CN104273184A - Insect-resistant pesticide for vegetables and preparation method of insect-resistant pesticide - Google Patents
Insect-resistant pesticide for vegetables and preparation method of insect-resistant pesticide Download PDFInfo
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- CN104273184A CN104273184A CN201410604954.3A CN201410604954A CN104273184A CN 104273184 A CN104273184 A CN 104273184A CN 201410604954 A CN201410604954 A CN 201410604954A CN 104273184 A CN104273184 A CN 104273184A
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Classifications
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses an insect-resistant pesticide for vegetables. The insect-resistant pesticide is prepared by taking a folium artemisiae argyi extracting solution, an iris japonica thumb extracting solution, a melia azedarach extracting solution, an euphorbia helioscopia extracting solution, a duranta repens extracting solution, a sweet wormwood extracting solution, white vinegar and pepper spray as raw materials. The insect-resistant pesticide can effectively prevent and kill vegetable worms such as aphids and snails, and enable the vegetables to grow luxuriantly, so as to improve the yield of the vegetables. Meanwhile, the liquid drug residual period of the insect-resistant pesticide is only 8-12 days, thus being non-toxic and harmless to people and livestock. The invention also provides a preparation method of the insect-resistant pesticide. The insect-resistant pesticide disclosed by the invention is remarkable in effect, low in cost, and green and pollution-free, thus having a broad market application prospect.
Description
Technical field
The present invention relates to a kind of insecticide, particularly a kind of vegetables insecticide and preparation method thereof.
Background technology
Vegetables are one of requisite food in people's conventional food.Vegetables can provide the necessary multivitamin of human body and mineral matter.One of requisite food in people's diet according to vegetables.Vegetables can provide the necessary multivitamin of human body and mineral matter.According to international food and agricultural organization nineteen ninety statistics, ascorbic 90%, the vitamin A of needed by human 60% from vegetables.In addition, in vegetables, also have diversified phytochemicals, be people generally acknowledge to the effective composition of health, as carotenoid, two propen compounds, methyl sulfide compound etc.Nutrient in current fruits and vegetables the many kinds of substance of effectively preventing chronic, degenerative disease can be studied discovery by people.Vegetables are dishes with, feed, the multipurpose breed such as view and admire, and easily, output is high, can repeatedly shell leaf to gather in cultivation, and the supply phase is long, and can go on the market when summer lacks leaf vegetables, the north can be cultivated at daylight energy-saving greenhouse.But vegetables are very easily insect infestation in process of growth, mainly contain the vegetables such as aphid, snail worm, if prevent not in time and kill vegetables worm, the seed output and quality of vegetables can be had a strong impact on.
At present, people are when preventing and treating vegetables worm, all generally adopt the agricultural chemicals of high concentration to spray, although control efficiency is fine, the farm chemical ingredients of Residues in Vegetables is too high, damages human body, the health of people is made easily to suffer from various illness, the immunocompetence of each function of human body is easily caused to decline, the vegetables that long-term edible remains of pesticide is too high, the generation of the various illness of easier hidden danger.
Summary of the invention
The object of the invention is to overcome above-mentioned deficiency existing in prior art, a kind of vegetables insecticide is provided.This insecticide is that raw material is prepared from by Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, WUDUOYUN extract, Bright Yellow extract, sweet wormwood extract, light-coloured vinegar, capsicum water, can effectively prevent and kill the vegetables such as aphid, snail worm, vegetables are made to look luxuriant, improve output, the liquor residue phase is short simultaneously, nontoxic to people and animals.
Another object of the present invention is to provide the preparation method of described insecticide.
In order to realize foregoing invention object, the invention provides following technical scheme:
Vegetables insecticide of the present invention is the medicament that raw material is prepared from by Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, WUDUOYUN extract, Bright Yellow extract, sweet wormwood extract, light-coloured vinegar, capsicum water.
Described Folium Artemisiae Argyi extractive liquid obtains by the following method: get tarragon, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain Folium Artemisiae Argyi extractive liquid.
