CN104920395A - Agricultural combination containing validamycin and botanical components and application - Google Patents
Agricultural combination containing validamycin and botanical components and application Download PDFInfo
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- CN104920395A CN104920395A CN201510287336.5A CN201510287336A CN104920395A CN 104920395 A CN104920395 A CN 104920395A CN 201510287336 A CN201510287336 A CN 201510287336A CN 104920395 A CN104920395 A CN 104920395A
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- botanical components
- antibiotics
- alkali
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- OCDGBSUVYYVKQZ-UHFFFAOYSA-N gramine Chemical compound C1=CC=C2C(CN(C)C)=CNC2=C1 OCDGBSUVYYVKQZ-UHFFFAOYSA-N 0.000 description 1
- 230000012010 growth Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 239000001102 lavandula vera Substances 0.000 description 1
- 235000018219 lavender Nutrition 0.000 description 1
- HDVAWXXJVMJBAR-VHSXEESVSA-N lupinine Chemical compound C1CCC[C@@H]2[C@H](CO)CCCN21 HDVAWXXJVMJBAR-VHSXEESVSA-N 0.000 description 1
- 229930014016 lupinine Natural products 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229930014456 matrine Natural products 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 229940041616 menthol Drugs 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 229960005181 morphine Drugs 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- NHOIBRJOQAYBJT-IMGVWCFESA-N nimbin Chemical compound C=1([C@@H]2C[C@H]3O[C@H]4[C@](C3=C2C)(C)[C@@H]([C@]2(C(=O)C=C[C@](C)([C@@H]2[C@H]4OC(C)=O)C(=O)OC)C)CC(=O)OC)C=COC=1 NHOIBRJOQAYBJT-IMGVWCFESA-N 0.000 description 1
- ZQIYJHBQRBBBRZ-UHFFFAOYSA-N nimbin Natural products COC(=O)CC1C2C(C(OC(=O)C)C3OC4CC(C(=C4C13C)C)c5cocc5)C(C)(C=CC2=O)C(=O)OC ZQIYJHBQRBBBRZ-UHFFFAOYSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002420 orchard Substances 0.000 description 1
- 229930015582 oxymatrine Natural products 0.000 description 1
- 229960001789 papaverine Drugs 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 239000005648 plant growth regulator Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- ZCCUUQDIBDJBTK-UHFFFAOYSA-N psoralen Chemical class C1=C2OC(=O)C=CC2=CC2=C1OC=C2 ZCCUUQDIBDJBTK-UHFFFAOYSA-N 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- OARRHUQTFTUEOS-UHFFFAOYSA-N safranin Chemical compound [Cl-].C=12C=C(N)C(C)=CC2=NC2=CC(C)=C(N)C=C2[N+]=1C1=CC=CC=C1 OARRHUQTFTUEOS-UHFFFAOYSA-N 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 229940084560 sanguinarine Drugs 0.000 description 1
- YZRQUTZNTDAYPJ-UHFFFAOYSA-N sanguinarine pseudobase Natural products C1=C2OCOC2=CC2=C3N(C)C(O)C4=C(OCO5)C5=CC=C4C3=CC=C21 YZRQUTZNTDAYPJ-UHFFFAOYSA-N 0.000 description 1
- 229930000044 secondary metabolite Natural products 0.000 description 1
- 229930004725 sesquiterpene Chemical class 0.000 description 1
- 150000004354 sesquiterpene derivatives Chemical class 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- YZHUMGUJCQRKBT-UHFFFAOYSA-M sodium chlorate Chemical compound [Na+].[O-]Cl(=O)=O YZHUMGUJCQRKBT-UHFFFAOYSA-M 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- SLRCCWJSBJZJBV-AJNGGQMLSA-N sparteine Chemical compound C1N2CCCC[C@H]2[C@@H]2CN3CCCC[C@H]3[C@H]1C2 SLRCCWJSBJZJBV-AJNGGQMLSA-N 0.000 description 1
- 229960001945 sparteine Drugs 0.000 description 1
- UINUUSQOLRQGNF-UHFFFAOYSA-N stemonine Chemical compound O1C2(C=C(C)C(=O)O2)C(CC)C(C2CC3)C1CCCN2C3C1CC(C)C(=O)O1 UINUUSQOLRQGNF-UHFFFAOYSA-N 0.000 description 1
- HTLBMAZNGBFLEY-UHFFFAOYSA-N stemonine-C17 Natural products O1C(=O)C(C)CC1C1N2CCCC3OC(=O)C(C)C3C2CC1 HTLBMAZNGBFLEY-UHFFFAOYSA-N 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 229960005322 streptomycin Drugs 0.000 description 1
- FWQHRZXEQNUCSY-UHFFFAOYSA-N tert-butyl N-[2-(ethoxycarbonylamino)-5-[(4-fluorophenyl)methyl-prop-2-ynylamino]phenyl]carbamate Chemical compound CCOC(=O)NC1=C(C=C(C=C1)N(CC#C)CC2=CC=C(C=C2)F)NC(=O)OC(C)(C)C FWQHRZXEQNUCSY-UHFFFAOYSA-N 0.000 description 1
- 239000001585 thymus vulgaris Substances 0.000 description 1
- 125000003639 thymyl group Chemical group C1(=CC(C)=CC=C1C(C)C)* 0.000 description 1
- REJLGAUYTKNVJM-SGXCCWNXSA-N tomatine Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@H]1[C@@H](CO)O[C@H]([C@@H]([C@H]1O)O)O[C@@H]1C[C@@H]2CC[C@H]3[C@@H]4C[C@H]5[C@@H]([C@]4(CC[C@@H]3[C@@]2(C)CC1)C)[C@@H]([C@@]1(NC[C@@H](C)CC1)O5)C)[C@@H]1OC[C@@H](O)[C@H](O)[C@H]1O REJLGAUYTKNVJM-SGXCCWNXSA-N 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/54—1,3-Diazines; Hydrogenated 1,3-diazines
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention belongs to the field of plant protection, and relates to an agricultural combination containing a validamycin and botanical components, wherein the botanical components comprise one or several of the crushed materials or the crude extract or the active ingredients of derris, tripterygium wilfordii, tobacco, pyrethrum, Tagetes erecta, Ageratina adenophora, Radix Stemonae, chillies, Macleaya cordata, Sophora flavescens and the like. The agricultural combination manifests a good synergistic effect within a certain matching range, and has good control efficiency to crop diseases and insect pests.
