CN103288552B - Compound fertilizer for preventing woodbine powdery mildew and preparation method thereof - Google Patents
Compound fertilizer for preventing woodbine powdery mildew and preparation method thereof Download PDFInfo
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- CN103288552B CN103288552B CN201310260518.4A CN201310260518A CN103288552B CN 103288552 B CN103288552 B CN 103288552B CN 201310260518 A CN201310260518 A CN 201310260518A CN 103288552 B CN103288552 B CN 103288552B
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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Abstract
The invention relates to a compound fertilizer for preventing woodbine powdery mildew and a preparation method thereof. The compound fertilizer is prepared from the following raw materials in parts by weight: 1-15 parts of stellera chamaejasme, 5-10 parts of hops, 25-30 parts of peppers and 25-30 parts of gingko seed coat. The compound fertilizer for preventing woodbine powdery mildew can be used for preventing and killing off farmland weeds, and is broad-spectrum in sterilization characteristics. Compared with the prior art, the dosage form disclosed by the invention has the characteristics of being good in weeding effect, safe to the environment and less in possibility of generating drug resistance by weeds and the like, and is board in application prospect.
Description
Technical field
The invention belongs to nuisanceless fertilizer technical field, relate to Chemical Mixed Fertilizer of a kind of control five leaf Root of Cream Clematis Powdery Mildews and preparation method thereof.
Background technology
Clematis (
clematisl.) approximately 300 kinds, the plant whole world, is widely distributed in north temperate zone, and approximately 110 kinds, China, is mainly distributed in southwest, the Northwest.This platymiscium is worth because strong adaptability, florescence length have very high ornamental plantation, but in China gardens, applies at present less.Five leaf Root of Cream Clematis (
clematis quinquefoliolatahutch.), have another name called willow leaf Radix Zanthoxyli Spinifolii, Ranunculaceae Clematis.This kind of herb can be used as medicine, can wind-damp dispelling, cure mainly chronic rheumatic arthritis, arthralgia etc.
With plant-growth regulator and temperature control processing seed, improve seed vitality, strengthen the emerge germination rate of seed in adverse circumstance, the treatment technology of plant seedlings being controlled to prosperous short weak, strong seedling strong sprout is well applied in other Root of Cream Clematis kind, such as uandarin clematis, Herba clematidis intricatae etc., but have not been reported for the research of five leaf Root of Cream Clematis fertilizer.Major Diseases is Powdery Mildew, wherein Powdery Mildew harm Japanese Honeysuckle blade and tender stem., there is circular white velvet-like mildew in blade their early stage, rear continuous expansion, connects in flakes, forms white amyloid plaque not of uniform size.Finally cause fallen flowers, the leaf that withers, make branch withered; At present single for the method for preventing and treating of Powdery Mildew, generally only prevent and treat by spraying chemical agent, but only Agro-chemicals control to be cured the symptoms, not the disease, effect is undesirable.
The fertilizer of currently available technology only has the trophic function of fertilizer, does not have the effect of killing plant insect.Market in urgent need one is conducive to environment protection, can effectively utilize organic waste, slow, sterilization, weeding, and can be applicable to the large nuisanceless bactericidal and herbicidal Chemical Mixed Fertilizer of plant of producing.
Summary of the invention
A kind of control five leaf Root of Cream Clematis Powdery Mildew Chemical Mixed Fertilizers and preparation method thereof, it is characterized in that, it is prepared by the raw material of following parts by weight: bacillus amyloliquefaciens 0.8-1 part, Bacillus thuringiensis 0.6-0.8 part, subtilis 0.5-0.7 part, milk-acid bacteria 0.4-0.8 part, substrate fermentation agent 1-3 part, maize straw 30-35 part, peat composed of rotten mosses 20-30 part, flyash 30-36 part, mushroom slag 10-20 part, expanded pig manure 30-40 part, methyl Synergistic Phosphorus pulvis 2-4 part, Piperonyl Butoxide pulvis 1-3 part, ethrel 0.4-0.6 part, urea 12-16 part, diammonium phosphate 10-12 part, potassium sulfate 6-8 part, Seed of Chinese Soapberry 55-60 part, three-coloured amaranth 10-20 part, Cortex Meliae 10-30 part, Rangooncreeper Fruit 15-25 part, Turkey-galls 1-15 part, Root of Pubescent Holly 5-15 part, matrine 5-10 part, fructus ulmi 10-15 part, camphor 5-15 part, Semen Momordicae 5-15 part, Golden Larch Bark 10-15 part.
