ATE282044T1 - Chromatographische reinigung von chlorinierter sukrose - Google Patents

Chromatographische reinigung von chlorinierter sukrose

Info

Publication number
ATE282044T1
ATE282044T1 AT98906453T AT98906453T ATE282044T1 AT E282044 T1 ATE282044 T1 AT E282044T1 AT 98906453 T AT98906453 T AT 98906453T AT 98906453 T AT98906453 T AT 98906453T AT E282044 T1 ATE282044 T1 AT E282044T1
Authority
AT
Austria
Prior art keywords
chlorinated sucrose
adsorbent
chromatographic purification
chlorinated
sucrose
Prior art date
Application number
AT98906453T
Other languages
English (en)
Inventor
Stephen J Catani
Duane Leinhos
Thomas O'connor
Original Assignee
Tate & Lyle Plc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate & Lyle Plc filed Critical Tate & Lyle Plc
Application granted granted Critical
Publication of ATE282044T1 publication Critical patent/ATE282044T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
AT98906453T 1997-02-13 1998-02-11 Chromatographische reinigung von chlorinierter sukrose ATE282044T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US4698097P 1997-02-13 1997-02-13
PCT/US1998/002927 WO1998035974A1 (en) 1997-02-13 1998-02-11 Chromatographic purification of chlorinated sucrose

Publications (1)

Publication Number Publication Date
ATE282044T1 true ATE282044T1 (de) 2004-11-15

Family

ID=21946404

Family Applications (1)

Application Number Title Priority Date Filing Date
AT98906453T ATE282044T1 (de) 1997-02-13 1998-02-11 Chromatographische reinigung von chlorinierter sukrose

Country Status (17)

