CN105379779B - Agriculturally useful compositions and application containing streptomycin sulphate and botanical components - Google Patents

Agriculturally useful compositions and application containing streptomycin sulphate and botanical components Download PDF

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CN105379779B
CN105379779B CN201510652057.4A CN201510652057A CN105379779B CN 105379779 B CN105379779 B CN 105379779B CN 201510652057 A CN201510652057 A CN 201510652057A CN 105379779 B CN105379779 B CN 105379779B
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botanical components
streptomycin sulphate
composition
useful compositions
agriculturally useful
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CN105379779A (en
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侯华民
张善学
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Hainan Zhengye Biotechnology Co ltd
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Hainan Zhengye Zhongnong Hi Tech Co Ltd
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/54—1,3-Diazines; Hydrogenated 1,3-diazines
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The invention belongs to plant protection art; it is related to the agriculturally useful compositions of streptomycin sulphate and botanical components, botanical components are the one or more in the crushed material or crude extract or active component of trifoliate jewelvine, tripterygium wilfordii, tobacco, Dalmatian chrysanthemum, marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng etc..The present composition shows good synergistic effect in certain ratio range, has excellent prevention effect to diseases and pests of agronomic crop.

Description

Agriculturally useful compositions and application containing streptomycin sulphate and botanical components
The application is the division of " agriculturally useful compositions and application containing antibiotic and botanical components " application for a patent for invention Application, original application day：On July 26th, 2013, application number：2013103211300
Technical field
The invention belongs to plant protection art, more particularly to the agriculturally useful compositions containing antibiotic and botanical components with Using the present composition can effectively prevent and treat diseases and pests of agronomic crop.
Background technology
In recent years, due to single and not Scientific Usage of Drugs, pest and disease damage has produced the different degrees of resistance to the action of a drug, and agriculture and forestry produce Still using chemical pesticide as main preventing and treating kind, environmental pollution and the serious of ecological environment is caused to destroy increasingly.As people live Horizontal raising and the enhancing of health perception, development and the exploitation of biological pesticide are progressively paid close attention to by agricultural chemical R＆D, It is the effective way for improving environment, reduction or delaying drug resistance and improving drug effect as the focus of agriculture and forestry sustainable development.Its In, farm antibiotics and botanical components turn into one of focus of biological pesticide research.
Farm antibiotics, refer to be produced by microbial fermentation, there is agricultural chemicals function, for agriculturally preventing and treating pest organism mouse etc. The secondary metabolite of harmful organism.The microorganisms such as actinomyces, fungi, bacterium can produce farm antibiotics, wherein actinomyces Caused farm antibiotics is most.The many important farm antibiotics being widely used at present all are isolated from streptomyces Actinomyces caused by.Earliest farm antibiotics is streptomysin, and has thus promoted antibiotic in application agriculturally, 20 Rapid development has been obtained after century 70.At present, farm antibiotics is almost throughout insecticide, bactericide, herbicide, plant The agricultural chemicals all spectra such as thing growth regulator.Such as the AVM of Insecticiding-miticiding effect, ivermectin, milbemectin, more sterilizations Element, macro tetrolide, nikkomycin etc., prevent and treat the polyoxin of fungal disease, kasugarnycin, jinggangmeisu, Ningnanmycin, go out powder Mycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin etc., streptomycin sulphate, the soil for preventing and treating bacteriosis are mould Element etc., there are the bialaphos of herbicidal effect, the gibberellin etc. with coordinate plant growth.
Having agricultural mainly has Meliaceae, composite family, pulse family, Rutaceae, aster section, lip using the plant of future and Development volue The certain plants of section, Annonaceae, Ranunculaceae, Euphorbiaceae, Araeceae, Myrsinacea, Papilionaceae etc., studying more has Trifoliate jewelvine, tripterygium wilfordii, tobacco, Dalmatian chrysanthemum, marigold, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, horse Mulberry, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, Argy wormwood, Chinese prickly ash, Cynanchum Komarovii, gleditsia sinensis, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, asarum, India red sandalwood, erythrina indica, plant Iron son or frutus cnidii etc..
Botanical components with desinsection, sterilization, fertilizer, fresh-keeping etc., including can directly using the root of plant, stem, leaf, The crushed materials such as flower, fruit, seed or crude extract or the active component for extracting plant.Plant source active component is divided into by chemical constitution Alkaloids, terpenes, flavonoids, essential oil class, light-activated toxin class and other class active components.
Containing alkaloid, there are Cephalotaxaceae, Ranunculaceae, Berberidaceae, Papaveraceae, pulse family, Loganiaceae, Apocynaceae, eggplant in more section Section, composite family, Liliaceae, Amaryllidaceae, Loganiaceae, Rutaceae, Lauraceae etc..