Description
The application is the divisional application of " agriculturally useful compositions containing antibiotic and botanical components and application " application for a patent for invention, original application day: on July 26th, 2013, application number: 2013103211300
Technical field
The invention belongs to plant protection art, particularly relate to the agriculturally useful compositions containing antibiotic and botanical components and application, the present composition effectively can prevent and treat diseases and pests of agronomic crop.
Background technology
In recent years, due to single and not Scientific Usage of Drugs, damage by disease and insect has produced pesticide resistance in various degree, and agriculture and forestry produce still with chemical pesticide for mainly to prevent and treat kind, cause seriously increasingly destroying of environmental pollution and ecotope.Along with the raising of people's living standard and the enhancing of health perception, the manufacture and exploit of biopesticide progressively receives the concern of agricultural chemicals R&D worker, becoming the focus of agriculture and forestry sustainable development, is the effective way of environmental protect, minimizing or delaying drug resistance and raising drug effect.Wherein, farm antibiotics and botanical components become one of focus of biopesticide research.
Farm antibiotics, refers to and is produced by fermentable, had agricultural chemicals function, for agriculturally preventing and treating the secondary metabolite of the pests such as Pest organism mouse.The microorganisms such as actinomycetes, fungi, bacterium all can produce farm antibiotics, and wherein the farm antibiotics of actinomycetes generation is maximum.The many important farm antibiotics of current extensive use is all from streptomyces, be separated the actinomycetes obtained produce.Farm antibiotics is the earliest streptomycin, and has promoted antibiotic thus in application agriculturally, obtains and develop rapidly after 20 century 70s.At present, farm antibiotics is almost throughout agricultural chemicals all spectras such as insecticide, bactericide, weed killer herbicide, plant growth regulator.As the Avermectin, ivermectin, milbemectin, pleocidin, macro tetrolide, nikkomycin etc. of Insecticiding-miticiding effect, the polyoxin, kasugarnycin, jinggangmeisu, Ningnanmycin, mildiomycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin etc. of control fungal disease, prevent and treat the streptomycin sulphate of bacteriosis, terramycin etc., there is the bialaphos of herbicidal effect, there is the gibberellin etc. of coordinate plant growth.
The plant of the agricultural use future of tool and Development volue mainly contains Meliaceae, composite family, pulse family, Rutaceae, aster section, Labiatae, Annonaceae, Ranunculaceae, Euphorbiaceae, Araeceae, Myrsinacea, the certain plants of Papilionaceae etc., studying more has trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, India red sandalwood, erythrina indica, plant iron son or frutus cnidii etc.
There is desinsection, sterilization, fertilizer, fresh-keeping etc. botanical components, comprise the crushed material such as root, stem, leaf, flower, fruit, seed or crude extract that directly can utilize plant or the active component extracting plant.Plant resource active component is divided into alkaloids, terpenes, flavonoids, essential oil class, light-activated toxin class and other class active components by chemical constitution.
Cephalotaxaceae, Ranunculaceae, Berberidaceae, Papaveraceae, pulse family, Loganiaceae, Apocynaceae, Solanaceae, composite family, Liliaceae, Amaryllidaceae, Loganiaceae, Rutaceae, Lauraceae etc. is had containing the section that alkaloid is more.
Terpenes active component, mainly contains monoterpenes, sesquiterpenoids, Diterpenes and triterpene compound.Monoterpene is modal terpene, it is the key component of plant volatile oil, in Cupressaceae plant, content is relatively high, sesquiterpenoids is more in Coriariaceae plant, Celastraceae plant Celastrus angulatus etc., diterpene-kind compound is more in Euphorbiaceae, Isolated From Thymelaeaceae Species, and the important representative of triterpene compound has insect anti-feedant nimbin.
Flavonoids also claims flavone class, the form that major part and sugar are combined into glycoside or carbon glycosyl in plant corpus exists, and also has to exist in a free form.Mainly be distributed in the plants such as pulse family, Papilionaceae, Rutaceae, Umbelliferae, Labiatae.The rotenone extracted from Derris and Baptisia plant, has powerful tagging and stomach poison function to insect, and insecticidal spectrum is wide, and insect not easily develops immunity to drugs.The pterocarpoid chromocor compound extracted from Pterocarpus, Erythrina, reticulate millettia platymiscium has very strong antimycotic and bacterial activity effect, can be used as important plant defense element.
