JP2017500409A5 - - Google Patents
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- JP2017500409A5 JP2017500409A5 JP2016541091A JP2016541091A JP2017500409A5 JP 2017500409 A5 JP2017500409 A5 JP 2017500409A5 JP 2016541091 A JP2016541091 A JP 2016541091A JP 2016541091 A JP2016541091 A JP 2016541091A JP 2017500409 A5 JP2017500409 A5 JP 2017500409A5
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- 125000000962 organic group Chemical group 0.000 claims description 21
- 229920005640 poly alpha-1,3-glucan Polymers 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 17
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- 150000001875 compounds Chemical class 0.000 claims description 14
- -1 ether compound Chemical class 0.000 claims description 14
- 238000006467 substitution reaction Methods 0.000 claims description 10
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 239000000416 hydrocolloid Substances 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- 229920001503 Glucan Polymers 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- GETQZCLCWQTVFV-UHFFFAOYSA-O trimethylammonium Chemical group C[NH+](C)C GETQZCLCWQTVFV-UHFFFAOYSA-O 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000002768 hydroxyalkyl group Chemical group 0.000 description 1
- KFZMGEQAYNKOFK-UHFFFAOYSA-N iso-propanol Chemical group CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 1
- 230000003472 neutralizing Effects 0.000 description 1
- 125000001453 quaternary ammonium group Chemical group 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Description
表5のデータは、四級アンモニウムグルカンポリマーが、異なる塩及びpH条件下で種々の種類の布地に吸着し得ることを示す。この吸着は、ポリマーへの曝露後に布地をすすいだ場合でも起こる。グルカンエーテルが、綿に吸着するのに加え、ポリエステル及びポリエステル/クレトンブレンドに吸着できたことは注目に値する。
このように、水性組成物中のポリα−1,3−グルカンエーテル誘導体は布地に吸着できる。
このように、水性組成物中のポリα−1,3−グルカンエーテル誘導体は布地に吸着できる。
以上、本発明を要約すると下記のとおりである。
1.以下の構造により表されるポリα−1,3−グルカンエーテル化合物を含む組成物:
(式中
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、且つ
(iii)前記化合物は、約0.05から約3.0の置換度を有する)。
2.少なくとも1種の正電荷を帯びた有機基が、置換されているアンモニウム基を含む、上記1に記載の組成物。
3.前記正電荷を帯びた有機基が、トリメチルアンモニウム基を含む、上記2に記載の組成物。
4.前記正電荷を帯びた有機基が、四級アンモニウム基である、上記2に記載の組成物。5.少なくとも1種の正電荷を帯びた有機基が、アルキル基又はヒドロキシアルキル基を含む、上記1に記載の組成物。
6.少なくとも1種の正電荷を帯びた有機基が、四級アンモニウムヒドロキシプロピル基である、上記5に記載の組成物。
7.ポリα−1,3−グルカンエーテル化合物を製造する方法であって、
(a)ポリα−1,3−グルカンを、アルカリ条件下での反応物中で、正電荷を帯びた有機基を含む少なくとも1種のエーテル化剤と接触させ、少なくとも1種の正電荷を帯びた有機基が前記ポリα−1,3−グルカンにエーテル化されて、それにより以下の構造により表されるポリα−1,3−グルカンエーテル化合物を製造すること:
(式中
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、且つ
(iii)前記化合物は、約0.05から約3.0の置換度を有する);及び
(b)任意選択で、工程(a)で製造された前記ポリα−1,3−グルカンエーテル化合物を単離すること
を含む方法。
8.前記アルカリ条件がアルカリ水酸化物溶液を含む、上記7に記載の方法。
9.前記反応物が有機溶媒を含む、上記7に記載の方法。
10.前記有機溶媒がイソプロパノールである、上記9に記載の方法。
11.工程(a)が、
(i)前記反応物を加熱すること;及び/又は
(ii)前記反応物のpHを中和すること
をさらに含む、上記7に記載の方法。
12.少なくとも1種の正電荷を帯びた有機基が、置換されているアンモニウム基を含む、上記7に記載の方法。
13.少なくとも1種の正電荷を帯びた有機基が、トリメチルアンモニウム基を含む、上記12に記載の方法。
14.以下の構造により表されるポリα−1,3−グルカンエーテル化合物を含む親水コロイド又は水溶液:
(式中
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、
(iii)前記化合物は、約0.05から約3.0の置換度を有し、且つ
(iv)前記親水コロイド又は水溶液は、少なくとも約10cPsの粘度を有する)。
15.水性組成物の粘度を増加させる方法であって、
ポリα−1,3−グルカンエーテル化合物を前記水性組成物と接触させることを含み、前記水性組成物の粘度が前記化合物により増加し、
前記化合物が以下の構造により表される方法:
(式中