The preparation method of special fertilizer, comprises the following steps:
(1) multiplication culture of microorganism: bacillus amyloliquefaciens, Bacillus thuringiensis, subtilis, lactic bacterium strains are inoculated into respectively on substratum, control the condition of fermentation separately well, final bacteria containing amount or gemma amount>=6 × 10 separately
9individual/ml, makes bacterium liquid;
(2) Bacillus thuringiensis, subtilis, lactic acid bacterial liquid and pig manure are carried out to solid fermentation, turning every day 1 time in solid fermentation process, make solid fermentation temperature be no more than 50 DEG C, through within 6-8 days, having fermented, Bacillus thuringiensis, subtilis, milk-acid bacteria continue to expand numerous simultaneously, obtain Bacillus thuringiensis microbial inoculum, bacillus subtilis microbial agent, milk-acid bacteria microbial inoculum, and the content of various microbial inoculums reaches 5 × 10
9individual/more than g;
(3) substrate fermentation agent is joined according to described ratio in the mixture of maize straw, the peat composed of rotten mosses, flyash, mushroom slag, throwing is turned in mechanize, the timed interval be 1-2 days once, control temperature well, solid fermentation temperature is no more than 60 DEG C, when finding that material is loose, there is no the original stink of material, and ammonia taste slightly, while producing white hypha in heap, ferment complete, general through within 8-10 days, obtaining the fermented product that moisture content is 35-40%, the microorganism in substrate fermentation agent obtains expanding numerous simultaneously;
(4) material step (2) and step (3) being made mixes, and after-ripening 2-3 days, and in After-ripening, once, turning 2-4 time altogether, is evaporated to the water content of microbial organic fertilizer below 30% under the last condition that is no more than 60 DEG C in temperature in turning every day;
(5) preparation of Extracts from Plant Recourses: get Seed of Chinese Soapberry, three-coloured amaranth, Cortex Meliae, Rangooncreeper Fruit, Turkey-galls, Root of Pubescent Holly, matrine, fructus ulmi, camphor, Semen Momordicae, Golden Larch Bark according to described parts by weight, in water, soak after 2 hours, being warmed to 50 DEG C keeps 20 minutes, then add the cellulase of (unit of activity of 10 parts is 150U) to carry out enzymolysis, enzyme digestion reaction temperature is 30 DEG C, the enzyme digestion reaction time is 1 hour, filters and obtains Chinese herbal medicine fluid; 300 parts of the described herbal liquid medicines making are added to 75% alcohol immersion 80min of 10 times of weight, be heated to 70 DEG C times and heat up in a steamer 45min, filter, collect extracting solution; Filter residue adds 70% ethanol of 5 times of weight again, is heated to 80 DEG C and returns and heat up in a steamer 65min, filters, and collects extracting solution, the medicinal extract that relative density is 1.6 in the time that (0.08Mpa, 60 DEG C) is evaporated to 65 DEG C, and spraying is dry, obtains dry extract;
(6), by urea, diammonium phosphate, potassium sulfate, methyl Synergistic Phosphorus pulvis, Piperonyl Butoxide pulvis, ethrel, mix according to described ratio with the dry extract preparing in step (5), add water dissolution; And then the material making with step (4) mixes, stir;
(7) dry, pulverize, make finished product: above-mentioned material is dried through fluidized-bed, and temperature is controlled at 90 DEG C below degree, and water content is controlled within the scope of 10-15%, pulverizes and sieves, and fineness reaches 80 orders; Then send into after crushed roller pelletizer with travelling belt, in cylinder, uperize makes heating material to 50-60 DEG C, is moved and is made material balling-up by not stall of cylinder; Then balling-up is sent into drying roller, input hot-air seasoning, more cooling, screening, canned one-tenth finished product.
Useful technique effect:
The polynary microorganism special fertilizer of this Powdery Mildew of control prepared by the present invention can make sickness rate greatly reduce, bacterium and the fungal disease of leaf portion are obviously reduced, and plant strain growth is more vigorous, and the output of asparagus is greatly enhanced, quality also improves, and the probiotic bacterium in soil also increases.
Embodiment
The present invention is described in further detail by the following examples, but should be appreciated that the present invention is not in following examples.
