CN102599200B - Chinese medicinal herb plant protecting agent and preparation method thereof - Google Patents
Chinese medicinal herb plant protecting agent and preparation method thereof Download PDFInfo
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- CN102599200B CN102599200B CN201210038619.2A CN201210038619A CN102599200B CN 102599200 B CN102599200 B CN 102599200B CN 201210038619 A CN201210038619 A CN 201210038619A CN 102599200 B CN102599200 B CN 102599200B
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
The invention discloses a Chinese medicinal herb plant protecting agent, which comprises the following raw materials: Euphorbia pekinensis, Rhizoma arisaematis, Pinellia ternate, Semen Strychni, Cortex Meliae, Fructus Toosendan, Litsea cubeba oil, castor oil, silicate, a surface active agent and a tackifier. A preparation method comprises the following steps: firstly decocting the Chinese medicinal herbs twice in water; merging filtrates and adding into an emulsifying reactor, then adding an emulsifying agent and uniformly mixing; then adding the Litsea cubeba oil and/or the castor oil for emulsifying; and finally adding a mixed seriflux of the tackifier and silicate, and fully mixing and homogenizing to obtain the product. The Chinese medicinal herb plant protecting agent is a novel pesticide preparation with the functions of killing insects, sterilizing and resisting viruses, can be singly used or/and used by being mixed with common pesticides, has effects of touch toxicity, intestine toxicity, nerve toxicity and sterilization on insects, keeps the advantages of low toxicity, high efficiency, easy degradation and no residual of Chinese medicinal herbs, has no drug resistance to insects or environmental pollution, has a good preventing and curing effect on horticultural plants and urban landscaping plants, and has good economic benefits, social benefits and environmental-protection benefits.
Description
Technical field
The invention belongs to agricultural insecticide bactericide technical field, relate to a kind of Chinese herbal medicine plant protection agent and preparation method thereof.
Background technology
Litsea cubeba oil (Litsea cubeba oil), has another name called Litsea cubeba oil, Litsea cubeba oil, the essential oil extracting from fruit of a cubeb litsea tree fruit with steam distillation.The fruit of a cubeb litsea tree is a kind of canella, and main product is in East Asia, and on the south China the Changjiang river, there are a large amount of plantations each province, main component: carbonyls (in citral) >=66%.Main component is citral, and content approximately reaches 60%-80%.Other composition comprises methyl heptenone, citronellal, citronellol, firpene, hesperidene, 1, 8-Cineole, amphene, linalool, 2-methyl-2 hexene-6-ketone, camphor, safrole, nerol, geraniol, terpineol, geranyl acetate, eugenol and p-cymene etc.Containing 26 kinds of above chemically reactive substances, there is broad-spectrum antibacterial action, its main component is citral, its Antibacterial Mechanism complexity is various.It can directly make bacterioprotein or enzyme denaturation, with some chemical group direct effects, DNA and RNA is produced to chemical action, destroy the institutional framework of bacterium, suppress biosynthesis, reduce permeability or the sealing cell wall of cell membrane, the approach performance antibacterial actions such as the katabolism of interference bacterium.
Printing Dong element (azadirachtin) is the main active insecticidal components of a kind of triterpene compound, in the positions such as seed, leaf, bark and branch, contains multiple insecticide active substance, wherein strong with the insecticidal activity of seal strain element.The insect in the multiple different length of times is demonstrated suppress to take food, the effect of repellent, toxicity and disturbance endocrine.Oneself uses for many years in developing country as natural botanical insecticide to print Dong seed oil.Printing Dong tree (Azadirachtaindica) is the autochthonal tropical trees in arid area, a kind of Asia, and on the south China the Changjiang river, there are a large amount of plantations each province.Now also by some country's cultivations of Central and South America.