Plants essential oil is often present in the oil droplet of plant or the resin of plant cavity tissue.Most of essential oil component is complicated, and chemical constituent can be divided into four classes substantially, and a class is terpene compound, is the key component of essential oil, is divided into monoterpene derivative, sesquiterpene derivative, forskolin.Equations of The Second Kind is aromatic compound, in essential oil, be only second to terpene compound.3rd class is aliphatic compound.4th class is sulfur-bearing nitrogen-containing compound.Essential oil is volatile at normal temperatures, has strong peat-reek, is oily liquids at normal temperatures, dissolves in the multiple organic solvent such as methyl alcohol, ethanol.
Plant light-activated toxin more mainly derives from the natural products of Rutaceae composite family, samphire, not high to pest activity when unglazed, then has very strong activity under light illumination.Plant light-activated toxin main Types has polyyne class, thiophene phenols and quinones etc., and its mechanism of action is very unique, is different from traditional any insecticides, therefore can not produce the problem of cross tolerance.
Research about the agriculturally useful compositions of antibiotic agents and botanical components is reported less.
Summary of the invention
The object of the invention is environmental protect, expand action spectrum, minimizing or delaying drug resistance, raising drug effect, the agriculturally useful compositions of a kind of antibiotics and botanical components is provided.
The present invention is achieved through the following technical solutions:
Containing antibiotics and botanical components agriculturally useful compositions, it is characterized in that said composition includes A and B of effective amount, A is selected from Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, macro tetrolide, polyoxin, kasugarnycin, jinggangmeisu, Ningnanmycin, mildiomycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin, bialaphos, gibberellin, streptomycin sulphate, one or more in terramycin, B is selected from trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, India red sandalwood, erythrina indica, one or more meal of the young and frutus cnidii of plant iron.Preferably, botanical components is selected from Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia.
In the present composition, A is selected from Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, macro tetrolide, polyoxin, kasugarnycin, jinggangmeisu, Ningnanmycin, mildiomycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin, bialaphos, gibberellin, streptomycin sulphate, one or more in terramycin, B is selected from trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, India red sandalwood, erythrina indica, alkaloids in the crude extract of one or more in the young and frutus cnidii of plant iron or active component, terpenes, flavonoids, essential oil class, one or more in light-activated toxin class.
The agriculturally useful compositions containing antibiotics and botanical components of the present invention, is characterized in that the feverfew in botanical components is selected from Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia.
Alkaloids in botanical components in the present composition, for datura total alkali, Chelidonine, the total alkaloids, camptothecine, aconitine, strychnia, total alkaloid of sophora alopecuroide, thunder godvine alkaloid, oxymatrine, nicotine, black false hellebore total alkali, capsaicine, matrine, sanguinarine, jamaicin, stemonine, papaverine, quinoline is peaceful, tomatin, lupinine, sparteine, the numb rope in ground, donaxine, morphine, kind art soft-shelled turtle alkali, gelsemium henbane amine, mufangchine, magnoflorine, aconitine, eulexine, atropine, black nightshade alkaloid, one or more alkaloids in dandelion alkaloid etc. or one or more components in above-mentioned total alkali.One or more alkaloids preferably in datura total alkali, Chelidonine, the total alkaloids, camptothecine, aconitine, strychnia, Cynanchum Komarovii alkali, solanine or dandelion alkali or biology total alkali one or more components interior.
Terpenes in botanical components in the present composition is one or more in the diterpene-kind compound in the Celastrus angulatus of the coriamyrtin of the monoterpene in the Chinese azalea extract in Ericaceae, the menthol in Labiatae, peppermint aldehyde, Cupressaceae plant, Coriariaceae plant, Celastraceae plant, Euphorbiaceae, Isolated From Thymelaeaceae Species and the triterpene compound in Meliaceae etc.Preferred terpenes is one in Chinese azalea extract and coriamyrtin or two kinds.
Flavonoids in botanical components in the present composition is one or more in the young flavones of chamaejasmine, rotenone, pterocarpoid, kuh-seng flavones and plant iron.Preferred flavonoids is one in chamaejasmine, pterocarpoid or two kinds.
Essential oil class in botanical components in the present composition is one or more in the terpene compound in thyme, Chinese cassia tree, lemongrass, cloves, Chinese anise, orange peel, tree-of-heaven bark, chilli powder, Siberian cocklebur, lavender, the fruit of a cubeb litsea tree, garlic, peppermint, cypress, Chinese prickly ash, Artemisia scoparia etc., aromatic compound, aliphatic compound, sulfur-bearing nitrogen-containing compound.Preferred essential oil is one in thymol and cinnamic acid or two kinds.
Plant Light activation endotoxin in botanical components in the present composition is one or more in furocoumarin class, polyyne class, thiophene phenols and quinones etc.
In the present composition, the ratio of quality and the number of copies of antibiotics and botanical components is 50:1-1:200.Preferably, the ratio of quality and the number of copies of antibiotics and botanical components is 30:1-1:20.
Above-mentioned composition process preparation of the present invention is wetting powder, water dispersible granules, aqueous emulsion, microemulsion, suspending agent, and the percentage that antibiotics and botanical components quality sum account for preparation gross mass is 0.05-80%.Preferably, antibiotics and botanical components quality sum account for the percentage of preparation gross mass is 0.1-40%
The preparation of above-mentioned composition processing of the present invention, with base manure, spraying, filling root, seed dressing, impregnating application, shows the purposes of preventing and treating various crop damage by disease and insect.
