CN106818948A - A kind of low-temperature-resistance growth substance and preparation method thereof - Google Patents

A kind of low-temperature-resistance growth substance and preparation method thereof Download PDF

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Publication number
CN106818948A
CN106818948A CN201710048909.8A CN201710048909A CN106818948A CN 106818948 A CN106818948 A CN 106818948A CN 201710048909 A CN201710048909 A CN 201710048909A CN 106818948 A CN106818948 A CN 106818948A
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China
Prior art keywords
parts
temperature
low
preparation
growth substance
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CN201710048909.8A
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Chinese (zh)
Inventor
施春华
张美芬
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Shengzhou City Paitepu Technology Development Co Ltd
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Shengzhou City Paitepu Technology Development Co Ltd
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Priority to CN201710048909.8A priority Critical patent/CN106818948A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/44Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Environmental Sciences (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Pest Control & Pesticides (AREA)
  • Pretreatment Of Seeds And Plants (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention provides a kind of, and the growth regulator includes following component and its weight portion:18 25 parts of the wall fern, 5 10 parts of eclipta, 8 15 parts of mulberry leaf, 10 15 parts of blackspiked lovegrass herb with root, 10 20 parts of achyranthes aspera, 10 23 parts of folium isatidis, 10 15 parts of cassia bark, 10 20 parts of polygala, 15 20 parts of trehalose, 0.2 0.7 parts of fennel seeds, 0.5 0.9 parts of wormwood, this low-temperature-resistance growth substance that the present invention is provided and preparation method thereof, prepare simple, operation strategies are wide, provide promote biological growth when and improve biology cold tolerance, prevent from making biological death during low temperature.

