CN103288552A - Compound fertilizer for preventing woodbine powdery mildew and preparation method thereof - Google Patents

Compound fertilizer for preventing woodbine powdery mildew and preparation method thereof Download PDF

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Publication number
CN103288552A
CN103288552A CN2013102605184A CN201310260518A CN103288552A CN 103288552 A CN103288552 A CN 103288552A CN 2013102605184 A CN2013102605184 A CN 2013102605184A CN 201310260518 A CN201310260518 A CN 201310260518A CN 103288552 A CN103288552 A CN 103288552A
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fermentation
parts
subtilis
agent
preparation
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CN103288552B (en
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吴志刚
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Suzhou Herun Agricultural Science & Technology Co Ltd
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Suzhou Herun Agricultural Science & Technology Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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Abstract

The invention relates to a compound fertilizer for preventing woodbine powdery mildew and a preparation method thereof. The compound fertilizer is prepared from the following raw materials in parts by weight: 1-15 parts of stellera chamaejasme, 5-10 parts of hops, 25-30 parts of peppers and 25-30 parts of gingko seed coat. The compound fertilizer for preventing woodbine powdery mildew can be used for preventing and killing off farmland weeds, and is broad-spectrum in sterilization characteristics. Compared with the prior art, the dosage form disclosed by the invention has the characteristics of being good in weeding effect, safe to the environment and less in possibility of generating drug resistance by weeds and the like, and is board in application prospect.

Description

A kind of control five leaf Root of Cream Clematis Powdery Mildew compound fertilizer and preparation method thereof
Technical field
The invention belongs to the nuisanceless fertilizer technical field, relate to compound fertilizer of a kind of control five leaf Root of Cream Clematis Powdery Mildews and preparation method thereof.
Background technology
Clematis ( ClematisL.) the plant whole world is about 300 kinds, is widely distributed in the north temperate zone, and about 110 kinds of China mainly is distributed in southwest, the Northwest.This platymiscium is strong because of adaptability, florescence length has very high ornamental plantation and is worth, but uses less at present in China gardens.Five leaf Root of Cream Clematis ( Clematis quinquefoliolataHutch.), have another name called the willow leaf Radix Zanthoxyli Spinifolii, the Ranunculaceae Clematis.This kind of herb can be used as medicine, but wind-damp dispelling cures mainly chronic rheumatic arthritis, arthralgia etc.
Handle seed with plant-growth regulator and temperature control, improve seed vitality, strengthen the emerge germination rate of seed in adverse circumstance, the treatment technology of plant seedlings being controlled prosperous short weak, strong seedling strong sprout is well used in other Root of Cream Clematis kind, such as uandarin clematis, Herba clematidis intricatae etc., but yet there are no report for the research of five leaf Root of Cream Clematis fertilizer.Main disease is Powdery Mildew, wherein Powdery Mildew harm Japanese Honeysuckle blade and tender stem.Circular white velvet-like mildew appears in the blade their early stage, after constantly enlarge, connect in flakes, form white amyloid plaque not of uniform size.Cause fallen flowers at last, the leaf that withers, make branch withered; At present single for the method for preventing and treating of Powdery Mildew, generally only prevent and treat by spraying chemical agent, yet only chemical agent to be cured the symptoms, not the disease, effect is undesirable.
The fertilizer of prior art only has the trophic function of fertilizer at present, does not have the effect of killing plant insect.Market in urgent need is a kind of to be conducive to environment protection, can effectively utilize organic waste, slow, sterilization, weeding, and can be fit to the big nuisanceless bactericidal and herbicidal compound of the plant fertilizer of producing.