Present invention also offers the composition of antibiotic and several composite family component and antibiotic and several alkaloid composition to the effect of citrus pest, cotton-plant pest-insects, antibiotic and several alkaloidal composition are to the effect of tomato disease, rice disease, several composition containing antibiotic and botanical components is to the effect of cotton nematode, the composition of antibiotic and terpenes component and antibiotic and flavones is to the effect of cabbage pests, cotton-plant pest-insects, and the composition of antibiotic and plants essential oil is to the effect of rice sheath blight disease.
Composition of the present invention compared with prior art, produces following beneficial effect:
1, purposes is widened: composition can prevent and treat the multiple damage by disease and insect of crops.
2, use cost is reduced: improve preventive effect because composition has, control spectrum increases, decrease Pesticide use number of times, reduce use cost.
3, delay pesticide resistance: be that the component of different mechanism of action is composite containing antibiotic and the composition of botanical components, damage by disease and insect not easily develops immunity to drugs.
4, environmental friendliness: to people and animals and non-target organism toxicity low, degraded is fast in the environment, and low-residual is free from environmental pollution.
Embodiment
Below described in embodiment only for explaining the present invention, for not departing from amendment that the present invention's spirit and principle make, replacement or improvement, all belong to the scope of protection of present invention.Antibiotic in following examples and botanical components are from commercial channel or prepare voluntarily.
The alkaloidal preparation method of embodiment 1 plant resource
Get plant material trifoliate jewelvine respectively, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, India red sandalwood, erythrina indica, one or more vegetable materials in the young and frutus cnidii of plant iron, clean, dry, pulverize, add 95% ethanol 43 DEG C backflow 2 × 1h/ time, reclaim ethanol to concentrate, with the acidifying of 0.4mol/L aqueous sulfuric acid, after use chloroform eccysis oil-soluble impurities, the acid liquid sodium carbonate obtained is neutralized to pH8.5 and uses chloroform extraction again, reclaim organic solvent, obtain the biology total alkali of botanical components.
The preparation of embodiment 2 botanical components flavonoids
Get plant trifoliate jewelvine respectively, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, India red sandalwood, erythrina indica, one or more vegetable materials in the young and frutus cnidii of plant iron, clean, dry, pulverize, crushed material and solvent are loaded in extractor and mixes, be placed in ultrasonoscope, 75-85 DEG C is extracted at least 25min, obtain suspension, first time filters to get filtrate and filter residue, filter residue and solvent are loaded in extractor and mix, be placed in ultrasonoscope, 82-94 DEG C is extracted at least 40min, obtains suspension, and second time filters to get filtrate and filter residue, the mixing of the filtrate of above-mentioned secondary is adopted decompression distillation, and the concentrate obtained is plant resource Flavonoid substances.Above-mentioned solvent adopts one or more in water, ethyl acetate, acetone, ethanol, methyl alcohol.
The preparation of embodiment 3 plant resource terpenes, essential oil material
Get one or more vegetable materials in plant trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, India red sandalwood, erythrina indica, plant iron son and frutus cnidii respectively, clean, dry, pulverizing.The steam distillation of this area routine, ethonal extraction method or acetone and water mixed solvent extraction method is adopted to be prepared terpenes, essential oil class.Also the steam distillation of this area routine can be adopted to prepare essential oil.
Embodiment 4 5% Avermectin Aztec marigold aqueous emulsion
0.5g Avermectin is dissolved with 5g dimethyl formamide, get the concentrate 4.5g of Aztec marigold through alcohol extract, distillation, fully dissolve with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 5% Avermectin Aztec marigold aqueous emulsion.
Embodiment 5 5% ivermectin Eupatorium adenophorum aqueous emulsion
With 5g acetic acid 0.5g ivermectin, get the concentrate 4.5g of Eupatorium adenophorum through alcohol extract, distillation, fully dissolve with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 5% ivermectin Eupatorium adenophorum aqueous emulsion.
Embodiment 6 5% milbemectin Dalmatian chrysanthemum aqueous emulsion
0.5g milbemectin is dissolved with 5g dimethyl formamide, get the concentrate 4.5g of Dalmatian chrysanthemum through alcohol extract, distillation, fully dissolve with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 5% milbemectin Dalmatian chrysanthemum aqueous emulsion.
Embodiment 7 5% pleocidin Artemisia scoparia aqueous emulsion
0.5g pleocidin is dissolved with 5g dimethyl formamide, get the concentrate 4.5g of Artemisia scoparia through alcohol extract, distillation, fully dissolve with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 5% pleocidin Artemisia scoparia aqueous emulsion.
Embodiment 8 5% nikkomycin Dalmatian chrysanthemum aqueous emulsion
0.5g nikkomycin is dissolved with 5g dimethyl formamide, get the concentrate 4.5g of Dalmatian chrysanthemum through alcohol extract, distillation, fully dissolve with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 5% nikkomycin Dalmatian chrysanthemum aqueous emulsion.
Embodiment 9 5% macro tetrolide fennel wormwood artemisia aqueous emulsion
0.5g macro tetrolide is dissolved with 5g dimethyl formamide, get the concentrate 4.5g of fennel wormwood artemisia through alcohol extract, distillation, fully dissolve with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 5% macro tetrolide fennel wormwood artemisia aqueous emulsion.
