CN105994450A - Chinese herbal medicine insecticide of tea and preparation method thereof - Google Patents
Chinese herbal medicine insecticide of tea and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/02—Sulfur; Selenium; Tellurium; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention provides a Chinese herbal medicine insecticide of tea and a preparation method thereof, belonging to the technical field of Chinese herbal medicine pesticides. The Chinese herbal medicine insecticide is prepared from the following raw materials: 5-15 parts of trifoliate jewelvine root or stem, 2-10 parts of sweet wormwood herb, 1-7 parts of lime, 1-5 parts of sulfur, 1-25 parts of plant vines, 3-12 parts of pepper leaf, 2-9 parts of leaf of common ginger, 2-8 parts of star anise, 1-6 parts of konjaku, 1-3 parts of leaf of sweet orange, 1-6 parts of camphor, 3-20 parts of wild chrysanthemum and 2-10 parts of pig's bile. The preparation method comprises the steps of raw material treatment, extraction, spray drying, drying and packaging. The Chinese herbal medicine insecticide has the beneficial effects that the Chinese herbal medicine insecticide not only has high killing rate but also takes effect quickly; the raw materials can also serve as leaf fertilizers to provide nutritive elements for plants after giving play to the effects, thus reducing the production input and increasing the utilization rates of agricultural byproducts.
Description
Technical field
The invention belongs to pesticide made of Chinese medicinal herbs technical field, particularly to Chinese herbal medicine pesticide of the insect pest of sucking property and acarid and preparation method thereof in a kind of Folium Camelliae sinensis.
Background technology
The step such as Tea planting method includes wholely, fertilising, field management, beta pruning, pest and disease damage are prevented and kill off, wherein pest and disease damage is prevented and kill off is the committed step in planting process, harm Pests of Tea-Plants reaches kind more than 40 at present, wherein in false eye leafhopper, Aleurocanthus spiniferus, tea aphid, pink tea rust mite etc., sucking property insect causes disaster generation, has a strong impact on the good quality and high output of Folium Camelliae sinensis.This class pest occurs hidden, and polypide is little, generation overlap, and reproduction speed is fast, either adult and nymph all can draw Camellia sinensis juice, hinder the normal conveying of Camellia sinensis nutrient substance, and Camellia sinensis of being injured photosynthetic efficiency reduces, and bud density declines, educating bud ability, rudiment is slow, and tea growth stops.Aleurocanthus spiniferus and aphid also drain honeydew, cause mycete generation, induce mildew, cause small worm to become terrible disaster, have a strong impact on the yield and quality of Folium Camelliae sinensis.
Tea growers for convenience and fast, mostly use insecticide, and insecticide is mainly used for preventing a class pesticide of agricultural pests.At present, wide in variety, the yield of product occupies insecticide first and a most widely used insecticides is organophosphorus insecticides, this insecticides is typically to make with chemical synthesis process, although it has the quick advantage of parasite killing, but persticide residue is big, it is eaten for a long time and used the food of this insecticides human body can be made to produce the problems such as chronic toxicity, especially Delayed onset neurotoxic, the living environment of the mankind is constituted a threat to；It addition, the extensively application of chemicals compromises the ecological agriculture, soil and water resource are caused serious pollution, the theory of the green of serious non-compliance Modern times call, environmental protection, health and sustainable development.
Chinese herbal medicine pesticide forms with pure combined Chinese herb, uses rear insecticidal effect notable, nontoxic to plant and people and animals and have no side effect, and is the insecticide of a kind of green, environmental protection, and therefore, Chinese herbal medicine pesticide is increasingly praised highly by people.
Summary of the invention
It is an object of the invention to, for solving the abuse of chemical pesticide during Tea planting, cause soil and the problem of water resource severe contamination, it is provided that Chinese herbal medicine pesticide of a kind of Folium Camelliae sinensis and preparation method thereof.The technical scheme used by realizing the object of the invention is:
The Chinese herbal medicine pesticide of a kind of Folium Camelliae sinensis, including the raw material of following parts by weight: Radix seu Caulis Derridis Trifoliatae 5-15 part, Herba Artemisiae Annuae 2-10 part, Calx 1-7 part, sulfur 1-5 part, plant tendril 1-25 part, Folium Capsici 3-12 part, Folium Zingiberis 2-9 part, anistree 2-8 part, Rhizoma amorphophalli 1-6 part, Folium citri sinensis 1-3 part, Camphora 1-6 part, Flos Chrysanthemi Indici 3-20 part and Fel Sus domestica 2-10 part.
