ATE316092T1 - Verfahren zur verbesserung der reinheit und ausbeute von sucralose - Google Patents

Verfahren zur verbesserung der reinheit und ausbeute von sucralose

Info

Publication number
ATE316092T1
ATE316092T1 AT03744178T AT03744178T ATE316092T1 AT E316092 T1 ATE316092 T1 AT E316092T1 AT 03744178 T AT03744178 T AT 03744178T AT 03744178 T AT03744178 T AT 03744178T AT E316092 T1 ATE316092 T1 AT E316092T1
Authority
AT
Austria
Prior art keywords
sucralose
purity
yield
improving
Prior art date
Application number
AT03744178T
Other languages
English (en)
Inventor
Steven J Catani
James Edwin Wiley
Nicholas M Vernon
Carolyn Merkel
Edward Micinski
Original Assignee
Tate & Lyle Plc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate & Lyle Plc filed Critical Tate & Lyle Plc
Application granted granted Critical
Publication of ATE316092T1 publication Critical patent/ATE316092T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Seasonings (AREA)
  • Saccharide Compounds (AREA)
  • Soy Sauces And Products Related Thereto (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
AT03744178T 2002-03-08 2003-03-06 Verfahren zur verbesserung der reinheit und ausbeute von sucralose ATE316092T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10/092,730 US6998480B2 (en) 2002-03-08 2002-03-08 Process for improving sucralose purity and yield

Publications (1)

Publication Number Publication Date
ATE316092T1 true ATE316092T1 (de) 2006-02-15

Family

ID=27804179

Family Applications (2)

Application Number Title Priority Date Filing Date
AT05027718T ATE375357T1 (de) 2002-03-08 2003-03-06 Verfahren zur gewinnung von sucralose mit hoher reinheit und hoher ausbeute
AT03744178T ATE316092T1 (de) 2002-03-08 2003-03-06 Verfahren zur verbesserung der reinheit und ausbeute von sucralose

Family Applications Before (1)

Application Number Title Priority Date Filing Date
AT05027718T ATE375357T1 (de) 2002-03-08 2003-03-06 Verfahren zur gewinnung von sucralose mit hoher reinheit und hoher ausbeute

Country Status (19)

Country Link
US (1) US6998480B2 (de)
EP (2) EP1657246B1 (de)
JP (1) JP4916089B2 (de)
KR (1) KR101025235B1 (de)
CN (1) CN1330659C (de)
AR (1) AR038902A1 (de)
AT (2) ATE375357T1 (de)
AU (6) AU2003216516B2 (de)
BR (1) BR0308292A (de)
CA (1) CA2481402A1 (de)
DE (2) DE60303305T2 (de)
DK (2) DK1657246T3 (de)
ES (2) ES2296057T3 (de)
IL (2) IL163717A0 (de)
MX (1) MXPA04009925A (de)
PT (2) PT1657246E (de)
RU (1) RU2324407C2 (de)
TW (1) TW200400196A (de)
WO (1) WO2003076454A1 (de)