Summary of the invention
A kind of control five leaf Root of Cream Clematis Powdery Mildew compound fertilizer and preparation method thereof, it is characterized in that it is obtained by the feedstock production of following parts by weight: bacillus amyloliquefaciens 0.8-1 part, Bacillus thuringiensis 0.6-0.8 part, subtilis 0.5-0.7 part, milk-acid bacteria 0.4-0.8 part, substrate fermentation agent 1-3 part, maize straw 30-35 part, peat composed of rotten mosses 20-30 part, flyash 30-36 part, mushroom slag 10-20 part, expanded pig manure 30-40 part, methyl synergy phosphorus powder agent 2-4 part, Piperonyl Butoxide pulvis 1-3 part, ethrel 0.4-0.6 part, urea 12-16 part, diammonium phosphate 10-12 part, vitriolate of tartar 6-8 part, Seed of Chinese Soapberry 55-60 part, three-coloured amaranth 10-20 part, Cortex Meliae 10-30 part, Rangooncreeper Fruit 15-25 part, Turkey-galls 1-15 part, Root of Pubescent Holly 5-15 part, matrine 5-10 part, fructus ulmi 10-15 part, camphor 5-15 part, Semen Momordicae 5-15 part, Golden Larch Bark 10-15 part.
Special-purpose fertile preparation method may further comprise the steps:
(1) multiplication culture of microorganism: bacillus amyloliquefaciens, Bacillus thuringiensis, subtilis, lactic bacterium strains are inoculated into respectively on the substratum, control the condition of fermentation separately well, final bacteria containing amount or gemma amount 〉=6 * 10 separately 9Individual/ml, make bacterium liquid;
(2) Bacillus thuringiensis, subtilis, lactic acid bacterial liquid and pig manure are carried out solid fermentation, turning every day is 1 time in the solid fermentation process, make the solid fermentation temperature be no more than 50 ℃, finish through fermentation in 6-8 days, Bacillus thuringiensis, subtilis, milk-acid bacteria continue to expand numerous simultaneously, obtain Bacillus thuringiensis microbial inoculum, bacillus subtilis microbial agent, milk-acid bacteria microbial inoculum, and the content of various microbial inoculums reaches 5 * 10 9Individual/more than the g;
(3) join the substrate fermentation agent in the mixture of maize straw, the peat composed of rotten mosses, flyash, mushroom slag according to described ratio, throwing is turned in mechanize, the timed interval be 1-2 days once, control temperature well, the solid fermentation temperature is no more than 60 ℃, when finding that material is loose, do not have the original stink of material, and the ammonia flavor is arranged slightly, fermentation finishes when producing white hypha in the heap, general process obtained the fermented product that moisture content is 35-40% in 8-10 days, and the microorganism in the substrate fermentation agent obtains expanding numerous simultaneously;
(4) material that step (2) and step (3) are made mixes, and after-ripening 2-3 days, in the after-ripening process turning every day once, turning is 2-4 time altogether, the last water content that is no more than in temperature under 60 ℃ the condition microbial organic fertilizer is evaporated to below 30%;
(5) preparation of plant-sourced extract: get Seed of Chinese Soapberry, three-coloured amaranth, Cortex Meliae, Rangooncreeper Fruit, Turkey-galls, Root of Pubescent Holly, matrine, fructus ulmi, camphor, Semen Momordicae, Golden Larch Bark according to described parts by weight, in water, soak after 2 hours, being warmed to 50 ℃ kept 20 minutes, the cellulase that adds (10 parts unit of activity is 150U) carries out enzymolysis then, the enzyme digestion reaction temperature is 30 ℃, the enzyme digestion reaction time is 1 hour, filters to obtain Chinese herbal medicine fluid; With 300 parts of 75% alcohol immersion 80min that add 10 times of weight of the described herbal liquid medicine that makes, be heated to 70 ℃ times and heat up in a steamer 45min, filter, collect extracting solution; Filter residue adds 70% ethanol of 5 times of weight again, is heated to 80 ℃ and returns and to heat up in a steamer 65min, filters, and collects extracting solution, and relative density is 1.6 medicinal extract when being evaporated to 65 ℃ through (0.08Mpa, 60 ℃), and spraying drying gets dry extract;
(6) with urea, diammonium phosphate, vitriolate of tartar, the agent of methyl synergy phosphorus powder, Piperonyl Butoxide pulvis, ethrel, with step (5) in the dry extract for preparing even according to described mixed, add water dissolving; And then mix with material that step (4) makes, stir;
(7) dry, pulverize, make finished product: above-mentioned material is dried through fluidized-bed, and temperature control is at 90 ℃ below the degree, and water content is controlled in the 10-15% scope, crushing screening, and fineness reaches 80 orders; Send into the cylinder tablets press after crushed with travelling belt then, uperize makes material be heated to 50-60 ℃ in cylinder, moves by not stall of cylinder and makes the material balling-up; Then drying roller is sent in balling-up, the input hot-air seasoning cools off, screening, canned one-tenth finished product again.
