BR0308292A - Processo para aperfeiçoar a pureza e o rendimento da sucralose - Google Patents
Processo para aperfeiçoar a pureza e o rendimento da sucraloseInfo
- Publication number
- BR0308292A BR0308292A BR0308292-0A BR0308292A BR0308292A BR 0308292 A BR0308292 A BR 0308292A BR 0308292 A BR0308292 A BR 0308292A BR 0308292 A BR0308292 A BR 0308292A
- Authority
- BR
- Brazil
- Prior art keywords
- compositions
- sucralose
- crystallization
- improve
- yield
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
- C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
Abstract
"PROCESSO PARA APERFEIçOAR A PUREZA E O RENDIMENTO DA SUCRALOSE". A presente invenção refere-se aos processos para purificar a sucralose pelo uso de um procedimento de purificação por não-cristalização inicial, seguido por três ou mais etapas de cristalização seq³enciais e reciclo do licor-mãe que permanece de cada etapa de cristalização para a alimentação de uma outra etapa de cristalização ou purificação. Esta invenção também refere-se às composições de sucralose, bem como às composições compreendendo as composições de sucralose da presente invenção. Estas composições podem estar altamente puras e ter um perfil de sabor superior.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/092,730 US6998480B2 (en) | 2002-03-08 | 2002-03-08 | Process for improving sucralose purity and yield |
PCT/US2003/006628 WO2003076454A1 (en) | 2002-03-08 | 2003-03-06 | Process for improving sucralose purity and yield |
Publications (1)
Publication Number | Publication Date |
---|---|
BR0308292A true BR0308292A (pt) | 2005-01-11 |
Family
ID=27804179
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR0308292-0A BR0308292A (pt) | 2002-03-08 | 2003-03-06 | Processo para aperfeiçoar a pureza e o rendimento da sucralose |
Country Status (19)
Country | Link |
---|---|
US (1) | US6998480B2 (pt) |
EP (2) | EP1487846B1 (pt) |
JP (1) | JP4916089B2 (pt) |
KR (1) | KR101025235B1 (pt) |
CN (1) | CN1330659C (pt) |
AR (1) | AR038902A1 (pt) |
AT (2) | ATE375357T1 (pt) |
AU (6) | AU2003216516B2 (pt) |
BR (1) | BR0308292A (pt) |
CA (1) | CA2481402A1 (pt) |
DE (2) | DE60316853T2 (pt) |
DK (2) | DK1657246T3 (pt) |
ES (2) | ES2256765T3 (pt) |
IL (2) | IL163717A0 (pt) |
MX (1) | MXPA04009925A (pt) |
PT (2) | PT1487846E (pt) |
RU (1) | RU2324407C2 (pt) |
TW (1) | TW200400196A (pt) |
WO (1) | WO2003076454A1 (pt) |
Families Citing this family (62)
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US20060088638A1 (en) * | 2002-07-29 | 2006-04-27 | Merkel Carolyn M | Method of improving sweetness delivery of sucralose |
US6943248B2 (en) | 2003-04-30 | 2005-09-13 | Tate & Lyle Public Limited Company | Crystalline form of sucralose, and method for producing it |
CA2558683A1 (en) * | 2004-03-05 | 2005-09-22 | Sunil Srivastava | High-intensity sweetener-polyol compositions |
US20060188629A1 (en) * | 2005-01-21 | 2006-08-24 | Greg Liesen | Method for the purification of sucralose |
CN102124017A (zh) * | 2005-06-01 | 2011-07-13 | V.B.医疗保险私人有限公司 | 利用溶剂萃取法纯化氯化蔗糖衍生物的方法 |
JP2009509925A (ja) * | 2005-08-30 | 2009-03-12 | ファームド メディケア プライヴェート リミテッド | 疎水性親和性クロマトグラフィに基づく塩素化スクロースの生成方法 |