Embodiment 10 1% Avermectin datura total alkali water dispersible granules
By Avermectin 0.5g, datura total alkali 0.5g, naphthalenesulfonate formaldehyde condensation compound 4g, sodium alkyl benzene sulfonate 1.5g, gum Arabic 0.5g, 100g mixing supplied by white carbon, mixture is carried out granulation after ultra-fine grinding, drying, screening, both 1% Avermectin datura total alkali water dispersible granules.
Embodiment 11 1% ivermectin Chelidonine water dispersible granules
Ivermectin 0.5g, Chelidonine 0.5g, naphthalenesulfonate formaldehyde condensation compound 10g, sodium alkyl benzene sulfonate 5g, white carbon are supplied 100g mixing, mixture is carried out granulation after ultra-fine grinding, drying, screening, both made 1% ivermectin Chelidonine water dispersible granules.
Embodiment 12 1% milbemectin the total alkaloids microemulsion
Milbemectin 0.5g dimethylbenzene 5g is dissolved, the total alkaloids 0.5g chloroform 3g and methyl alcohol 5g fully dissolves, and adds phenethyl phenol polyethenoxy ether 5g and agriculture breast 500#5g, is stirred by mixture in agitator, water complements to 100g, both obtains 1% milbemectin the total alkaloids microemulsion.
Embodiment 13 1% pleocidin camptothecine aqueous emulsion
Pleocidin 0.5g dimethylbenzene 5g is dissolved, camptothecine 0.5g ethyl acetate 3g and ethanol 10g fully dissolves, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, complement to 100g with water, both obtain 1% pleocidin camptothecine aqueous emulsion.
Embodiment 14 1% nikkomycin aconitine wetting powder
Nikkomycin 0.5g, aconitine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 1% nikkomycin aconitine wetting powder.
Embodiment 15 1% macro tetrolide strychnia wetting powder
Macro tetrolide 0.5g, strychnia 0.5g, sodium lignin sulfonate 2g, white carbon are supplied 100g mixing, each component is dry, cooling, levigate, both must be mixed with 1% macro tetrolide strychnia wetting powder.
Embodiment 16 1.5% Ningnanmycin Cynanchum Komarovii alkali wetting powder
Ningnanmycin 1g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 1.5% Ningnanmycin Cynanchum Komarovii alkali wetting powder.
Embodiment 17 1.5% Ningnanmycin solanine microemulsion
Ningnanmycin 1g use water 10g is dissolved, solanine 0.5g chloroform 3g and methyl alcohol 5g fully dissolves, and adds phenethyl phenol polyethenoxy ether 5g and agriculture breast 500#5g, is stirred by mixture in agitator, water complements to 100g, both obtains 1.5% Ningnanmycin solanine microemulsion.
Embodiment 18 1.5% Ningnanmycin dandelion buck emulsion
Ningnanmycin element 1g use water 10g is dissolved, dandelion alkali 0.5g ethyl acetate 3g and ethanol 10g fully dissolves, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, complement to 100g with water, both obtain 1.5% Ningnanmycin dandelion buck emulsion.
Embodiment 19 2.5% jinggangmeisu Cynanchum Komarovii alkali wetting powder
Jinggangmeisu 2g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 2.5% jinggangmeisu Cynanchum Komarovii alkali wetting powder.
Embodiment 20 2.5% jinggangmeisu solanine wetting powder
Jinggangmeisu 2g, solanine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 2.5% jinggangmeisu solanine wetting powder.
Embodiment 21 2.5% jinggangmeisu dandelion alkali wetting powder
Jinggangmeisu 2g, dandelion alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 2.5% jinggangmeisu dandelion alkali wetting powder.
Embodiment 22 3% kasugarnycin Cynanchum Komarovii alkali wetting powder
Kasugarnycin 2.5g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 3% kasugarnycin Cynanchum Komarovii alkali wetting powder.
Embodiment 23 3% kasugarnycin solanine wetting powder
Kasugarnycin 2.5g, solanine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 3% kasugarnycin solanine wetting powder.
Embodiment 24 3% kasugarnycin dandelion alkali wetting powder
Kasugarnycin 2.5g, dandelion alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 3% kasugarnycin dandelion alkali wetting powder.
Embodiment 25 36% streptomycin sulphate Cynanchum Komarovii alkali wetting powder
Streptomycin sulphate 35g, Cynanchum Komarovii alkali 1g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 36% streptomycin sulphate Cynanchum Komarovii alkali wetting powder.
Embodiment 26 3.5% polyoxin Cynanchum Komarovii alkali wetting powder
Polyoxin 3g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 3.5% polyoxin Cynanchum Komarovii alkali wetting powder.
Embodiment 27 3.5% polyoxin solanine wetting powder
Polyoxin 3g, solanine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 3.5% polyoxin solanine wetting powder.
Embodiment 28 3.5% polyoxin dandelion alkali wetting powder
Polyoxin 3g, dandelion alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 3.5% polyoxin dandelion alkali wetting powder.
Embodiment 29 36% streptomycin sulphate solanine wetting powder
Streptomycin sulphate 35g, solanine 1g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 36% streptomycin sulphate Cynanchum Komarovii alkali wetting powder.
Embodiment 30 36% streptomycin sulphate dandelion alkali wetting powder
Streptomycin sulphate 35g, dandelion alkali 1g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mixing, each component is dry, cooling, levigate, be both mixed with 36% streptomycin sulphate dandelion alkali wetting powder.