Useful technique effect:
The special-purpose fertilizer of the polynary microorganism of this Powdery Mildew of control of the present invention's preparation can make sickness rate reduce greatly, bacterium and the fungal disease of leaf portion are obviously reduced, and plant strain growth is more vigorous, and the output of asparagus is greatly enhanced, quality also improves, and the probiotic bacterium in the soil also increases.
Embodiment
The present invention is described in further detail by the following examples, but should be appreciated that the present invention is not in following examples.
Embodiment 1:
A kind of control five leaf Root of Cream Clematis Powdery Mildew compound fertilizer and preparation method thereof, it is characterized in that it is obtained by the feedstock production of following parts by weight: bacillus amyloliquefaciens 0.8-1 part, Bacillus thuringiensis 0.6-0.8 part, subtilis 0.5-0.7 part, milk-acid bacteria 0.4-0.8 part, substrate fermentation agent 1-3 part, maize straw 30-35 part, peat composed of rotten mosses 20-30 part, flyash 30-36 part, mushroom slag 10-20 part, expanded pig manure 30-40 part, methyl synergy phosphorus powder agent 2-4 part, Piperonyl Butoxide pulvis 1-3 part, ethrel 0.4-0.6 part, urea 12-16 part, diammonium phosphate 10-12 part, vitriolate of tartar 6-8 part, Seed of Chinese Soapberry 55-60 part, three-coloured amaranth 10-20 part, Cortex Meliae 10-30 part, Rangooncreeper Fruit 15-25 part, Turkey-galls 1-15 part, Root of Pubescent Holly 5-15 part, matrine 5-10 part, fructus ulmi 10-15 part, camphor 5-15 part, Semen Momordicae 5-15 part, Golden Larch Bark 10-15 part.
Special-purpose fertile preparation method may further comprise the steps:
(1) multiplication culture of microorganism: bacillus amyloliquefaciens, Bacillus thuringiensis, subtilis, lactic bacterium strains are inoculated into respectively on the substratum, control the condition of fermentation separately well, final bacteria containing amount or gemma amount 〉=6 * 10 separately 9Individual/ml, make bacterium liquid;
(2) Bacillus thuringiensis, subtilis, lactic acid bacterial liquid and pig manure are carried out solid fermentation, turning every day is 1 time in the solid fermentation process, make the solid fermentation temperature be no more than 50 ℃, finish through fermentation in 6-8 days, Bacillus thuringiensis, subtilis, milk-acid bacteria continue to expand numerous simultaneously, obtain Bacillus thuringiensis microbial inoculum, bacillus subtilis microbial agent, milk-acid bacteria microbial inoculum, and the content of various microbial inoculums reaches 5 * 10 9Individual/more than the g;
(3) join the substrate fermentation agent in the mixture of maize straw, the peat composed of rotten mosses, flyash, mushroom slag according to described ratio, throwing is turned in mechanize, the timed interval be 1-2 days once, control temperature well, the solid fermentation temperature is no more than 60 ℃, when finding that material is loose, do not have the original stink of material, and the ammonia flavor is arranged slightly, fermentation finishes when producing white hypha in the heap, general process obtained the fermented product that moisture content is 35-40% in 8-10 days, and the microorganism in the substrate fermentation agent obtains expanding numerous simultaneously;
(4) material that step (2) and step (3) are made mixes, and after-ripening 2-3 days, in the after-ripening process turning every day once, turning is 2-4 time altogether, the last water content that is no more than in temperature under 60 ℃ the condition microbial organic fertilizer is evaporated to below 30%;
