MY189272A - Process for the regeneration of a titanium zeolite catalyst for propylene epoxidation - Google Patents

Process for the regeneration of a titanium zeolite catalyst for propylene epoxidation

Info

Publication number
MY189272A
MY189272A MYPI2017001194A MYPI2017001194A MY189272A MY 189272 A MY189272 A MY 189272A MY PI2017001194 A MYPI2017001194 A MY PI2017001194A MY PI2017001194 A MYPI2017001194 A MY PI2017001194A MY 189272 A MY189272 A MY 189272A
Authority
MY
Malaysia
Prior art keywords
catalyst
regeneration
reactor
feed stream
zeolite catalyst
Prior art date
Application number
MYPI2017001194A
Other languages
English (en)
Inventor
Riedel Dominic Dr
Teles Joaquim Henrique Dr
Urbanczyk Daniel Dr
Ulrike Wegerle
Spiske Luise Dr
Parvulescu Andrei-Nicolae Dr
Schroeder Alexander Dr
Mueller Ulrich Dr
Weidenbach Meinolf Dr
Werner J Witzl
Original Assignee
Dow Global Technologies Llc
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies Llc, Basf Se filed Critical Dow Global Technologies Llc
Publication of MY189272A publication Critical patent/MY189272A/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/90—Regeneration or reactivation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/02—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/12—Treating with free oxygen-containing gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/183—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself in framework positions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B01J35/647—2-50 nm
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/08—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the aluminium atoms being wholly replaced
    • C01B39/085—Group IVB- metallosilicates
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Epoxy Compounds (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
MYPI2017001194A 2015-02-13 2016-02-12 Process for the regeneration of a titanium zeolite catalyst for propylene epoxidation MY189272A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201562115658P 2015-02-13 2015-02-13
EP15154998 2015-02-13
PCT/EP2016/052983 WO2016128538A1 (en) 2015-02-13 2016-02-12 Process for the regeneration of a titanium zeolite catalyst for propylene epoxidation

Publications (1)

Publication Number Publication Date
MY189272A true MY189272A (en) 2022-01-31

Family

ID=52472215

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI2017001194A MY189272A (en) 2015-02-13 2016-02-12 Process for the regeneration of a titanium zeolite catalyst for propylene epoxidation

Country Status (11)

Country Link
US (1) US10195598B2 (enExample)
EP (1) EP3256252B1 (enExample)
JP (1) JP6685315B2 (enExample)
KR (1) KR102512661B1 (enExample)
CN (2) CN119456024A (enExample)
BR (1) BR112017017269B1 (enExample)
MX (1) MX2017010402A (enExample)
MY (1) MY189272A (enExample)
PL (1) PL3256252T3 (enExample)
SG (1) SG11201706530RA (enExample)
WO (1) WO2016128538A1 (enExample)

