CN102796033B - 一种清洁的d,l-蛋氨酸制备方法 - Google Patents
一种清洁的d,l-蛋氨酸制备方法 Download PDFInfo
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- CN102796033B CN102796033B CN201210320297.0A CN201210320297A CN102796033B CN 102796033 B CN102796033 B CN 102796033B CN 201210320297 A CN201210320297 A CN 201210320297A CN 102796033 B CN102796033 B CN 102796033B
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- methionine
- solution
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- ether
- methylmercaptoethyl
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- SNDPXSYFESPGGJ-UHFFFAOYSA-N CCCC(C(O)=O)N Chemical compound CCCC(C(O)=O)N SNDPXSYFESPGGJ-UHFFFAOYSA-N 0.000 description 1
- FFEARJCKVFRZRR-UHFFFAOYSA-N CSCCC(C(O)=O)N Chemical compound CSCCC(C(O)=O)N FFEARJCKVFRZRR-UHFFFAOYSA-N 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
- C07C323/50—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
- C07C323/51—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
- C07C323/57—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups
- C07C323/58—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups with amino groups bound to the carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
- C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
- C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D207/30—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having two double bonds between ring members or between ring members and non-ring members
- C07D207/34—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D207/36—Oxygen or sulfur atoms
- C07D207/38—2-Pyrrolones
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (6)
Priority Applications (14)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210320297.0A CN102796033B (zh) | 2012-09-03 | 2012-09-03 | 一种清洁的d,l-蛋氨酸制备方法 |
EP13833235.8A EP2894147B1 (en) | 2012-09-03 | 2013-01-06 | Clean method for preparing d,l-methionine |
US14/425,310 US9206120B2 (en) | 2012-09-03 | 2013-01-06 | Clean method for preparing D,L-methionine |
JP2015528838A JP6026663B2 (ja) | 2012-09-03 | 2013-01-06 | クリーンなdl−メチオニンの製造方法 |
RU2015111118/04A RU2604064C2 (ru) | 2012-09-03 | 2013-01-06 | Чистый метод приготовления d, l-метионина |
AU2013307993A AU2013307993B2 (en) | 2012-09-03 | 2013-01-06 | Clean method for preparing D,L-methionine |
ES13833235.8T ES2687247T3 (es) | 2012-09-03 | 2013-01-06 | Método de limpieza para preparar D,L-metionina |
KR1020157007639A KR101689366B1 (ko) | 2012-09-03 | 2013-01-06 | 청정 d,l-메티오닌 제조 방법 |
MX2015002752A MX362811B (es) | 2012-09-03 | 2013-01-06 | Método limpio de preparación de una d,l-metionina. |
BR112015004487A BR112015004487B1 (pt) | 2012-09-03 | 2013-01-06 | método para preparar d,l-metionina |
MYPI2015700650A MY191517A (en) | 2012-09-03 | 2013-01-06 | A clean method for preparing d, l-methionine |
PCT/CN2013/070129 WO2014032401A1 (zh) | 2012-09-03 | 2013-01-06 | 一种清洁的d,l-蛋氨酸制备方法 |
SG11201501553PA SG11201501553PA (en) | 2012-09-03 | 2013-01-06 | Clean method for preparing d,l-methionine |