Terpenes active component, mainly there are monoterpenes, sesquiterpenoids, Diterpenes and triterpene compound.Monoterpene is most normal The terpene seen, it is the key component of plant volatile oil, content is of a relatively high in cupressaceae plant, and sesquiterpenoids is in Coriariaceae More in plant, Celastraceae plant Celastrus angulatus etc., diterpene-kind compound is more in Euphorbiaceae, Isolated From Thymelaeaceae Species, triterpenes The important representative of compound has insect anti-feedant nimbin.
Flavonoids is also referred to as flavone class, and most of form for being combined into glycoside or carbon glycosyl with sugar is present in plant, Also have existing in a free form.It is mainly distributed in the plants such as pulse family, Papilionaceae, Rutaceae, Umbelliferae, Labiatae.From The rotenone extracted in Derris and bastard indigo platymiscium, have to insect it is powerful tag and stomach poison function, insecticidal spectrum is wide, and evil Worm is not likely to produce the resistance to the action of a drug.The pterocarpoid chromocor compound extracted from Pterocarpus, Erythrina, reticulate millettia platymiscium has very Strong antimycotic and bacterial activity effect, can be as important plant defense element.
Plants essential oil is normally present in the oil droplet of plant or the resin of plant cavity tissue.Most of essential oil components are complicated, Chemical constituent is basically divided into four classes, and one kind is terpene compound, is the key component of essential oil, be divided into monoterpene derivative, times Half triterpene derivative, forskolin.Second class is aromatic compound, and terpene compound is only second in essential oil.3rd class It is aliphatic compound.4th class is sulfur-bearing nitrogen-containing compound.Essential oil is volatile at normal temperatures, there is strong peat-reek, It is oily liquids under normal temperature, dissolves in a variety of organic solvents such as methanol, ethanol.
Plant light-activated toxin is mainly that some derive from the natural products for having Rutaceae composite family, samphire, in nothing It is not high to pest activity in the case of light, then there is very strong activity under light illumination.Plant light-activated toxin main Types have polyyne Class, thiophene phenols and quinones etc., its mechanism of action is very unique, different from traditional any kind insecticide, therefore will not produce The problem of cross tolerance.
Research report on antibiotic agents and the agriculturally useful compositions of botanical components is less.
The content of the invention
The purpose of the present invention is to improve environment, expand action spectrum, reduction or delaying drug resistance, improve drug effect, there is provided Yi Zhongkang The agriculturally useful compositions of raw plain class and botanical components.
The present invention is achieved through the following technical solutions：
Contain antibioticses and botanical components agriculturally useful compositions, it is characterised in that said composition include effective dose A and It is mould that B, A are selected from AVM, ivermectin, milbemectin, pleocidin, nikkomycin, macro tetrolide, polyoxin, spring thunder Element, jinggangmeisu, Ningnanmycin, mildiomycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin, double third ammonia One or more in phosphine, gibberellin, streptomycin sulphate, terramycin, B are selected from trifoliate jewelvine, tripterygium wilfordii, tobacco, Dalmatian chrysanthemum, Wan Shou Chrysanthemum, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, yellow Du Cuckoo flower, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Gleditsia sinensis, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, asarum, India red sandalwood, erythrina indica, plant iron are young and frutus cnidii is a kind of or several The coarse powder of kind.Preferably, botanical components are selected from marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia.
In the present composition, A is selected from AVM, ivermectin, milbemectin, pleocidin, nikkomycin, Liuyang Mycin, polyoxin, kasugarnycin, jinggangmeisu, Ningnanmycin, mildiomycin, cycloheximide, blasticidin, valida, go out One or more in pest element, Qinlingmycin, bialaphos, gibberellin, streptomycin sulphate, terramycin, B are selected from trifoliate jewelvine, Thunder God Rattan, tobacco, Dalmatian chrysanthemum, marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, horse Mulberry, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, Argy wormwood, Chinese prickly ash, Cynanchum Komarovii, gleditsia sinensis, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, asarum, India red sandalwood, erythrina indica, plant Iron is young and one or more of crude extract in frutus cnidii or active component in alkaloids, terpenes, flavonoids, essential oil class, One or more in light-activated toxin class.
The agriculturally useful compositions containing antibioticses and botanical components of the present invention, it is characterised in that in botanical components Feverfew is selected from marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia.
The alkaloids in botanical components in the present composition, it is datura total alkali, Chelidonine, macleaya cordata total Alkali, camptothecine, aconitine, strychnia, total alkaloid of sophora alopecuroide, thunder godvine alkaloid, oxymatrine, nicotine, black false hellebore are total Alkali, capsaicine, matrine, sanguinarine, jamaicin, stemonine, papaverine, quinoline are peaceful, tomatin, lupinine, sparteine, Numb rope, donaxine, morphine, kind art soft-shelled turtle alkali, gelsemium henbane amine, mufangchine, magnoflorine, aconitine, eulexine, atropine, black nightshade One or more of components in one or more of alkaloids or above-mentioned total alkali in alkaloid, dandelion alkaloid etc..Preferably For datura total alkali, Chelidonine, the total alkaloids, camptothecine, aconitine, strychnia, Cynanchum Komarovii alkali, solanine or Pu One or more of components in one or more of alkaloids or biology total alkali in public English alkali.