Embodiment 31 1% Avermectin Chinese azalea extract aqueous emulsion
Avermectin 0.5g dimethylbenzene 4g is fully dissolved, Chinese azalea extract 0.5g ethyl acetate 1g, chloroform 1g fully dissolve, mix the first two solution, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, complement to 100g with water, both obtain 1% Avermectin Chinese azalea extract aqueous emulsion.
Embodiment 32 1.5% pleocidin coriamyrtin aqueous emulsion
Pleocidin 0.5g dimethylbenzene 4g is fully dissolved, coriamyrtin 1g ethyl acetate 1g, chloroform 1g fully dissolve, mix the first two solution, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, complement to 100g with water, both obtain 1.5% pleocidin coriamyrtin aqueous emulsion.
Embodiment 33 1.5% Avermectin chamaejasmine suspending agent
Avermectin 0.5g, chamaejasmine 1g, sodium lignin sulfonate 3g, the withered powder 5g of tea, bentonite 5g, Magnesiumaluminumsilicate 2g, ethylene glycol 10g are fully mixed, the 25g that adds water fully grinds, and water complements to 100g, is mixed with 1.5% Avermectin chamaejasmine suspending agent.
Embodiment 34 1.5% pleocidin chamaejasmine suspending agent
Pleocidin 0.5g, chamaejasmine 1g, sodium lignin sulfonate 3g, the withered powder 5g of tea, bentonite 5g, Magnesiumaluminumsilicate 2g, ethylene glycol 10g are fully mixed, the 25g that adds water fully grinds, and water complements to 100g, is mixed with 1.5% pleocidin chamaejasmine suspending agent.
Embodiment 35 1.5% magnificent light rhzomorph pterocarpin suspending agent
Magnificent light rhzomorph 0.5g, pterocarpin 1g, sodium lignin sulfonate 3g, the withered powder 5g of tea, bentonite 5g, Magnesiumaluminumsilicate 2g, ethylene glycol 10g are fully mixed, the 25g that adds water fully grinds, and water complements to 100g, is mixed with 1.5% magnificent light rhzomorph pterocarpin suspending agent.
Embodiment 36 1.5% macro tetrolide pterocarpin suspending agent
Macro tetrolide 0.5g, pterocarpin 1g, sodium lignin sulfonate 3g, the withered powder 5g of tea, bentonite 5g, Magnesiumaluminumsilicate 2g, ethylene glycol 10g are fully mixed, the 25g that adds water fully grinds, and water complements to 100g, is mixed with 1.5% macro tetrolide pterocarpin suspending agent.
Embodiment 37 2% polyoxin thymol aqueous emulsion
Fully dissolved by polyoxin 1.5g water, thymol 0.5g ethanol 5g fully dissolves, and mixes the first two solution, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 2% polyoxin thymol aqueous emulsion.
Embodiment 38 10% jinggangmeisu thymol aqueous emulsion
Fully dissolved by jinggangmeisu 9.5g water, thymol 0.5g ethanol 5g fully dissolves, and mixes the first two solution, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 10% jinggangmeisu thymol aqueous emulsion.
Embodiment 39 2% polyoxin cinnamic acid aqueous emulsion
Fully dissolved by polyoxin 1.5g water, cinnamic acid 0.5g ethanol 5g fully dissolves, and mixes the first two solution, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 2% polyoxin cinnamic acid aqueous emulsion.
Embodiment 40 10% jinggangmeisu cinnamic acid aqueous emulsion
Fully dissolved by jinggangmeisu 9.5g water, cinnamic acid 0.5g ethanol 5g fully dissolves, and mixes the first two solution, add phenethyl phenol polyethenoxy ether 5g, agriculture breast 500#5g, water slowly adds and stirs, and complements to 100g with water, both obtains 10% jinggangmeisu cinnamic acid aqueous emulsion.
Embodiment 41 contains the composition of antibiotic and botanical components to the effect of cotton nematode
Dissolved by quantitative antibiotic and mix with the Aztec marigold pulverized and sieved, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia respectively, interpolation auxiliary agent is made into and treats articles for use respectively.Dissolved by quantitative antibiotic and mix with alkaloid respectively, interpolation auxiliary agent is made into and treats articles for use respectively.Above-mentionedly treat that articles for use are mixed into compost with sterilized soil and sterilizing river sand respectively, get quantitative culture soil and be mixed into quantitative compositions or single dose, fully mix thoroughly, add clear water and make water content 40%, load basin alms bowl, the cotton seedling of 10d is had to be transplanted in basin growth, every pot transplanting 10 strain, 7d after transplanting, every basin access Meloidogyne incognita 2 instar larvae 100, be placed in greenhouse, quantitative watering manages.If every chemicals treatment 6 basin, and set and be not mixed into chemicals treatment as blank.After 20d, when blank plant rhizosphere has a large amount of root knot, investigate plant height and the root knot number of 3 basin cottons, and carry out classification by Liu Weizhi (1995): 0 grade, without root knot; 1 grade, 1-2 root knot; 2 grades, 3-10 root knot; 3 grades, 11-30 root knot; 4 grades, 31-100 root knot; 5 grades, more than 100 root knots.20d " Invest, Then Investigate " often processes the incidence of another 3 basin cotton verticillium wilts.The results are shown in Table 1.