Described fringed iris rhizome extract obtains by the following method: get fringed iris rhizome, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain fringed iris rhizome extract.
Described China tree extract obtains by the following method: get China tree, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain China tree extract.
Described WUDUOYUN extract obtains by the following method: get WUDUOYUN, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain WUDUOYUN extract.
Described Bright Yellow extract obtains by the following method: get Bright Yellow, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain Bright Yellow extract.
Described sweet wormwood extract obtains by the following method: get sweet wormwood, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain sweet wormwood extract.
Natural plants tarragon, fringed iris rhizome, China tree, WUDUOYUN, Bright Yellow, sweet wormwood are adopted water soaking 15 ~ 40 days by the present invention respectively, and effective ingredient is fully dissolved in water, filter and obtain extract.When soak time is less than 15 days, effective ingredient cannot fully be dissolved in water; When soak time is greater than 40 days, drug smell runs off, and drug effect reduces.Preferably, soak time is 35 days to the best.
Described capsicum water obtains by the following method: the red pepper of getting fresh mature, smashs to pieces, adds the water of 1 ~ 3 times of weight, soaking at room temperature 7 ~ 15 days, filters, gets filtrate, obtain capsicum water.Preferably, described capsicum water obtains by the following method: the red pepper of getting fresh mature, smashs to pieces, adds the water of 2 times of weight, soaking at room temperature 10 days, filters, gets filtrate, obtain capsicum water.Preferably, described capsicum is qi xing paprika, and qi xing paprika has the strong characteristic of pungent.
Tarragon is the dried leaves of feverfew Chinese mugwort Artemisia argyi Levl.et Vant., main containing compositions such as volatile oil, flavonoids, triterpenes, tannins, have the physiologically actives such as hemostasis, anti-bacteria and anti-virus, scavenging free radicals, analgesia, Folium Artemisiae Argyi extractive liquid has penetrating odor, can expelling parasite.Fringed iris rhizome is the rhizome shape of Jris herbaceous plant fringed iris, mainly be distributed in the ground such as East China, south China, southwest and Hebei, Shaanxi, Gansu, being a kind of ornamental plants, is also traditional traditional Chinese medicine, in traditional medicine for the desinsection that helps digestion, clearing away heat and loosing the bowels, control food abdominal distension etc.China tree is not only material with plant, and be also medicinal plant, its flower, leaf, fruit, root skin all can be used as medicine, can ascarifuge, hookworm etc., makes ointment can control favus of the scalp by chinaberry.Preferably, China tree extract of the present invention is Folium Meliae extract and/or chinaberry root extract.WUDUOYUN, has another name called wartwort, Euphorbia esula L, is a kind of herbaceos perennial opening five flowers, has anti-inflammatory, insecticidal action.Bright Yellow has another name called gold leaf Duranta repens Linn, the long oval of leaf, and coloured gold is yellow to yellowish green, and evergreen shrubs, southern china is widely cultivated, leaf bitter and puckery flavor, can strengthen the property of medicine and the penetrating odor of insecticide of the present invention.Light-coloured vinegar effectively can regulate the pH value of insecticide, makes it be highly acid, plays agent efficacy better.Capsicum water can strengthen insect protected and insecticidal power.
Applicant is found by lot of experiments, by natural plants Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, WUDUOYUN extract, Bright Yellow extract, sweet wormwood extract and light-coloured vinegar, capsicum water compatibility, the effect of Synergistic can be played, the insecticide obtained has micro-poison, effectively can kill the vegetables worms such as aphid, but little to people and animals' toxic and side effect; This insecticide has very strong pungent odor simultaneously, effectively can drive the vegetables such as aphid, snail worm, to reach the object preventing and kill the vegetables such as aphid, snail worm.