Preferably, described Chinese herbal medicine pesticide also includes parthenocissus 1-7 part.
Preferably, described plant tendril includes one or more of Caulis Cucurbitae, Caulis Cucumidis sativiv and Caulis Momordicae Charantiae.
Preferably, described plant tendril includes following parts by weight raw material: Caulis Cucurbitae 1-8 part, Caulis Cucumidis sativiv 1-7 part and Caulis Momordicae Charantiae 1-10 part.
Preferably, described Radix seu Caulis Derridis Trifoliatae 5-8 part, Herba Artemisiae Annuae 2-6 part, Calx 1-3 part, sulfur 1-2 part, Caulis Cucurbitae 3-8 part, Caulis Cucumidis sativiv 1-5 part and Caulis Momordicae Charantiae 1-4 part, Folium Capsici 3-8 part, Folium Zingiberis 2-7 part, anistree 2-6 part, Rhizoma amorphophalli 1-3 part, Folium citri sinensis 1-2 part, Camphora 1-3 part, Flos Chrysanthemi Indici 3-8 part and Fel Sus domestica 2-4 part.
Preferably, described Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, plant tendril, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora and Flos Chrysanthemi Indici is the raw material being dried after drying.
Preferably, described raw material need to be through broken, and being crushed to particle diameter is 1-35mm.
The preparation method of the Chinese herbal medicine pesticide of a kind of Folium Camelliae sinensis, including Feedstock treating, extracts, is spray-dried, is dried and packs, and concrete preparation process is as follows:
1) Feedstock treating: Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, Calx, sulfur, plant tendril, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora and Flos Chrysanthemi Indici are crushed to particle diameter is 1-35mm, obtains mixture of Chinese herbal medicines；
2) extracting: mixture of Chinese herbal medicines and Fel Sus domestica being mixed, boiling material, the amount added water is 3-10 times of Traditional Chinese drug mixture and Fel Sus domestica, decocts to ripe rotten, and decocting time is 2-7 hour, decoct after terminating, filter, filtrate concentrates, and obtains concentrated filtrate, standby；
3) being spray-dried: sent into by concentrated filtrate in spray dryer, preparation forms extract powder；
4) being dried: being dried by extract powder, temperature is 60-80 DEG C, water content control, below 5%, obtains solid particle, sieves, obtain uniform solid particle after solid particle cooling；
5) packaging: the uniform solid particle of above-mentioned acquisition is loaded air-locked aluminium foil bag, seals and preserves, i.e. finished product.
Preferably, the amount that described extraction adds water is 3-5 times of raw material, and decocting time is 3-6 hour.
The using method of the Chinese herbal medicine pesticide of described Folium Camelliae sinensis is to be diluted by product around the 300-500 times of stem and leaf being sprayed on Camellia sinensis and root, prevents and treats the insects such as false eye leafhopper, Aleurocanthus spiniferus, tea aphid, pink tea rust mite.
The present invention selects the performance of raw material and effect thereof to be summarized as follows:
Radix seu Caulis Derridis Trifoliatae, its root is containing insecticide active substance rotenone and the like, and rotenone and the like can make crops pesticide, may further be used to kill mosquito class larva, and rotenone is spectrum insecticide, can prevent and treat 800 various pests, is one of three great tradition pesticide plants.
Herba Artemisiae Annuae includes chemical composition sesquiterpenoids lactone: arteannuin series compound, such as arteannuin, Herba Artemisiae Annuae first, second, artemisilactone and flavonoid: Rhizoma Kaempferiae flavin (nimbecetin), Quercetin.Having the effect killing spray testis trematodiasis, also have raising lymhocyte transformation rate, the effect of enhancing human body immunity power, the material that Herba Artemisiae Annuae decocting extracts has antibacterial action to various bacteria.