ZA2015/02259A ZA201502259B (en) | 2012-09-03 | 2015-04-07 | Clean method for preparing d,l-methionine |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210320297.0A CN102796033B (zh) | 2012-09-03 | 2012-09-03 | 一种清洁的d,l-蛋氨酸制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102796033A CN102796033A (zh) | 2012-11-28 |
CN102796033B true CN102796033B (zh) | 2014-02-26 |
Family
ID=47195373
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201210320297.0A Active CN102796033B (zh) | 2012-09-03 | 2012-09-03 | 一种清洁的d,l-蛋氨酸制备方法 |
Country Status (14)
Country | Link |
---|---|
US (1) | US9206120B2 (zh) |
EP (1) | EP2894147B1 (zh) |
JP (1) | JP6026663B2 (zh) |
KR (1) | KR101689366B1 (zh) |
CN (1) | CN102796033B (zh) |
AU (1) | AU2013307993B2 (zh) |
BR (1) | BR112015004487B1 (zh) |
ES (1) | ES2687247T3 (zh) |
MX (1) | MX362811B (zh) |
MY (1) | MY191517A (zh) |
RU (1) | RU2604064C2 (zh) |
SG (1) | SG11201501553PA (zh) |
WO (1) | WO2014032401A1 (zh) |
ZA (1) | ZA201502259B (zh) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102796033B (zh) | 2012-09-03 | 2014-02-26 | 浙江新和成股份有限公司 | 一种清洁的d,l-蛋氨酸制备方法 |
JP2014108956A (ja) * | 2012-12-04 | 2014-06-12 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
CN105061193B (zh) * | 2015-08-10 | 2017-03-22 | 蓝星(北京)技术中心有限公司 | 蛋氨酸生产废水处理中回收有机物的方法 |
CN105296557A (zh) * | 2015-10-31 | 2016-02-03 | 高大元 | 一种D,L-α-蛋氨酸钙的合成方法 |
CN106119311A (zh) * | 2016-07-11 | 2016-11-16 | 雷春生 | 一种腐乳废水制备高纯蛋氨酸的方法 |
CN106432018A (zh) * | 2016-09-14 | 2017-02-22 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种d,l‑蛋氨酸的环保清洁生产方法 |
CN106432020B (zh) * | 2016-09-14 | 2018-11-20 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种d,l-蛋氨酸的分离纯化方法 |
CN106565608A (zh) * | 2016-09-30 | 2017-04-19 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种高纯度5‑(2‑甲硫基乙基)‑乙内酰脲的制备方法 |
EP3725770B1 (en) | 2017-12-13 | 2022-08-10 | Sumitomo Chemical Company, Limited | Method for producing methionine |
CN111491917B (zh) * | 2017-12-19 | 2022-03-22 | 住友化学株式会社 | 甲硫氨酸的制造方法 |
US20210017129A1 (en) * | 2017-12-27 | 2021-01-21 | Sumitomo Chemical Company, Limited | Refined methionine production method |
EP3733645B1 (en) * | 2017-12-28 | 2022-07-20 | Sumitomo Chemical Company, Limited | Method for producing methionine |
CN109232335B (zh) * | 2018-10-15 | 2021-02-26 | 天宝动物营养科技股份有限公司 | 一种蛋氨酸制备方法 |
KR20200138606A (ko) | 2019-06-01 | 2020-12-10 | 장환석 | 치약 칫솔 |
CN112445254B (zh) * | 2019-09-05 | 2022-11-08 | 中石油吉林化工工程有限公司 | 脱氢氰酸塔塔顶冷凝器液位与塔顶温度的控制系统及方法 |
CN111362453B (zh) * | 2020-03-18 | 2020-11-03 | 北京百灵天地环保科技股份有限公司 | 一种高矿化度煤矿矿井水达标处理及资源化利用装置及其使用方法 |
CN112661682B (zh) * | 2020-12-21 | 2023-08-01 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种生产dl-蛋氨酸的方法 |
CN112679399A (zh) * | 2020-12-22 | 2021-04-20 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种蛋氨酸结晶母液后处理方法及分离设备 |
CN112694428B (zh) * | 2020-12-24 | 2023-09-26 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种蛋氨酸生产中油相杂质的处理方法 |
CN116535338B (zh) * | 2023-04-25 | 2023-11-03 | 重庆渝化新材料有限责任公司 | 一种d,l-蛋氨酸生产过程中钾盐回收循环工艺 |