Description

A kind of low-temperature-resistance growth substance and preparation method thereof
Technical field
The present invention relates to promote biological growth field, a kind of especially low-temperature-resistance growth substance and preparation method thereof.
Background technology
During biological culture, in order to improve the growth ability of biology, promote biological growth speed, people often exist A certain amount of growth regulator is keyed in fertilising or feeding feed.
A kind of a kind of plant growth substances and application thereof in the art, CN101019559A, pyrolkigneous liquid plant helps Agent long and application thereof, is made up of pyrolkigneous liquid and carrier water, wherein the weight proportion of described pyrolkigneous liquid and carrier water be 1: 200~ 700, a kind of described plant growth substances is spraying, pour or immersion way releases the hazard of pesticides in plant, promotees root growth side The application in face., better than conventional plant hormone and growth regulator in terms of promoting root growth system growth result, price advantage is more for the present invention Substantially;The invention has special effect in terms of the hazard of pesticides is released.
Certain effect is served to plant growth there is provided a kind of growth regulator to plant in the invention, but is not being planted The cold tolerance of plant is improved in thing growth course, causes some plants to be adapted in low temperature and withered.
The content of the invention
The technical problems to be solved by the invention are that a kind of increase growth ability promotion of offer grows and clearing damp is scattered to be improved Resistance, cold-resistant effect is particularly evident, low-temperature-resistance growth substance of protection against cold and freezing conditions wound and preparation method thereof.
To solve above-mentioned existing technical problem, the present invention uses following scheme:A kind of low-temperature-resistance growth substance, the growth encourage Agent includes following component and its weight portion:Wall fern 18-25 parts, eclipta 5-10 parts, mulberry leaf 8-15 parts, blackspiked lovegrass herb with root 10-15 parts, Achyranthes aspera 10-20 parts, folium isatidis 10-23 parts, cassia bark 10-15 parts, polygala 10-20 parts, trehalose 15-20 parts, fennel seeds 0.2- 0.7 part, wormwood 0.5-0.9 parts.
A kind of preparation method of low-temperature-resistance growth substance, comprises the following steps:
1)Dried process after being chosen each composition, cleaned with clear water by above-mentioned weight portion;
2)Dried fennel seeds and wormwood are used into supercritical carbon dioxide cyclic countercurrent extraction method, fennel seeds and Chinese mugwort is obtained The extract of grass, it is standby;
3)By the wall fern, eclipta, mulberry leaf, blackspiked lovegrass herb with root, achyranthes aspera, folium isatidis, cassia bark, polygala, trehalose, 150- is crushed to 230 mesh, soak, stirring, ultrasonic-leaching after adding the ethanol of 73-83%;
4)Filtered after ultrasonic-leaching, concentration is stirred after the extract that fennel seeds and wormwood are added in filtered fluid;
5)The concentrate that will be obtained is sterilized using moist hear heat test, obtains preservation after growth regulator.
Preferably, the method for dried process is to be placed in the environment of 50-63 DEG C in step 1, with 72-84 DEG C of hot air drying Dry, drying time is 27-46min, the moisture on removal Chinese herbal medicine surface, prevents Chinese herbal medicine surface bacteria from growing.
Preferably, in step 3 during ultrasonic-leaching under 58-64 DEG C of counterflow condition, extraction time is 10-23h, is adopted Solubility of the Chinese herbal medicine in ethanol solution is improved with ultrasonic-leaching, extraction can be more easy under 58-64 DEG C of counterflow condition.
Preferably, the quality that ethanol is added in step 3 is 3.4-5.3 times of Chinese herbal medicine quality, Chinese herbal medicine is improved in second Solubility in alcoholic solution.
Preferably, soak time is 21-43h in step 3, Chinese herbal medicine is promoted fully to dissolve.
Preferably, it is 0.2- with the mass ratio of filtered fluid that the quality of the extract of fennel seeds and wormwood is added in step 4 0.4:1, cold-resistant Chinese herbal medicine is added in growth regulator, improve the biological cold tolerance in growth.
Preferably, sterilising temp is 119-130 DEG C in step 5, sterilize 20-30min, eliminates the fungi in growth regulator, Improve the effect of growth regulator.
Preferably, the mode of preservation is dried, lucifuge to be placed in 10-25 DEG C in step 5.
Beneficial effect:This low-temperature-resistance growth substance that the present invention is provided and preparation method thereof, prepares simple, operation strategies Extensively, provide promote biological growth when and improve biology cold tolerance, prevent from making biological death during low temperature.Fennel seeds and wormwood Addition, associated with by with eclipta, mulberry leaf, blackspiked lovegrass herb with root, produce unexpected effect, improve the resistance energy of plant, especially It is particularly evident to cold-resistant effect, and a kind of low-temperature-resistance growth substance and its preparation side are provided present invention employs above-mentioned technical proposal Method, compensate for the deficiencies in the prior art, reasonable in design, easy to operate.
Specific embodiment
Following examples are described in further detail:
Embodiment 1:
A kind of low-temperature-resistance growth substance, the growth regulator includes following component and its weight portion:18 parts of the wall fern, 7 parts of eclipta, mulberry 10 parts of leaf, 13 parts of blackspiked lovegrass herb with root, 18 parts of achyranthes aspera, 13 parts of folium isatidis, 14 parts of cassia bark, 16 parts of polygala, 18 parts of trehalose, fennel seeds 0.2 part, 0.9 part of wormwood.
A kind of preparation method of low-temperature-resistance growth substance, comprises the following steps:
1)Dried process after being chosen each composition, cleaned with clear water by above-mentioned weight portion;
2)Dried fennel seeds and wormwood are used into supercritical carbon dioxide cyclic countercurrent extraction method, fennel seeds and Chinese mugwort is obtained The extract of grass, it is standby;
3)By the wall fern, eclipta, mulberry leaf, blackspiked lovegrass herb with root, achyranthes aspera, folium isatidis, cassia bark, polygala, trehalose, 230 mesh are crushed to, Soaked after adding 73% ethanol, stirring, ultrasonic-leaching;
4)Filtered after ultrasonic-leaching, concentration is stirred after the extract that fennel seeds and wormwood are added in filtered fluid;
5)The concentrate that will be obtained is sterilized using moist hear heat test, obtains preservation after growth regulator.
To be placed in the environment of 62 DEG C, with 76 DEG C of heated-air drying, drying time is the method for dried process in step 1 35min, the moisture on removal Chinese herbal medicine surface prevents Chinese herbal medicine surface bacteria from growing.
In step 3 during ultrasonic-leaching under 58 DEG C of counterflow condition, extraction time is 20h, is carried using ultrasonic-leaching Solubility of the Chinese herbal medicine high in ethanol solution, can more be easy to extraction under 58 DEG C of counterflow condition.
It is 4.3 times of Chinese herbal medicine quality that the quality of ethanol is added in step 3, improves dissolving of the Chinese herbal medicine in ethanol solution Degree.
Soak time is 32h in step 3, promotes Chinese herbal medicine fully to dissolve.
The quality of extract and the mass ratio of filtered fluid that fennel seeds and wormwood are added in step 4 are 0.2-0.4:1, helping Cold-resistant Chinese herbal medicine is added in agent long, the biological cold tolerance in growth is improved.
Sterilising temp is 119 DEG C in step 5, and sterilize 20min, eliminates the fungi in growth regulator, improves the effect of growth regulator.
The mode of preservation is dried, lucifuge to be placed in 20 DEG C in step 5.
Embodiment 2:
A kind of occupation mode in plant of low-temperature-resistance growth substance of the invention is poured for immersion, foliar spray or soil, is pressed The formula of above-mentioned growth regulator chooses 25 parts of the Chinese herbal medicine wall fern, 8 parts of eclipta, 15 parts of mulberry leaf, 10 parts of blackspiked lovegrass herb with root, achyranthes aspera 10 Part, 23 parts of folium isatidis, 10 parts of cassia bark, 20 parts of polygala, 15 parts of trehalose, 0.7 part of fennel seeds, 0.6 part of wormwood, are prepared into growth encourage Agent, then chooses the good rice seedlings of growing way and is divided into some regions and be placed in a low temperature of 9 DEG C, will encourage 500 times of dilution agent, 1000 times, 1500, be sprayed on Rice Leaf in the form of foliar spray respectively, with sprinkling in every 4 days once, contrasted after sprinkling 5 times Table one shown in:
The different multiples growth regulator of table one is sprayed at field rice growth result situation
Extension rate 500 times 1000 times 1500 times Do not spray growth regulator
Survival rate 100% 93.72% 86.54% 35.67%
By the gained of table one, the growth using the growth regulator of 500 times of dilution to paddy rice most has effect.
Specific embodiment described herein is only to explanation for example of the invention.The technical field of the invention Technical staff can be made various modifications or supplement to described specific embodiment or be substituted using similar mode, but Without departing from of the invention or surmount scope defined in appended claims.