Calx main component is calcium carbonate, and common field trash is silicic acid, ferrum, aluminum, magnesium etc..Calx acrid in the mouth, temperature, poisonous, there is dampness, parasite killing, hemostasis, analgesic therapy, erosion evil meat, control scabies, eczema, wound hemorrhage, the burning hot wound of soup, hemorrhoid, proctoptosis, wart etc. acts on.
Sulfur is yellow solid or powder, has obvious abnormal smells from the patient, can volatilize.Sulfur aqueous suspensions is subacidity, water insoluble, generates polysulfide with alkali reaction.Send cyan flame during sulfur burning, produce sulfur dioxide gas with burning.Often sulfur being processed into colloidal suspending agent for prevention and elimination of disease and pests in production, it is to people, animal safety, is difficult to make crop produce poisoning.Sulfur belongs to multipurpose agent, in addition to having bactericidal action, moreover it is possible to mite killing and parasite killing.For preventing and treating powdery mildew and the leaf Scarabaeiform etc. of various crop, the lasting period up to first quarter moon about.Sulfur belongs to multipurpose agent, in addition to having bactericidal action, moreover it is possible to mite killing and parasite killing.For preventing and treating powdery mildew and the leaf Scarabaeiform etc. of various crop, the lasting period up to first quarter moon about.
Caulis Cucurbitae is annual draft of overgrowing；Taking root in stem often joint portion, elongation reaches 2-5 rice, close by white short bristle.Caulis Cucurbitae has effect of removing damp-heat, anthelmintic, has the effect controlling and killing to schistosomicide, and Pedicellus Melo has antiabortive effect, radical cure toothache.
Caulis Cucumidis sativiv is annual overgrowing or climbing herb, and general rattan is short and does not has side shoot or little side shoot.Caulis Cucumidis sativiv is medicinal, can antiinflammatory, eliminate the phlegm, antispasmodic effect.
Caulis Momordicae Charantiae is annual draft of climbing up by holding on to, and multi-branched has fine and soft hair, tendril not branch.Ye great, the kidney shape is circular, length and width the most about 5-12cm, usual 5-7 drastic crack, and sliver ovum shape is oval, and base portion shrinks, edge tool wave-formed mouth, and two sides is bordering on smooth or hairiness, and primary efficacy heat-clearing and toxic substances removing, for tackling the insect of hotness class.
Folium Capsici is the leaf of solanaceae plant pepper, is the plant of a kind of medicine-food two-purpose.Folium Capsici, as medicine, has detumescence and washs network, effect of killing parasites for relieving itching.Folium Capsici contains abundant calcareous, carotene, multivitamin and other nutrient substance, analyzes according to nutrition man, containing calcium substance in Folium Capsici.This is that a kind of natural plant is replenished the calcium, and is particularly effective for the insect fearing high calcium class.
Folium Zingiberis is the leaf of zingiber, has and controls blood stasis of injuring, warming the lung, heart disease, the liver benefiting, spleen invigorating, stomach function regulating, strong muscle, beauty care, logical blood, effect of regulating menstruation.
Rhizoma amorphophalli is cold in nature, pungent, poisonous；Can blood circulation promoting and blood stasis dispelling, removing toxic substances and promoting subsidence of swelling, wide intestinal relieving constipation, resolving phlegm and softening hard masses；Cure mainly the diseases such as blood pressure lowering, blood sugar lowering, scrofula sucutaneous nodule, damage congestive edema, constipation stomachache, laryngopharynx swelling and pain, gingival swelling and pain.It addition, Rhizoma amorphophalli also has and replenishes the calcium, balances the effect such as salinity, clean stomach, whole intestinal, toxin expelling.Rhizoma amorphophalli can form antibacterial film possibly together with a kind of natural antibiotics, Rhizoma amorphophalli, can prevent and treat bacteria attack on insecticide surface.
Folium citri sinensis is the leaf of rutaceae Fructus Citri sinensis, eliminating stasis to stop pain, and main skin infection swells and ache.Folium citri sinensis contains volatile oil 0.2～0.3%, therein is mainly composed of linalool, citral and limonene etc..
Camphora has orifice opening, qi stagnation removing, wards off foul, effect of killing parasites for relieving itching, reducing swelling and alleviating pain, cures mainly the symptoms such as scabies pruritus, traumatic pain, toothache.