Preferably, the weight of described each raw material is: Folium Artemisiae Argyi extractive liquid 3 ~ 10 parts, fringed iris rhizome extract 3 ~ 10 parts, China tree extract 3 ~ 10 parts, WUDUOYUN extract 1 ~ 8 part, Bright Yellow extract 1 ~ 8 part, sweet wormwood extract 1 ~ 8 part, light-coloured vinegar 0.05 ~ 2 part, capsicum water 1 ~ 4 part.Insecticide of the present invention with Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, WUDUOYUN extract, Bright Yellow extract, sweet wormwood extract, light-coloured vinegar and capsicum water for raw material, effect of insect protected, desinsection should be played, reduce its toxic action to people and animals again, this just brings very large difficulty for the screening of parts by weight of raw materials proportioning.Applicant is through repeatedly replica test discovery, and insecticide of the present invention, under above-mentioned weight, can effectively prevent and kill the vegetables such as aphid, snail worm, significantly improve the output of vegetables, and the liquor residue phase is short.
Further preferably, the weight of described each raw material is: fringed iris rhizome extract 3 ~ 10 parts, Folium Artemisiae Argyi extractive liquid 4 ~ 8 parts, China tree extract 3 ~ 9 parts, WUDUOYUN extract 2 ~ 7 parts, Bright Yellow extract 1 ~ 6 part, sweet wormwood extract 2 ~ 6 parts, light-coloured vinegar 0.05 ~ 1.5 part, capsicum water 1 ~ 3 part.
Still more preferably, the weight of described each raw material is: fringed iris rhizome extract 3 ~ 8 parts, Folium Artemisiae Argyi extractive liquid 4 ~ 7 parts, China tree extract 3 ~ 9 parts, WUDUOYUN extract 2 ~ 7 parts, Bright Yellow extract 2 ~ 6 parts, sweet wormwood extract 2 ~ 5 parts, light-coloured vinegar 0.08 ~ 1.0 part, capsicum water 1 ~ 3 part.
Still more preferably, the weight of described each raw material is: fringed iris rhizome extract 3 ~ 7 parts, Folium Artemisiae Argyi extractive liquid 4 ~ 7 parts, China tree extract 4 ~ 8 parts, WUDUOYUN extract 2 ~ 6 parts, Bright Yellow extract 2 ~ 6 parts, sweet wormwood extract 3 ~ 5 parts, light-coloured vinegar 0.08 ~ 0.8 part, capsicum water 1 ~ 3 part.
Still more preferably, the weight of described each raw material is: fringed iris rhizome extract 4 ~ 6 parts, Folium Artemisiae Argyi extractive liquid 4 ~ 7 parts, China tree extract 5 ~ 7 parts, WUDUOYUN extract 4 ~ 6 parts, Bright Yellow extract 3 ~ 5 parts, sweet wormwood extract 3 ~ 5 parts, light-coloured vinegar 0.1 ~ 0.5 part and capsicum water 1 ~ 2 part.
Preferably, the weight of described each raw material is the best: fringed iris rhizome extract 6 parts, Folium Artemisiae Argyi extractive liquid 6 parts, China tree extract 5 parts, WUDUOYUN extract 5 parts, Bright Yellow extract 4 parts, sweet wormwood extract 4 parts, light-coloured vinegar 0.2 part and capsicum water 1.8 parts.
By preferably above, the synergistic function between each raw material components can be played further, strengthen the efficacy of drugs of medicament, strengthen the strong sharp aroma of medicament simultaneously, thus prevent and kill the vegetables such as aphid, snail worm better, significantly improve the output of vegetables.
The preparation method of vegetables insecticide of the present invention, concrete steps are as follows: by ratio of weight and the number of copies, Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, WUDUOYUN extract, Bright Yellow extract and sweet wormwood extract are mixed, then light-coloured vinegar and capsicum water is added, mixing, obtains vegetables insecticide.
During use, vegetables of the present invention insecticide sprayer is evenly sprayed on vegetables.If fine day, can spray again once after 3 days; If the rainy day, wait and become a fine day rear continuation spray.