Pesticide species is in the market various, and great majority are chemical pesticides, and these toxicity of pesticide are strong, and power is large, and crop insecticide, sterilization are played a role.But, because these agricultural chemicals are due to strong toxicity, be difficult for decomposing, the use of the crops such as edible grain, melon and fruit and vegetables is produced to very large side effect, often can cause food poisoning and slow iron poisoning, the whole nation is every year met not freshly because of food vegetables, the poisoning accident of melon and fruit, and the incidence of disease of other difficult strange illnesses such as the cancer that chronic poisoning causes sharply increases, by serious harm people's physical and mental health; Meanwhile, owing to using chemical pesticide, plant is developed immunity to drugs, in order to reach control efficiency, have to increase year by year every mu of dosage, cost is constantly raise, and control efficiency is general.People wish to have a kind of new nontoxic, pollution-free and non-harmful biopesticide to come for chemical pesticide.Utilize that the exploitation of natural pesticide plant is efficient, low toxicity and vegetable insecticide free from environmental pollution, be subject to just gradually people's great attention.By literature search, the pesticide species of exploitation has natural plant type and natural plants and chemical pesticide compound, and existing extracts is as follows:
Chinese patent CN 00113939.8 plant insecticide and preparation method thereof, it is characterized in that said preparation is formed and printed Dong element 0.1-90%, oxymatrine 0.1-98%, matrine 0.1-98% and other plant extracts 0.5% by the composition of following weight ratio, all the other are auxiliary agent.The auxiliary agent adopting has: surfactant can be selected: the rare and sldium lauryl sulfate of tween, sapn, OP-10, polyoxy second; Stabilizing agent: epoxidized vegetable oil; Organic solvent; Methyl alcohol, ethanol and butanone; PH adjusting agent: sodium hydroxid and acetic acid; Preservative: benzoic acid is received.
Chinese patent CN00114227.5 prints Dong extract plant insects agent formulation, prints each composition weight proportion in Dong element cream preparation to be: to print Dong cellulose content be 0.1-92%, print Dong oil content is that 0.5-60%, surface-active contents are that 1-40%, cosolvent content are that 0.2-20%, sun-screening agent content are that 1-2.5%, antiseptic content are that 0.1-2%, stabiliser content are that 0.1-30%, synergist content are that 0.5-10%, organic solvent content are 5.40%, penetrating agent content is that 0.1-24% and pH value conditioning agent content are 0.01-0.5%.
Chinese patent CN 01119394.8 prints the pesticidal preparations of Dong element and rotenone mixture, and this invention utilization prints Dong seed and carries out lixiviate, becomes and contains certain density seal Dong element extract, and extract becomes concentrate after concentrated evaporate to dryness.The seal Dong element that the present invention utilizes plant to print in Dong seed is active insecticidal components, by with biopesticide rotenone mixture, and allocate appropriate amount of addition agent into and be prepared into and print an element ten rotenone emulsifiable solution formulations.Agricultural chemicals prints each composition weight proportion in Dong element ten rotenone emulsifiable solution formulations: print Dong cellulose content and be 0.1-80%, rotenone content and be 0.1-20%, surface-active contents and be 1-40%, cosolvent content and be 0.2-20%, sun-screening agent content and be 1-2.5%, antiseptic content and be 0.1-2%, stabiliser content and be 0.1-30%, synergist content and be 0.5-10%, organic solvent content and be 5.40%, penetrating agent content is that 0.1-24% and pH value conditioning agent content are 0.01-0.5%.
Chinese patent CN 01119399.9 prints the pesticidal preparations of Dong element and pyrethroid mixture, mixed insecticide prints each component content weight proportion in Dong element ten pyrethroid cream preparations: printing Dong cellulose content is 0.1-80%, pyrethroid ester content is 0.3-25%, surface-active contents is 1-40%, cosolvent content is 0.2-20%, sun-screening agent content is 1-2.5%, antiseptic content is 0.1-2%, stabiliser content is 0.1-30%, synergist content is 0.5-10%, organic solvent content is 5-40%, penetrating agent content is that 0.1-24% and pH value conditioning agent content are 0.01-0.5%, each component summation is 100%.