Anistree dry mature fruit contains containing aromatic oil, fatty oil, protein, resin etc., and extract is Oleum Anisi Stellati, and wherein containing anise-oil 1.7%-2.7% in seed, the star anise oil content of dry fruit and cured leaf is respectively 12%-13%, 1.6%-1.8%.Oleum Anisi Stellati be mainly composed of methoxybenzene (Anethole), anisaldehyde (Anisaldehyde) and fenchone (Anisylacetone), safrole (Safrole), phellandrene etc..
The root of parthenocissus, stem can be used as medicine, and have removing blood stasis, muscle hemostasis of living, effect of detumescence poison.The poisonous plants that this species Chinese Plants spectrum data storehouse is included, its toxicity is that herb is poisonous.There is dispelling wind and removing obstruction in the collateral, the effect of promoting blood circulation and detoxication.
The leaf of Herba Dendranthematis indici, flower and all herbal medicine.Bitter in the mouth, pungent, cool, heat-clearing and toxic substances removing, wind-dispelling heat-dissipating, dissipating blood stasis, improving eyesight, blood pressure lowering.Prevent and treat epidemic cerebrospinal meningitis, prevent influenza, flu, treatment hypertension, hepatitis, dysentery, carbuncle furuncle treatment skin ulcer to have positive effect.The immersion of Flos Chrysanthemi Indici is to killing wriggler and fly larvae is the most highly effective.
Fel Sus domestica is mainly composed of bile acids, bile pigments, mucin, lipid and inorganic matter etc..It mainly tackles the insect being suitable for growing in the basic conditions in Camellia sinensis.
The invention have the benefit that
1, the raw material of the insecticide of the present invention is the Nature material, and composition is nontoxic, and noresidue is nuisanceless, and insecticide production method of the present invention is simple, it is easy to operation, production cost is low, easy to use.
2, the insecticide of the present invention is to can effectively prevent and treat the insects such as false eye leafhopper, Aleurocanthus spiniferus, tea aphid, pink tea rust mite, and one time killing rate reaches more than 95%；And also to Euproctis pseudoconspersa, tea geometrid, killing rate reach more than 70%；Killing rate of cutworm is reached more than 60%, and this insecticide is not easy drug resistance, can persistently use.
3, Chinese herbal medicine pesticide of the present invention not only killing rate is high, and the raw material after drug effect volatilization is alternatively arranged as foliage fertilizer provides nutrient for plant, and its content of organic matter is more than 2 times of fertilizer, improves the photosynthesis of Camellia sinensis, and is obviously improved Folium Camelliae sinensis mouthfeel.This insecticide, possibly together with substantial amounts of C4 material, uses rear insecticidal effect notable, and effect of increasing production is obvious.Therefore Chinese herbal medicine pesticide not only killing rate of the present invention is high, and decrease Productive statistics, improve the utilization rate of agricultural by product.
Detailed description of the invention
Being described in further detail the present invention program below in conjunction with embodiment, its content, merely to explain the present invention, is not defined by the description below.
Embodiment 1
Raw material: Radix seu Caulis Derridis Trifoliatae 5kg, Herba Artemisiae Annuae 2kg, Calx 1kg, sulfur 1 kg, Caulis Cucurbitae 1 kg, Folium Capsici 3 kg, Folium Zingiberis 2 kg, anistree 2 kg, Rhizoma amorphophalli 1 kg, Folium citri sinensis 1 kg, Camphora 1 kg, Flos Chrysanthemi Indici 3 kg and Fel Sus domestica 2 kg, preparation method is as follows:
1) Feedstock treating: dry Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, Calx, sulfur, Caulis Cucurbitae, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora and Flos Chrysanthemi Indici are crushed to particle diameter is 5mm, obtains mixture of Chinese herbal medicines；
2) extracting: mixture of Chinese herbal medicines and Fel Sus domestica being mixed, boiling material, the amount added water is 125kg, decocts to ripe rotten, and it's 6 hours pasts decocting time, decoct after terminating, filter, filtrate concentrates, and obtains concentrated filtrate, standby；
3) being spray-dried: sent into by concentrated filtrate in spray dryer, preparation forms extract powder；
4) being dried: being dried by extract powder, temperature is 60 DEG C, water content control, below 5%, obtains solid particle, sieves, obtain uniform solid particle after solid particle cooling；
5) packaging: the uniform solid particle of above-mentioned acquisition is loaded air-locked aluminium foil bag, seals and preserves, i.e. finished product.