WO2007052302A2 (en) * | 2005-08-30 | 2007-05-10 | Pharmed Medicare Pvt. Ltd. | Removal of pyridine and pyridine analogs from reaction mass containing sucrose esters |
US8956677B2 (en) * | 2005-11-23 | 2015-02-17 | The Coca-Cola Company | High-potency sweetener composition with glucosamine and compositions sweetened therewith |
US20070116831A1 (en) * | 2005-11-23 | 2007-05-24 | The Coca-Cola Company | Dental Composition with High-Potency Sweetener |
US20070134391A1 (en) * | 2005-11-23 | 2007-06-14 | The Coca-Cola Company | High-Potency Sweetener Composition for Treatment and/or Prevention of Autoimmune Disorders and Compositions Sweetened Therewith |
US8956678B2 (en) * | 2005-11-23 | 2015-02-17 | The Coca-Cola Company | High-potency sweetener composition with preservative and compositions sweetened therewith |
US9101160B2 (en) | 2005-11-23 | 2015-08-11 | The Coca-Cola Company | Condiments with high-potency sweetener |
US20070116822A1 (en) * | 2005-11-23 | 2007-05-24 | The Coca-Cola Company | High-potency sweetener composition with saponin and compositions sweetened therewith |
US20070116836A1 (en) * | 2005-11-23 | 2007-05-24 | The Coca-Cola Company | High-Potency Sweetener Composition for Treatment and/or Prevention of Osteoporosis and Compositions Sweetened Therewith |
KR20080071606A (ko) * | 2005-11-23 | 2008-08-04 | 더 코카콜라 컴파니 | 시간 특성 및/또는 향미 특성이 개선된 인공 감미료조성물과 이들의 제제 방법 및 용도 |
US9144251B2 (en) * | 2005-11-23 | 2015-09-29 | The Coca-Cola Company | High-potency sweetener composition with mineral and compositions sweetened therewith |
US8993027B2 (en) * | 2005-11-23 | 2015-03-31 | The Coca-Cola Company | Natural high-potency tabletop sweetener compositions with improved temporal and/or flavor profile, methods for their formulation, and uses |
US20070116825A1 (en) * | 2005-11-23 | 2007-05-24 | The Coca-Cola Company | Confection with High-Potency Sweetener |
US7741477B2 (en) * | 2006-01-10 | 2010-06-22 | Alembic Limited | Process for purification of sucralose |
CN100372859C (zh) * | 2006-03-17 | 2008-03-05 | 广西大学 | 医药级蔗糖的制备方法 |
US8791253B2 (en) * | 2006-06-19 | 2014-07-29 | The Coca-Cola Company | Rebaudioside A composition and method for purifying rebaudioside A |
US9012626B2 (en) * | 2006-06-19 | 2015-04-21 | The Coca-Cola Company | Rebaudioside a composition and method for purifying rebaudioside a |
JP2009542625A (ja) * | 2006-07-06 | 2009-12-03 | アレムビック・リミテッド | 高純度スクラロースの改良製造法 |
US8258291B2 (en) * | 2006-10-25 | 2012-09-04 | Mamtek International Limited | Process for the preparation of sucralose by the chlorination of sugar with triphosgene (BTC) |
US20080103295A1 (en) * | 2006-10-25 | 2008-05-01 | David Losan Ho | Process for the preparation of sucrose-6-ester by esterification in the presence of solid superacid catalyst |
US20080107787A1 (en) * | 2006-11-02 | 2008-05-08 | The Coca-Cola Company | Anti-Diabetic Composition with High-Potency Sweetener |
US8017168B2 (en) | 2006-11-02 | 2011-09-13 | The Coca-Cola Company | High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith |
US9101161B2 (en) * | 2006-11-02 | 2015-08-11 | The Coca-Cola Company | High-potency sweetener composition with phytoestrogen and compositions sweetened therewith |