Compared with prior art, beneficial effect of the present invention is:
(1) insecticide of the present invention with natural plants Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, WUDUOYUN extract, Bright Yellow extract, sweet wormwood extract and light-coloured vinegar, capsicum water for raw material components, further by the weight of each raw material components of screening, each raw material components is made to play the effect of Synergistic, the micro-poison had by it and strong pungent odor effectively kill the vegetables such as aphid, snail worm, reach more than 90% to the preventing efficiency of the various vegetable fields such as eggplant, radish, Chinese cabbage, cabbage, capsicum.
(2) vegetables of the present invention effectively prevent with insecticide and kill the vegetables such as aphid, snail worm, make vegetables growing way better, output increased more than 10%; The liquor residue phase is short, only 8 ~ 12 days.
(2) preparation method of insecticide of the present invention fully remains the active drug composition of each raw material components, and technique is simple, and cost is low.
Embodiment
Below in conjunction with test example and embodiment, the present invention is described in further detail.But this should be interpreted as that the scope of the above-mentioned theme of the present invention is only limitted to following embodiment, all technology realized based on content of the present invention all belong to scope of the present invention.
Embodiment 1
(1) preparation of raw material
The preparation of Folium Artemisiae Argyi extractive liquid: get tarragon, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, gets filtrate, obtain Folium Artemisiae Argyi extractive liquid.
The preparation of fringed iris rhizome extract: get fringed iris rhizome, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, gets filtrate, obtain fringed iris rhizome extract.
The preparation of China tree extract: get chinaberry root, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, gets filtrate, obtain China tree extract.
WUDUOYUN extract: get WUDUOYUN, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, gets filtrate, obtain WUDUOYUN extract.
The preparation of Bright Yellow extract: get Bright Yellow, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, gets filtrate, obtain Bright Yellow extract.
The preparation of sweet wormwood extract: get sweet wormwood, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, gets filtrate, obtain sweet wormwood extract.
The preparation of capsicum water: the qi xing paprika getting the maturation redness of just plucking is smashed to pieces, adds the water of 2 times of weight, soaking at room temperature 10 days, filters, gets filtrate, obtain capsicum water.
(2) preparation of insecticide
By ratio of weight and the number of copies, get Folium Artemisiae Argyi extractive liquid 6 parts, fringed iris rhizome extract 6 parts, China tree extract 5 parts, WUDUOYUN extract 5 parts, Bright Yellow extract 4 parts and sweet wormwood extract 4 parts mixing, then add light-coloured vinegar 0.2 part and capsicum water 1.8 parts, mixing, obtains vegetables insecticide.
Embodiment 2
(1) preparation of raw material
The preparation of Folium Artemisiae Argyi extractive liquid: get tarragon, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, gets filtrate, obtain Folium Artemisiae Argyi extractive liquid.
The preparation of fringed iris rhizome extract: get fringed iris rhizome, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, gets filtrate, obtain fringed iris rhizome extract.
The preparation of China tree extract: get Folium Meliae, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, gets filtrate, obtain China tree extract.
WUDUOYUN extract: get WUDUOYUN, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, gets filtrate, obtain WUDUOYUN extract.
The preparation of Bright Yellow extract: get Bright Yellow, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, gets filtrate, obtain Bright Yellow extract.
The preparation of sweet wormwood extract: get sweet wormwood, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, gets filtrate, obtain sweet wormwood extract.
The preparation of capsicum water: smashed to pieces by the qi xing paprika of the maturation redness of just having plucked, add the water of 1 times of weight, soaking at room temperature 7 days, filters, gets filtrate, obtain capsicum water.
(2) preparation of insecticide
By ratio of weight and the number of copies, get Folium Artemisiae Argyi extractive liquid 3 parts, fringed iris rhizome extract 3 parts, China tree extract 3 parts, WUDUOYUN extract 1 part, Bright Yellow extract 1 part and sweet wormwood extract 1 part mixing, then add light-coloured vinegar 0.05 part and capsicum water 1 part, mixing, obtains vegetables insecticide.
Embodiment 3
(1) preparation of raw material
The preparation of Folium Artemisiae Argyi extractive liquid: get tarragon, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, gets filtrate, obtain Folium Artemisiae Argyi extractive liquid.