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CN107735392B (zh) 2015-05-04 2021-12-03 巴斯夫欧洲公司 制备甜瓜醛的方法
EP3322685A1 (en) 2015-07-15 2018-05-23 Basf Se Process for preparing an arylpropene
BR112018000606B1 (pt) 2015-07-22 2022-01-18 Basf Se Processo para preparação de ácido furan-2,5- dicarboxílico e uso de um catalisador
EP3170828A1 (de) 2015-11-23 2017-05-24 Basf Se Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten
JP2018538284A (ja) 2015-11-27 2018-12-27 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 金属−有機骨格体の超高速高空時収量合成
MX2018007068A (es) 2015-12-08 2018-08-01 Basf Se Un material zeolitico con contenido de estaño que tiene una estructura de armazon de bea.
EP3178788A1 (en) 2015-12-08 2017-06-14 Basf Se A tin-containing zeolitic material having a bea framework structure
US10618873B2 (en) 2016-02-01 2020-04-14 Basf Se Method for producing C4-C15 lactams
MX2018016297A (es) 2016-06-29 2019-09-16 Basf Se Proceso para la preparacion de aldehidos alfa, beta insaturados mediante oxidacion de alcoholes en presencia de una fase liquida.
JP6986063B2 (ja) 2016-07-08 2021-12-22 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 有機スルホンの製造方法
SG11201811020XA (en) 2016-07-20 2019-02-27 Basf Se A process for purifying propylene oxide
KR102445812B1 (ko) 2016-07-29 2022-09-21 바스프 코포레이션 FAU-타입 골격 구조를 갖는 제올라이트성 물질의 제조 방법 및 NOx의 선택적 접촉 환원에서의 이의 용도
WO2018096171A1 (en) 2016-11-28 2018-05-31 Basf Se Catalyst composite comprising an alkaline earth metal containing cha zeolite and use thereof in a process for the conversion of oxygenates to olefins
US11091425B2 (en) 2016-11-30 2021-08-17 Basf Se Process for the conversion of ethylene glycol to ethylenediamine employing a zeolite catalyst
WO2018099964A1 (en) 2016-11-30 2018-06-07 Basf Se Process for the conversion of monoethanolamine to ethylenediamine employing a copper-modified zeolite of the mor framework structure
BR112019010134B1 (pt) 2016-12-13 2022-11-29 Basf Se Processo para preparar um material zeolítico, material zeolítico, e, uso do material
BR112020010507A2 (pt) * 2017-12-21 2020-11-10 Basf Se processo para a preparação de aldeídos alfa, beta insaturados
EP3604222A1 (en) * 2018-07-30 2020-02-05 Evonik Operations GmbH Process for the purification of hydrogen cyanide
US20210403333A1 (en) * 2018-11-15 2021-12-30 Dalian Institute Of Chemical Physics, Chinese Academy Of Sciences Method for preparing hierarchical porous titanosilicate ts-1 molecular sieve
TW202045484A (zh) * 2019-02-08 2020-12-16 德商贏創運營有限公司 有機化合物的氧化
CN110252393A (zh) * 2019-05-21 2019-09-20 江西农业大学 一种用于合成环氧大豆油的钛硅沸石负载镉催化剂、制备方法及应用
CN110075914A (zh) * 2019-05-28 2019-08-02 江苏扬农化工集团有限公司 一种hppo工艺失活钛硅分子筛催化剂器内再生的方法
EP3812375A1 (en) * 2019-10-21 2021-04-28 Evonik Operations GmbH Process for the epoxidation of propene
CN112354557B (zh) * 2020-11-16 2023-03-24 华东师范大学 一种整体式钛沸石催化剂制备方法及其应用
CN112678866B (zh) * 2020-12-24 2023-07-04 中国石油化工股份有限公司 一种烯烃聚合工业废酸渣资源化处理方法
CN112844468A (zh) * 2021-01-19 2021-05-28 中国科学院大连化学物理研究所 一种用于丙烯气相环氧化制环氧丙烷的催化剂及其制备方法
US20240279194A1 (en) * 2021-06-15 2024-08-22 Basf Se Shutdown method for a process for preparing an olefin oxide
CN113368895B (zh) * 2021-07-13 2023-09-29 福州大学 一种具有高转化率的丙烯气相环氧化催化剂的制备方法
WO2023056231A1 (en) * 2021-09-30 2023-04-06 Basf Corporation Pretreatment of porous metal oxide catalysts for use in dehydrogenation and other reactions
CN118022856B (zh) * 2022-11-04 2026-04-07 万华化学集团股份有限公司 一种双氧水法环氧氯丙烷环氧化用催化剂的再生工艺
WO2024115737A1 (en) 2022-12-02 2024-06-06 Basf Se Process for regeneration of an epoxidation reactor
CN117504927B (zh) * 2023-11-10 2025-04-29 江西师范大学 一种负载型Ti-MWW分子筛与金属氧化物的复合催化剂及其制备与应用
CN119034224B (zh) * 2024-07-19 2026-08-11 华陆工程科技有限责任公司 一种多晶硅渣浆的回收系统和方法

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CN102791376A (zh) * 2010-03-18 2012-11-21 住友化学株式会社 钛硅酸盐催化剂的再生方法
EP3216520B1 (en) 2012-02-07 2024-07-17 Basf Se Molding containing a zeolitic mww type material containing ti and zn and use thereof as a catalyst
CN104014365B (zh) * 2013-02-28 2016-08-24 中国石油化工股份有限公司 一种钛硅分子筛的再生方法
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Also Published As

Publication number Publication date
KR102512661B1 (ko) 2023-03-21
BR112017017269B1 (pt) 2022-05-24
US10195598B2 (en) 2019-02-05
EP3256252A1 (en) 2017-12-20
KR20170117509A (ko) 2017-10-23
US20180036723A1 (en) 2018-02-08
WO2016128538A1 (en) 2016-08-18
CN119456024A (zh) 2025-02-18
JP6685315B2 (ja) 2020-04-22
SG11201706530RA (en) 2017-09-28
JP2018511459A (ja) 2018-04-26
EP3256252B1 (en) 2021-04-07
BR112017017269A2 (en) 2018-04-17
MX2017010402A (es) 2018-05-28
CN107530693A (zh) 2018-01-02
PL3256252T3 (pl) 2021-10-25

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