Embodiment 1:
A kind of control five leaf Root of Cream Clematis Powdery Mildew Chemical Mixed Fertilizers and preparation method thereof, it is characterized in that, it is prepared by the raw material of following parts by weight: bacillus amyloliquefaciens 0.8-1 part, Bacillus thuringiensis 0.6-0.8 part, subtilis 0.5-0.7 part, milk-acid bacteria 0.4-0.8 part, substrate fermentation agent 1-3 part, maize straw 30-35 part, peat composed of rotten mosses 20-30 part, flyash 30-36 part, mushroom slag 10-20 part, expanded pig manure 30-40 part, methyl Synergistic Phosphorus pulvis 2-4 part, Piperonyl Butoxide pulvis 1-3 part, ethrel 0.4-0.6 part, urea 12-16 part, diammonium phosphate 10-12 part, potassium sulfate 6-8 part, Seed of Chinese Soapberry 55-60 part, three-coloured amaranth 10-20 part, Cortex Meliae 10-30 part, Rangooncreeper Fruit 15-25 part, Turkey-galls 1-15 part, Root of Pubescent Holly 5-15 part, matrine 5-10 part, fructus ulmi 10-15 part, camphor 5-15 part, Semen Momordicae 5-15 part, Golden Larch Bark 10-15 part.
The preparation method of special fertilizer, comprises the following steps:
(1) multiplication culture of microorganism: bacillus amyloliquefaciens, Bacillus thuringiensis, subtilis, lactic bacterium strains are inoculated into respectively on substratum, control the condition of fermentation separately well, final bacteria containing amount or gemma amount>=6 × 10 separately
9individual/ml, makes bacterium liquid;
(2) Bacillus thuringiensis, subtilis, lactic acid bacterial liquid and pig manure are carried out to solid fermentation, turning every day 1 time in solid fermentation process, make solid fermentation temperature be no more than 50 DEG C, through within 6-8 days, having fermented, Bacillus thuringiensis, subtilis, milk-acid bacteria continue to expand numerous simultaneously, obtain Bacillus thuringiensis microbial inoculum, bacillus subtilis microbial agent, milk-acid bacteria microbial inoculum, and the content of various microbial inoculums reaches 5 × 10
9individual/more than g;
(3) substrate fermentation agent is joined according to described ratio in the mixture of maize straw, the peat composed of rotten mosses, flyash, mushroom slag, throwing is turned in mechanize, the timed interval be 1-2 days once, control temperature well, solid fermentation temperature is no more than 60 DEG C, when finding that material is loose, there is no the original stink of material, and ammonia taste slightly, while producing white hypha in heap, ferment complete, general through within 8-10 days, obtaining the fermented product that moisture content is 35-40%, the microorganism in substrate fermentation agent obtains expanding numerous simultaneously;
(4) material step (2) and step (3) being made mixes, and after-ripening 2-3 days, and in After-ripening, once, turning 2-4 time altogether, is evaporated to the water content of microbial organic fertilizer below 30% under the last condition that is no more than 60 DEG C in temperature in turning every day;
(5) preparation of Extracts from Plant Recourses: get Seed of Chinese Soapberry, three-coloured amaranth, Cortex Meliae, Rangooncreeper Fruit, Turkey-galls, Root of Pubescent Holly, matrine, fructus ulmi, camphor, Semen Momordicae, Golden Larch Bark according to described parts by weight, in water, soak after 2 hours, being warmed to 50 DEG C keeps 20 minutes, then add the cellulase of (unit of activity of 10 parts is 150U) to carry out enzymolysis, enzyme digestion reaction temperature is 30 DEG C, the enzyme digestion reaction time is 1 hour, filters and obtains Chinese herbal medicine fluid; 300 parts of the described herbal liquid medicines making are added to 75% alcohol immersion 80min of 10 times of weight, be heated to 70 DEG C times and heat up in a steamer 45min, filter, collect extracting solution; Filter residue adds 70% ethanol of 5 times of weight again, is heated to 80 DEG C and returns and heat up in a steamer 65min, filters, and collects extracting solution, the medicinal extract that relative density is 1.6 in the time that (0.08Mpa, 60 DEG C) is evaporated to 65 DEG C, and spraying is dry, obtains dry extract;
(6), by urea, diammonium phosphate, potassium sulfate, methyl Synergistic Phosphorus pulvis, Piperonyl Butoxide pulvis, ethrel, mix according to described ratio with the dry extract preparing in step (5), add water dissolution; And then the material making with step (4) mixes, stir;
(7) dry, pulverize, make finished product: above-mentioned material is dried through fluidized-bed, and temperature is controlled at 90 DEG C below degree, and water content is controlled within the scope of 10-15%, pulverizes and sieves, and fineness reaches 80 orders; Then send into after crushed roller pelletizer with travelling belt, in cylinder, uperize makes heating material to 50-60 DEG C, is moved and is made material balling-up by not stall of cylinder; Then balling-up is sent into drying roller, input hot-air seasoning, more cooling, screening, canned one-tenth finished product.