The terpenes in botanical components in the present composition, in the Chinese azalea extract in Ericaceae, Labiatae Menthol, peppermint aldehyde, the monoterpene in cupressaceae plant, the coriamyrtin of Coriariaceae plant, the Celastrus angulatus, big of Celastraceae plant One or more in triterpene compound in diterpene-kind compound and Meliaceae in halberd section, Isolated From Thymelaeaceae Species etc..Preferably Terpenes are one kind or two kinds in Chinese azalea extract and coriamyrtin.
The flavonoids in botanical components in the present composition is chamaejasmine, rotenone, pterocarpoid, kuh-seng flavones With the one or more in plant iron son's flavones.Preferable flavonoids is chamaejasmine, one kind in pterocarpoid or two kinds.
Essential oil class in botanical components in the present composition, it is thyme, Chinese cassia tree, lemongrass, cloves, anistree fennel In perfume, orange peel, tree-of-heaven bark, chilli powder, Siberian cocklebur, lavender, the fruit of a cubeb litsea tree, garlic, peppermint, cypress, Chinese prickly ash, Artemisia scoparia etc. One or more in terpene compound, aromatic compound, aliphatic compound, sulfur-bearing nitrogen-containing compound.Preferable essence Oil is one kind or two kinds in thymol and cinnamic acid.
Plant photoactivation endotoxin in botanical components in the present composition be furocoumarin class, polyacetylene, One or more in thiophene phenols and quinones etc..
In the present composition, the quality parts ratio of antibioticses and botanical components is 50:1-1:200.Preferably, resist Raw plain class and the quality parts ratio of botanical components are 30:1-1:20.
The above-mentioned composition process preparation of the present invention is wettable powder, water dispersible granules, aqueous emulsion, microemulsion, suspension The percentage that agent, antibioticses and botanical components quality sum account for preparation gross mass is 0.05-80%.Preferably, antibiotic The percentage that class and botanical components quality sum account for preparation gross mass is 0.1-40%
The preparation of the above-mentioned composition processing of the present invention shows to prevent with base manure, spraying, pouring root, seed dressing, impregnating application Plant the purposes of crop disease and insect in Zhiduo County.
Present invention also offers the composition and antibiotic of antibiotic and several composite family components and several alkaloid compositions To citrus pest, the effect of cotton-plant pest-insects, the composition of antibiotic and several alkaloids is to tomato disease, the effect of rice disease Fruit, several compositions containing antibiotic and botanical components are to the effect of cotton nematode, antibiotic and terpenes component and antibiosis Element and the compositions of flavones are to cabbage pests, the effect of cotton-plant pest-insects, and the composition of antibiotic and plants essential oil is to water The effect of the sheath and culm blight of rice.
The composition of the present invention compared with prior art, produces following beneficial effect：
1st, purposes is widened：Composition can prevent and treat a variety of pest and disease damages of crops.
2nd, use cost is reduced：Preventive effect, preventing and treating spectrum increase are improved because composition has, reduces Pesticide use number, drops Low use cost.
3rd, the resistance to the action of a drug is delayed：Compounded containing antibiotic from the component that the composition of botanical components is different mechanism of action, disease Insect pest is not likely to produce the resistance to the action of a drug.
4th, it is environment-friendly：Low to people and animals and non-target organism toxicity, degraded is fast in the environment, and low-residual is free from environmental pollution.
Embodiment
Be only used for explaining the present invention described in example below, for made without departing from spirit of the invention and principle modification, Replace or improve, belong to the scope of protection of present invention.Antibiotic and botanical components in following examples come from business Industry channel is voluntarily prepared.
The preparation method of the plant source alkaloid of embodiment 1
Plant material trifoliate jewelvine, tripterygium wilfordii are taken respectively, tobacco, Dalmatian chrysanthemum, marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, win Return, be kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, thin Lotus, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, gleditsia sinensis, datura, ginkgo, camphor tree, chicken One or more of vegetable materials in blood rattan, elscholtiza, asarum, India red sandalwood, erythrina indica, plant iron son and frutus cnidii, clean, are dry Dry, crushing, add 43 DEG C of 95% ethanol to flow back 2 × 1h/ times, recovery ethanol to concentrate, be acidified with 0.4mol/L aqueous sulfuric acids, Oil-soluble impurities is removed with chloroform afterwards, obtained acid liquid is neutralized to pH8.5 with sodium carbonate and extracted again with chloroform, and recovery is organic molten Agent, obtain the biology total alkali of botanical components.
