ATE540962T1 - Extraktive verfahren zur aufreinigung von sucralose - Google Patents
Extraktive verfahren zur aufreinigung von sucraloseInfo
- Publication number
- ATE540962T1 ATE540962T1 AT03744177T AT03744177T ATE540962T1 AT E540962 T1 ATE540962 T1 AT E540962T1 AT 03744177 T AT03744177 T AT 03744177T AT 03744177 T AT03744177 T AT 03744177T AT E540962 T1 ATE540962 T1 AT E540962T1
- Authority
- AT
- Austria
- Prior art keywords
- sucralose
- purification
- extractive process
- extractive
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
- C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Extraction Or Liquid Replacement (AREA)
- Saccharide Compounds (AREA)
- Seasonings (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/092,715 US7049435B2 (en) | 2002-03-08 | 2002-03-08 | Extractive methods for purifying sucralose |
| PCT/US2003/006627 WO2003076453A1 (en) | 2002-03-08 | 2003-03-06 | Extractive methods for purifying sucralose |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE540962T1 true ATE540962T1 (de) | 2012-01-15 |
Family
ID=27804178
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT03744177T ATE540962T1 (de) | 2002-03-08 | 2003-03-06 | Extraktive verfahren zur aufreinigung von sucralose |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US7049435B2 (de) |
| EP (2) | EP2039699A3 (de) |
| JP (1) | JP5196702B2 (de) |
| KR (1) | KR101024882B1 (de) |
| CN (1) | CN1318437C (de) |
| AR (1) | AR038901A1 (de) |
| AT (1) | ATE540962T1 (de) |
| AU (1) | AU2003216515B2 (de) |
| BR (1) | BR0308261A (de) |
| CA (1) | CA2481405A1 (de) |
| IL (1) | IL163662A0 (de) |
| MX (1) | MXPA04009842A (de) |
| RU (1) | RU2326887C2 (de) |
| TW (1) | TW200408647A (de) |
| WO (1) | WO2003076453A1 (de) |
Families Citing this family (47)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6890581B2 (en) * | 2002-04-05 | 2005-05-10 | Tate & Lyle Public Limited Company | Methods for buffer stabilized aqueous deacylation |
| WO2005087020A1 (en) * | 2004-03-05 | 2005-09-22 | Richmond Chemical Corporation | High-intensity sweetener-polyol compositions |
| WO2006061855A2 (en) * | 2004-12-10 | 2006-06-15 | Pharmed Medicare Private Limited | Salts assisted selective extraction of 6-acetyl-4.1', 6' trichlorogalactosucrose and 4, 1 ', 6' trichlorogalactosucrose from aqueous reaction mixture |
| US20060188629A1 (en) * | 2005-01-21 | 2006-08-24 | Greg Liesen | Method for the purification of sucralose |
| CN102124017A (zh) * | 2005-06-01 | 2011-07-13 | V.B.医疗保险私人有限公司 | 利用溶剂萃取法纯化氯化蔗糖衍生物的方法 |
| CN101253187A (zh) * | 2005-08-30 | 2008-08-27 | 法马德医疗保险私人有限公司 | 含有蔗糖酯的反应物中吡啶及其类似物的除去方法 |
| US9101160B2 (en) | 2005-11-23 | 2015-08-11 | The Coca-Cola Company | Condiments with high-potency sweetener |
| US7741477B2 (en) * | 2006-01-10 | 2010-06-22 | Alembic Limited | Process for purification of sucralose |
| US9012626B2 (en) * | 2006-06-19 | 2015-04-21 | The Coca-Cola Company | Rebaudioside a composition and method for purifying rebaudioside a |
| US8791253B2 (en) * | 2006-06-19 | 2014-07-29 | The Coca-Cola Company | Rebaudioside A composition and method for purifying rebaudioside A |
| US20090312538A1 (en) * | 2006-07-06 | 2009-12-17 | Alembic Limited | process for the preparation of sucralose of high purity |
| US8017168B2 (en) | 2006-11-02 | 2011-09-13 | The Coca-Cola Company | High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith |
| US8030481B2 (en) | 2007-05-21 | 2011-10-04 | The Coca-Cola Company | Stevioside polymorphic and amorphous forms, methods for their formulation, and uses |
| AR070082A1 (es) * | 2008-01-04 | 2010-03-10 | Tate & Lyle Technology Ltd | Metodo para la produccion de sucralosa |
| WO2009117317A1 (en) * | 2008-03-20 | 2009-09-24 | Tate & Lyle Technology Ltd | Removal of acids from tertiary amide solvents |
| US8436157B2 (en) * | 2008-03-26 | 2013-05-07 | Tate & Lyle Technology Limited | Method for the production of sucralose |
| AR071134A1 (es) * | 2008-04-03 | 2010-05-26 | Tate & Lyle Technology Ltd | Cristalizacion de sucralosa a partir de chorros que contienen sucralosa |
| US20090299055A1 (en) * | 2008-04-03 | 2009-12-03 | Tate & Lyle Technology Limited | Purification of Sucralose Containing Feed Streams for Sucralose Crystallization |
| WO2009124113A1 (en) * | 2008-04-03 | 2009-10-08 | Tate & Lyle Technology Ltd. | Extraction of less polar impurities from sucralose containing aqueous feed streams |
| US8497367B2 (en) * | 2008-04-03 | 2013-07-30 | Tate & Lyle Technology Limited | Sucralose purification process |
| US8212022B2 (en) * | 2008-04-03 | 2012-07-03 | Tate & Lyle Technology Limited | Effect of carbohydrate concentration on sucralose extraction efficiency |
| GB2468936B (en) | 2009-03-27 | 2011-09-07 | Mohamad Rami Radwan Jaber | Chlorination of sucrose-6-esters |
| GB2469157B (en) | 2009-03-30 | 2011-07-06 | John Kerr | Process for removing dimethylamine during sucralose production |
| GB2469158B (en) | 2009-03-31 | 2011-09-28 | Peter J Seaberg | Base-assisted formation of tin-sucrose adducts |
| US8609805B2 (en) | 2009-04-15 | 2013-12-17 | Invista North America S.A R.L. | Copolyether glycol manufacturing process |
| GB2474311B (en) * | 2009-10-12 | 2012-10-17 | Tate & Lyle Technology Ltd | Low temperature, single solvent process for the production of sucrose-6-ester |
| GB2474310B (en) | 2009-10-12 | 2012-02-29 | Tate & Lyle Technology Ltd | Process for the production of sucrose-6-ester |
| GB201110520D0 (en) | 2011-05-10 | 2011-08-03 | Tate & Lyle Technology Ltd | Extraction of carboxylic acids with tin compounds |
| HUE027876T2 (en) * | 2011-10-14 | 2016-10-28 | Lexington Pharmaceuticals Laboratories Llc | Carbohydrate chlorination and carbohydrate derivatives |
| CN102391319B (zh) * | 2011-10-14 | 2015-01-07 | 山东三和维信生物科技有限公司 | 三氯蔗糖的结晶方法 |
| CN102391320B (zh) * | 2011-12-23 | 2014-03-19 | 盐城捷康三氯蔗糖制造有限公司 | 溶剂热回流纯化三氯蔗糖的方法 |
| CN105829332B (zh) | 2013-12-16 | 2018-10-02 | 塔特和莱利技术有限公司 | 蔗糖-6-酯的氯化 |
| GB2544217B (en) | 2014-08-08 | 2020-03-25 | Tate & Lyle Tech Ltd | Chlorination of sucrose-6-esters |
| CN104387427A (zh) * | 2014-10-30 | 2015-03-04 | 安徽金禾实业股份有限公司 | 一种三氯蔗糖的生产方法 |
| GB2536480B (en) | 2015-03-17 | 2019-09-04 | Tate & Lyle Tech Ltd | DMF Distillation |
| CN104861003A (zh) * | 2015-04-24 | 2015-08-26 | 吉安市新琪安科技有限公司 | 一种三氯蔗糖母液的处理方法 |
| GB2551591B (en) * | 2016-06-23 | 2019-08-07 | Tate & Lyle Tech Ltd | Liquid-liquid extraction of DMF |
| CN116854579A (zh) * | 2016-12-07 | 2023-10-10 | 孟山都技术公司 | 纯化、回收和转化氯苯酚盐以及制备和回收由氯苯酚盐制得的产品的工艺 |
| CN106674292B (zh) * | 2016-12-09 | 2019-02-22 | 福建科宏生物工程股份有限公司 | 一种三氯蔗糖水结晶母液的提纯处理方法 |
| CN108264527A (zh) * | 2018-01-15 | 2018-07-10 | 山东三和维信生物科技有限公司 | 一种提高三氯蔗糖纯度的方法 |
| CN109315745A (zh) * | 2018-10-28 | 2019-02-12 | 四川泰之味食品有限公司 | 一种泡椒花生及其制备方法 |
| CN111499672B (zh) * | 2019-01-30 | 2021-07-20 | 山东新和成精化科技有限公司 | 一种用于纯化三氯蔗糖的萃取方法 |
