WO2009008393A1 - 強制超薄膜回転式処理法を用いたナノ粒子の製造方法 - Google Patents

強制超薄膜回転式処理法を用いたナノ粒子の製造方法 Download PDF

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Publication number
WO2009008393A1
WO2009008393A1 PCT/JP2008/062236 JP2008062236W WO2009008393A1 WO 2009008393 A1 WO2009008393 A1 WO 2009008393A1 JP 2008062236 W JP2008062236 W JP 2008062236W WO 2009008393 A1 WO2009008393 A1 WO 2009008393A1
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WO
WIPO (PCT)
Prior art keywords
thin film
producing nanoparticles
rotary processing
film rotary
forced
Prior art date
Application number
PCT/JP2008/062236
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English (en)
French (fr)
Inventor
Masakazu Enomura
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M.Technique Co., Ltd.
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Publication date
Application filed by M.Technique Co., Ltd. filed Critical M.Technique Co., Ltd.
Priority to EP08790916.4A priority Critical patent/EP2184109B1/en
Priority to JP2009522636A priority patent/JP4817154B2/ja
Priority to US12/668,013 priority patent/US9211510B2/en
Priority to KR1020097027663A priority patent/KR101402734B1/ko
Priority to CN200880105423.2A priority patent/CN101795772B/zh
Publication of WO2009008393A1 publication Critical patent/WO2009008393A1/ja

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1887—Stationary reactors having moving elements inside forming a thin film
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/41—Emulsifying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50—Mixing liquids with solids
    • B01F23/53—Mixing liquids with solids using driven stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/70—Spray-mixers, e.g. for mixing intersecting sheets of material
    • B01F25/74—Spray-mixers, e.g. for mixing intersecting sheets of material with rotating parts, e.g. discs
    • B01F25/741—Spray-mixers, e.g. for mixing intersecting sheets of material with rotating parts, e.g. discs with a disc or a set of discs mounted on a shaft rotating about a vertical axis, on top of which the material to be thrown outwardly is fed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
    • B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
    • B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
    • B01F27/2712—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator provided with ribs, ridges or grooves on one surface
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
    • B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
    • B01F27/2714—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator the relative position of the stator and the rotor, gap in between or gap with the walls being adjustable
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C7/00—Crushing or disintegrating by disc mills
    • B02C7/11—Details
    • B02C7/14—Adjusting, applying pressure to, or controlling distance between, discs
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B22F1/056—Submicron particles having a size above 100 nm up to 300 nm
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    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
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    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
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    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
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    • C09B67/0001—Post-treatment of organic pigments or dyes
    • C09B67/0022—Wet grinding of pigments
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    • B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
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    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Manufacturing & Machinery (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Crushing And Grinding (AREA)
  • Silicon Compounds (AREA)
  • Disintegrating Or Milling (AREA)

Abstract

　接近・離反可能な相対的に回転する２つの処理用面間に１ｍｍ以下の微小間隔を維持し、この微小間隔に維持された２つの処理用面間を被処理流動体の流路とすることによって、被処理流動体の強制薄膜を形成し、この強制薄膜中においてナノ粒子の析出を行うことを特徴とするナノ粒子の製造方法を提供する。
PCT/JP2008/062236 2007-07-06 2008-07-04 強制超薄膜回転式処理法を用いたナノ粒子の製造方法 WO2009008393A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP08790916.4A EP2184109B1 (en) 2007-07-06 2008-07-04 Method for producing nanoparticles by forced ultra-thin film rotary processing
JP2009522636A JP4817154B2 (ja) 2007-07-06 2008-07-04 強制超薄膜回転式処理法を用いたナノ粒子の製造方法
US12/668,013 US9211510B2 (en) 2007-07-06 2008-07-04 Method for producing nanoparticles by forced ultrathin film rotary processing
KR1020097027663A KR101402734B1 (ko) 2007-07-06 2008-07-04 강제 초박막 회전식 처리법을 사용한 나노입자의 제조방법
CN200880105423.2A CN101795772B (zh) 2007-07-06 2008-07-04 使用强制超薄膜旋转式处理法的纳米粒子的制造方法

Applications Claiming Priority (24)

Application Number Priority Date Filing Date Title
JP2007179103 2007-07-06
JP2007-179102 2007-07-06
JP2007179100 2007-07-06
JP2007179102 2007-07-06
JP2007-179101 2007-07-06
JP2007179104 2007-07-06
JP2007179099 2007-07-06
JP2007-179098 2007-07-06
JP2007-179103 2007-07-06
JP2007179101 2007-07-06
JP2007-179104 2007-07-06
JP2007-179099 2007-07-06
JP2007179098 2007-07-06
JP2007-179100 2007-07-06
JP2007-180349 2007-07-09
JP2007180349 2007-07-09
JP2007203850 2007-08-06
JP2007-203850 2007-08-06
JP2007207426 2007-08-09
JP2007-207426 2007-08-09
JP2007214821 2007-08-21
JP2007-214821 2007-08-21
JP2007-233557 2007-09-10
JP2007233557 2007-09-10

Publications (1)

Publication Number Publication Date
WO2009008393A1 true WO2009008393A1 (ja) 2009-01-15

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PCT/JP2008/062236 WO2009008393A1 (ja) 2007-07-06 2008-07-04 強制超薄膜回転式処理法を用いたナノ粒子の製造方法

Country Status (6)

Country Link
US (1) US9211510B2 (ja)
EP (1) EP2184109B1 (ja)
JP (3) JP2009082902A (ja)
KR (1) KR101402734B1 (ja)
TW (1) TWI441672B (ja)
WO (1) WO2009008393A1 (ja)

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JP2011140432A (ja) * 2009-12-08 2011-07-21 Toyota Motor Corp 金属複合酸化物の合成方法、及び、当該合成方法により得られる金属複合酸化物
JP2011177037A (ja) * 2010-02-26 2011-09-15 Kishu Hosokawa:Kk 有機酸の中和方法
WO2011158537A1 (ja) * 2010-06-16 2011-12-22 エム・テクニック株式会社 新規なキナクリドン顔料組成物及びキナクリドン微粒子の製造方法
US20120006230A1 (en) * 2009-03-03 2012-01-12 M. Technique Co., Ltd. Method for treating surface of pigment microparticles
JP4868558B1 (ja) * 2011-04-28 2012-02-01 エム・テクニック株式会社 酸化物・水酸化物の製造方法
WO2012014530A1 (ja) * 2010-07-28 2012-02-02 エム・テクニック株式会社 粒子径を制御された微粒子の製造方法
WO2012128273A1 (ja) * 2011-03-23 2012-09-27 エム・テクニック株式会社 微粒子の製造方法
WO2012137628A1 (ja) * 2011-04-01 2012-10-11 エム・テクニック株式会社 バリウムチタニル塩及びチタン酸バリウムの製造方法
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