Chinese patent CN 96118296.2 disease-resistant, insect-prevention, increasing-production agent for plants, technical scheme is: adopt the percentage proportioning of main component to be: litsea cubeba oil: 1-10%, tea oil: 1-15%, tung oil: 3-35%, castor oil: 2-12%, eucalyptus citriodora oil: 1-6%, propylene glycol fatty acid: 1-8% and lytic agent: 5-8%.Lytic agent adopts purified petroleum benzin 5-18%, pyridine 2-16%, methyl alcohol 5-38%, acetone 1-34% and ether 4-5%.Compound method is: first purified petroleum benzin, methyl alcohol precentagewise proportioning example in dissolving punishment are entered in container, then precentagewise proportioning is progressively poured litsea cubeba oil, tea oil, tung oil, castor oil, eucalyptus citriodora oil and propylene glycol fatty acid in this container respectively, 6-10 minute stirs, again acetone ether in lytic agent also precentagewise proportioning example is entered in container, stir 10 minutes, be sampled in test tube, carry out aqueous dispersion timing and reach the pesticidal emulsifiable standard of national regulation.This invention also can also can add cedar oil, wooden leaf oils on the basis of above-mentioned Main Ingredients and Appearance litsea cubeba oil, tea oil, tung oil, castor oil, eucalyptus citriodora oil, propylene glycol fatty acid and lytic agent, the cedar oil adding can be by 0.1-5%, and wooden leaf oils can be carried out proportioning by 0.5-8% and be added.
Chinese patent CN 200310110556.8 public nuisance free yellow lemon emulsified oil biological pesticides, its formula sassafras oil (shiu oil) 1-30%, citral (going out grey seed oil) 15-50%, emulsifier 15-20%, stabilizing agent 5-15%, bleeding agent 10-15% and synergist 10-15%.Technique is that above-mentioned medicament is first used after technical grade sassafras oil dissolved dilution under 10-37 degree normal temperature, add again after citral dissolved dilution, evenly adding to stir after 30 minutes adds auxiliary material emulsifier, stabilizing agent, bleeding agent and synergist to stir successively 30 minutes again, suction stabilization pond detects mark by the analysis of agricultural drugs after 4 hours and suppresses after the each qualified of detection, sub-bottle packaging.Main feature is high effect nontoxic, without residual hazard, to person poultry harmless, harmless to crops, and chronic administration does not form destruction to environment and ecology.The chemical pesticide that can effectively prevent high poison and high residue works the mischief to people and animals, crops and ecotope.
The preparation method of Chinese patent CN 200410040319.3 water soluble compound natural insecticides, its natural pyrethrin of filling a prescription: print Dong element: organic solvent: cyclodextrine=0.001-100: 0.001-100: 800-3000: 2000-5000.Preparation method is dissolved in natural pyrethrin and seal Dong element in organic solvent at normal temperatures, make the composition of natural pyrethrin-Yin Dong element, in the combination of natural pyrethrin-Yin Dong element, add cyclodextrine, stir, be dried, make the inclusion compound of water Rong natural pyrethrin-Yin Dong element, make water-soluble natural insecticide, this inclusion compound can be half dry or powder, soluble in water, also can further dilute.
200610029814.3 1 kinds of highly effective environment-friendly type biological insecticides of Chinese patent CN, it all utilizes natural plant extracts, plain as main compositions useful taking d mono-citrene and seal Dong, its component and weight package are containing (R)-4-isopropenyl-1-methyl-1-cyclohexene 10-40%, seal Dong element 0.1-5%, emulsifier 10-25% and solvent 30-74.9%.
Show from domestic and international large quantity research, in the position such as seed, leaf, bark and branch that prints Dong, contain multiple insecticide active substance, wherein strong to print the insecticidal activity of Dong element.But, as the natural seal Dong element of natural active products, there is easy photodissociation and hydrolysis, easily oxidized, the responsive and non-water-soluble shortcoming to pH value.These shortcomings are that processing and the use of natural seal Dong element product brings negative effect.Printing Dong element is food refusal to the effect main manifestations of insect, and speed of action is invaded, but the residence time is longer, and also has unique worm spectrum.