The preparation of the botanical components flavonoids of embodiment 2
Plant trifoliate jewelvine, tripterygium wilfordii, tobacco, Dalmatian chrysanthemum, marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, hardship are taken respectively Ginseng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, Chang Pu, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, gleditsia sinensis, datura, ginkgo, camphor tree, reticulate millettia, One or more of vegetable materials in elscholtiza, asarum, India red sandalwood, erythrina indica, plant iron son and frutus cnidii, clean, dry, powder It is broken, crushed material and solvent are fitted into extractor and mixed, ultrasonoscope is placed in, 75-85 DEG C of extraction at least 25min, is suspended Liquid, filters to get filtrate and filter residue for the first time；Filter residue and solvent are fitted into extractor and mixed, is placed in ultrasonoscope, 82-94 DEG C carries At least 40min is taken, obtains suspension, is filtered to get filtrate for the second time and filter residue；Above-mentioned secondary filtrate is mixed and steamed using decompression Evaporate, obtained concentrate is plant source Flavonoid substances.Above-mentioned solvent is using water, ethyl acetate, acetone, ethanol, methanol In one or more.
The preparation of embodiment 3 plant source terpenes, essential oil material
Plant trifoliate jewelvine, tripterygium wilfordii, tobacco, Dalmatian chrysanthemum, marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, hardship are taken respectively Ginseng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, Chang Pu, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, gleditsia sinensis, datura, ginkgo, camphor tree, reticulate millettia, One or more of vegetable materials in elscholtiza, asarum, India red sandalwood, erythrina indica, plant iron son and frutus cnidii, clean, dry, powder It is broken.Using this area conventional steam distillation, ethonal extraction method or acetone and water mixed solvent extraction method system Standby terpenes, essential oil class.Also the steam distillation that this area can be used conventional prepares essential oil.
The AVM marigold aqueous emulsion of embodiment 4 5%
With 5g dimethylformamides dissolving 0.5g AVMs, the concentrate 4.5g for take marigold to be extracted through ethanol, distilling, Fully dissolved with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds Enter and stir, 100g is complemented to water, both obtain 5% AVM marigold aqueous emulsion.
The ivermectin Eupatorium adenophorum aqueous emulsion of embodiment 5 5%
With 5g acetic acid 0.5g ivermectins, the concentrate 4.5g for take Eupatorium adenophorum to be extracted through ethanol, distilling, ethanol is used 10g fully dissolves, and mixes the first two dissolved matter, adds phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, and water is slowly added to and stirred Mix, 100g is complemented to water, both obtain 5% ivermectin Eupatorium adenophorum aqueous emulsion.
The milbemectin Dalmatian chrysanthemum aqueous emulsion of embodiment 6 5%
With 5g dimethylformamides dissolving 0.5g milbemectins, the concentrate 4.5g for take Dalmatian chrysanthemum to be extracted through ethanol, distilling, Fully dissolved with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slow Add and stir, 100g is complemented to water, both obtain 5% milbemectin Dalmatian chrysanthemum aqueous emulsion.
The pleocidin Artemisia scoparia aqueous emulsion of embodiment 7 5%
With 5g dimethylformamides dissolving 0.5g pleocidin, the concentrate 4.5g for take Artemisia scoparia to be extracted through ethanol, distilling, Fully dissolved with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds Enter and stir, 100g is complemented to water, both obtain 5% pleocidin Artemisia scoparia aqueous emulsion.
The nikkomycin Dalmatian chrysanthemum aqueous emulsion of embodiment 8 5%
With 5g dimethylformamides dissolving 0.5g nikkomycins, the concentrate 4.5g for take Dalmatian chrysanthemum to be extracted through ethanol, distilling, Fully dissolved with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slow Add and stir, 100g is complemented to water, both obtain 5% nikkomycin Dalmatian chrysanthemum aqueous emulsion.
The macro tetrolide fennel wormwood artemisia aqueous emulsion of embodiment 9 5%
0.5g macro tetrolides are dissolved with 5g dimethylformamides, the concentrate 4.5g for take fennel wormwood artemisia to be extracted through ethanol, distilling, are used Ethanol 10g is fully dissolved, and mixes the first two dissolved matter, adds phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, and water is slowly added to And stir, 100g is complemented to water, both obtains 5% macro tetrolide fennel wormwood artemisia aqueous emulsion.
The AVM datura total alkali water dispersible granules of embodiment 10 1%
By AVM 0.5g, datura total alkali 0.5g, naphthalenesulfonate formaldehyde condensation compound 4g, sodium alkyl benzene sulfonate 1.5g, Arabic gum 0.5g, white carbon supply 100g mix, will mixture carry out ultra-fine grinding after be granulated, dry, screening, both 1% Ah Tie up rhzomorph datura total alkali water dispersible granules.
The ivermectin Chelidonine water dispersible granules of embodiment 11 1%
By ivermectin 0.5g, Chelidonine 0.5g, naphthalenesulfonate formaldehyde condensation compound 10g, sodium alkyl benzene sulfonate 5g, hard charcoal It is black to supply 100g mixing, mixture be granulated after ultra-fine grinding, dried, screening, 1% ivermectin greater celandine had both been made Buck dispersible granule.