| EP4206211B1 (de) | 2020-09-30 | 2025-12-31 | Anhui Jinhe Industrial Co., Ltd. | Verfahren zur reinigung von sucralose |
| EP4215538A4 (de) * | 2020-11-13 | 2023-10-11 | Anhui Jinhe Industrial Co., Ltd. | Verfahren zur reinigung von sucralose |
| CN115996936A (zh) * | 2022-10-19 | 2023-04-21 | 安徽金禾实业股份有限公司 | 一种利用改进的醇水碱解体系制备三氯蔗糖粗品的方法 |
| CN115956082A (zh) * | 2022-10-19 | 2023-04-11 | 安徽金禾实业股份有限公司 | 一种利用水解体系制备三氯蔗糖粗品的方法 |
| CN116134043A (zh) * | 2022-10-19 | 2023-05-16 | 安徽金禾实业股份有限公司 | 一种利用改进的水解体系制备三氯蔗糖粗品的方法 |
Family Cites Families (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ZA807578B (en) * | 1979-12-18 | 1981-11-25 | Tate & Lyle Patent Holdings | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
| EP0030804B1 (de) | 1979-12-18 | 1983-10-19 | TATE & LYLE PUBLIC LIMITED COMPANY | Kristallin-4,1',6'-trichlor-4,1',6'-trideoxy-galactosucrose |
| GB2065646B (en) * | 1979-12-18 | 1983-10-05 | Tate & Lyle Ltd | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxygalactosucrose |
| EP0031651B1 (de) | 1979-12-20 | 1983-03-23 | TATE & LYLE PUBLIC LIMITED COMPANY | Verfahren zur Herstellung von 4,1',6'-Trichlor-4,1',6'-trideoxy-galactosucrose |
| EP0043649B1 (de) * | 1980-07-08 | 1984-09-12 | TATE & LYLE PUBLIC LIMITED COMPANY | Verfahren zur Herstellung von 4,1',6'-Trichlor-4,1',6'-trideoxygalactosucrose (TGS) |
| CA1183133A (en) | 1980-10-28 | 1985-02-26 | Tate & Lyle Public Limited Company | Sweet chlorine-substituted disaccharides |
| GB8525871D0 (en) | 1985-10-21 | 1985-11-27 | Tate & Lyle Plc | Chemical compound |
| GB2222827B (en) * | 1988-09-16 | 1992-08-19 | Tate & Lyle Plc | Chlorination of sugars |
| GB8822673D0 (en) | 1988-09-27 | 1988-11-02 | Tate & Lyle Plc | Selective acylation of sugars |
| GB8822674D0 (en) | 1988-09-27 | 1988-11-02 | Tate & Lyle Plc | Preparation of acylated sucrose derivatives |
| NZ234143A (en) | 1989-06-28 | 1991-10-25 | Mcneil Ppc Inc | Aqueous pharmaceutical suspension formulation for administering substantially insoluble pharmaceutical agents |
| US4980463A (en) * | 1989-07-18 | 1990-12-25 | Noramco, Inc. | Sucrose-6-ester chlorination |
| US5034551A (en) | 1990-04-23 | 1991-07-23 | Noramco, Inc. | Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds |
| NZ240818A (en) * | 1990-12-14 | 1993-08-26 | Mcneil Ppc Inc | Liquid sucralose concentrate compositions containing preservative, buffer and liquid |
| US5272137A (en) | 1992-02-14 | 1993-12-21 | Mcneil-Pfc, Inc. | Aqueous pharmaceutical suspension for pharmaceutical actives |
| US5270071A (en) | 1992-06-18 | 1993-12-14 | Mcneil-Ppc, Inc. | Reduced calorie fruit spreads |
| US5397588A (en) | 1992-06-18 | 1995-03-14 | Mcneil-Ppc, Inc. | Reduced calorie fruit spreads |
| US5354902A (en) | 1992-10-26 | 1994-10-11 | Mcneil-Ppc, Inc. | Stabilized sorbic acid or salt thereof |
| CA2110313C (en) | 1992-12-01 | 2004-10-26 | Edward John Roche | Pharmaceutical compositions containing a guanidinothiazole compound and antacids |
| US5530106A (en) | 1993-03-12 | 1996-06-25 | Mcneil-Ppc, Inc. | Recovery of sucralose intermediates |
| US5298611A (en) | 1993-03-12 | 1994-03-29 | Mcneil-Ppc, Inc. | Sucralose pentaester production |
| CA2121435C (en) | 1993-04-16 | 2002-01-22 | Sheila M. Ratnaraj | Aqueous pharmaceutical suspension and process for preparation thereof |