Polynary microbial fertilizer prepared by table 1 the present invention and comparing
Powdery Mildew reduction (%) | Fresh weight increment (%) | Soil probiotics increment (%) | |
Embodiment 1 | 69 | 21 | 40 |
Result shows, the polynary microorganism special fertilizer of this Powdery Mildew of control prepared by the present invention can make sickness rate greatly reduce, bacterium and the fungal disease of leaf portion are obviously reduced, plant strain growth is more vigorous, the output of asparagus is greatly enhanced, quality also improves, and the probiotic bacterium in soil also increases.
Claims (2)
1. control five leaf Root of Cream Clematis Powdery Mildew Chemical Mixed Fertilizers, it is characterized in that, it is prepared by the raw material of following parts by weight: bacillus amyloliquefaciens 0.8-1 part, Bacillus thuringiensis 0.6-0.8 part, subtilis 0.5-0.7 part, milk-acid bacteria 0.4-0.8 part, substrate fermentation agent 1-3 part, maize straw 30-35 part, peat composed of rotten mosses 20-30 part, flyash 30-36 part, mushroom slag 10-20 part, expanded pig manure 30-40 part, methyl Synergistic Phosphorus pulvis 2-4 part, Piperonyl Butoxide pulvis 1-3 part, ethrel 0.4-0.6 part, urea 12-16 part, diammonium phosphate 10-12 part, potassium sulfate 6-8 part, Seed of Chinese Soapberry 55-60 part, three-coloured amaranth 10-20 part, Cortex Meliae 10-30 part, Rangooncreeper Fruit 15-25 part, Turkey-galls 1-15 part, Root of Pubescent Holly 5-15 part, matrine 5-10 part, fructus ulmi 10-15 part, camphor 5-15 part, Semen Momordicae 5-15 part, Golden Larch Bark 10-15 part.
2. the preparation method of control five leaf Root of Cream Clematis Powdery Mildew Chemical Mixed Fertilizers according to claim 1, is characterized in that, comprises the following steps:
(1) multiplication culture of microorganism: bacillus amyloliquefaciens, Bacillus thuringiensis, subtilis, lactic bacterium strains are inoculated into respectively on substratum, control the condition of fermentation separately well, final bacteria containing amount or gemma amount>=6 × 10 separately
9individual/ml, makes bacterium liquid;
(2) bacillus amyloliquefaciens bacterium liquid, Bacillus thuringiensis bacterium liquid, subtilis bacterium liquid, lactic acid bacterial liquid and expanded pig manure are carried out to solid fermentation, turning every day 1 time in solid fermentation process, make solid fermentation temperature be no more than 50 DEG C, through within 6-8 days, having fermented, bacillus amyloliquefaciens, Bacillus thuringiensis, subtilis, milk-acid bacteria continue to expand numerous simultaneously, obtain bacillus amyloliquefaciens microbial inoculum, Bacillus thuringiensis microbial inoculum, bacillus subtilis microbial agent, milk-acid bacteria microbial inoculum, and the content of various microbial inoculums reaches 5 × 10
9individual/more than g;
(3) substrate fermentation agent is joined according to described ratio in the mixture of maize straw, the peat composed of rotten mosses, flyash, mushroom slag, throwing is turned in mechanize, the timed interval be 1-2 days once, control temperature well, solid fermentation temperature is no more than 60 DEG C, when finding that material is loose, there is no the original stink of material, and ammonia taste slightly, while producing white hypha in heap, ferment complete, through within 8-10 days, obtaining the fermented product that moisture content is 35-40%, the microorganism in substrate fermentation agent obtains expanding numerous simultaneously;
(4) material step (2) and step (3) being made mixes, and after-ripening 2-3 days, and in After-ripening, once, turning 2-4 time altogether, is evaporated to the water content of microbial organic fertilizer below 30% under the last condition that is no more than 60 DEG C in temperature in turning every day;
