BR9807377B1 - processo para separação de fase lìquida de uma sacarose clorada a partir de uma mistura de reação de sacarose clorada. - Google Patents

processo para separação de fase lìquida de uma sacarose clorada a partir de uma mistura de reação de sacarose clorada.

Info

Publication number
BR9807377B1
BR9807377B1 BRPI9807377-0A BR9807377A BR9807377B1 BR 9807377 B1 BR9807377 B1 BR 9807377B1 BR 9807377 A BR9807377 A BR 9807377A BR 9807377 B1 BR9807377 B1 BR 9807377B1
Authority
BR
Brazil
Prior art keywords
chlorinated sucrose
reaction mixture
separating
liquid phase
chlorinated
Prior art date
Application number
BRPI9807377-0A
Other languages
English (en)
Other versions
BR9807377A (pt
Inventor
Stephen J Catani
Duane A Leinhos
Thomas O'connor
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Publication of BR9807377A publication Critical patent/BR9807377A/pt
Publication of BR9807377B1 publication Critical patent/BR9807377B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
BRPI9807377-0A 1997-02-13 1998-02-11 processo para separação de fase lìquida de uma sacarose clorada a partir de uma mistura de reação de sacarose clorada. BR9807377B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US4698097P 1997-02-13 1997-02-13
PCT/US1998/002927 WO1998035974A1 (en) 1997-02-13 1998-02-11 Chromatographic purification of chlorinated sucrose

Publications (2)

Publication Number Publication Date
BR9807377A BR9807377A (pt) 2001-06-19
BR9807377B1 true BR9807377B1 (pt) 2009-12-01

Family

ID=21946404

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI9807377-0A BR9807377B1 (pt) 1997-02-13 1998-02-11 processo para separação de fase lìquida de uma sacarose clorada a partir de uma mistura de reação de sacarose clorada.

Country Status (17)

Country Link
US (1) US5977349A (pt)
EP (1) EP0970096B1 (pt)
JP (2) JP4623763B2 (pt)
KR (2) KR100531261B1 (pt)
AT (1) ATE282044T1 (pt)
AU (1) AU6167598A (pt)
BR (1) BR9807377B1 (pt)
CA (1) CA2280784A1 (pt)
DE (1) DE69827482T2 (pt)
DK (1) DK0970096T3 (pt)
ES (1) ES2231964T3 (pt)
IL (1) IL131394A0 (pt)
NO (1) NO313553B1 (pt)
NZ (1) NZ337573A (pt)
PT (1) PT970096E (pt)
TR (1) TR199902413T2 (pt)
WO (1) WO1998035974A1 (pt)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DK0970096T3 (da) * 1997-02-13 2005-03-21 Tate & Lyle Plc Kromatografisk oprensning af chloreret saccharose
US6998480B2 (en) * 2002-03-08 2006-02-14 Tate & Lyle Public Limited Company Process for improving sucralose purity and yield
US7049435B2 (en) * 2002-03-08 2006-05-23 Tate & Lyle Public Limited Company Extractive methods for purifying sucralose
US6890581B2 (en) * 2002-04-05 2005-05-10 Tate & Lyle Public Limited Company Methods for buffer stabilized aqueous deacylation
GB2437442B (en) * 2004-12-10 2010-03-31 Pharmed Medicare Pvt Ltd Improved process for purification of 6 acetyl 4,1',6' trichlorogalactosucrose and 4,1'6' trichlorogalactosucrose by chromatography on silanized silica gel
WO2006088017A1 (ja) * 2005-02-16 2006-08-24 National University Corporation Hokkaido University ４位ハロゲン化ガラクトース含有糖鎖及びその応用
US20060276639A1 (en) * 2005-06-01 2006-12-07 Healthy Brands, Llc Conversion of sucralose-6-ester to sucralose
US20100197906A1 (en) * 2005-06-06 2010-08-05 Pharmed Medicare Private Limited Method for purification of chlorinated sucrose derivatives from reaction mixture by chromatography
CA2620869A1 (en) * 2005-08-30 2007-05-10 Pharmed Medicare Pvt. Ltd. Process for production of chlorinated sucrose based on hydrophobic affinity chromatography
JP2009538293A (ja) * 2006-05-23 2009-11-05 ヴイ ビー メディケア プライヴェート リミテッド トリクロロガラクトスクロース製造のプロセスストリームからのジメチルホルムアミド及び他の溶媒の回収
CN101029062B (zh) * 2007-04-09 2011-06-15 淄博联技甜味剂有限公司 三氯蔗糖的合成工艺
US8436156B2 (en) * 2008-01-04 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
WO2009117317A1 (en) * 2008-03-20 2009-09-24 Tate & Lyle Technology Ltd Removal of acids from tertiary amide solvents
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
CN101981044B (zh) * 2008-04-03 2014-08-06 塔特和莱利技术有限公司 碳水化合物浓度对三氯半乳蔗糖萃取效率的影响
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
WO2009124113A1 (en) * 2008-04-03 2009-10-08 Tate & Lyle Technology Ltd. Extraction of less polar impurities from sucralose containing aqueous feed streams
GB2468936B (en) 2009-03-27 2011-09-07 Mohamad Rami Radwan Jaber Chlorination of sucrose-6-esters
GB2469157B (en) 2009-03-30 2011-07-06 John Kerr Process for removing dimethylamine during sucralose production
GB2469158B (en) 2009-03-31 2011-09-28 Peter J Seaberg Base-assisted formation of tin-sucrose adducts
GB2474310B (en) 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
GB2474311B (en) * 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
US20120034366A1 (en) * 2010-08-05 2012-02-09 Tate & Lyle Ingredients Americas, Inc. Carbohydrate compositions
GB201110520D0 (en) 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
CN102830197B (zh) * 2012-07-25 2015-07-15 湖北省宏源药业科技股份有限公司 一种中控监测单酯法合成三氯蔗糖过程的方法
CN105829332B (zh) 2013-12-16 2018-10-02 塔特和莱利技术有限公司 蔗糖-6-酯的氯化
GB2544217B (en) 2014-08-08 2020-03-25 Tate & Lyle Tech Ltd Chlorination of sucrose-6-esters
GB2536480B (en) 2015-03-17 2019-09-04 Tate & Lyle Tech Ltd DMF Distillation
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF

Family Cites Families (13)

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Publication number Priority date Publication date Assignee Title
ZA807578B (en) * 1979-12-18 1981-11-25 Tate & Lyle Patent Holdings Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
EP0043649B1 (en) * 1980-07-08 1984-09-12 TATE & LYLE PUBLIC LIMITED COMPANY Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs)
ZA817425B (en) * 1980-10-28 1982-10-27 Tate & Lyle Patent Holdings Sweet chlorine-substituted disaccharides
DE3262120D1 (en) * 1981-05-22 1985-03-14 Tate & Lyle Plc Brominated sucrose derivatives
GB8316201D0 (en) * 1982-09-13 1983-07-20 Tate & Lyle Plc Sucrose derivatives
GB8822673D0 (en) * 1988-09-27 1988-11-02 Tate & Lyle Plc Selective acylation of sugars
US4980463A (en) * 1989-07-18 1990-12-25 Noramco, Inc. Sucrose-6-ester chlorination
JPH06253879A (ja) * 1993-03-01 1994-09-13 Snow Brand Milk Prod Co Ltd グルクロン酸結合オリゴ糖の分離方法
US5298611A (en) * 1993-03-12 1994-03-29 Mcneil-Ppc, Inc. Sucralose pentaester production
US5530106A (en) * 1993-03-12 1996-06-25 Mcneil-Ppc, Inc. Recovery of sucralose intermediates
EP0687491A1 (en) * 1994-06-16 1995-12-20 Daicel Chemical Industries, Ltd. Simulated moving bed chromatographic separation process
US5498709A (en) * 1994-10-17 1996-03-12 Mcneil-Ppc, Inc. Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
DK0970096T3 (da) * 1997-02-13 2005-03-21 Tate & Lyle Plc Kromatografisk oprensning af chloreret saccharose

Also Published As

Publication number Publication date
NO313553B1 (no) 2002-10-21
ATE282044T1 (de) 2004-11-15
NZ337573A (en) 2000-06-23
CA2280784A1 (en) 1998-08-20
AU6167598A (en) 1998-09-08
JP2001511812A (ja) 2001-08-14
WO1998035974A1 (en) 1998-08-20
KR100619874B1 (ko) 2006-09-06
DK0970096T3 (da) 2005-03-21
EP0970096B1 (en) 2004-11-10
EP0970096A1 (en) 2000-01-12
PT970096E (pt) 2005-03-31
KR100531261B1 (ko) 2005-11-28
TR199902413T2 (xx) 2000-01-21
NO993920L (no) 1999-10-11
JP2010090160A (ja) 2010-04-22
US5977349A (en) 1999-11-02
IL131394A0 (en) 2001-01-28
ES2231964T3 (es) 2005-05-16
BR9807377A (pt) 2001-06-19
DE69827482T2 (de) 2005-12-15
DE69827482D1 (de) 2004-12-16
JP5132665B2 (ja) 2013-01-30
NO993920D0 (no) 1999-08-13
KR20050093860A (ko) 2005-09-23
JP4623763B2 (ja) 2011-02-02
KR20000071081A (ko) 2000-11-25

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B25A Requested transfer of rights approved

Owner name: TATE AND LYLE PUBLIC LIMITED COMPANY (GB)

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B06A Patent application procedure suspended [chapter 6.1 patent gazette]
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B09A Decision: intention to grant [chapter 9.1 patent gazette]
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Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 15/12/2009, OBSERVADAS AS CONDICOES LEGAIS.

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Owner name: TATE AND LYLE TECHNOLOGY LIMITED (GB)

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