The milbemectin the total alkaloids microemulsion of embodiment 12 1%
Milbemectin 0.5g dimethylbenzene 5g are dissolved, the total alkaloids 0.5g is fully dissolved with chloroform 3g and methanol 5g, Phenethyl phenol polyethenoxy ether 5g and agriculture breast 500#5g is added, mixture is stirred in agitator, water complements to 100g, both 1% milbemectin the total alkaloids microemulsion.
The pleocidin camptothecine aqueous emulsion of embodiment 13 1%
Pleocidin 0.5g dimethylbenzene 5g are dissolved, camptothecine 0.5g is fully dissolved with ethyl acetate 3g and ethanol 10g, The first two dissolved matter is mixed, adds phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slowly added to and stirred, supplied with water To 100g, 1% pleocidin camptothecine aqueous emulsion is both obtained.
The nikkomycin aconitine wettable powder of embodiment 14 1%
Nikkomycin 0.5g, aconitine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each component Dry, cool down, be levigate, be both configured to 1% nikkomycin aconitine wettable powder.
The macro tetrolide strychnia wettable powder of embodiment 15 1%
Macro tetrolide 0.5g, strychnia 0.5g, sodium lignin sulfonate 2g, white carbon supply 100g are mixed, by each group Divide and dry, cool down, be levigate, must both be configured to 1% macro tetrolide strychnia wettable powder.
The Ningnanmycin Cynanchum Komarovii alkali wettable powder of embodiment 16 1.5%
Ningnanmycin 1g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each group Divide and dry, cool down, be levigate, be both configured to 1.5% Ningnanmycin Cynanchum Komarovii alkali wettable powder.
The Ningnanmycin solanine microemulsion of embodiment 17 1.5%
Ningnanmycin 1g water 10g are dissolved, solanine 0.5g is fully dissolved with chloroform 3g and methanol 5g, adds phenethyl Phenol polyethenoxy ether 5g and agriculture breast 500#5g, mixture is stirred in agitator, water complements to 100g, both obtains 1.5% Ningnan Mycin solanine microemulsion.
The Ningnanmycin dandelion buck emulsion of embodiment 18 1.5%
Ningnanmycin element 1g water 10g are dissolved, dandelion alkali 0.5g is fully dissolved with ethyl acetate 3g and ethanol 10g, The first two dissolved matter is mixed, adds phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slowly added to and stirred, supplied with water To 100g, 1.5% Ningnanmycin dandelion buck emulsion is both obtained.
The jinggangmeisu Cynanchum Komarovii alkali wettable powder of embodiment 19 2.5%
Jinggangmeisu 2g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each group Divide and dry, cool down, be levigate, be both configured to 2.5% jinggangmeisu Cynanchum Komarovii alkali wettable powder.
The jinggangmeisu solanine wettable powder of embodiment 20 2.5%
Jinggangmeisu 2g, solanine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, each component is done It is dry, cooling, it is levigate, be both configured to 2.5% jinggangmeisu solanine wettable powder.
The jinggangmeisu dandelion alkali wettable powder of embodiment 21 2.5%
Jinggangmeisu 2g, dandelion alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each component Dry, cool down, be levigate, be both configured to 2.5% jinggangmeisu dandelion alkali wettable powder.
The kasugarnycin Cynanchum Komarovii alkali wettable powder of embodiment 22 3%
Kasugarnycin 2.5g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, will be each Component is dry, cools down, be levigate, has both been configured to 3% kasugarnycin Cynanchum Komarovii alkali wettable powder.
The kasugarnycin solanine wettable powder of embodiment 23 3%
Kasugarnycin 2.5g, solanine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each component Dry, cool down, be levigate, be both configured to 3% kasugarnycin solanine wettable powder.
The kasugarnycin dandelion alkali wettable powder of embodiment 24 3%
Kasugarnycin 2.5g, dandelion alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each group Divide and dry, cool down, be levigate, be both configured to 3% kasugarnycin dandelion alkali wettable powder.
The streptomycin sulphate Cynanchum Komarovii alkali wettable powder of embodiment 25 36%
Streptomycin sulphate 35g, Cynanchum Komarovii alkali 1g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each group Divide and dry, cool down, be levigate, be both configured to 36% streptomycin sulphate Cynanchum Komarovii alkali wettable powder.
The polyoxin Cynanchum Komarovii alkali wettable powder of embodiment 26 3.5%
Polyoxin 3g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each group Divide and dry, cool down, be levigate, be both configured to 3.5% polyoxin Cynanchum Komarovii alkali wettable powder.
The polyoxin solanine wettable powder of embodiment 27 3.5%
Polyoxin 3g, solanine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, each component is done It is dry, cooling, it is levigate, be both configured to 3.5% polyoxin solanine wettable powder.
The polyoxin dandelion alkali wettable powder of embodiment 28 3.5%
Polyoxin 3g, dandelion alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each component Dry, cool down, be levigate, be both configured to 3.5% polyoxin dandelion alkali wettable powder.
