JP2018516952A - ジアリールスルホンを製造するための改良された方法 - Google Patents

ジアリールスルホンを製造するための改良された方法 Download PDF

Info

Publication number
JP2018516952A
JP2018516952A JP2017563946A JP2017563946A JP2018516952A JP 2018516952 A JP2018516952 A JP 2018516952A JP 2017563946 A JP2017563946 A JP 2017563946A JP 2017563946 A JP2017563946 A JP 2017563946A JP 2018516952 A JP2018516952 A JP 2018516952A
Authority
JP
Japan
Prior art keywords
aryl
alkyl
hours
minutes
coupling step
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2017563946A
Other languages
English (en)
Japanese (ja)
Inventor
ムルガン，ラミア
エー． ヘイ，デビッド
エー． ヘイ，デビッド
Original Assignee
ヴァーテラス ホールディングス エルエルシー
ヴァーテラス ホールディングス エルエルシー
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ヴァーテラス ホールディングス エルエルシー, ヴァーテラス ホールディングス エルエルシー filed Critical ヴァーテラス ホールディングス エルエルシー
Publication of JP2018516952A publication Critical patent/JP2018516952A/ja
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C315/00—Preparation of sulfones; Preparation of sulfoxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C315/00—Preparation of sulfones; Preparation of sulfoxides
    • C07C315/04—Preparation of sulfones; Preparation of sulfoxides by reactions not involving the formation of sulfone or sulfoxide groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B01J21/04—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/066—Zirconium or hafnium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/06—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of zinc, cadmium or mercury
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/18—Arsenic, antimony or bismuth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0215—Sulfur-containing compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0255—Phosphorus containing compounds
    • B01J31/0257—Phosphorus acids or phosphorus acid esters
    • B01J31/0258—Phosphoric acid mono-, di- or triesters ((RO)(R'O)2P=O), i.e. R= C, R'= C, H
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
    • C07C303/06—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with sulfuric acid or sulfur trioxide
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C315/00—Preparation of sulfones; Preparation of sulfoxides
    • C07C315/06—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C317/00—Sulfones; Sulfoxides
    • C07C317/14—Sulfones; Sulfoxides having sulfone or sulfoxide groups bound to carbon atoms of six-membered aromatic rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2017563946A 2015-06-09 2016-06-09 ジアリールスルホンを製造するための改良された方法 Pending JP2018516952A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201562173283P 2015-06-09 2015-06-09
US62/173,283 2015-06-09
PCT/US2016/036587 WO2016201039A1 (en) 2015-06-09 2016-06-09 Improved process for making diaryl sulfones

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2020190852A Division JP7027509B2 (ja) 2015-06-09 2020-11-17 ジアリールスルホンを製造するための改良された方法

Publications (1)

Publication Number Publication Date
JP2018516952A true JP2018516952A (ja) 2018-06-28

Family

ID=57504373

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2017563946A Pending JP2018516952A (ja) 2015-06-09 2016-06-09 ジアリールスルホンを製造するための改良された方法
JP2020190852A Active JP7027509B2 (ja) 2015-06-09 2020-11-17 ジアリールスルホンを製造するための改良された方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2020190852A Active JP7027509B2 (ja) 2015-06-09 2020-11-17 ジアリールスルホンを製造するための改良された方法

Country Status (6)

Country Link
US (2) US10745348B2 (enExample)
EP (2) EP3805202A1 (enExample)
JP (2) JP2018516952A (enExample)
KR (1) KR102629634B1 (enExample)
CN (1) CN107922325B (enExample)
WO (1) WO2016201039A1 (enExample)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10809947B2 (en) * 2016-04-06 2020-10-20 Emerge Print Management, Llc Apparatus and method for metering and monitoring printer related data on non-networked printers
EP3441393B1 (en) * 2017-08-07 2020-03-18 Rhodia Operations New cycloadduct precursors of dihalodiphenylsulfones and preparations thereof
WO2021037797A1 (en) * 2019-08-27 2021-03-04 Basf Se (c)crystal composition (cc) comprising 4,4'-dichlorodiphenylsulfone crystals (c)
US20220388949A1 (en) 2019-11-13 2022-12-08 Basf Se A process for working up water containing 4,4'-dichlorodiphenyl sulfoxide and/or 4,4'-dichlorodiphenyl sulfone as impurities

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5785363A (en) * 1980-11-18 1982-05-28 Mitsui Toatsu Chem Inc Preparation of diaryl sulfone
JPS6368556A (ja) * 1986-09-09 1988-03-28 New Japan Chem Co Ltd ジアリ−ルスルホン類の製造方法
US4937387A (en) * 1986-09-05 1990-06-26 Amoco Corporation Processes for preparing diaryl sulfones
US4983773A (en) * 1988-10-19 1991-01-08 Basf Aktiengesellschaft Preparation of bis-(4-chlorophenyl) sulfone
JPH04221336A (ja) * 1990-04-04 1992-08-11 Imperial Chem Ind Plc <Ici> 芳香族化合物の製造方法
JPH1017542A (ja) * 1996-06-28 1998-01-20 New Japan Chem Co Ltd ジアリールスルホン類の製造方法
JP2015500312A (ja) * 2011-12-15 2015-01-05 ソルベイ スペシャルティ ポリマーズ ユーエスエー， エルエルシー ジハロジアリールスルホンの異性体の混合物からハロアリール化合物を製造する方法