(5) preparation of plant-sourced extract: get Seed of Chinese Soapberry, three-coloured amaranth, Cortex Meliae, Rangooncreeper Fruit, Turkey-galls, Root of Pubescent Holly, matrine, fructus ulmi, camphor, Semen Momordicae, Golden Larch Bark according to described parts by weight, in water, soak after 2 hours, being warmed to 50 ℃ kept 20 minutes, the cellulase that adds (10 parts unit of activity is 150U) carries out enzymolysis then, the enzyme digestion reaction temperature is 30 ℃, the enzyme digestion reaction time is 1 hour, filters to obtain Chinese herbal medicine fluid; With 300 parts of 75% alcohol immersion 80min that add 10 times of weight of the described herbal liquid medicine that makes, be heated to 70 ℃ times and heat up in a steamer 45min, filter, collect extracting solution; Filter residue adds 70% ethanol of 5 times of weight again, is heated to 80 ℃ and returns and to heat up in a steamer 65min, filters, and collects extracting solution, and relative density is 1.6 medicinal extract when being evaporated to 65 ℃ through (0.08Mpa, 60 ℃), and spraying drying gets dry extract;
(6) with urea, diammonium phosphate, vitriolate of tartar, the agent of methyl synergy phosphorus powder, Piperonyl Butoxide pulvis, ethrel, with step (5) in the dry extract for preparing even according to described mixed, add water dissolving; And then mix with material that step (4) makes, stir;
(7) dry, pulverize, make finished product: above-mentioned material is dried through fluidized-bed, and temperature control is at 90 ℃ below the degree, and water content is controlled in the 10-15% scope, crushing screening, and fineness reaches 80 orders; Send into the cylinder tablets press after crushed with travelling belt then, uperize makes material be heated to 50-60 ℃ in cylinder, moves by not stall of cylinder and makes the material balling-up; Then drying roller is sent in balling-up, the input hot-air seasoning cools off, screening, canned one-tenth finished product again.
The polynary microbial fertilizer of table 1 the present invention preparation and comparing
Powdery Mildew reduction (%) Fresh weight increment (%) Soil probiotics increment (%)
Embodiment 1 69 21 40
The result shows, the special-purpose fertilizer of the polynary microorganism of this Powdery Mildew of control of the present invention's preparation can make sickness rate reduce greatly, bacterium and the fungal disease of leaf portion are obviously reduced, plant strain growth is more vigorous, the output of asparagus is greatly enhanced, quality also improves, and the probiotic bacterium in the soil also increases.

Claims (2)

1. prevent and treat five leaf Root of Cream Clematis Powdery Mildew compound fertilizer and preparation method thereof for one kind, it is characterized in that it is obtained by the feedstock production of following parts by weight: bacillus amyloliquefaciens 0.8-1 part, Bacillus thuringiensis 0.6-0.8 part, subtilis 0.5-0.7 part, milk-acid bacteria 0.4-0.8 part, substrate fermentation agent 1-3 part, maize straw 30-35 part, peat composed of rotten mosses 20-30 part, flyash 30-36 part, mushroom slag 10-20 part, expanded pig manure 30-40 part, methyl synergy phosphorus powder agent 2-4 part, Piperonyl Butoxide pulvis 1-3 part, ethrel 0.4-0.6 part, urea 12-16 part, diammonium phosphate 10-12 part, vitriolate of tartar 6-8 part, Seed of Chinese Soapberry 55-60 part, three-coloured amaranth 10-20 part, Cortex Meliae 10-30 part, Rangooncreeper Fruit 15-25 part, Turkey-galls 1-15 part, Root of Pubescent Holly 5-15 part, matrine 5-10 part, fructus ulmi 10-15 part, camphor 5-15 part, Semen Momordicae 5-15 part, Golden Larch Bark 10-15 part.