| CA2128820A1 (en) | 1993-07-27 | 1995-01-28 | Walter G. Gowan, Jr. | Rapidly disintegrating pharmaceutical dosage form and process for preparation thereof |
| US5674522A (en) | 1993-10-07 | 1997-10-07 | Mcneil-Ppc, Inc. | Beverage concentrate for drug delivery |
| US5498709A (en) * | 1994-10-17 | 1996-03-12 | Mcneil-Ppc, Inc. | Production of sucralose without intermediate isolation of crystalline sucralose-6-ester |
| US5593696A (en) | 1994-11-21 | 1997-01-14 | Mcneil-Ppc, Inc. | Stabilized composition of famotidine and sucralfate for treatment of gastrointestinal disorders |
| KR100531261B1 (ko) | 1997-02-13 | 2005-11-28 | 테이트 앤드 라일 퍼블릭 리미티드 컴파니 | 염소화된 슈크로즈의 크로마토그래피 정제법 |
| AU753587B2 (en) | 1997-11-14 | 2002-10-24 | Johnson & Johnson Consumer Companies, Inc. | Highly flavored dental floss |
| ES2229722T3 (es) | 1998-07-07 | 2005-04-16 | Mcneil-Ppc, Inc. | Procedimiento para mejorar el efecto edulcorante de la sucralosa. |
| US6090401A (en) | 1999-03-31 | 2000-07-18 | Mcneil-Ppc, Inc. | Stable foam composition |
| US6211246B1 (en) | 1999-06-10 | 2001-04-03 | Mcneil-Ppc, Inc. | Rapidly absorbed liquid compositions |
| US6277409B1 (en) | 2000-02-11 | 2001-08-21 | Mcneil-Ppc, Inc. | Protective coating for tablet |
| US6258381B1 (en) | 2000-02-11 | 2001-07-10 | Mcneil-Ppc, Inc. | Tablet and process for making the same |
-
2002
- 2002-03-08 US US10/092,715 patent/US7049435B2/en not_active Expired - Lifetime
-
2003
- 2003-03-06 IL IL16366203A patent/IL163662A0/xx unknown
- 2003-03-06 BR BR0308261-0A patent/BR0308261A/pt not_active IP Right Cessation
- 2003-03-06 KR KR1020047014006A patent/KR101024882B1/ko not_active Expired - Fee Related
- 2003-03-06 CA CA002481405A patent/CA2481405A1/en not_active Abandoned
- 2003-03-06 WO PCT/US2003/006627 patent/WO2003076453A1/en not_active Ceased
- 2003-03-06 EP EP08011594A patent/EP2039699A3/de not_active Withdrawn
- 2003-03-06 RU RU2004129749/04A patent/RU2326887C2/ru not_active IP Right Cessation
- 2003-03-06 AT AT03744177T patent/ATE540962T1/de active
- 2003-03-06 EP EP03744177A patent/EP1483278B1/de not_active Expired - Lifetime
- 2003-03-06 MX MXPA04009842A patent/MXPA04009842A/es active IP Right Grant
- 2003-03-06 AU AU2003216515A patent/AU2003216515B2/en not_active Ceased
- 2003-03-06 JP JP2003574668A patent/JP5196702B2/ja not_active Expired - Fee Related
- 2003-03-06 CN CNB038055279A patent/CN1318437C/zh not_active Expired - Lifetime
- 2003-03-07 AR ARP030100792A patent/AR038901A1/es not_active Application Discontinuation
- 2003-03-07 TW TW092104871A patent/TW200408647A/zh unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AU2003216515B2 (en) | 2008-07-10 |
| KR101024882B1 (ko) | 2011-03-31 |
| IL163662A0 (en) | 2005-12-18 |
| CN1318437C (zh) | 2007-05-30 |
| KR20040099305A (ko) | 2004-11-26 |
| WO2003076453A1 (en) | 2003-09-18 |
| CN1646551A (zh) | 2005-07-27 |
| RU2326887C2 (ru) | 2008-06-20 |
| CA2481405A1 (en) | 2003-09-18 |
| TW200408647A (en) | 2004-06-01 |
| EP2039699A2 (de) | 2009-03-25 |
| RU2004129749A (ru) | 2005-04-20 |
| AU2003216515A1 (en) | 2003-09-22 |
| AR038901A1 (es) | 2005-02-02 |
| EP1483278B1 (de) | 2012-01-11 |
| EP2039699A3 (de) | 2010-11-17 |
| BR0308261A (pt) | 2005-01-04 |
| EP1483278A1 (de) | 2004-12-08 |
| US7049435B2 (en) | 2006-05-23 |
| US20030171574A1 (en) | 2003-09-11 |
| JP2005526075A (ja) | 2005-09-02 |
| MXPA04009842A (es) | 2005-06-17 |
| JP5196702B2 (ja) | 2013-05-15 |
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