The streptomycin sulphate solanine wettable powder of embodiment 29 36%
Streptomycin sulphate 35g, solanine 1g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, each component is done It is dry, cooling, it is levigate, be both configured to 36% streptomycin sulphate Cynanchum Komarovii alkali wettable powder.
The streptomycin sulphate dandelion alkali wettable powder of embodiment 30 36%
Streptomycin sulphate 35g, dandelion alkali 1g, sodium alkyl benzene sulfonate 2g, kaolin are supplied into 100g to mix, by each component Dry, cool down, be levigate, be both configured to 36% streptomycin sulphate dandelion alkali wettable powder.
The AVM Chinese azalea extract aqueous emulsion of embodiment 31 1%
AVM 0.5g is fully dissolved with dimethylbenzene 4g, Chinese azalea extract 0.5g ethyl acetate 1g, chloroform 1g are abundant Dissolving, the first two solution is mixed, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slowly added to and stirred, mended with water Foot both obtains 1% AVM Chinese azalea extract aqueous emulsion to 100g.
The pleocidin coriamyrtin aqueous emulsion of embodiment 32 1.5%
Pleocidin 0.5g is fully dissolved with dimethylbenzene 4g, coriamyrtin 1g ethyl acetate 1g, chloroform 1g are fully molten Solution, the first two solution is mixed, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slowly added to and stirred, supplied with water To 100g, 1.5% pleocidin coriamyrtin aqueous emulsion is both obtained.
The AVM chamaejasmine suspending agent of embodiment 33 1.5%
By AVM 0.5g, chamaejasmine 1g, sodium lignin sulfonate 3g, tea seed cake powder 5g, bentonite 5g, Magnesiumaluminumsilicate 2g, Ethylene glycol 10g is sufficiently mixed, and adds water 25g to be fully ground, and water complements to 100g, is configured to 1.5% AVM chamaejasmine and is hanged Floating agent.
The pleocidin chamaejasmine suspending agent of embodiment 34 1.5%
By pleocidin 0.5g, chamaejasmine 1g, sodium lignin sulfonate 3g, tea seed cake powder 5g, bentonite 5g, Magnesiumaluminumsilicate 2g, Ethylene glycol 10g is sufficiently mixed, and adds water 25g to be fully ground, and water complements to 100g, is configured to 1.5% pleocidin chamaejasmine and is hanged Floating agent.
The magnificent light rhzomorph pterocarpin suspending agent of embodiment 35 1.5%
By magnificent light rhzomorph 0.5g, pterocarpin 1g, sodium lignin sulfonate 3g, tea seed cake powder 5g, bentonite 5g, Magnesiumaluminumsilicate 2g, Ethylene glycol 10g is sufficiently mixed, and adds water 25g to be fully ground, and water complements to 100g, is configured to 1.5% magnificent light rhzomorph pterocarpin and is hanged Floating agent.
The macro tetrolide pterocarpin suspending agent of embodiment 36 1.5%
By macro tetrolide 0.5g, pterocarpin 1g, sodium lignin sulfonate 3g, tea seed cake powder 5g, bentonite 5g, Magnesiumaluminumsilicate 2g, Ethylene glycol 10g is sufficiently mixed, and adds water 25g to be fully ground, and water complements to 100g, is configured to 1.5% macro tetrolide pterocarpin and is hanged Floating agent.
The polyoxin thymol aqueous emulsion of embodiment 37 2%
Polyoxin 1.5g is fully dissolved with water, thymol 0.5g is fully dissolved with ethanol 5g, is mixed the first two solution, is added Enter phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slowly added to and stirred, and 100g is complemented to water, and it is anti-both to have obtained more than 2% Mycin thymol aqueous emulsion.
The jinggangmeisu thymol aqueous emulsion of embodiment 38 10%
Jinggangmeisu 9.5g is fully dissolved with water, thymol 0.5g is fully dissolved with ethanol 5g, is mixed the first two solution, is added Enter phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slowly added to and stirred, and 100g is complemented to water, both obtains 10% well Ridge mycin thymol aqueous emulsion.
The polyoxin cinnamic acid aqueous emulsion of embodiment 39 2%
Polyoxin 1.5g is fully dissolved with water, cinnamic acid 0.5g is fully dissolved with ethanol 5g, is mixed the first two solution, is added Enter phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slowly added to and stirred, and 100g is complemented to water, and it is anti-both to have obtained more than 2% Mycin cinnamic acid aqueous emulsion.
The jinggangmeisu cinnamic acid aqueous emulsion of embodiment 40 10%
Jinggangmeisu 9.5g is fully dissolved with water, cinnamic acid 0.5g is fully dissolved with ethanol 5g, is mixed the first two solution, is added Enter phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water is slowly added to and stirred, and 100g is complemented to water, both obtains 10% well Ridge mycin cinnamic acid aqueous emulsion.