2. the special-purpose fertile preparation method of complex microorganism according to claim 1 is characterized in that, may further comprise the steps:
(1) multiplication culture of microorganism: bacillus amyloliquefaciens, Bacillus thuringiensis, subtilis, lactic bacterium strains are inoculated into respectively on the substratum, control the condition of fermentation separately well, final bacteria containing amount or gemma amount 〉=6 * 10 separately 9Individual/ml, make bacterium liquid;
(2) Bacillus thuringiensis, subtilis, lactic acid bacterial liquid and pig manure are carried out solid fermentation, turning every day is 1 time in the solid fermentation process, make the solid fermentation temperature be no more than 50 ℃, finish through fermentation in 6-8 days, Bacillus thuringiensis, subtilis, milk-acid bacteria continue to expand numerous simultaneously, obtain Bacillus thuringiensis microbial inoculum, bacillus subtilis microbial agent, milk-acid bacteria microbial inoculum, and the content of various microbial inoculums reaches 5 * 10 9Individual/more than the g;
(3) join the substrate fermentation agent in the mixture of maize straw, the peat composed of rotten mosses, flyash, mushroom slag according to described ratio, throwing is turned in mechanize, the timed interval be 1-2 days once, control temperature well, the solid fermentation temperature is no more than 60 ℃, when finding that material is loose, do not have the original stink of material, and the ammonia flavor is arranged slightly, fermentation finishes when producing white hypha in the heap, general process obtained the fermented product that moisture content is 35-40% in 8-10 days, and the microorganism in the substrate fermentation agent obtains expanding numerous simultaneously;
(4) material that step (2) and step (3) are made mixes, and after-ripening 2-3 days, in the after-ripening process turning every day once, turning is 2-4 time altogether, the last water content that is no more than in temperature under 60 ℃ the condition microbial organic fertilizer is evaporated to below 30%;
(5) preparation of plant-sourced extract: get Seed of Chinese Soapberry, three-coloured amaranth, Cortex Meliae, Rangooncreeper Fruit, Turkey-galls, Root of Pubescent Holly, matrine, fructus ulmi, camphor, Semen Momordicae, Golden Larch Bark according to described parts by weight, in water, soak after 2 hours, being warmed to 50 ℃ kept 20 minutes, the cellulase that adds (10 parts unit of activity is 150U) carries out enzymolysis then, the enzyme digestion reaction temperature is 30 ℃, the enzyme digestion reaction time is 1 hour, filters to obtain Chinese herbal medicine fluid; With 300 parts of 75% alcohol immersion 80min that add 10 times of weight of the described herbal liquid medicine that makes, be heated to 70 ℃ times and heat up in a steamer 45min, filter, collect extracting solution; Filter residue adds 70% ethanol of 5 times of weight again, is heated to 80 ℃ and returns and to heat up in a steamer 65min, filters, and collects extracting solution, and relative density is 1.6 medicinal extract when being evaporated to 65 ℃ through (0.08Mpa, 60 ℃), and spraying drying gets dry extract;
(6) with urea, diammonium phosphate, vitriolate of tartar, the agent of methyl synergy phosphorus powder, Piperonyl Butoxide pulvis, ethrel, with step (5) in the dry extract for preparing even according to described mixed, add water dissolving; And then mix with material that step (4) makes, stir;
(7) dry, pulverize, make finished product: above-mentioned material is dried through fluidized-bed, and temperature control is at 90 ℃ below the degree, and water content is controlled in the 10-15% scope, crushing screening, and fineness reaches 80 orders; Send into the cylinder tablets press after crushed with travelling belt then, uperize makes material be heated to 50-60 ℃ in cylinder, moves by not stall of cylinder and makes the material balling-up; Then drying roller is sent in balling-up, the input hot-air seasoning cools off, screening, canned one-tenth finished product again.