Summary of the invention
The object of the invention is for above-mentioned weak point, provide a kind of preparation method simple, there is Chinese herbal medicine plant protection agent of low, the free from environmental pollution and synergistic function of desinsection, sterilization, toxicity and preparation method thereof.
The object of the invention is to realize like this:
A kind of Chinese herbal medicine plant protection agent, comprises raw material components and parts by weight: root of Beijing euphorbia 10-20 part, rhizoma arisaematis 10-20 part, tuber of pinellia 10-20 part, Semen Strychni 0-20 part, bitter Dong skin 5-10 part, river Dong 0-20 part, litsea cubeba oil 0.3-0.6 part, castor oil 0.1-0.3 part, silicate 3-5 part, surfactant 0.3-1.0 part, tackifier 5-10 part and water are appropriate;
Described silicate comprises any one or more in sodium silicate, asbestos, clay and cement;
Described surfactant adopts sodium dodecylbenzene and calcium dodecyl benzene sulfonate;
Described tackifier comprise any one or more in shitosan, polyvinyl alcohol, carboxymethyl cellulose, carboxyethyl cellulose and methylcellulose.
Described Chinese herbal medicine plant protection agent, raw material components and parts by weight: root of Beijing euphorbia 15-18 part, rhizoma arisaematis 15-18 part, tuber of pinellia 14-16 part, bitter Dong skin 8-10 part, litsea cubeba oil 0.5-0.6 part, castor oil 0.2-0.3 part, silicate 3-4 part, surfactant 0.6-1.0 part, tackifier 8-10 part and water are appropriate.
The preparation method of Chinese herbal medicine plant protection agent, comprise first by twice of former plant medicine boiling, filtrate merging is added in emulsion reactor, add again emulsifier to mix, then litsea cubeba oil and/or castor oil are added to emulsification, finally add tackifier fully to mix homogeneous with silicate mixed serum, obtain Chinese herbal medicine plant protection agent product of the present invention, processing step is as follows:
(1) decoct: by Chinese herbal medicine boiling twice, merging filtrate;
(2) emulsification: surfactant is added in filtrate, then add litsea cubeba oil and castor oil emulsification to obtain emulsion;
(3) dissolve: tackifier raw material is added water to heat to dissolve makes slurries, then adds silicate to obtain mixed serum;
(4) homogeneous: mixed serum is added and mixes homogeneous in emulsion and obtain product.
Described decoction, controls temperature 80-100 DEG C, each decocting time 1.5-3.5 hour; Decocting for the first time amount of water is the former medicine total weight parts of plant 4-6 times, and amount of water is the former medicine total weight parts of plant 3-5 times for the second time.
In the present invention, the root of Beijing euphorbia (Euphorbia pekinensis), nature and flavor: toil, cold, poisonous; Enter lung, spleen, kidney channel.Rhizoma arisaematis (RHIZOMA ARISAEMATIS), nature and flavor: hardship, pungent, temperature, poisonous; Return lung, liver, the spleen channel.The tuber of pinellia (Rhizoma Pinelliae), nature and flavor: warm in nature, taste is pungent, poisonous; Return the spleen channel, stomach warp, lung channel.Bitter Dong skin hardship, cold; Poisonous; Return liver, spleen, stomach warp.River Dong nature and flavor: cold, slightly poisonous; Return liver, stomach, small intestinl channel.Castor-oil plant (Ricinus communis L.), complete stool is poisonous, and seed toxicity is large.Children eat 3～4, and adult eats 20 and draws and can be poisoned to death.General calomel poisoning person shows languishment after half a day, and that severe one has is nauseating, stomachache, vomiting and diarrhoea, hyperthermia, accelerated breathing, tic of limbs, spasm, stupor death.Ox, horse, pig etc. are eaten castor bean by mistake, can cause poor appetite, vomiting, diarrhea, colic, spasm, death when serious.Domestic animal is eaten castor bean lethal dose by mistake: horse 36～50g, ox 350～450g, calf 20g, sheep 30g, goat 105～140g, pig 60g, piglet 15～20g, rabbit 1.5g, goose 1g, chicken 18g (Chen Jisheng, 1987).Semen Strychni (Semen Strychni), nature and flavor: hardship, cold, poison greatly; Return liver, spleen two warps.Can there is intoxicating phenomenon with 5～10 milligrams in adult, can lethally die for 30 milligrams.Occur that at first headache, dizziness, agitation, breathing strengthen, crick sense, swallow difficult, breathing increases the weight of, myosis, feeling of distension and oppression over the chest, unsmooth breath, whole body is felt nervous, then extensor and musculus flexor do extremely to shrink simultaneously, to listening, look, the tetchiness such as taste, sensation, then there is typical convulsions symptom, it is last that respiratory muscle is tetanic is choked to death.