The preparation of fringed iris rhizome extract: get fringed iris rhizome, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, gets filtrate, obtain fringed iris rhizome extract.
The preparation of China tree extract: get chinaberry root, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, gets filtrate, obtain China tree extract.
WUDUOYUN extract: get WUDUOYUN, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, gets filtrate, obtain WUDUOYUN extract.
The preparation of Bright Yellow extract: get Bright Yellow, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, gets filtrate, obtain Bright Yellow extract.
The preparation of sweet wormwood extract: get sweet wormwood, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, gets filtrate, obtain sweet wormwood extract.
The preparation of capsicum water: the qi xing paprika getting the maturation redness of just plucking is smashed to pieces, adds the water of 3 times of weight, soaking at room temperature 15 days, filters, gets filtrate, obtain capsicum water.
(2) preparation of insecticide
By ratio of weight and the number of copies, get Folium Artemisiae Argyi extractive liquid 10 parts, fringed iris rhizome extract 10 parts, China tree extract 10 parts, WUDUOYUN extract 8 parts, Bright Yellow extract 8 parts and sweet wormwood extract 8 parts mixing, then add light-coloured vinegar 2 parts and capsicum water 3 parts, mixing, obtains vegetables insecticide.
Embodiment 4
(1) preparation of raw material
The preparation of Folium Artemisiae Argyi extractive liquid: get tarragon, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, gets filtrate, obtain Folium Artemisiae Argyi extractive liquid.
The preparation of fringed iris rhizome extract: get fringed iris rhizome, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, gets filtrate, obtain fringed iris rhizome extract.
The preparation of China tree extract: get Folium Meliae, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, gets filtrate, obtain China tree extract.
WUDUOYUN extract: get WUDUOYUN, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, gets filtrate, obtain WUDUOYUN extract.
The preparation of Bright Yellow extract: get Bright Yellow, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, gets filtrate, obtain Bright Yellow extract.
The preparation of sweet wormwood extract: get sweet wormwood, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, gets filtrate, obtain sweet wormwood extract.
The preparation of capsicum water: get the red qi xing paprika of the maturation of just plucking and smash to pieces, add the water of 2 times of weight, soaking at room temperature 8 days, filter, get filtrate, obtain capsicum water.
(2) preparation of insecticide
By ratio of weight and the number of copies, get Folium Artemisiae Argyi extractive liquid 8 parts, fringed iris rhizome extract 5 parts, China tree extract 7 parts, WUDUOYUN extract 4 parts, Bright Yellow extract 3 parts and sweet wormwood extract 5 parts mixing, then add light-coloured vinegar 1 part and capsicum water 2 parts, mixing, obtains vegetables insecticide.
Insecticide prepared by embodiment 1 ~ 4 is acid, in faint yellow, has very strong pungent odor.
Comparative example 1
By ratio of weight and the number of copies, get Folium Artemisiae Argyi extractive liquid 6 parts, China tree extract 5 parts, WUDUOYUN extract 5 parts, Bright Yellow extract 4 parts and sweet wormwood extract 4 parts mixing, then add light-coloured vinegar 0.2 part and capsicum water 1.8 parts, mixing, obtains vegetables insecticide.The preparation method of described Folium Artemisiae Argyi extractive liquid, China tree extract, WUDUOYUN extract, Bright Yellow extract, sweet wormwood extract and capsicum water is with embodiment 1.
Comparative example 2
By ratio of weight and the number of copies, get Folium Artemisiae Argyi extractive liquid 6 parts, fringed iris rhizome extract 6 parts, China tree extract 5 parts, WUDUOYUN extract 5 parts and sweet wormwood extract 4 parts mixing, then add light-coloured vinegar 0.2 part and capsicum water 1.8 parts, mixing, obtains vegetables insecticide.The preparation method of described Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, WUDUOYUN extract, sweet wormwood extract and capsicum water is with embodiment 1.