CN201310260518.4A 2013-06-27 2013-06-27 Compound fertilizer for preventing woodbine powdery mildew and preparation method thereof Expired - Fee Related CN103288552B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103570471A (en) * 2013-11-08 2014-02-12 苏州市相城区渭塘凤凰泾农业发展有限公司 Nanometer carrier fertilizer for preventing and controlling powdery mildew of woodbind and preparation method thereof
CN103636599A (en) * 2013-11-19 2014-03-19 湖北省生物农药工程研究中心 Preparation method of high-content dry Bacillus thuringiensis suspension
CN104030850A (en) * 2014-06-30 2014-09-10 桂林丰茂源农业技术开发有限公司 Lentinula edodes culture medium in which hop residues are added and preparing method thereof
CN105191638A (en) * 2015-10-14 2015-12-30 吉首大学 Method for returning all maize straw to field during harvesting
CN105384527A (en) * 2015-11-25 2016-03-09 高青山 Organic-inorganic compound fertilizer for high-yield paddy rice
CN105481560A (en) * 2015-12-23 2016-04-13 成都新柯力化工科技有限公司 Multifunctional organic water soluble fertilizer resisting plant diseases and insect pests and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1119178A (en) * 1995-08-31 1996-03-27 金尧 Yeast microbial fertilizer and producing process thereof
CN1238321A (en) * 1998-06-08 1999-12-15 张显军 Formula and process for preparing efficient biofertilizer
CN101200390A (en) * 2007-12-26 2008-06-18 李珍发 Production technique of organic fertilizer
CN101468933A (en) * 2007-12-24 2009-07-01 韩庆岭 Biological silicon fertilizer
CN101619001A (en) * 2008-07-03 2010-01-06 许吉雷 Preparation method of culture fertilizer for cultivating amaranth

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1119178A (en) * 1995-08-31 1996-03-27 金尧 Yeast microbial fertilizer and producing process thereof
CN1238321A (en) * 1998-06-08 1999-12-15 张显军 Formula and process for preparing efficient biofertilizer
CN101468933A (en) * 2007-12-24 2009-07-01 韩庆岭 Biological silicon fertilizer
CN101200390A (en) * 2007-12-26 2008-06-18 李珍发 Production technique of organic fertilizer
CN101619001A (en) * 2008-07-03 2010-01-06 许吉雷 Preparation method of culture fertilizer for cultivating amaranth

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103570471A (en) * 2013-11-08 2014-02-12 苏州市相城区渭塘凤凰泾农业发展有限公司 Nanometer carrier fertilizer for preventing and controlling powdery mildew of woodbind and preparation method thereof
CN103636599A (en) * 2013-11-19 2014-03-19 湖北省生物农药工程研究中心 Preparation method of high-content dry Bacillus thuringiensis suspension
CN103636599B (en) * 2013-11-19 2015-03-18 湖北省生物农药工程研究中心 Preparation method of high-content dry Bacillus thuringiensis suspension
CN104030850A (en) * 2014-06-30 2014-09-10 桂林丰茂源农业技术开发有限公司 Lentinula edodes culture medium in which hop residues are added and preparing method thereof
CN104030850B (en) * 2014-06-30 2016-03-30 桂林丰茂源农业技术开发有限公司 A kind of mushroom culture medium adding hop residue and preparation method thereof
CN105191638A (en) * 2015-10-14 2015-12-30 吉首大学 Method for returning all maize straw to field during harvesting
CN105384527A (en) * 2015-11-25 2016-03-09 高青山 Organic-inorganic compound fertilizer for high-yield paddy rice
CN105481560A (en) * 2015-12-23 2016-04-13 成都新柯力化工科技有限公司 Multifunctional organic water soluble fertilizer resisting plant diseases and insect pests and preparation method thereof

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