Effect of composition of the embodiment 41 containing antibiotic and botanical components to cotton nematode
The dissolving of quantitative antibiotic is mixed with marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, the fennel wormwood artemisia to pulverize and sieve respectively Close, addition auxiliary agent, which is made into, respectively treats articles for use.Quantitative antibiotic dissolving is mixed with alkaloid respectively, addition auxiliary agent, which is made into, respectively treats Articles for use.It is above-mentioned to treat that articles for use are mixed into compost with sterilized soil and sterilizing river sand respectively, take quantitative culture soil to be mixed into quantitative compositions Or single dose, fully mix thoroughly, adding clear water makes water content 40%, loads basin alms bowl, and the cotton seedling that growth has 10d is transplanted in basin, Per 10 plants, 7d after transplanting of pot transplanting, per basin, 2 instar larvae of access Meloidogyne incognita 100, is placed in greenhouse, quantitative watering management. If per the basin of chemicals treatment 6, and set and be not mixed into chemicals treatment as blank control.After 20d, when blank control plant rhizosphere has a large amount of roots During knot, the plant height and root knot number of 3 basin cottons are investigated, and is classified by Liu Weizhi (1995)：0 grade, no root knot；1 grade, 1-2 roots Knot；2 grades, 3-10 root knot；3 grades, 11-30 root knot；4 grades, 31-100 root knot；5 grades, more than 100 root knots.Adjusted after 20d Look into the incidence of every another 3 basin cotton verticillium wilt of processing.It the results are shown in Table 1.
Effect of several compositions containing antibiotic and botanical components of table 1 to cotton nematode
Table 1 shows, compared with the processing of corresponding single dose, AVM containing antibiotic, ivermectin, milbemectin, kills more Rhzomorph, nikkomycin, the compositions-treated of macro tetrolide and several feverfew components, antibiotic Ningnanmycin, jinggangmeisu, Kasugarnycin, polyoxin, the processing root knot number of streptomycin sulphate and the composition of several alkaloids are less, and plant height is higher, and The blade verticillium wilt incidence of disease is relatively low, illustrates composition, the group of antibiotic and several alkaloids of antibiotic and several composite family components Compound can effectively prevent and treat nematode, reduce the generation of verticillium wilt.
The antibiotic of embodiment 42 is with the composition and antibiotic of several composite family components and the composition of several alkaloids to mandarin orange Tangerine, the effect of cotton
According to scheme, built agent and single dose are prepared, and carry out activity preliminary experiment.According to activity test determination trial, by preparation It is configured to the concentration needed.Before experiment, cell, listed, investigation red spider, aphid base are set in citrus orchard and Cotton Fields respectively Number, and corresponding single dose and blank control are set, using manual sprayer routine conventional spray.The listed processing red spider of 7d investigation after medicine And the quantity of aphid.Using Abbot formula, percentage is converted into preventive effect.
In theoretical effect, x is the effect of substance A when concentration is a, and y is the effect of substance B when concentration is b, compares reason By effect and actual effect, the synergy of composition is evaluated.It the results are shown in Table 2, table 3.
The antibiotic of table 2 is with the composition and antibiotic of several composite family components and several alkaloid compositions to citrus pest Field efficacy
Note：In table 2, marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia are the concentrate after extractive distillation.
The antibiotic of table 3 is with the composition and antibiotic of several composite family components and several alkaloid compositions to cotton-plant pest-insects Field efficacy
Note：In table 3, marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia are the concentrate after extractive distillation.
Find out from table 2, table 3, antibiotic AVM, ivermectin, milbemectin, pleocidin, nikkomycin, Liuyang Mycin and several Asteraceae plants and with the compositions of several alkaloids to citrus red mite and aphid, to cotton red spider And the actual effect of aphid is higher than theoretical effect, show that composition has obvious synergistic function.
The composition of the antibiotic of embodiment 43 and several alkaloids is to tomato disease and the effect of rice disease
According to scheme, built agent and unit dose preparation are prepared, and carry out activity preliminary experiment., will according to activity test determination trial Preparation is configured to the concentration needed.Corresponding single dose and blank control are set in tomato field and rice terrace before experiment, using hand-held spraying Device routine conventional spray, 50 plants are sprayed per medicament.7-10d dispenser 1 time again after 1st dispenser.10-20d after 2nd dispenser, investigation Listing tomato plant disease and rice plant disease incidence.Using Abbot formula, percentage is converted into preventive effect.
In theoretical effect, x is the effect of substance A when concentration is a, and y is the effect of substance B when concentration is b, compares reason By effect and actual effect, the synergy of composition is evaluated.Knot of the composition to tomato plant disease and rice plant disease Fruit is shown in Table 4 and table 5 respectively.