Embodiment 2
Raw material: Radix seu Caulis Derridis Trifoliatae 15kg, Herba Artemisiae Annuae 10kg, Calx 7kg, sulfur 5 kg, Caulis Cucurbitae 8 kg, Caulis Cucumidis sativiv 7kg, Caulis Momordicae Charantiae 10kg, Folium Capsici 12 kg, Folium Zingiberis 9 kg, anistree 8 kg, Rhizoma amorphophalli 6 kg, Folium citri sinensis 3 kg, Camphora 6 kg, Flos Chrysanthemi Indici 20 kg and Fel Sus domestica 10 kg, preparation method is as follows:
1) Feedstock treating: dry Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, Calx, sulfur, Caulis Cucurbitae, Caulis Cucumidis sativiv, Caulis Momordicae Charantiae, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora and Flos Chrysanthemi Indici are crushed to particle diameter is 35mm, obtains mixture of Chinese herbal medicines；
2) extracting: mixture of Chinese herbal medicines and Fel Sus domestica being mixed, boiling material, the amount added water is 408kg, decocts to ripe rotten, and it's 3 hours pasts decocting time, decoct after terminating, filter, filtrate concentrates, and obtains concentrated filtrate, standby；
3) being spray-dried: sent into by concentrated filtrate in spray dryer, preparation forms extract powder；
4) being dried: being dried by extract powder, temperature is 80 DEG C, water content control, below 5%, obtains solid particle, sieves, obtain uniform solid particle after solid particle cooling；
5) packaging: the uniform solid particle of above-mentioned acquisition is loaded air-locked aluminium foil bag, seals and preserves, i.e. finished product.
Embodiment 3
Raw material: Radix seu Caulis Derridis Trifoliatae 5kg, Herba Artemisiae Annuae 2kg, Calx 3kg, sulfur 2kg, Caulis Cucurbitae 3 kg, Caulis Cucumidis sativiv 1kg, Caulis Momordicae Charantiae 4kg, Folium Capsici 5 kg, Folium Zingiberis 2 kg, anistree 4kg, Rhizoma amorphophalli 1 kg, Folium citri sinensis 2 kg, Camphora 3 kg, Flos Chrysanthemi Indici 5 kg, parthenocissus 1kg and Fel Sus domestica 2 kg, preparation method is as follows:
1) Feedstock treating: dry Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, Calx, sulfur, Caulis Cucurbitae, Caulis Cucumidis sativiv, Caulis Momordicae Charantiae, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora, Flos Chrysanthemi Indici and parthenocissus are crushed to particle diameter is 10mm, obtains mixture of Chinese herbal medicines；
2) extracting: mixture of Chinese herbal medicines and Fel Sus domestica being mixed, boiling material, the amount added water is 270kg, decocts to ripe rotten, and it's 5 hours pasts decocting time, decoct after terminating, filter, filtrate concentrates, and obtains concentrated filtrate, standby；
3) being spray-dried: sent into by concentrated filtrate in spray dryer, preparation forms extract powder；
4) being dried: being dried by extract powder, temperature is 70 DEG C, water content control, below 5%, obtains solid particle, sieves, obtain uniform solid particle after solid particle cooling；
5) packaging: the uniform solid particle of above-mentioned acquisition is loaded air-locked aluminium foil bag, seals and preserves, i.e. finished product.