Claims (9)

1. a kind of low-temperature-resistance growth substance, it is characterised in that the growth regulator includes following component and its weight portion:Wall fern 18- 25 parts, eclipta 5-10 parts, mulberry leaf 8-15 parts, blackspiked lovegrass herb with root 10-15 parts, achyranthes aspera 10-20 parts, folium isatidis 10-23 parts, cassia bark 10-15 parts, polygala 10-20 parts, trehalose 15-20 parts, fennel seeds 0.2-0.7 parts, wormwood 0.5-0.9 parts.
2. a kind of preparation method of low-temperature-resistance growth substance, it is characterised in that comprise the following steps:
1)Dried process after being chosen each composition, cleaned with clear water by above-mentioned weight portion;
2)Dried fennel seeds and wormwood are used into supercritical carbon dioxide cyclic countercurrent extraction method, fennel seeds and Chinese mugwort is obtained The extract of grass, it is standby;
3)By the wall fern, eclipta, mulberry leaf, blackspiked lovegrass herb with root, achyranthes aspera, folium isatidis, cassia bark, polygala, trehalose, 150-230 is crushed Mesh, soaks, stirring, ultrasonic-leaching after adding the ethanol of 73-83%;
4)Filtered after ultrasonic-leaching, concentration is stirred after the extract that fennel seeds and wormwood are added in filtered fluid;
5)The concentrate that will be obtained is sterilized using moist hear heat test, obtains preservation after growth regulator.
3. the preparation method of a kind of low-temperature-resistance growth substance according to claim 1, it is characterised in that:Done in the step 1 To be placed in the environment of 50-63 DEG C, with 72-84 DEG C of heated-air drying, drying time is 27-46min to the method for dry treatment.
4. the preparation method of a kind of low-temperature-resistance growth substance according to claim 1, it is characterised in that:Surpass in the step 3 During sound wave extraction under 58-64 DEG C of counterflow condition, extraction time is 10-23h.
5. the preparation method of a kind of low-temperature-resistance growth substance according to claim 1, it is characterised in that:Add in the step 3 The quality for entering ethanol is 3.4-5.3 times of Chinese herbal medicine quality.
6. the preparation method of a kind of low-temperature-resistance growth substance according to claim 1, it is characterised in that:Soaked in the step 3 The bubble time is 21-43h.
7. the preparation method of a kind of low-temperature-resistance growth substance according to claim 1, it is characterised in that:Add in the step 4 The quality of extract and the mass ratio of filtered fluid for entering fennel seeds and wormwood are 0.2-0.4:1.
8. the preparation method of a kind of low-temperature-resistance growth substance according to claim 1, it is characterised in that:Gone out in the step 5 Bacterium temperature is 119-130 DEG C, and sterilize 20-30min.
9. the preparation method of a kind of low-temperature-resistance growth substance according to claim 1, it is characterised in that:Protected in the step 5 The mode of Tibetan is dried, lucifuge to be placed in 10-25 DEG C.
CN201710048909.8A 2017-01-23 2017-01-23 A kind of low-temperature-resistance growth substance and preparation method thereof Pending CN106818948A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102763691A (en) * 2012-06-28 2012-11-07 乌鲁木齐木易联华生物科技有限公司 Preparation method of nuisanceless plant pesticide
CN103349007A (en) * 2013-07-26 2013-10-16 海南正业中农高科股份有限公司 Agricultural composition containing antibiotics and plant source materials and application thereof
CN103733921A (en) * 2013-12-05 2014-04-23 时洪良 Anti-freezing agent for trees
CN105104450A (en) * 2015-09-18 2015-12-02 王素敏 Spraying fluid capable of preventing trunk from freezing and bursting

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102763691A (en) * 2012-06-28 2012-11-07 乌鲁木齐木易联华生物科技有限公司 Preparation method of nuisanceless plant pesticide
CN103349007A (en) * 2013-07-26 2013-10-16 海南正业中农高科股份有限公司 Agricultural composition containing antibiotics and plant source materials and application thereof
CN103733921A (en) * 2013-12-05 2014-04-23 时洪良 Anti-freezing agent for trees
CN105104450A (en) * 2015-09-18 2015-12-02 王素敏 Spraying fluid capable of preventing trunk from freezing and bursting

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
邓如福等: "海藻糖对水稻幼苗抗寒性研究", 《西南农业大学学报》 *

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Application publication date: 20170613