US8030481B2 (en) | 2007-05-21 | 2011-10-04 | The Coca-Cola Company | Stevioside polymorphic and amorphous forms, methods for their formulation, and uses |
US8436156B2 (en) * | 2008-01-04 | 2013-05-07 | Tate & Lyle Technology Limited | Method for the production of sucralose |
CN101236182B (zh) * | 2008-01-11 | 2012-01-18 | 西北大学 | 三氯蔗糖中间体的分析检测方法 |
KR20100130219A (ko) * | 2008-03-20 | 2010-12-10 | 테이트 앤드 라일 테크놀러지 리미티드 | 3급 아미드 용매로부터 산을 제거하는 방법 |
US8436157B2 (en) * | 2008-03-26 | 2013-05-07 | Tate & Lyle Technology Limited | Method for the production of sucralose |
US20090259036A1 (en) * | 2008-04-03 | 2009-10-15 | Tate & Lyle Technology Limited | Extraction of less polar impurities from sucralose containing aqueous feed streams |
AR071134A1 (es) * | 2008-04-03 | 2010-05-26 | Tate & Lyle Technology Ltd | Cristalizacion de sucralosa a partir de chorros que contienen sucralosa |
WO2009137193A2 (en) * | 2008-04-03 | 2009-11-12 | Tate & Lyte Technology Ltd | Effect of carbohydrate concentration on sucralose extraction efficiency |
US8497367B2 (en) * | 2008-04-03 | 2013-07-30 | Tate & Lyle Technology Limited | Sucralose purification process |
US20100022765A1 (en) * | 2008-07-23 | 2010-01-28 | David Losan Ho | Methods for extracting and purifying sucralose intermediate |
GB2468936B (en) | 2009-03-27 | 2011-09-07 | Mohamad Rami Radwan Jaber | Chlorination of sucrose-6-esters |
GB2469157B (en) | 2009-03-30 | 2011-07-06 | John Kerr | Process for removing dimethylamine during sucralose production |
GB2469158B (en) | 2009-03-31 | 2011-09-28 | Peter J Seaberg | Base-assisted formation of tin-sucrose adducts |
US20110027445A1 (en) * | 2009-07-28 | 2011-02-03 | Heartland Sweeteners, LLC | No-calorie sweetener compositions |
US20110027444A1 (en) * | 2009-07-28 | 2011-02-03 | Heartland Sweeteners, LLC | No-calorie sweetener compositions |
US20110027446A1 (en) * | 2009-07-28 | 2011-02-03 | Heartland Sweeteners, LLC | No-calorie sweetener compositions |
GB2474311B (en) * | 2009-10-12 | 2012-10-17 | Tate & Lyle Technology Ltd | Low temperature, single solvent process for the production of sucrose-6-ester |
GB2474310B (en) | 2009-10-12 | 2012-02-29 | Tate & Lyle Technology Ltd | Process for the production of sucrose-6-ester |
US20120034366A1 (en) * | 2010-08-05 | 2012-02-09 | Tate & Lyle Ingredients Americas, Inc. | Carbohydrate compositions |
GB201110520D0 (en) | 2011-05-10 | 2011-08-03 | Tate & Lyle Technology Ltd | Extraction of carboxylic acids with tin compounds |
CN102391319B (zh) * | 2011-10-14 | 2015-01-07 | 山东三和维信生物科技有限公司 | 三氯蔗糖的结晶方法 |
CN102391320B (zh) * | 2011-12-23 | 2014-03-19 | 盐城捷康三氯蔗糖制造有限公司 | 溶剂热回流纯化三氯蔗糖的方法 |
CN102687887A (zh) * | 2012-06-18 | 2012-09-26 | 陕西咸阳淳化中富实业有限公司 | 果蔬汁三次萃取新工艺 |
CN102977157A (zh) * | 2012-12-05 | 2013-03-20 | 溧阳维信生物科技有限公司 | 一种三氯蔗糖的结晶方法 |
US10227367B2 (en) | 2013-12-16 | 2019-03-12 | Tate & Lyle Technology Limited | Chlorination of sucrose-6-esters |
WO2016020635A1 (en) | 2014-08-08 | 2016-02-11 | Tate & Lyle Technology Limited | Chlorination of sucrose-6-esters |
US20160115560A1 (en) * | 2014-10-23 | 2016-04-28 | Amalgamated Research Llc | Methods of separating components using multi-scale simulated moving bed chromatography |