Embodiment 4
Raw material: Radix seu Caulis Derridis Trifoliatae 8kg, Herba Artemisiae Annuae 6kg, Calx 2kg, sulfur 1 kg, Caulis Cucurbitae 8 kg, Caulis Cucumidis sativiv 5kg, Caulis Momordicae Charantiae 2kg, Folium Capsici 5 kg, Folium Zingiberis 6 kg, anistree 4kg, Rhizoma amorphophalli 2 kg, Folium citri sinensis 2 kg, Camphora 1 kg, Flos Chrysanthemi Indici 5 kg, parthenocissus 7kg and Fel Sus domestica 4 kg, preparation method is as follows:
1) Feedstock treating: dry Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, Calx, sulfur, Caulis Cucurbitae, Caulis Cucumidis sativiv, Caulis Momordicae Charantiae, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora, Flos Chrysanthemi Indici and parthenocissus are crushed to particle diameter is 1mm, obtains mixture of Chinese herbal medicines；
2) extracting: mixture of Chinese herbal medicines and Fel Sus domestica being mixed, boiling material, the amount added water is 272kg, decocts to ripe rotten, and it's 4 hours pasts decocting time, decoct after terminating, filter, filtrate concentrates, and obtains concentrated filtrate, standby；
3) being spray-dried: sent into by concentrated filtrate in spray dryer, preparation forms extract powder；
4) being dried: being dried by extract powder, temperature is 65 DEG C, water content control, below 5%, obtains solid particle, sieves, obtain uniform solid particle after solid particle cooling；
5) packaging: the uniform solid particle of above-mentioned acquisition is loaded air-locked aluminium foil bag, seals and preserves, i.e. finished product.
Embodiment 5
Raw material: Radix seu Caulis Derridis Trifoliatae 10kg, Herba Artemisiae Annuae 3kg, Calx 3kg, sulfur 2 kg, Caulis Cucumidis sativiv 1 kg, Folium Capsici 5 kg, Folium Zingiberis 3 kg, anistree 5 kg, Rhizoma amorphophalli 2 kg, Folium citri sinensis 2kg, Camphora 1 kg, Flos Chrysanthemi Indici 8 kg and Fel Sus domestica 2 kg, preparation method is as follows:
1) Feedstock treating: dry Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, Calx, sulfur, Caulis Cucumidis sativiv, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora and Flos Chrysanthemi Indici are crushed to particle diameter is 25mm, obtains mixture of Chinese herbal medicines；
2) extracting: mixture of Chinese herbal medicines and Fel Sus domestica being mixed, boiling material, the amount added water is 235kg, decocts to ripe rotten, and it's 5 hours pasts decocting time, decoct after terminating, filter, filtrate concentrates, and obtains concentrated filtrate, standby；
3) being spray-dried: sent into by concentrated filtrate in spray dryer, preparation forms extract powder；
4) being dried: being dried by extract powder, temperature is 75 DEG C, water content control, below 5%, obtains solid particle, sieves, obtain uniform solid particle after solid particle cooling；
5) packaging: the uniform solid particle of above-mentioned acquisition is loaded air-locked aluminium foil bag, seals and preserves, i.e. finished product.
Embodiment 6
Raw material: Radix seu Caulis Derridis Trifoliatae 5kg, Herba Artemisiae Annuae 6kg, Calx 1kg, sulfur 1 kg, Caulis Momordicae Charantiae 4 kg, Folium Capsici 3 kg, Folium Zingiberis 2 kg, anistree 2 kg, Rhizoma amorphophalli 1 kg, Folium citri sinensis 2kg, Camphora 1 kg, Flos Chrysanthemi Indici 3 kg, parthenocissus 5kg and Fel Sus domestica 3 kg, preparation method is as follows:
1) Feedstock treating: dry Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, Calx, sulfur, Caulis Momordicae Charantiae, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora, Flos Chrysanthemi Indici and parthenocissus are crushed to particle diameter is 20mm, obtains mixture of Chinese herbal medicines；
2) extracting: mixture of Chinese herbal medicines and Fel Sus domestica being mixed, boiling material, the amount added water is 156kg, decocts to ripe rotten, and it's 7 hours pasts decocting time, decoct after terminating, filter, filtrate concentrates, and obtains concentrated filtrate, standby；
3) being spray-dried: sent into by concentrated filtrate in spray dryer, preparation forms extract powder；
4) being dried: being dried by extract powder, temperature is 70 DEG C, water content control, below 5%, obtains solid particle, sieves, obtain uniform solid particle after solid particle cooling；
5) packaging: the uniform solid particle of above-mentioned acquisition is loaded air-locked aluminium foil bag, seals and preserves, i.e. finished product.
The above, the only detailed description of the invention of the present invention, but protection scope of the present invention is not limited thereto, any change expected without creative work or replacement, all should contain within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain that claims are limited.