Family Cites Families (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2971985A (en) 1958-07-05 1961-02-14 Roussel Uclaf Process for the preparation of 4, 4'-dichlorodiphenylsulfone
GB895464A (en) * 1958-07-05 1962-05-02 U C L A F Improvements in or relating to sulphones
US3309409A (en) 1964-04-10 1967-03-14 Stauffer Chemical Co Purification of acidic chlorophenylsulfones
US3355497A (en) 1965-02-01 1967-11-28 Plains Chemical Dev Co Manufacture of 4, 4'-dichlorodiphenyl sulfone
CH497396A (de) 1968-11-06 1970-10-15 Inventa Ag Verfahren zum Reinigen von Halogendiphenylsulfonen
US3855312A (en) * 1970-02-06 1974-12-17 Ici Ltd Production of di-4-chlorophenyl sulphone
JPS5182237A (en) 1975-01-16 1976-07-19 Nippon Soda Co 4*4** jikurofuenirusurupponnoseizojiniokeru jimechiruryusannokaishuhoho
JPS5188938A (en) 1975-01-31 1976-08-04 Kojundo 4*4** jikurorujifuenirusurupponnobunrihoho
US4778932A (en) * 1986-07-16 1988-10-18 New Japan Chemical Co., Ltd. Process for preparing diarylsulfones
DE3704932A1 (de) 1987-02-17 1988-09-01 Basf Ag Verfahren zur herstellung von 4,4'-dichlordiphenylsulfon
US4822916A (en) * 1987-09-21 1989-04-18 Akzo America Inc. Preparation of diaryl sulfones
US4876390A (en) 1988-08-19 1989-10-24 Uop Process for separating dichlorodiphenylsulfone isomers
DE3902894A1 (de) * 1989-02-01 1990-08-02 Basf Ag Verfahren zur herstellung von bis-(4-chlorphenyl)-sulfon
DE3902890A1 (de) 1989-02-01 1990-08-02 Basf Ag Verfahren zur herstellung von bis-(4-chlorphenyl)-sulfon
JPH06116231A (ja) * 1992-10-06 1994-04-26 Ube Ind Ltd ４，４’−ジクロロジフェニルスルホンの精製法
JPH09143150A (ja) 1995-11-28 1997-06-03 Tokuyama Corp 芳香族スルホンの製造方法
JPH09157246A (ja) 1995-12-13 1997-06-17 Tokuyama Corp ４，４’−ジクロロジフェニルスルホンの単離方法
JPH09165366A (ja) 1995-12-15 1997-06-24 Tokuyama Corp 芳香族スルホンの製造方法
JP3188173B2 (ja) 1996-01-10 2001-07-16 株式会社トクヤマ 芳香族スルホンの製造方法
RO113981B1 (ro) 1998-01-30 1998-12-30 Inst Cercetari Chim Procedeu de obținere a 4,4' -diclor
CN1623982A (zh) 2003-12-02 2005-06-08 马炳荣 4，4’－二氯二苯砜的制备方法
GB0921069D0 (en) * 2009-12-01 2010-01-13 Bandodkar Hemant R Process for the production of a sulfone polymer
WO2011107465A1 (de) 2010-03-05 2011-09-09 Basf Se Verfahren zur herstellung von 4-chlorbenzolsulfonsäure und 4,4'-dichlordiphenylsulfon
EP2383256A1 (de) 2010-04-22 2011-11-02 Basf Se Verfahren zur Herstellung von 4,4'-Dichlordiphenylsulfon
US20110263902A1 (en) 2010-04-22 2011-10-27 Basf Se Process for preparing 4,4'-dichlorodiphenyl sulfone
EP2383257A1 (de) 2010-04-22 2011-11-02 Basf Se Verfahren zur Herstellung von 4,4'-Dichlordiphenylsulfon
US20110263903A1 (en) 2010-04-22 2011-10-27 Basf Se Process for preparing 4,4'-dichlorodiphenyl sulfone
CN103619810B (zh) 2011-04-18 2017-02-15 索维特殊聚合物有限责任公司 用于制造二卤代二苯砜的方法
CN102351759A (zh) 2011-08-25 2012-02-15 吴江市北厍盛源纺织品助剂厂 改进的制备4.4-二氯二苯砜的三氧化硫方法
WO2013153412A1 (en) 2012-04-12 2013-10-17 Hemant Ratanakar Bandodkar Process for the conversion of isomeric mixture of dichlorodiphenyl sulfones to chlorobenzene