Field efficacy of the composition of the antibiotic of table 4 and several alkaloids to tomato disease
Field efficacy of the composition of the antibiotic of table 5 and several alkaloids to rice disease
As seen from Table 4, antibiotic Ningnanmycin, jinggangmeisu, kasugarnycin, polyoxin, streptomycin sulphate with it is several The composition of alkaloid is higher than theoretical effect to the actual effect of tomato virus disease, graw mold of tomato and bacterial wilt of tomato, shows Composition has obvious synergistic function.
As seen from Table 5, antibiotic Ningnanmycin, jinggangmeisu, kasugarnycin, polyoxin, streptomycin sulphate with it is several The composition of alkaloid is imitated to the actual effect of stripe disease, rice blast and banded sclerotial blight higher than the theoretical of corresponding medicament Fruit, show that composition has obvious synergistic function.
The composition of the composition of the antibiotic of embodiment 44 and terpenes component, antibiotic and flavones to wild cabbage, The effect of cotton-plant pest-insects
According to testing program, built agent and single dose are prepared, and carry out active trial test., will according to activity test determination trial Preparation is configured to the concentration needed.Before experiment, cell, listed, investigation cabbage field diamondback moth, dish are set in cabbage field and Cotton Fields Blue or green worm and Cotton Fields prodenia litura radix, and corresponding single dose and blank control are set, using manual sprayer routine conventional spray.Medicine 7d investigates effect of the medicament to diamondback moth, cabbage caterpillar and prodenia litura afterwards.Using Abbot formula, percentage is converted into preventive effect.
In theoretical effect, x is the effect of substance A when concentration is a, and y is the effect of substance B when concentration is b, compares reason By effect and actual effect, the synergy of composition is evaluated.It the results are shown in Table 6, table 7.
Field efficacy of composition of the table 6 containing antibiotic to cabbage pests
Field efficacy of composition of the table 7 containing antibiotic to cotton prodenia litura
Find out from table 6, table 7, AVM, ivermectin, pleocidin, milbemectin, nikkomycin in antibiotic, Macro tetrolide respectively the composition with the Chinese azalea extract of terpenes, with the composition of coriamyrtin and with the chamaejasmine of flavonoids Composition and the composition with pterocarpin, it is notable to the preventive effect of wild cabbage diamondback moth, cabbage caterpillar and cotton prodenia litura, to insect Actual effect be above theoretical effect, show obvious synergistic function.
Effect of the composition of the antibiotic of embodiment 45 and plants essential oil to rice sheath blight disease
According to scheme, built agent and unit dose preparation are prepared, and carry out active trial test., will according to active trial test result Preparation is configured to the concentration needed.Manual sprayer routine conventional spray is used in rice terrace before experiment, 50 plants of the spray per medicament, and Corresponding single dose and blank control are set, 7-10d dispenser 1 time again after the 1st dispenser, 10-20d after the 2nd dispenser, investigate listed water Rice plants banded sclerotial blight incidence.Using Abbot formula, percentage is converted into preventive effect.
In theoretical effect, x is the effect of substance A when concentration is a, and y is the effect of substance B when concentration is b, compares reason By effect and actual effect, the synergy of composition is evaluated.Rice plant banded sclerotial blight situation the results are shown in Table 8.
Field efficacy of composition of the table 8 containing antibiotic to rice sheath blight disease
As seen from Table 8, the Ningnanmycin in antibiotic, jinggangmeisu, kasugarnycin, polyoxin, streptomycin sulphate point Rice sheath blight disease is not prevented with the composition of the thymol of plants essential oil class and with the composition of the cinnamic acid of plants essential oil class Effect is notable, is above theoretical effect to the actual effect of banded sclerotial blight, shows obvious synergistic function.

Claims (5)

1. the agriculturally useful compositions containing streptomycin sulphate and botanical components, it is characterised in that said composition includes the sulphur of effective dose The quality parts ratio of sour streptomysin and alkaloid, streptomycin sulphate and alkaloid is 25:1-1:9, alkaloid be Cynanchum Komarovii alkali, One or more of alkaloids in solanine or dandelion alkali.
2. the agriculturally useful compositions of streptomycin sulphate according to claim 1 and botanical components, it is characterised in that composition The preparation of processing is wettable powder, water dispersible granules, aqueous emulsion, microemulsion, suspending agent, antibioticses and botanical components matter The percentage that amount sum accounts for preparation gross mass is 0.05-80%.
3. the agriculturally useful compositions according to claim 2 containing streptomycin sulphate and botanical components, it is characterised in that anti- The percentage that raw plain class and the quality sum of botanical components account for preparation gross mass is 0.1-40%.
4. the purposes of the agriculturally useful compositions containing streptomycin sulphate and botanical components described in claim 3, it is characterised in that With base manure, spraying, pouring root, seed dressing, immersion applications, show to prevent and treat the purposes of various crop pest and disease damage.
5. the purposes of the agriculturally useful compositions according to claim 4 containing streptomycin sulphate and botanical components, its feature Be the processing of composition has positive effect to cotton nematode and verticillium wilt, has synergy effect to tomato disease, rice disease Fruit.
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