(5) preparation of Extracts from Plant Recourses: get Seed of Chinese Soapberry, three-coloured amaranth, Cortex Meliae, Rangooncreeper Fruit, Turkey-galls, Root of Pubescent Holly, matrine, fructus ulmi, camphor, Semen Momordicae, Golden Larch Bark according to described parts by weight, in water, soak after 2 hours, being warmed to 50 DEG C keeps 20 minutes, then the cellulase that the unit of activity that adds 10 parts is 150U carries out enzymolysis, enzyme digestion reaction temperature is 30 DEG C, the enzyme digestion reaction time is 1 hour, filters and obtains Chinese herbal medicine fluid; 300 parts of the described herbal liquid medicines making are added to 75% alcohol immersion 80min of 10 times of weight, be heated to 70 DEG C times and heat up in a steamer 45min, filter, collect extracting solution; Filter residue adds 70% ethanol of 5 times of weight again, is heated to 80 DEG C and returns and heat up in a steamer 65min, filters, and collects extracting solution, the medicinal extract that relative density is 1.6 in the time that 0.08Mpa, 60 DEG C are evaporated to 65 DEG C, and spraying is dry, obtains dry extract;
(6), by urea, diammonium phosphate, potassium sulfate, methyl Synergistic Phosphorus pulvis, Piperonyl Butoxide pulvis, ethrel, mix according to described ratio with the dry extract preparing in step (5), add water dissolution; And then the material making with step (4) mixes, stir;
(7) dry, pulverize, make finished product: above-mentioned material is dried through fluidized-bed, and temperature is controlled at below 90 DEG C, and water content is controlled within the scope of 10-15%, pulverizes and sieves, and fineness reaches 80 orders; Then send into after crushed roller pelletizer with travelling belt, in cylinder, uperize makes heating material to 50-60 DEG C, is moved and is made material balling-up by not stall of cylinder; Then balling-up is sent into drying roller, input hot-air seasoning, more cooling, screening, canned one-tenth finished product.
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CN103570471A (en) * | 2013-11-08 | 2014-02-12 | 苏州市相城区渭塘凤凰泾农业发展有限公司 | Nanometer carrier fertilizer for preventing and controlling powdery mildew of woodbind and preparation method thereof |
CN103636599B (en) * | 2013-11-19 | 2015-03-18 | 湖北省生物农药工程研究中心 | Preparation method of high-content dry Bacillus thuringiensis suspension |
CN104030850B (en) * | 2014-06-30 | 2016-03-30 | 桂林丰茂源农业技术开发有限公司 | A kind of mushroom culture medium adding hop residue and preparation method thereof |
CN105191638B (en) * | 2015-10-14 | 2017-09-12 | 吉首大学 | A kind of method of total crop return during maize straw harvest |
CN105384527A (en) * | 2015-11-25 | 2016-03-09 | 高青山 | Organic-inorganic compound fertilizer for high-yield paddy rice |
CN105481560A (en) * | 2015-12-23 | 2016-04-13 | 成都新柯力化工科技有限公司 | Multifunctional organic water soluble fertilizer resisting plant diseases and insect pests and preparation method thereof |
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CN1119178A (en) * | 1995-08-31 | 1996-03-27 | 金尧 | Yeast microbial fertilizer and producing process thereof |
CN1238321A (en) * | 1998-06-08 | 1999-12-15 | 张显军 | Formula and process for preparing efficient biofertilizer |
CN101200390A (en) * | 2007-12-26 | 2008-06-18 | 李珍发 | Production technique of organic fertilizer |
CN101468933A (en) * | 2007-12-24 | 2009-07-01 | 韩庆岭 | Biological silicon fertilizer |
CN101619001A (en) * | 2008-07-03 | 2010-01-06 | 许吉雷 | Preparation method of culture fertilizer for cultivating amaranth |
-
2013
- 2013-06-27 CN CN201310260518.4A patent/CN103288552B/en not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1119178A (en) * | 1995-08-31 | 1996-03-27 | 金尧 | Yeast microbial fertilizer and producing process thereof |
CN1238321A (en) * | 1998-06-08 | 1999-12-15 | 张显军 | Formula and process for preparing efficient biofertilizer |
CN101468933A (en) * | 2007-12-24 | 2009-07-01 | 韩庆岭 | Biological silicon fertilizer |
CN101200390A (en) * | 2007-12-26 | 2008-06-18 | 李珍发 | Production technique of organic fertilizer |
CN101619001A (en) * | 2008-07-03 | 2010-01-06 | 许吉雷 | Preparation method of culture fertilizer for cultivating amaranth |
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