CN116675631B (zh) * | 2023-06-07 | 2023-12-12 | 重庆渝化新材料有限责任公司 | 一种d,l-蛋氨酸的循环生产方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3833651A (en) * | 1970-08-12 | 1974-09-03 | Degussa | Process for the preparation of dl-methionine |
US4069251A (en) * | 1969-02-08 | 1978-01-17 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler | Continuous process for the manufacture of methionine |
CN1160043A (zh) * | 1995-12-18 | 1997-09-24 | 底古萨股份公司 | 制备d,l-甲硫氨酸或其盐的方法 |
DE102005060316A1 (de) * | 2005-12-16 | 2007-06-21 | Kiefer, Hans, Dr. | Verfahren zur Herstellung von Methionin |
CN102399177A (zh) * | 2010-09-15 | 2012-04-04 | 李宽义 | 连续化合成蛋氨酸的环保清洁工艺方法 |
Family Cites Families (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN85108505A (zh) | 1985-11-14 | 1987-05-20 | 西北大学 | 5-(β-甲硫基乙基)海因的催化一步合成法 |
CN85108531A (zh) | 1985-11-14 | 1987-05-20 | 西北大学 | 5-(β-甲硫基乙基)海因水解制备蛋氨酸的方法 |
DE4235295A1 (de) | 1992-10-20 | 1994-04-21 | Degussa | Kontinuierlich durchführbares Verfahren zur Herstellung von Methionin oder Methioninderivaten |
JP3292119B2 (ja) * | 1997-11-26 | 2002-06-17 | 住友化学工業株式会社 | メチオニンの製造方法 |
EP1457486A4 (en) * | 2001-11-29 | 2006-04-05 | Nippon Soda Co | PROCESS FOR THE PRODUCTION OF METHIONINE |
DE10238212A1 (de) | 2002-08-21 | 2004-03-04 | Degussa Ag | Verfahren zur Herstellung von α-Aminosäuren durch Hydrolyse von Hydantoinen bei erhöhtem Druck und erhöhter Temperatur |
ATE509908T1 (de) * | 2004-02-14 | 2011-06-15 | Evonik Degussa Gmbh | Verfahren zur herstellung von methionin |
JP4997729B2 (ja) | 2005-08-29 | 2012-08-08 | 住友化学株式会社 | メチオニンの製造方法 |
JP2008266298A (ja) * | 2007-03-27 | 2008-11-06 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
JP2009292796A (ja) * | 2008-06-09 | 2009-12-17 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
JP5307512B2 (ja) * | 2008-11-07 | 2013-10-02 | 住友化学株式会社 | メチオニンの製造方法 |
JP2010111640A (ja) * | 2008-11-07 | 2010-05-20 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
JP2010111642A (ja) * | 2008-11-07 | 2010-05-20 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
FR2938535B1 (fr) * | 2008-11-20 | 2012-08-17 | Arkema France | Procede de fabrication de methylmercaptopropionaldehyde et de methionine a partir de matieres renouvelables |
JP2011126794A (ja) * | 2009-12-15 | 2011-06-30 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
JP5524736B2 (ja) * | 2010-06-29 | 2014-06-18 | 住友化学株式会社 | メチオニンの製造方法 |
CN102796033B (zh) * | 2012-09-03 | 2014-02-26 | 浙江新和成股份有限公司 | 一种清洁的d,l-蛋氨酸制备方法 |
-
2012
- 2012-09-03 CN CN201210320297.0A patent/CN102796033B/zh active Active
-
2013
- 2013-01-06 MX MX2015002752A patent/MX362811B/es active IP Right Grant
- 2013-01-06 WO PCT/CN2013/070129 patent/WO2014032401A1/zh active Application Filing
- 2013-01-06 US US14/425,310 patent/US9206120B2/en active Active
- 2013-01-06 KR KR1020157007639A patent/KR101689366B1/ko active IP Right Grant
- 2013-01-06 EP EP13833235.8A patent/EP2894147B1/en active Active
- 2013-01-06 AU AU2013307993A patent/AU2013307993B2/en active Active
- 2013-01-06 JP JP2015528838A patent/JP6026663B2/ja active Active