Comparative example 3
By ratio of weight and the number of copies, get Folium Artemisiae Argyi extractive liquid 6 parts, fringed iris rhizome extract 6 parts, China tree extract 5 parts, Bright Yellow extract 4 parts and sweet wormwood extract 4 parts mixing, then add capsicum water 1.8 parts, mixing, obtains vegetables insecticide.The preparation method of described Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, Bright Yellow extract, sweet wormwood extract and capsicum water is with embodiment 1.
Embodiment 5
Vegetables prepared by above-described embodiment 1 ~ 4 are carried out insect protected test with insecticide: to also not occurring that the cabbage ground of aphid, snail insect pest etc. monthly sprays twice insecticide of the present invention, each fountain height is 20kg/ mu, and second time is carried out after first time spray medicine for 3 days.Not spray the vegetable field of any insecticide for reference, evaluate the preventing efficiency of insecticide of the present invention on vegetables insect pest and the impact on yield of vegetables, simultaneously to spray the vegetable field of insecticide described in comparative example 1 ~ 3 for comparative example.
The wherein evaluation method of preventing efficiency: continuous spraying medicine is after 2 months, and random selecting 200 cabbages, observe the total amount of the vegetables such as aphid, snail worm on 200 cabbages.The computing formula of preventing efficiency is: preventing efficiency=(not spraying the worm total quantity of the worm total quantity-spray medicine vegetable field of medicine vegetable field) ÷ does not spray worm total quantity × 100% of medicine vegetable field.
Wherein the evaluation method of vegetable increase production rate is: timely collecting after vegetable ripeness, weighs.The computing formula of vegetable increase production rate is: vegetable increase production rate=(per mu yield of the per mu yield of spray medicine vegetable field-do not spray medicine vegetable field) ÷ sprays per mu yield × 100% of medicine vegetable field.
Experimental result result is as shown in table 1.
Table 1 insect protected is tested
| Group | Preventing efficiency (%) | Vegetable increase production rate (%) |
| Embodiment 1 | 98 | 18 |
| Embodiment 2 | 94 | 15 |
| Embodiment 3 | 93 | 15 |
| Embodiment 4 | 93 | 14 |
| Comparative example 1 | 78 | 7 |
| Comparative example 2 | 80 | 8 |
| Comparative example 3 | 76 | 5 |
Embodiment 6
Vegetables prepared by above-described embodiment 1 ~ 4 are carried out insecticidal test with insecticide, concrete grammar is: to occurring that the vegetable field of aphid, snail insect pest etc. monthly sprays 2 insecticides of the present invention, each fountain height is 20kg/ mu, and second time is carried out after first time spray medicine for 3 days.Not spray the vegetable field of any insecticide for reference, evaluate the preventing efficiency of insecticide of the present invention on vegetables insect pest and the impact on yield of vegetables, simultaneously to spray the vegetable field of insecticide described in comparative example 1 ~ 3 for comparative example, its result is as shown in table 2.Wherein the evaluation method of preventing efficiency and vegetable increase production rate is with embodiment 5.Experimental result is as shown in table 2.
Table 2 insecticidal test
| Group | Preventing efficiency (%) | Vegetable increase production rate (%) |
| Embodiment 1 | 95 | 15 |
| Embodiment 2 | 91 | 11 |
| Embodiment 3 | 92 | 11 |
| Embodiment 4 | 90 | 10 |
| Comparative example 1 | 76 | 6 |
| Comparative example 2 | 76 | 5 |
| Comparative example 3 | 74 | 4 |
In the experimentation of the present embodiment, applicant find when to occur aphid, snail insect pest etc. vegetable field sprinkling the embodiment of the present invention 1 ~ 4 described in insecticide after, aphid starts in 5 minutes to run chaotically on leaf, in 1h, the aphid of more than 85% stops running, and in 24h, the lethality of aphid is more than 90%.Show that insecticide of the present invention effectively can kill aphid, and instant effect.But the reaction of snail and aphid are had any different, after spraying insecticide of the present invention, snail climbs rapidly from vegetable leaf, starts to drain foreign matter after 2h.Show that insecticide of the present invention mainly has by it that strong pungent odor prevents and treats snail.