Advantage of the present invention and good effect:
1, this Chinese herbal medicine plant protection agent, has good control efficiency to gardening plant and urban greenery plants, is a kind of collection desinsection, sterilizing and antiviral novel agrochemical formulations, and the single use of energy is or/and common pesticide mixes use.Through evidence: there is special efficacy in all kinds of insect pests such as control greening vegetation and flower plants and nursery stocks, reach the object of protection greening vegetation and flower plants and nursery stock.
2, this botanical plant-protecting agent is taking plant resource as raw material; reasonable recipe; the effect of touching poison, malicious, the neural poison of intestines and sterilization is played in cooperation between them to plant insect; Chinese herbal medicine low toxicity, efficient, easily degraded, noresidue are kept; to insect be difficult for developing immunity to drugs, advantage free from environmental pollution, its raw material sources are abundant, do not produce in process of production and do not discharge any pollutant; preserve the ecological environment, alleviate the toxic action to people and animals.
3, the technological process of production of the present invention is simple, and cost is low, has good economic benefit, social benefit and environmental benefit.
Embodiment
Embodiment 1
(1) raw material components and parts by weight:
800 parts, 18 parts of the roots of Beijing euphorbia, 16 parts of rhizoma arisaematis, 15 parts of the tuber of pinellia, 10 parts of bitter Dong skins, 0.6 part of litsea cubeba oil, 0.3 part of castor oil, 1 part of sodium silicate, 2 parts, asbestos, 1.0 parts of sodium dodecylbenzenes, 8 parts of carboxymethyl celluloses and water.
(2) preparation method:
First Chinese herbal medicine is added in decoction pot, then the water of half is added, heat up, control 96 DEG C of temperature, decocting time completes for the first time and decocts for 3 hours, leaches decoction liquor; Add remaining carrying out to decoct for the second time, control 96 DEG C of temperature, decocting time 2 hours, leaches decoction liquor and merges with decoction liquor for the first time.Decoction liquor is added in stainless steel still or enamel still, start and stir, add surfactant, then add litsea cubeba oil and castor oil emulsification to obtain emulsion; Tackifier raw material is added to appropriate emulsion dissolving and make slurries, then add silicate to obtain mixed serum, mixed serum is dropped in stainless steel still or enamel still and mixed all, after homogeneous, obtain product.
(3) application test:
In in June, 2011 roadside greening vegetation dispenser to green belt and the two supports road in XinXingYuan community, Qingxiu District, Nanning City, by 2 kilograms of amount of formulation, dilute even spraying with the clear water of 350 and 450 times according to every mu respectively.After dispenser, have tag, the effect such as intestines poison, neural poison and sterilization, in two days, reach desinsection peak, after desinsection, in 60 days, have no the generation of insect pest, solve a Liao Yuan this area desinsection difficult problem seemingly-dead and that existing agricultural chemicals used is developed immunity to drugs.
Embodiment 2
(1) raw material components and parts by weight:
600 parts, 10 parts of the roots of Beijing euphorbia, 10 parts of rhizoma arisaematis, 20 parts of the tuber of pinellia, 10 parts of bitter Dong skins, 0.3 part, 0.3 part of litsea cubeba oil, clay part, 2 parts of cement, 0.7 part of calcium dodecyl benzene sulfonate, 5 parts of polyvinyl alcohol and water.