Country Link
US (1) US5977349A (de)
EP (1) EP0970096B1 (de)
JP (2) JP4623763B2 (de)
KR (2) KR100531261B1 (de)
AT (1) ATE282044T1 (de)
AU (1) AU6167598A (de)
BR (1) BR9807377B1 (de)
CA (1) CA2280784A1 (de)
DE (1) DE69827482T2 (de)
DK (1) DK0970096T3 (de)
ES (1) ES2231964T3 (de)
IL (1) IL131394A0 (de)
NO (1) NO313553B1 (de)
NZ (1) NZ337573A (de)
PT (1) PT970096E (de)
TR (1) TR199902413T2 (de)
WO (1) WO1998035974A1 (de)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1998035974A1 (en) * 1997-02-13 1998-08-20 Mcneil-Ppc Inc. Chromatographic purification of chlorinated sucrose
US7049435B2 (en) * 2002-03-08 2006-05-23 Tate & Lyle Public Limited Company Extractive methods for purifying sucralose
US6998480B2 (en) * 2002-03-08 2006-02-14 Tate & Lyle Public Limited Company Process for improving sucralose purity and yield
US6890581B2 (en) * 2002-04-05 2005-05-10 Tate & Lyle Public Limited Company Methods for buffer stabilized aqueous deacylation
WO2006061856A2 (en) * 2004-12-10 2006-06-15 Pharmed Medicare Private Limited Improved process for purificaton of 6 acetyl 4,1’,6’ trichlorogalactosucrose and 4,1’,6’ trichlorogalactosucrose by chromatography on silanized silica gel
WO2006088017A1 (ja) * 2005-02-16 2006-08-24 National University Corporation Hokkaido University ４位ハロゲン化ガラクトース含有糖鎖及びその応用
US20060276639A1 (en) * 2005-06-01 2006-12-07 Healthy Brands, Llc Conversion of sucralose-6-ester to sucralose
WO2007023505A2 (en) * 2005-06-06 2007-03-01 Pharmed Medicare Private Limited Method for purification of chlorinated sucrose derivatives from reaction mixture by chromatography
JP2009509925A (ja) * 2005-08-30 2009-03-12 ファームド メディケア プライヴェート リミテッド 疎水性親和性クロマトグラフィに基づく塩素化スクロースの生成方法
EP2029522A2 (de) * 2006-05-23 2009-03-04 V.B. Medicare Pvt. Ltd. Rückgewinnung von dimethylformamid und anderen lösungsmitteln aus verfahrensströmen aus der herstellung von trichlorgalactosaccharose
CN101029062B (zh) * 2007-04-09 2011-06-15 淄博联技甜味剂有限公司 三氯蔗糖的合成工艺
US8436156B2 (en) * 2008-01-04 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
KR20100130219A (ko) * 2008-03-20 2010-12-10 테이트 앤드 라일 테크놀러지 리미티드 ３급 아미드 용매로부터 산을 제거하는 방법
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
WO2009137193A2 (en) * 2008-04-03 2009-11-12 Tate & Lyte Technology Ltd Effect of carbohydrate concentration on sucralose extraction efficiency
US20090259036A1 (en) * 2008-04-03 2009-10-15 Tate & Lyle Technology Limited Extraction of less polar impurities from sucralose containing aqueous feed streams
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
GB2468936B (en) 2009-03-27 2011-09-07 Mohamad Rami Radwan Jaber Chlorination of sucrose-6-esters
GB2469157B (en) * 2009-03-30 2011-07-06 John Kerr Process for removing dimethylamine during sucralose production
GB2469158B (en) 2009-03-31 2011-09-28 Peter J Seaberg Base-assisted formation of tin-sucrose adducts
GB2474310B (en) 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
GB2474311B (en) * 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
US20120034366A1 (en) * 2010-08-05 2012-02-09 Tate & Lyle Ingredients Americas, Inc. Carbohydrate compositions
GB201110520D0 (en) 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
CN102830197B (zh) * 2012-07-25 2015-07-15 湖北省宏源药业科技股份有限公司 一种中控监测单酯法合成三氯蔗糖过程的方法
US10227367B2 (en) 2013-12-16 2019-03-12 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
WO2016020635A1 (en) 2014-08-08 2016-02-11 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
GB2536480B (en) 2015-03-17 2019-09-04 Tate & Lyle Tech Ltd DMF Distillation
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ZA807578B (en) * 1979-12-18 1981-11-25 Tate & Lyle Patent Holdings Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3165986D1 (en) * 1980-07-08 1984-10-18 Tate & Lyle Plc Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs)
ZA817425B (en) * 1980-10-28 1982-10-27 Tate & Lyle Patent Holdings Sweet chlorine-substituted disaccharides
DE3262120D1 (en) * 1981-05-22 1985-03-14 Tate & Lyle Plc Brominated sucrose derivatives
GB8316201D0 (en) * 1982-09-13 1983-07-20 Tate & Lyle Plc Sucrose derivatives
GB8822673D0 (en) * 1988-09-27 1988-11-02 Tate & Lyle Plc Selective acylation of sugars
US4980463A (en) * 1989-07-18 1990-12-25 Noramco, Inc. Sucrose-6-ester chlorination
JPH06253879A (ja) * 1993-03-01 1994-09-13 Snow Brand Milk Prod Co Ltd グルクロン酸結合オリゴ糖の分離方法
US5298611A (en) * 1993-03-12 1994-03-29 Mcneil-Ppc, Inc. Sucralose pentaester production
US5530106A (en) * 1993-03-12 1996-06-25 Mcneil-Ppc, Inc. Recovery of sucralose intermediates
EP0687491A1 (de) * 1994-06-16 1995-12-20 Daicel Chemical Industries, Ltd. Chromatographisches simuliertes Wanderbetttrennungsverfahren
US5498709A (en) * 1994-10-17 1996-03-12 Mcneil-Ppc, Inc. Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
WO1998035974A1 (en) * 1997-02-13 1998-08-20 Mcneil-Ppc Inc. Chromatographic purification of chlorinated sucrose