Claims (9)
1. the Chinese herbal medicine pesticide of a Folium Camelliae sinensis, it is characterized in that, including the raw material of following parts by weight: Radix seu Caulis Derridis Trifoliatae 5-15 part, Herba Artemisiae Annuae 2-10 part, Calx 1-7 part, sulfur 1-5 part, plant tendril 1-25 part, Folium Capsici 3-12 part, Folium Zingiberis 2-9 part, anistree 2-8 part, Rhizoma amorphophalli 1-6 part, Folium citri sinensis 1-3 part, Camphora 1-6 part, Flos Chrysanthemi Indici 3-20 part and Fel Sus domestica 2-10 part.
The Chinese herbal medicine pesticide of Folium Camelliae sinensis the most according to claim 1, it is characterised in that described Chinese herbal medicine pesticide also includes parthenocissus 1-7 part.
The Chinese herbal medicine pesticide of Folium Camelliae sinensis the most according to claim 1 or claim 2, it is characterised in that described plant tendril includes one or more of Caulis Cucurbitae, Caulis Cucumidis sativiv and Caulis Momordicae Charantiae.
The Chinese herbal medicine pesticide of Folium Camelliae sinensis the most according to claim 3, it is characterised in that described plant tendril includes following parts by weight raw material: Caulis Cucurbitae 1-8 part, Caulis Cucumidis sativiv 1-7 part and Caulis Momordicae Charantiae 1-10 part.
The Chinese herbal medicine pesticide of Folium Camelliae sinensis the most according to claim 4, it is characterized in that, described Radix seu Caulis Derridis Trifoliatae 5-8 part, Herba Artemisiae Annuae 2-6 part, Calx 1-3 part, sulfur 1-2 part, Caulis Cucurbitae 3-8 part, Caulis Cucumidis sativiv 1-5 part and Caulis Momordicae Charantiae 1-4 part, Folium Capsici 3-8 part, Folium Zingiberis 2-7 part, anistree 2-6 part, Rhizoma amorphophalli 1-3 part, Folium citri sinensis 1-2 part, Camphora 1-3 part, Flos Chrysanthemi Indici 3-8 part and Fel Sus domestica 2-4 part.
6. according to the Chinese herbal medicine pesticide of Folium Camelliae sinensis according to any one of claim 1-5, it is characterised in that described Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, plant tendril, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora and Flos Chrysanthemi Indici is the raw material being dried after drying.
The Chinese herbal medicine pesticide of Folium Camelliae sinensis the most according to claim 6, it is characterised in that described raw material need to be through broken, and being crushed to particle diameter is 1-35mm.
The most according to claim 1, the preparation method of the Chinese herbal medicine pesticide of Folium Camelliae sinensis, including Feedstock treating, extract, be spray-dried, be dried and pack, it is characterised in that concrete preparation process is as follows:
1) Feedstock treating: Radix seu Caulis Derridis Trifoliatae, Herba Artemisiae Annuae, Calx, sulfur, plant tendril, Folium Capsici, Folium Zingiberis, anise, Rhizoma amorphophalli, Folium citri sinensis, Camphora and Flos Chrysanthemi Indici are crushed to particle diameter is 1-35mm, obtains mixture of Chinese herbal medicines；
2) extracting: mixture of Chinese herbal medicines and Fel Sus domestica being mixed, boiling material, the amount added water is 3-6 times of Traditional Chinese drug mixture and Fel Sus domestica, decocts to ripe rotten, and decocting time is 3-7 hour, decoct after terminating, filter, filtrate concentrates, and obtains concentrated filtrate, standby；
3) being spray-dried: sent into by concentrated filtrate in spray dryer, preparation forms extract powder；
4) being dried: being dried by extract powder, temperature is 60-80 DEG C, water content control, below 5%, obtains solid particle, sieves, obtain uniform solid particle after solid particle cooling；
5) packaging: uniform for above-mentioned acquisition solid particle is loaded air-locked aluminium foil bag, seals and preserves, i.e. finished product.
The most according to claim 8, the preparation method of the Chinese herbal medicine pesticide of Folium Camelliae sinensis, it is characterised in that the amount that described extraction adds water is 3-5 times of raw material, decocting time is 4-6 hour.
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