Several composition containing antibiotic and botanical components of table 1 is to the effect of cotton nematode
Table 1 shows, compared with corresponding single dose process, containing antibiotic Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, the compositions-treated of macro tetrolide and several feverfew component, antibiotic Ningnanmycin, jinggangmeisu, kasugarnycin, polyoxin, the process root knot number of streptomycin sulphate and several alkaloidal composition is less, plant height is higher, and the blade verticillium wilt incidence of disease is lower, the composition of antibiotic and several composite family component is described, antibiotic and several alkaloidal composition effectively can prevent and treat nematode, reduce the generation of verticillium wilt.
The composition of embodiment 42 antibiotic and several composite family component and antibiotic and several alkaloidal composition are to the effect of oranges and tangerines, cotton
According to scheme, preparation built agent and single dose, and carry out active preliminary experiment.According to determination of activity trial test, by the concentration that Formulation becomes to need.Before test, community is set at citrus orchard and Cotton Fields, lists respectively, investigation two spotted spider mite, aphid radix, and establish corresponding single dose and blank, adopt the conventional conventional spray of manual sprayer.After medicine, 7d investigation is listed and is processed the quantity of two spotted spider mite and aphid.Use Abbot formula, convert percentage to preventive effect.
In theoretical effect, the effect of the substance A that x is concentration when being a, the effect of the substance B that y is concentration when being b, compares theoretical effect and actual effect, evaluates the synergy of composition.The results are shown in Table 2, table 3.
The composition of table 2 antibiotic and several composite family component and antibiotic and several alkaloid composition are to the field efficacy of citrus pest
Note: in table 2, Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia are the concentrate after extractive distillation.
The composition of table 3 antibiotic and several composite family component and antibiotic and several alkaloid composition are to the field efficacy of cotton-plant pest-insects
Note: in table 3, Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia are the concentrate after extractive distillation.
Find out from table 2, table 3, antibiotic Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, macro tetrolide and several Asteraceae plants and with several alkaloidal composition to citrus red mite and aphid, to the actual effect of cotton red spider and aphid higher than theoretical effect, show that composition has obvious synergistic function.
Embodiment 43 antibiotic and several alkaloidal composition are to the effect of tomato disease and rice disease
According to scheme, preparation built agent and unit dose preparation, and carry out active preliminary experiment.According to determination of activity trial test, by the concentration that Formulation becomes to need.Establish corresponding single dose and blank in tomato field and paddy field before test, adopt the conventional conventional spray of manual sprayer, every medicament sprays 50 strains.7-10d dispenser 1 time again after 1st dispenser.10-20d after 2nd dispenser, investigates list tomato plant disease and rice plant disease incidence.Use Abbot formula, convert percentage to preventive effect.
In theoretical effect, the effect of the substance A that x is concentration when being a, the effect of the substance B that y is concentration when being b, compares theoretical effect and actual effect, evaluates the synergy of composition.Composition to the result of tomato plant disease and rice plant disease respectively in table 4 and table 5.
Table 4 antibiotic and several alkaloidal composition are to the field efficacy of tomato disease
Table 5 antibiotic and several alkaloidal composition are to the field efficacy of rice disease
As seen from Table 4, antibiotic Ningnanmycin, jinggangmeisu, kasugarnycin, polyoxin, streptomycin sulphate and several alkaloidal composition higher than theoretical effect, show that composition has obvious synergistic function to the actual effect of tomato virus disease, graw mold of tomato and bacterial wilt of tomato.
As seen from Table 5, antibiotic Ningnanmycin, jinggangmeisu, kasugarnycin, polyoxin, streptomycin sulphate and several alkaloidal composition, to the theoretical effect of the actual effect of stripe disease, rice blast and banded sclerotial blight higher than corresponding medicament, show that composition has obvious synergistic function.
The composition of the composition of embodiment 44 antibiotic and terpenes component, antibiotic and flavones is to the effect of wild cabbage, cotton-plant pest-insects
According to testing program, preparation built agent and single dose, and carry out active trial test.According to determination of activity trial test, by the concentration that Formulation becomes to need.Before test, community is set at cabbage field and Cotton Fields, lists, investigation cabbage field diamond-back moth, cabbage caterpillar and Cotton Fields prodenia litura radix, and establish corresponding single dose and blank, adopt the conventional conventional spray of manual sprayer.After medicine, 7d investigates the effect of medicament to diamond-back moth, cabbage caterpillar and prodenia litura.Use Abbot formula, convert percentage to preventive effect.
In theoretical effect, the effect of the substance A that x is concentration when being a, the effect of the substance B that y is concentration when being b, compares theoretical effect and actual effect, evaluates the synergy of composition.The results are shown in Table 6, table 7.
Table 6 contains antibiotic composition to the field efficacy of cabbage pests
Table 7 contains antibiotic composition to the field efficacy of cotton prodenia litura
Find out from table 6, table 7, Avermectin in antibiotic, ivermectin, pleocidin, milbemectin, nikkomycin, macro tetrolide respectively with the composition of the Chinese azalea extract of terpenes, with the composition of coriamyrtin and with the composition of the chamaejasmine of flavonoids and the composition with pterocarpin, remarkable to the preventive effect of wild cabbage diamond-back moth, cabbage caterpillar and cotton prodenia litura, to the actual effect of insect all higher than theoretical effect, show obvious synergistic function.