(2) preparation method:
First Chinese herbal medicine is added in decoction pot, then 6/10ths water is added, heat up, control 90 DEG C of temperature, decocting time completes for the first time and decocts for 2.5 hours, leaches decoction liquor; Add remaining carrying out to decoct for the second time, control 90 DEG C of temperature, 2.5 hours, leach decoction liquor and merge with decoction liquor for the first time.Decoction liquor is added in stainless steel still or enamel still, start and stir, add surfactant, then add litsea cubeba oil and castor oil emulsification to obtain emulsion; Tackifier raw material is added to appropriate emulsion dissolving and make slurries, then add silicate to obtain mixed serum, mixed serum is dropped in stainless steel still or enamel still and mixed all, after homogeneous, obtain product.
(3) application test:
In May, 2011, in Xixiangtang District, Nanning City, friendly road central plaza, to the landscape tree dispenser in green belt, by 2 kilograms of amount of formulation, dilutes even spraying with the clear water of 300 times according to every mu.After dispenser, have tag, the effect such as intestines poison, neural poison and sterilization, in one day, reach desinsection peak, after desinsection, in 2 months, have no the generation of insect evil, solve a Liao Yuan square trees desinsection difficult problem seemingly-dead and that existing agricultural chemicals used is developed immunity to drugs.
Embodiment 3
(1) raw material components and parts by weight:
700 parts, 20 parts of the roots of Beijing euphorbia, 14 parts of rhizoma arisaematis, 12 parts of the tuber of pinellia, 5 parts of Semen Strychnis, 6 parts of bitter Dong skins, 8 parts of river Dong, 0.5 part of litsea cubeba oil, 1.5 parts, asbestos, 2 parts of clays, 0.4 part of sodium dodecylbenzene, 7 parts of methylcellulose and water.
(2) preparation method:
First Chinese herbal medicine is added in decoction pot, then the water of half is added, heat up, control 85 DEG C of temperature, decocting time completes for the first time and decocts for 3.5 hours, leaches decoction liquor; Add remaining carrying out to decoct for the second time, control 85 DEG C of temperature, decocting time 2 hours, leaches decoction liquor and merges with decoction liquor for the first time.Decoction liquor is added in stainless steel still or enamel still, start and stir, add surfactant, then add the emulsification of litsea cubeba oil oil to obtain emulsion; Tackifier raw material is added to appropriate emulsion dissolving and make slurries, then add silicate to obtain mixed serum, mixed serum is dropped in stainless steel still or enamel still and mixed all, after homogeneous, obtain product.
(3) application test:
In May, 2011, in Xingning District, Nanning City, northern lake garden spot is to 60 mu of dispensers of the nursery stock in garden, and every mu by 1.5 kilograms of amount of formulation, by the clear water dilution even spraying of 500 times.After dispenser, have tag, the effect such as intestines poison, neural poison and sterilization, in two days, reach desinsection peak, after desinsection, in 45 days, have no the generation again of insect pest, solve a desinsection difficult problem seemingly-dead and that existing agricultural chemicals used is developed immunity to drugs in Liao Yuangai garden.
Claims (4)
1. a Chinese herbal medicine plant protection agent, is characterized in that: be prepared from by following raw material components and parts by weight: 800 parts, 18 parts of the roots of Beijing euphorbia, 16 parts of rhizoma arisaematis, 15 parts of the tuber of pinellia, 10 parts of azedaraches, 0.6 part of litsea cubeba oil, 0.3 part of castor oil, 1 part of sodium silicate, 2 parts, asbestos, 1.0 parts of sodium dodecylbenzenes, 8 parts of carboxymethyl celluloses and water.