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5785363A (en) * 1980-11-18 1982-05-28 Mitsui Toatsu Chem Inc Preparation of diaryl sulfone
US4937387A (en) * 1986-09-05 1990-06-26 Amoco Corporation Processes for preparing diaryl sulfones
JPS6368556A (ja) * 1986-09-09 1988-03-28 New Japan Chem Co Ltd ジアリ−ルスルホン類の製造方法
US4983773A (en) * 1988-10-19 1991-01-08 Basf Aktiengesellschaft Preparation of bis-(4-chlorophenyl) sulfone
JPH04221336A (ja) * 1990-04-04 1992-08-11 Imperial Chem Ind Plc <Ici> 芳香族化合物の製造方法
JPH1017542A (ja) * 1996-06-28 1998-01-20 New Japan Chem Co Ltd ジアリールスルホン類の製造方法
JP2015500312A (ja) * 2011-12-15 2015-01-05 ソルベイ スペシャルティ ポリマーズ ユーエスエー， エルエルシー ジハロジアリールスルホンの異性体の混合物からハロアリール化合物を製造する方法

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
CHEMICAL COMMUNICATIONS (CAMBRIDGE, UNITED KINGDOM), vol. (17), JPN6020015651, 2001, pages 1696 - 1697, ISSN: 0004431513 *
JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, vol. 2(1), JPN6020015656, 2005, pages 47 - 53, ISSN: 0004431516 *
PHOSPHORUS, SULFUR AND SILICON AND THE RELATED ELEMENTS, vol. 180(9), JPN6020015654, 2005, pages 2029 - 2034, ISSN: 0004431515 *
SYNTHESIS, vol. (4), JPN6020015652, 1984, pages 323 - 5, ISSN: 0004431514 *

Also Published As

Publication number Publication date
US20210171457A1 (en) 2021-06-10
EP3307710A4 (en) 2018-12-19
CN107922325B (zh) 2021-09-07
EP3805202A1 (en) 2021-04-14
EP3307710B1 (en) 2020-09-30
KR20180016425A (ko) 2018-02-14
KR102629634B1 (ko) 2024-01-25
CN107922325A (zh) 2018-04-17
JP7027509B2 (ja) 2022-03-01
JP2021042221A (ja) 2021-03-18
EP3307710A1 (en) 2018-04-18
WO2016201039A1 (en) 2016-12-15
US10745348B2 (en) 2020-08-18
US20180179153A1 (en) 2018-06-28

Similar Documents

Publication Publication Date Title
JP7027509B2 (ja) ジアリールスルホンを製造するための改良された方法
EP3157930B1 (en) Methods for the preparation of 1,3-benzodioxole heterocyclic compounds
JP5016575B2 (ja) ストロンチウムラネレートおよびその水和物の新規な合成法
JPH0460466B2 (enExample)
IE912543A1 (en) Production of acetaminophen
JP2002241363A (ja) スルホニウム塩の製造方法
JPH04145061A (ja) 高純度４，４´―ジヒドロキシジフェニルスルホンの製造法
JPS5962543A (ja) ２，２−ビス（４−ヒドロキシフエニル）プロパンの製法
JPS642577B2 (enExample)
JP3570760B2 (ja) ２−ｔ−ブチルハイドロキノンの製造方法
JP2815071B2 (ja) ジクロロジフェニルスルホンの製造方法
JPH05500813A (ja) アルキル―〔３クロロフェニル〕―スルホンの製造方法
JPS5965039A (ja) ２，４−ジヒドロキシアセトフエノンの製造方法
JPS5962542A (ja) 精製２，２−ビス（４−ヒドロキシフエニル）プロパンのフエノ−ル付加物の製法
JP2000344699A (ja) ビスフェノールａの製造方法
JPH02304061A (ja) 含硫黄脂肪族カルボン酸エステル及びその酸の製造方法
JP4807690B2 (ja) ジフェニルスルホン化合物の製造方法
JP6439219B2 (ja) 含フッ素フェノールの製造法
KR101081115B1 (ko) 베타카로텐의 제조방법
JP2002145851A (ja) ４，４’−ビスフェノールスルホンの製造方法
JPS62135B2 (enExample)
JP2649722B2 (ja) ４，４’‐（１―フェニルエチリデン）ビスフェノールの製造方法
JPS6354356A (ja) 芳香族チオ−ルの製造法
JP4011364B2 (ja) ２，４’−ジヒドロキシジフェニルスルホンの製造方法
JPH0318617B2 (enExample)

Legal Events

Date Code Title Description
RD03 Notification of appointment of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7423

Effective date: 20180329

RD04 Notification of resignation of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7424

Effective date: 20180330

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20190603

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20200312

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20200518

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20200818

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20210125