The composition of embodiment 45 antibiotic and plants essential oil is to the effect of rice sheath blight disease
According to scheme, preparation built agent and unit dose preparation, and carry out active trial test.According to active trial test result, by the concentration that Formulation becomes to need.Adopt the conventional conventional spray of manual sprayer at paddy field before test, every medicament sprays 50 strains, and arranges corresponding single dose and blank, 7-10d dispenser 1 time again after the 1st dispenser, 10-20d after the 2nd dispenser, and investigation is listed rice plant banded sclerotial blight incidence.Use Abbot formula, convert percentage to preventive effect.
In theoretical effect, the effect of the substance A that x is concentration when being a, the effect of the substance B that y is concentration when being b, compares theoretical effect and actual effect, evaluates the synergy of composition.Rice plant banded sclerotial blight situation the results are shown in Table 8.
Table 8 contains antibiotic composition to the field efficacy of rice sheath blight disease
As seen from Table 8, Ningnanmycin in antibiotic, jinggangmeisu, kasugarnycin, polyoxin, streptomycin sulphate respectively with the composition of the thymol of plants essential oil class and remarkable with the preventive effect of composition to rice sheath blight disease of the cinnamic acid of plants essential oil class, to the actual effect of banded sclerotial blight all higher than theoretical effect, show obvious synergistic function.
Claims (6)
1. contain the agriculturally useful compositions of antibiotics and botanical components, it is characterized in that said composition includes A and B of effective amount, A is selected from jinggangmeisu, B is selected from trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, India red sandalwood, erythrina indica, alkaloid in the young and frutus cnidii active component of plant iron, alkaloid is datura total alkali, Chelidonine, the total alkaloids, camptothecine, aconitine, strychnia, Cynanchum Komarovii alkali, one or more alkaloids in solanine or dandelion alkali, the ratio of quality and the number of copies of antibiotics and botanical components is 50:1-1:200.
2. the agriculturally useful compositions containing antibiotics and botanical components according to claim 1, is characterized in that alkaloid is one or more alkaloids in Cynanchum Komarovii alkali, solanine or dandelion alkali.
3. the agriculturally useful compositions containing antibiotics and botanical components according to claim 2, it is characterized in that the preparation that composition is processed is wetting powder, water dispersible granules, aqueous emulsion, microemulsion, suspending agent, the percentage that antibiotics and botanical components quality sum account for preparation gross mass is 0.05-80%.
4. the agriculturally useful compositions containing antibiotics and botanical components according to claim 3, is characterized in that the percentage that the quality sum of antibiotics and botanical components accounts for preparation gross mass is 0.1-40%.
5. the purposes containing the agriculturally useful compositions of antibiotics and botanical components according to claim 4, is characterized in that, with base manure, spraying, filling root, seed dressing, immersion applications, showing the purposes of preventing and treating various crop damage by disease and insect.
6. the purposes containing the agriculturally useful compositions of antibiotics and botanical components according to claim 5, is characterized in that the process of composition has positive effect to cotton nematode and verticillium wilt, has synergistic effect to tomato disease, rice disease.
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106614804A (en) * | 2016-12-23 | 2017-05-10 | 芜湖福民生物药业股份有限公司 | Validamycin composition for controlling rice sheath blight disease and preparation method thereof |
| CN106614805A (en) * | 2016-12-23 | 2017-05-10 | 芜湖福民生物药业股份有限公司 | Validamycin compound for preventing and treating rice sheath blight disease and preparation method thereof |
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| CN106614804A (en) * | 2016-12-23 | 2017-05-10 | 芜湖福民生物药业股份有限公司 | Validamycin composition for controlling rice sheath blight disease and preparation method thereof |
| CN106614805A (en) * | 2016-12-23 | 2017-05-10 | 芜湖福民生物药业股份有限公司 | Validamycin compound for preventing and treating rice sheath blight disease and preparation method thereof |
| CN106665680A (en) * | 2016-12-23 | 2017-05-17 | 芜湖福民生物药业股份有限公司 | Validamycin composition for preventing and controlling rice sheath blight disease and preparation method of validamycin composition |
| CN106818921A (en) * | 2016-12-23 | 2017-06-13 | 芜湖福民生物药业股份有限公司 | Validamycin composition and preparation method thereof for preventing and treating rice sheath blight disease |
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| CN107628838B (en) * | 2017-10-24 | 2020-10-09 | 山东省农业科学院 | Ecological-friendly foliar fertilizer applied to vegetables or fruits and preparation method thereof |
| CN109197320A (en) * | 2018-09-04 | 2019-01-15 | 横县校椅供销卫民种养专业合作社联合社 | A kind of high-yield planting method of perfume lemon |
| CN110269068A (en) * | 2019-05-29 | 2019-09-24 | 贵州梵净山农业高科技股份有限公司 | A kind of macleaya cordata aqueous suspension agent biological pesticide and preparation method thereof |
| CN111480653A (en) * | 2020-04-02 | 2020-08-04 | 宁夏工商职业技术学院（宁夏化工技工学校、宁夏机电工程学校、宁夏农业机械化学校） | Pesticide composition for preventing and treating rice sheath blight disease and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103349007B (en) | 2015-12-02 |
| CN103349007A (en) | 2013-10-16 |
| CN105265501A (en) | 2016-01-27 |
| CN104920395B (en) | 2018-03-09 |
| CN105379779A (en) | 2016-03-09 |
| CN105379779B (en) | 2017-11-21 |
| CN105191995B (en) | 2017-11-21 |
| CN105191995A (en) | 2015-12-30 |
| CN105265501B (en) | 2017-12-08 |
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