Also Published As

Publication number Publication date
NO993920D0 (no) 1999-08-13
DK0970096T3 (da) 2005-03-21
JP5132665B2 (ja) 2013-01-30
NO993920L (no) 1999-10-11
JP2010090160A (ja) 2010-04-22
EP0970096A1 (de) 2000-01-12
PT970096E (pt) 2005-03-31
AU6167598A (en) 1998-09-08
ES2231964T3 (es) 2005-05-16
TR199902413T2 (xx) 2000-01-21
KR100619874B1 (ko) 2006-09-06
BR9807377B1 (pt) 2009-12-01
JP4623763B2 (ja) 2011-02-02
KR20050093860A (ko) 2005-09-23
DE69827482T2 (de) 2005-12-15
BR9807377A (pt) 2001-06-19
JP2001511812A (ja) 2001-08-14
US5977349A (en) 1999-11-02
NZ337573A (en) 2000-06-23
EP0970096B1 (de) 2004-11-10
NO313553B1 (no) 2002-10-21
IL131394A0 (en) 2001-01-28
CA2280784A1 (en) 1998-08-20
KR20000071081A (ko) 2000-11-25
WO1998035974A1 (en) 1998-08-20
DE69827482D1 (de) 2004-12-16
KR100531261B1 (ko) 2005-11-28

Similar Documents

Publication Publication Date Title
ATE282044T1 (de) Chromatographische reinigung von chlorinierter sukrose
MY107040A (en) Continuous process and apparatus for the chromatographic separation of a mixture of at least three constituents into three effluents purified by means of two solvents
DK0658164T3 (da) Fremgangsmåde til chromatografisk oprensning og adskillelse af nukleinsyreblandinger
MX9707909A (es) Purificacion de anticuerpos.
EP0658615A3 (de) Verfahren zur Rückwinnung von Benzenen aus Kohlenwasserstoffgemischen.
DE69206171D1 (de) Verfahren zum Trennen von Vielkomponentengasmischungen durch selektive Adsorption.
NZ336688A (en) Method for separating paraxylene comprising adsorption with water injection and crystallisation
IL127180A (en) Method for fractionation of a solution by a chromatographic simulated moving bed process
TW327611B (en) Process for purifying fluids by temperature swing adsorption process
ES8205570A1 (es) Un procedimiento de separacion con material adsorbente en lecho solido
MY137242A (en) Process for co-producing paraxylene and metaxylene, comprising two separation steps.
ATE182085T1 (de) Verfahren zur trennung eines materials von einer mischung durch verdrängungschromatographie
DE3880819T2 (de) Gastrennung.
ATE267635T1 (de) Flüssigphasen-adsorptions-verfahren zur entfernung und aufkonzentration heteroatomarer verbindungen in kohlenwasserstoffen
NO824313L (no) Vaeskefaseprosess for selektiv separering av hydrokarbonkomponenter.
US5603837A (en) Separation of a multicomponent mixture into components thereof
NO942721L (no) Fremgangsmåte for separering av komponenter i en væskeblanding
EP0187479A3 (de) Extraktion von Aromaten mit Ethylacetoacetat
DK0942921T3 (da) Forögede udbytter af krystalliseret protein ved anvendelse af et fast adsorptionsmateriale
EP0182673A3 (de) Verfahren zur Erhöhung der Abtrennung von Paraxylol aus einem anderen Xylol und Ethylbenzol enthaltenden Strom
KR930012070A (ko) 분말 활성탄에 의한 희박 용액의 탈색 방법
DK0698038T3 (da) Fremgangsmåde til separering af glycosylerede og ikke-glycosylerede proteiner
JPH01232259A (ja) イオンクロマトグラフ装置
DE60100306D1 (de) Verfahren zur Trennung in der Gasphase mittels Molekularsieben von Mischungen von Kohlenwasserstoffenisomeren
JPH04265857A (ja) カラムクロマトグラフ法による精製方法

Legal Events

Date Code Title Description
RER Ceased as to paragraph 5 lit. 3 law introducing patent treaties