CN104387427A (zh) * | 2014-10-30 | 2015-03-04 | 安徽金禾实业股份有限公司 | 一种三氯蔗糖的生产方法 |
GB2536480B (en) | 2015-03-17 | 2019-09-04 | Tate & Lyle Tech Ltd | DMF Distillation |
ES2946184T3 (es) * | 2015-12-08 | 2023-07-13 | Biomatrica Inc | Reducción de la velocidad de eritrosedimentación |
GB2551591B (en) | 2016-06-23 | 2019-08-07 | Tate & Lyle Tech Ltd | Liquid-liquid extraction of DMF |
CN108264527A (zh) * | 2018-01-15 | 2018-07-10 | 山东三和维信生物科技有限公司 | 一种提高三氯蔗糖纯度的方法 |
CN110527854B (zh) * | 2019-09-11 | 2021-06-11 | 广东先导稀材股份有限公司 | 一种制备粒径可控的超高纯铼酸铵晶体的方法 |
MX2023003704A (es) | 2020-09-30 | 2023-05-09 | Anhui Jinhe Ind Co Ltd | Método de purificación de sucralosa. |
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-
2002
- 2002-03-08 US US10/092,730 patent/US6998480B2/en not_active Expired - Lifetime
-
2003
- 2003-03-06 MX MXPA04009925A patent/MXPA04009925A/es active IP Right Grant
- 2003-03-06 PT PT03744178T patent/PT1487846E/pt unknown
- 2003-03-06 DE DE60316853T patent/DE60316853T2/de not_active Expired - Fee Related
- 2003-03-06 CN CNB038055287A patent/CN1330659C/zh not_active Expired - Lifetime
- 2003-03-06 AU AU2003216516A patent/AU2003216516B2/en not_active Ceased
- 2003-03-06 ES ES03744178T patent/ES2256765T3/es not_active Expired - Lifetime
- 2003-03-06 AT AT05027718T patent/ATE375357T1/de not_active IP Right Cessation
- 2003-03-06 PT PT05027718T patent/PT1657246E/pt unknown
- 2003-03-06 EP EP03744178A patent/EP1487846B1/en not_active Expired - Lifetime
- 2003-03-06 DE DE60303305T patent/DE60303305T2/de not_active Expired - Fee Related
- 2003-03-06 WO PCT/US2003/006628 patent/WO2003076454A1/en active Application Filing
- 2003-03-06 IL IL16371703A patent/IL163717A0/xx unknown
- 2003-03-06 EP EP05027718A patent/EP1657246B1/en not_active Expired - Lifetime
- 2003-03-06 CA CA002481402A patent/CA2481402A1/en not_active Abandoned
- 2003-03-06 DK DK05027718T patent/DK1657246T3/da active
- 2003-03-06 JP JP2003574669A patent/JP4916089B2/ja not_active Expired - Fee Related
- 2003-03-06 AT AT03744178T patent/ATE316092T1/de not_active IP Right Cessation
- 2003-03-06 KR KR1020047014007A patent/KR101025235B1/ko not_active IP Right Cessation
- 2003-03-06 DK DK03744178T patent/DK1487846T3/da active
- 2003-03-06 ES ES05027718T patent/ES2296057T3/es not_active Expired - Lifetime
- 2003-03-06 RU RU2004129750/04A patent/RU2324407C2/ru not_active IP Right Cessation
- 2003-03-06 BR BR0308292-0A patent/BR0308292A/pt not_active IP Right Cessation
- 2003-03-07 AR ARP030100793A patent/AR038902A1/es unknown
- 2003-03-07 TW TW092104872A patent/TW200400196A/zh unknown
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2008
- 2008-03-18 IL IL190247A patent/IL190247A0/en unknown
- 2008-11-24 AU AU2008249185A patent/AU2008249185A1/en not_active Abandoned
- 2008-11-24 AU AU2008249184A patent/AU2008249184A1/en not_active Abandoned
- 2008-11-24 AU AU2008249188A patent/AU2008249188A1/en not_active Abandoned
- 2008-11-24 AU AU2008249186A patent/AU2008249186A1/en not_active Abandoned
- 2008-11-25 AU AU2008249208A patent/AU2008249208A1/en not_active Abandoned
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