From embodiment 5 and 6, insecticide described in embodiment 1 ~ 4 is compared with the insecticide described in comparative example 1 ~ 3, it is to also not occurring the vegetable field of aphid, snail insect pest etc. and improve about 19% respectively to the preventing efficiency of the vegetable field occurring aphid, snail insect pest etc., and vegetable increase production rate improves about 10%.Show that in insecticide of the present invention, each raw material components is Synergistic.The preventing efficiency of the insecticide described in comparing embodiment 1 ~ 4 and known on the impact of yield of vegetables, insecticide described in embodiment 1 is compared with the insecticide described in embodiment 2 ~ 4, it is to also not occurring the vegetable field of aphid, snail insect pest etc. and improve about 4% respectively to the preventing efficiency of the vegetable field occurring aphid, snail insect pest etc., and vegetable increase production rate improves about 4%.Show that the insecticide in insecticide of the present invention described in embodiment 1 is optimum implementation of the present invention.
Embodiment 7
Vegetables prepared by above-described embodiment 1 ~ 4 are carried out the test of liquor residue phase with insecticide: be sprayed on vegetables leaf respectively by the vegetables insecticide described in the embodiment of the present invention 1 ~ 4, fountain height is 20kg/ mu.Vegetables leaf respectively after different time plucks spray medicine, prepare vegetable leaf extract, adopt TLC-colorimetric method to measure the residual quantity detecting margosine in vegetable leaf extract, agents useful for same is and analyzes pure, margosine reference substance is chromatographically pure, and its result is as shown in table 3.
The table 3 liquor residue phase tests
As shown in Table 3, only about the 8 days margosine residual life of vegetables insecticide of the present invention, also that is to say that the medicament residue phase of vegetables insecticide of the present invention is short, only about 8 days.
Embodiment 8
Vegetables prepared by above-described embodiment 1 ~ 4 are carried out animal toxicity test with insecticide: get Kunming mouse 50, male and female are use all, body weight 18 ~ 22g, is divided into five groups at random, often organize 10, the insecticide 1000mg/kg described in the other acute oral embodiment 1 ~ 4 of first ~ Four composition; The other acute oral of BSA commercially available agricultural chemicals (dimehypo) 350mg/kg.Observe the death condition of mouse in 5 days, insecticide of the present invention and commercially available agricultural chemicals is evaluated to the toxicity of kunming mice with this, result draws, insecticide prepared by the embodiment of the present invention 1 ~ 4 only shows low toxicity reaction to kunming mice, does not have dead mouse.And commercially available agricultural insecticide biconjugate kunming mice shows high poison reaction, 10 mouse are all dead.
From embodiment 7 and 8, insecticide of the present invention is little to people and animals' toxic and side effect, and the liquor residue phase is short, only about 8 days, can use safely.
Claims (10)
1. a vegetables insecticide, is characterized in that: it is the medicament that raw material is prepared from by Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, WUDUOYUN extract, Bright Yellow extract, sweet wormwood extract, light-coloured vinegar, capsicum water.
2. vegetables insecticide according to claim 1, is characterized in that: described Folium Artemisiae Argyi extractive liquid obtains by the following method: get tarragon, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain Folium Artemisiae Argyi extractive liquid; Described fringed iris rhizome extract obtains by the following method: get fringed iris rhizome, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain fringed iris rhizome extract; Described China tree extract obtains by the following method: get China tree, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain China tree extract; Described WUDUOYUN extract obtains by the following method: get WUDUOYUN, adds the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain WUDUOYUN extract; Described Bright Yellow extract obtains by the following method: get Bright Yellow, add the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filters, gets filtrate, obtain Bright Yellow extract: described sweet wormwood extract obtains by the following method: get sweet wormwood, add the water of 2 ~ 4 times of weight, soaking at room temperature 15 ~ 40 days, filter, get filtrate, obtain sweet wormwood extract.