2. a kind of Chinese herbal medicine plant protection agent according to claim 1, it is characterized in that: described preparation is first 10 parts of 18 parts of the Chinese herbal medicine roots of Beijing euphorbia, 16 parts of rhizoma arisaematis, 15 parts of the tuber of pinellia, azedarach to be added in decoction pot, then the water of half is added, heat up, control 96 DEG C of temperature, decocting time completes for the first time and decocts for 3 hours, leaches decoction liquor; Add remaining water to decoct for the second time, control 96 DEG C of temperature, decocting time 2 hours, leaches decoction liquor and merges with decoction liquor for the first time; Decoction liquor is added in stainless steel still or enamel still, start and stir, add 1.0 parts of surfactant sodium dodecylbenzenes, then add 0.6 part of litsea cubeba oil and 0.3 part of emulsification of castor oil to obtain emulsion; 8 parts of tackifier raw material carboxymethyl celluloses are added to emulsion and dissolve and make slurries, then add 2 parts of 1 part of sodium silicate, asbestos mixed serum, mixed serum is dropped in stainless steel still or enamel still and is mixed all, after homogeneous, obtain product.
3. a Chinese herbal medicine plant protection agent, is characterized in that: be prepared from by following raw material components and parts by weight: 700 parts, 20 parts of the roots of Beijing euphorbia, 14 parts of rhizoma arisaematis, 12 parts of the tuber of pinellia, 5 parts of Semen Strychnis, 6 parts of azedaraches, 8 parts of Fructus meliae toosendans, 0.5 part of litsea cubeba oil, 1.5 parts, asbestos, 2 parts of clays, 0.4 part of sodium dodecylbenzene, 7 parts of methylcellulose and water.
4. a kind of Chinese herbal medicine plant protection agent according to claim 3, it is characterized in that: described preparation is first 8 parts of 20 parts of the Chinese herbal medicine roots of Beijing euphorbia, 14 parts of rhizoma arisaematis, 12 parts of the tuber of pinellia, 5 parts of Semen Strychnis, 6 parts of azedaraches, Fructus meliae toosendan to be added in decoction pot, then the water of half is added, heat up, control 85 DEG C of temperature, decocting time completes for the first time and decocts for 3.5 hours, leaches decoction liquor; Add remaining water to decoct for the second time, control 85 DEG C of temperature, decocting time 2 hours, leach decoction liquor and merge with decoction liquor for the first time, decoction liquor is added in stainless steel still or enamel still, start and stir, add 0.4 part of surfactant sodium dodecylbenzene, then add 0.5 part of emulsification of litsea cubeba oil to obtain emulsion; 7 parts of tackifier raw material methylcellulose are added to emulsion dissolving and make slurries, then add 1.5 parts, asbestos to obtain mixed serum with 2 parts of clays, mixed serum is dropped in stainless steel still or enamel still and mixed all, after homogeneous, obtain product.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1108887A (en) * | 1995-01-14 | 1995-09-27 | 李瑛� | Insecticide made from Chinese medical herbs and its preparation |
| US20020076428A1 (en) * | 2000-12-19 | 2002-06-20 | Wharton Steven P. | Compositions for mole control |
| CN101223892A (en) * | 2008-01-25 | 2008-07-23 | 辛贵有 | Toosendanin-containing compound pesticide and preparing method thereof |
| CN101926372A (en) * | 2010-07-12 | 2010-12-29 | 重庆东方农药有限公司 | Nicotinamide-matrine aqua vegetable insecticide and preparation method thereof |
| CN102283258A (en) * | 2011-07-22 | 2011-12-21 | 南宁冠华农业科技有限公司 | Plant protecting agent for plant source and preparation method thereof |
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2012
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1108887A (en) * | 1995-01-14 | 1995-09-27 | 李瑛� | Insecticide made from Chinese medical herbs and its preparation |
| US20020076428A1 (en) * | 2000-12-19 | 2002-06-20 | Wharton Steven P. | Compositions for mole control |
| CN101223892A (en) * | 2008-01-25 | 2008-07-23 | 辛贵有 | Toosendanin-containing compound pesticide and preparing method thereof |
| CN101926372A (en) * | 2010-07-12 | 2010-12-29 | 重庆东方农药有限公司 | Nicotinamide-matrine aqua vegetable insecticide and preparation method thereof |
| CN102283258A (en) * | 2011-07-22 | 2011-12-21 | 南宁冠华农业科技有限公司 | Plant protecting agent for plant source and preparation method thereof |
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