- 2013-01-06 BR BR112015004487A patent/BR112015004487B1/pt active IP Right Grant
- 2013-01-06 ES ES13833235.8T patent/ES2687247T3/es active Active
- 2013-01-06 SG SG11201501553PA patent/SG11201501553PA/en unknown
- 2013-01-06 RU RU2015111118/04A patent/RU2604064C2/ru active
- 2013-01-06 MY MYPI2015700650A patent/MY191517A/en unknown
-
2015
- 2015-04-07 ZA ZA2015/02259A patent/ZA201502259B/en unknown
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4069251A (en) * | 1969-02-08 | 1978-01-17 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler | Continuous process for the manufacture of methionine |
US3833651A (en) * | 1970-08-12 | 1974-09-03 | Degussa | Process for the preparation of dl-methionine |
CN1160043A (zh) * | 1995-12-18 | 1997-09-24 | 底古萨股份公司 | 制备d,l-甲硫氨酸或其盐的方法 |
DE102005060316A1 (de) * | 2005-12-16 | 2007-06-21 | Kiefer, Hans, Dr. | Verfahren zur Herstellung von Methionin |
CN102399177A (zh) * | 2010-09-15 | 2012-04-04 | 李宽义 | 连续化合成蛋氨酸的环保清洁工艺方法 |
Non-Patent Citations (4)
Title |
---|
温尔玺.蛋氨酸的制备和应用.《化工之友》.1998,(第3期),第29页. |
蛋氨酸生产工艺及核心制备技术研究进展;高文亮等;《化工进展》;20120430;第31卷(第4期);第29页 * |
蛋氨酸的制备和应用;温尔玺;《化工之友》;19980331(第3期);第866-872页 * |
高文亮等.蛋氨酸生产工艺及核心制备技术研究进展.《化工进展》.2012,第31卷(第4期),第866-872页. |
Also Published As
Publication number | Publication date |
---|---|
KR101689366B1 (ko) | 2016-12-26 |
US20150284323A1 (en) | 2015-10-08 |
ZA201502259B (en) | 2016-06-29 |
JP6026663B2 (ja) | 2016-11-16 |
KR20150084774A (ko) | 2015-07-22 |
MX2015002752A (es) | 2015-09-25 |
SG11201501553PA (en) | 2015-05-28 |
RU2604064C2 (ru) | 2016-12-10 |
CN102796033A (zh) | 2012-11-28 |
ES2687247T3 (es) | 2018-10-24 |
EP2894147A1 (en) | 2015-07-15 |
EP2894147B1 (en) | 2018-07-18 |
JP2015526485A (ja) | 2015-09-10 |
US9206120B2 (en) | 2015-12-08 |
BR112015004487B1 (pt) | 2020-04-14 |
RU2015111118A (ru) | 2016-10-27 |
AU2013307993A1 (en) | 2015-04-30 |
BR112015004487A2 (pt) | 2017-08-08 |
MY191517A (en) | 2022-06-28 |
MX362811B (es) | 2019-02-13 |
WO2014032401A1 (zh) | 2014-03-06 |
EP2894147A4 (en) | 2016-05-25 |
AU2013307993B2 (en) | 2017-02-02 |
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Owner name: SHANDONG XINHECHENG AMINO ACID CO., LTD. Free format text: FORMER OWNER: ZHEJIANG XINHECHENG CO., LTD. Effective date: 20150616 Owner name: ZHEJIANG XINHECHENG CO., LTD. ZHEJIANG UNIVERSITY Free format text: FORMER OWNER: ZHEJIANG UNIVERSITY Effective date: 20150616 |
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Effective date of registration: 20150616 Address after: 261108, Weifang Shandong Binhai Economic Development Zone, advanced manufacturing industrial park, Zhujiang West Three Street North, Hanjiang West Street South, west of Hailin Road, Dan River East Patentee after: SHANDONG XINHECHENG AMINO ACID CO., LTD. Patentee after: Zhejiang Xinhecheng Co., Ltd. Patentee after: Zhejiang University Address before: Zhejiang Jiangbei Road 312500 city of Shaoxing province Xinchang County habayashi Street No. 4 Patentee before: Zhejiang Xinhecheng Co., Ltd. Patentee before: Zhejiang University |