3. vegetables insecticide according to claim 1, is characterized in that, described capsicum water obtains by the following method: get fresh chilli, smashs to pieces, adds the water of 1 ~ 3 times of weight, soaking at room temperature 7 ~ 15 days, filters, gets filtrate, obtain capsicum water.
4. vegetables insecticide according to claim 1, is characterized in that: the weight of described each raw material is: fringed iris rhizome extract 3 ~ 10 parts, Folium Artemisiae Argyi extractive liquid 3 ~ 10 parts, China tree extract 3 ~ 10 parts, WUDUOYUN extract 1 ~ 8 part, Bright Yellow extract 1 ~ 8 part, sweet wormwood extract 1 ~ 8 part, light-coloured vinegar 0.05 ~ 2 part, capsicum water 1 ~ 4 part.
5. vegetables insecticide according to claim 4, is characterized in that: the weight of described each raw material is: fringed iris rhizome extract 3 ~ 10 parts, Folium Artemisiae Argyi extractive liquid 4 ~ 8 parts, China tree extract 3 ~ 9 parts, WUDUOYUN extract 2 ~ 7 parts, Bright Yellow extract 1 ~ 6 part, sweet wormwood extract 2 ~ 6 parts, light-coloured vinegar 0.05 ~ 1.5 part, capsicum water 1 ~ 3 part.
6. vegetables insecticide according to claim 5, is characterized in that: the weight of described each raw material is: fringed iris rhizome extract 3 ~ 8 parts, Folium Artemisiae Argyi extractive liquid 4 ~ 7 parts, China tree extract 3 ~ 9 parts, WUDUOYUN extract 2 ~ 7 parts, Bright Yellow extract 2 ~ 6 parts, sweet wormwood extract 2 ~ 5 parts, light-coloured vinegar 0.08 ~ 1.0 part, capsicum water 1 ~ 3 part.
7. vegetables insecticide according to claim 6, is characterized in that: the weight of described each raw material is: fringed iris rhizome extract 3 ~ 7 parts, Folium Artemisiae Argyi extractive liquid 4 ~ 7 parts, China tree extract 4 ~ 8 parts, WUDUOYUN extract 2 ~ 6 parts, Bright Yellow extract 2 ~ 6 parts, sweet wormwood extract 3 ~ 5 parts, light-coloured vinegar 0.08 ~ 0.8 part, capsicum water 1 ~ 3 part.
8. vegetables insecticide according to claim 7, is characterized in that: the weight of described each raw material is: fringed iris rhizome extract 4 ~ 6 parts, Folium Artemisiae Argyi extractive liquid 4 ~ 7 parts, China tree extract 5 ~ 7 parts, WUDUOYUN extract 4 ~ 6 parts, Bright Yellow extract 3 ~ 5 parts, sweet wormwood extract 3 ~ 5 parts, light-coloured vinegar 0.1 ~ 0.5 part and capsicum water 1 ~ 2 part.
9. vegetables insecticide according to claim 8, is characterized in that: the weight of described each raw material is: fringed iris rhizome extract 6 parts, Folium Artemisiae Argyi extractive liquid 6 parts, China tree extract 5 parts, WUDUOYUN extract 5 parts, Bright Yellow extract 4 parts, sweet wormwood extract 4 parts, light-coloured vinegar 0.2 part and capsicum water 1.8 parts.
10. the preparation method of the vegetables insecticide as described in any one of claim 1 ~ 9, it is characterized in that, concrete steps are as follows: by ratio of weight and the number of copies, Folium Artemisiae Argyi extractive liquid, fringed iris rhizome extract, China tree extract, WUDUOYUN extract, Bright Yellow extract and sweet wormwood extract are mixed, then light-coloured vinegar and capsicum water is added, mixing, obtains vegetables insecticide.
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| CN108308208A (en) * | 2018-04-09 | 2018-07-24 | 何新桥 | A kind of nontoxic insectifuge for crops and preparation method thereof and use |
| CN109258714A (en) * | 2018-10-30 | 2019-01-25 | 大新县科学技术情报研究所 | A kind of biological insecticides and preparation method thereof for preventing and treating vegetable aphid |
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