8 parts, beggar-ticks 1-7 parts, perilla leaf 2-8 parts, eucalyptus oil 2-8 parts, synergist 5-10 parts, emulsifying agent 6-11 parts, remaining is nothing
Water-ethanol.
2. a kind of plants and flowers plant source efficient pesticides according to claim 1, it is characterised in that by following weight
The raw material of part is prepared：
Wilfordine 17-24 parts, pokeberry root 9-13 parts, freeze green 7-10 parts, baeckea frutescen 8-10 parts, fructus viticis 4-5 parts, Eupatorium adenophorum 4-
6 parts, Eclipta prostrata 3-5 parts, matrine 16-20 parts, tallow-seed oil 8-11 parts, root of Chinese clematis herb 7-11 parts, azalea 2-4 parts, folder bamboo
Peach 4-7 parts, beggar-ticks 2-6 parts, perilla leaf 3-7 parts, eucalyptus oil 3-7 parts, synergist 6-9 parts, emulsifying agent 7-10 parts, remaining is anhydrous
Ethanol.
3. a kind of plants and flowers plant source efficient pesticides according to claim 1, it is characterised in that by following weight
The raw material of part is prepared：
19 parts of wilfordine, 11 parts of pokeberry root, freeze green 8 parts, be 9 parts of baeckea frutescen, 4 parts of fructus viticis, 4 parts of Eupatorium adenophorum, 4 parts of Eclipta prostrata, bitter
Join 17 parts of alkali, 9 parts of tallow-seed oil, 8 parts of root of Chinese clematis herb, 3 parts of azalea, 5 parts of oleander, 5 parts of beggar-ticks, 6 parts of perilla leaf, eucalyptus
5 parts of oil, 9 parts of synergist, 8 parts of emulsifying agent, remaining is absolute ethyl alcohol.
A kind of 4. preparation method of plants and flowers plant source efficient pesticides according to claim 1, it is characterised in that
It is made up of following steps：
S1：Pokeberry root 9-13 parts, the green 7-10 parts of jelly, oleander 4-7 parts, root of Chinese clematis herb 7-11 parts are passed through into airslide disintegrating mill powder
After broken, the 3-5 times of absolute ethyl alcohol weighed is added, it is 7-9 to adjust pH value with sodium bicarbonate, is extracted for 0 .5 hours, filtering, decompression, concentration
After obtain extract solution A；
S2:By wilfordine 17-24 parts, baeckea frutescen 8-10 parts, fructus viticis 4-5 parts, Eupatorium adenophorum 4-6 parts, Eclipta prostrata 3-5 parts, kuh-seng
Alkali 16-20 parts, tallow-seed oil 8-11 parts, beggar-ticks 2-6 parts, perilla leaf 3-7 parts, the impurity elimination of eucalyptus oil 3-7 part selection of crude drugs, meter
Amount, mixing, load diafiltration kettle after crushing, add the organic solvent of 3-7 times of bulk drug weight, be heated to 66-88 DEG C, heating 2-5 is small
When after be percolated to obtain percolate B；
S3:After azalea mechanical crushing, the mass fraction for adding 2 times of weights carries out the .5 of refluxing extraction 0 for 20-30% glacial acetic acid
Hour, obtain extract solution C after filtering, decompression, concentration；
S4：The obtained extract solution C of extract solution A, step S2 that step S1 is obtained obtained percolate B and step S3 are added to steaming
Evaporate kettle concentration, circulation diafiltration extraction；Liquid phase is obtained just to expect；
S5：The material at the beginning of step S4 liquid phase, add emulsifying agent 7-10 parts and be sufficiently mixed stirring 15-30min, be then concentrated into no alcohol
Taste, heat same weight water dissolving；This product is made.
A kind of 5. preparation method of plants and flowers plant source efficient pesticides according to claim 4, it is characterised in that
The emulsifying agent is one or both of ethoxylated dodecyl alcohol and aliphatic amine polyoxyethylene ether nonionic emulsifier.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710894443.3A CN107646893A (en) | 2017-09-28 | 2017-09-28 | A kind of plants and flowers plant source efficient pesticides and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710894443.3A CN107646893A (en) | 2017-09-28 | 2017-09-28 | A kind of plants and flowers plant source efficient pesticides and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107646893A true CN107646893A (en) | 2018-02-02 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108341716A (en) * | 2018-04-02 | 2018-07-31 | 青岛元汇丰企业管理咨询服务有限公司 | A kind of antibacterial growth-promoting elongated biological pesticide of plant source |
| CN108633690A (en) * | 2018-04-16 | 2018-10-12 | 安徽梅兰园林景观工程有限公司 | A kind of soilless cultivation substrate of flowers and preparation method thereof |
| CN110506763A (en) * | 2019-09-18 | 2019-11-29 | 浙江省农业科学院 | A kind of novel environment friendly pesticide reagent and preparation method thereof |
| CN114766517A (en) * | 2022-03-28 | 2022-07-22 | 河北农业大学 | Application of vitex rotundifolia extract, pesticide and preparation method of pesticide |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104542749A (en) * | 2015-01-26 | 2015-04-29 | 李善宽 | Plant-based agricultural insecticide |
| CN106234426A (en) * | 2016-07-15 | 2016-12-21 | 广西顺帆投资有限公司 | One vegetative insecticide and preparation method thereof |
| CN106614801A (en) * | 2016-11-11 | 2017-05-10 | 芜湖国苑苗木服务有限公司 | Multifunctional and environment-friendly insecticide for seedlings and preparation method of insecticide |
-
2017
- 2017-09-28 CN CN201710894443.3A patent/CN107646893A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104542749A (en) * | 2015-01-26 | 2015-04-29 | 李善宽 | Plant-based agricultural insecticide |
| CN106234426A (en) * | 2016-07-15 | 2016-12-21 | 广西顺帆投资有限公司 | One vegetative insecticide and preparation method thereof |
| CN106614801A (en) * | 2016-11-11 | 2017-05-10 | 芜湖国苑苗木服务有限公司 | Multifunctional and environment-friendly insecticide for seedlings and preparation method of insecticide |
Non-Patent Citations (2)
| Title |
|---|
| 姜传义: "《中国杀虫植物志》", 31 December 1999, 新疆科技卫生出版社 * |
| 成卓敏: "《农业生物灾害预防与控制研究》", 31 October 2005, 中国农业科学技术出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108341716A (en) * | 2018-04-02 | 2018-07-31 | 青岛元汇丰企业管理咨询服务有限公司 | A kind of antibacterial growth-promoting elongated biological pesticide of plant source |
| CN108633690A (en) * | 2018-04-16 | 2018-10-12 | 安徽梅兰园林景观工程有限公司 | A kind of soilless cultivation substrate of flowers and preparation method thereof |
| CN110506763A (en) * | 2019-09-18 | 2019-11-29 | 浙江省农业科学院 | A kind of novel environment friendly pesticide reagent and preparation method thereof |
| CN114766517A (en) * | 2022-03-28 | 2022-07-22 | 河北农业大学 | Application of vitex rotundifolia extract, pesticide and preparation method of pesticide |
| CN114766517B (en) * | 2022-03-28 | 2024-09-13 | 河北农业大学 | Application of fructus viticis extract, pesticide and preparation method thereof |
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