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JP2009509925A (ja) * 2005-08-30 2009-03-12 ファームド メディケア プライヴェート リミテッド 疎水性親和性クロマトグラフィに基づく塩素化スクロースの生成方法
US8956677B2 (en) * 2005-11-23 2015-02-17 The Coca-Cola Company High-potency sweetener composition with glucosamine and compositions sweetened therewith
US20070116822A1 (en) * 2005-11-23 2007-05-24 The Coca-Cola Company High-potency sweetener composition with saponin and compositions sweetened therewith
US20070116825A1 (en) * 2005-11-23 2007-05-24 The Coca-Cola Company Confection with High-Potency Sweetener
EP1965667A2 (de) * 2005-11-23 2008-09-10 The Coca-Cola Company Synthetische süssmittelzusammensetzungen mit verbessertem zeitverlaufsprofil und/oder geschmacksprofil, verfahren zu ihrer formulierung und ihre verwendungen
US9101160B2 (en) 2005-11-23 2015-08-11 The Coca-Cola Company Condiments with high-potency sweetener
US9144251B2 (en) * 2005-11-23 2015-09-29 The Coca-Cola Company High-potency sweetener composition with mineral and compositions sweetened therewith
US8956678B2 (en) * 2005-11-23 2015-02-17 The Coca-Cola Company High-potency sweetener composition with preservative and compositions sweetened therewith
US20070116836A1 (en) * 2005-11-23 2007-05-24 The Coca-Cola Company High-Potency Sweetener Composition for Treatment and/or Prevention of Osteoporosis and Compositions Sweetened Therewith
US8993027B2 (en) * 2005-11-23 2015-03-31 The Coca-Cola Company Natural high-potency tabletop sweetener compositions with improved temporal and/or flavor profile, methods for their formulation, and uses
US20070134391A1 (en) * 2005-11-23 2007-06-14 The Coca-Cola Company High-Potency Sweetener Composition for Treatment and/or Prevention of Autoimmune Disorders and Compositions Sweetened Therewith
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CN100372859C (zh) * 2006-03-17 2008-03-05 广西大学 医药级蔗糖的制备方法
US9012626B2 (en) * 2006-06-19 2015-04-21 The Coca-Cola Company Rebaudioside a composition and method for purifying rebaudioside a
US8791253B2 (en) * 2006-06-19 2014-07-29 The Coca-Cola Company Rebaudioside A composition and method for purifying rebaudioside A
US20090312538A1 (en) * 2006-07-06 2009-12-17 Alembic Limited process for the preparation of sucralose of high purity
US20080103295A1 (en) * 2006-10-25 2008-05-01 David Losan Ho Process for the preparation of sucrose-6-ester by esterification in the presence of solid superacid catalyst
US8258291B2 (en) * 2006-10-25 2012-09-04 Mamtek International Limited Process for the preparation of sucralose by the chlorination of sugar with triphosgene (BTC)
US8017168B2 (en) 2006-11-02 2011-09-13 The Coca-Cola Company High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith
US9101161B2 (en) * 2006-11-02 2015-08-11 The Coca-Cola Company High-potency sweetener composition with phytoestrogen and compositions sweetened therewith
US20080107787A1 (en) * 2006-11-02 2008-05-08 The Coca-Cola Company Anti-Diabetic Composition with High-Potency Sweetener
US8030481B2 (en) 2007-05-21 2011-10-04 The Coca-Cola Company Stevioside polymorphic and amorphous forms, methods for their formulation, and uses
AR070082A1 (es) * 2008-01-04 2010-03-10 Tate & Lyle Technology Ltd Metodo para la produccion de sucralosa
CN101236182B (zh) * 2008-01-11 2012-01-18 西北大学 三氯蔗糖中间体的分析检测方法
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US20110027444A1 (en) * 2009-07-28 2011-02-03 Heartland Sweeteners, LLC No-calorie sweetener compositions
US20110027445A1 (en) * 2009-07-28 2011-02-03 Heartland Sweeteners, LLC No-calorie sweetener compositions
US20110027446A1 (en) * 2009-07-28 2011-02-03 Heartland Sweeteners, LLC No-calorie sweetener compositions
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CN102391319B (zh) * 2011-10-14 2015-01-07 山东三和维信生物科技有限公司 三氯蔗糖的结晶方法
CN102391320B (zh) * 2011-12-23 2014-03-19 盐城捷康三氯蔗糖制造有限公司 溶剂热回流纯化三氯蔗糖的方法
CN102687887A (zh) * 2012-06-18 2012-09-26 陕西咸阳淳化中富实业有限公司 果蔬汁三次萃取新工艺
CN102977157A (zh) * 2012-12-05 2013-03-20 溧阳维信生物科技有限公司 一种三氯蔗糖的结晶方法
US10227367B2 (en) 2013-12-16 2019-03-12 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
WO2016020635A1 (en) 2014-08-08 2016-02-11 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
US20160115560A1 (en) * 2014-10-23 2016-04-28 Amalgamated Research Llc Methods of separating components using multi-scale simulated moving bed chromatography
CN104387427A (zh) * 2014-10-30 2015-03-04 安徽金禾实业股份有限公司 一种三氯蔗糖的生产方法
GB2536480B (en) 2015-03-17 2019-09-04 Tate & Lyle Tech Ltd DMF Distillation
JP6827048B2 (ja) * 2015-12-08 2021-02-10 バイオマトリカ，インク． 赤血球沈降速度の低下
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF
CN108264527A (zh) * 2018-01-15 2018-07-10 山东三和维信生物科技有限公司 一种提高三氯蔗糖纯度的方法
CN110527854B (zh) * 2019-09-11 2021-06-11 广东先导稀材股份有限公司 一种制备粒径可控的超高纯铼酸铵晶体的方法
CN112543760A (zh) 2020-09-30 2021-03-23 安徽金禾实业股份有限公司 三氯蔗糖的纯化方法

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Also Published As

Publication number Publication date
EP1487846B1 (de) 2006-01-18
CN1639179A (zh) 2005-07-13
PT1487846E (pt) 2006-05-31
DE60316853T2 (de) 2008-07-17
DK1487846T3 (da) 2006-05-22
JP4916089B2 (ja) 2012-04-11
AU2003216516B2 (en) 2009-01-08
PT1657246E (pt) 2008-01-14
CN1330659C (zh) 2007-08-08
IL163717A0 (en) 2005-12-18
DE60303305D1 (de) 2006-04-06
AR038902A1 (es) 2005-02-02
EP1657246A1 (de) 2006-05-17
AU2008249208A1 (en) 2008-12-18
US6998480B2 (en) 2006-02-14
AU2008249184A1 (en) 2008-12-11
DK1657246T3 (da) 2008-02-11
KR101025235B1 (ko) 2011-04-01
RU2324407C2 (ru) 2008-05-20
ES2256765T3 (es) 2006-07-16
IL190247A0 (en) 2008-11-03
TW200400196A (en) 2004-01-01
ES2296057T3 (es) 2008-04-16
AU2008249188A1 (en) 2008-12-11
KR20040099306A (ko) 2004-11-26
WO2003076454A1 (en) 2003-09-18
ATE375357T1 (de) 2007-10-15
MXPA04009925A (es) 2005-07-01
DE60316853D1 (de) 2007-11-22
CA2481402A1 (en) 2003-09-18
EP1657246B1 (de) 2007-10-10
BR0308292A (pt) 2005-01-11
AU2003216516A1 (en) 2003-09-22
AU2008249185A1 (en) 2008-12-11
AU2008249186A1 (en) 2008-12-11
RU2004129750A (ru) 2005-04-20
DE60303305T2 (de) 2006-09-21
EP1487846A1 (de) 2004-12-22
US20030171575A1 (en) 2003-09-11
AU2003216516A2 (en) 2003-09-22
JP2005526767A (ja) 2005-09-08

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