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、且つ
(iii)前記化合物は、約0.05から約3.0の置換度を有する)。
16.材料を処理する方法であって、
材料を、以下の構造により表されるポリα−1,3−グルカンエーテル化合物を含む水性組成物と接触させることを含む方法:
(式中
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、且つ
(iii)前記化合物は、約0.05から約3.0の置換度を有する)。
1.以下の構造により表されるポリα−1,3−グルカンエーテル化合物を含む組成物:
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、且つ
(iii)前記化合物は、約0.05から約3.0の置換度を有する)。
2.少なくとも1種の正電荷を帯びた有機基が、置換されているアンモニウム基を含む、上記1に記載の組成物。
3.前記正電荷を帯びた有機基が、トリメチルアンモニウム基を含む、上記2に記載の組成物。
4.前記正電荷を帯びた有機基が、四級アンモニウム基である、上記2に記載の組成物。5.少なくとも1種の正電荷を帯びた有機基が、アルキル基又はヒドロキシアルキル基を含む、上記1に記載の組成物。
6.少なくとも1種の正電荷を帯びた有機基が、四級アンモニウムヒドロキシプロピル基である、上記5に記載の組成物。
7.ポリα−1,3−グルカンエーテル化合物を製造する方法であって、
(a)ポリα−1,3−グルカンを、アルカリ条件下での反応物中で、正電荷を帯びた有機基を含む少なくとも1種のエーテル化剤と接触させ、少なくとも1種の正電荷を帯びた有機基が前記ポリα−1,3−グルカンにエーテル化されて、それにより以下の構造により表されるポリα−1,3−グルカンエーテル化合物を製造すること:
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、且つ
(iii)前記化合物は、約0.05から約3.0の置換度を有する);及び
(b)任意選択で、工程(a)で製造された前記ポリα−1,3−グルカンエーテル化合物を単離すること
を含む方法。
8.前記アルカリ条件がアルカリ水酸化物溶液を含む、上記7に記載の方法。
9.前記反応物が有機溶媒を含む、上記7に記載の方法。
10.前記有機溶媒がイソプロパノールである、上記9に記載の方法。
11.工程(a)が、
(i)前記反応物を加熱すること;及び/又は
(ii)前記反応物のpHを中和すること
をさらに含む、上記7に記載の方法。
12.少なくとも1種の正電荷を帯びた有機基が、置換されているアンモニウム基を含む、上記7に記載の方法。
13.少なくとも1種の正電荷を帯びた有機基が、トリメチルアンモニウム基を含む、上記12に記載の方法。
14.以下の構造により表されるポリα−1,3−グルカンエーテル化合物を含む親水コロイド又は水溶液:
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、
(iii)前記化合物は、約0.05から約3.0の置換度を有し、且つ
(iv)前記親水コロイド又は水溶液は、少なくとも約10cPsの粘度を有する)。
15.水性組成物の粘度を増加させる方法であって、
ポリα−1,3−グルカンエーテル化合物を前記水性組成物と接触させることを含み、前記水性組成物の粘度が前記化合物により増加し、
前記化合物が以下の構造により表される方法:
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、且つ
(iii)前記化合物は、約0.05から約3.0の置換度を有する)。
16.材料を処理する方法であって、
材料を、以下の構造により表されるポリα−1,3−グルカンエーテル化合物を含む水性組成物と接触させることを含む方法:
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、且つ
(iii)前記化合物は、約0.05から約3.0の置換度を有する)。
Claims (5)
- ポリα−1,3−グルカンエーテル化合物を製造する方法であって、
(a)ポリα−1,3−グルカンを、アルカリ条件下での反応物中で、正電荷を帯びた有機基を含む少なくとも1種のエーテル化剤と接触させ、少なくとも1種の正電荷を帯びた有機基が前記ポリα−1,3−グルカンにエーテル化されて、それにより以下の構造により表されるポリα−1,3−グルカンエーテル化合物を製造すること:
(i)nは少なくとも6であり、
(ii)各Rは、独立に、H又は正電荷を帯びた有機基であり、且つ
(iii)前記化合物は、約0.05から約3.0の置換度を有する);及び
(b)任意選択で、工程(a)で製造された前記ポリα−1,3−グルカンエーテル化合物を単離すること
を含む方法。
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201361917507P | 2013-12-18 | 2013-12-18 | |
US61/917,507 | 2013-12-18 | ||
US201462014273P | 2014-06-19 | 2014-06-19 | |
US62/014,273 | 2014-06-19 | ||
PCT/US2014/070906 WO2015095358A1 (en) | 2013-12-18 | 2014-12-17 | Cationic poly alpha-1,3-glucan ethers |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2017500409A JP2017500409A (ja) | 2017-01-05 |
JP2017500409A5 true JP2017500409A5 (ja) | 2018-01-25 |
JP6559139B2 JP6559139B2 (ja) | 2019-08-14 |
Family
ID=52293259
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2016541091A Active JP6559139B2 (ja) | 2013-12-18 | 2014-12-17 | カチオン性ポリα−1,3−グルカンエーテル |
Country Status (11)
Country | Link |
---|---|
US (3) | US9957334B2 (ja) |
EP (2) | EP3789407B1 (ja) |
JP (1) | JP6559139B2 (ja) |
KR (1) | KR102410391B1 (ja) |
CN (1) | CN106029700B (ja) |
AU (1) | AU2014364772B2 (ja) |
BR (1) | BR112016014014B1 (ja) |
CA (1) | CA2932501C (ja) |
ES (1) | ES2835703T3 (ja) |
MX (1) | MX2016007920A (ja) |
WO (1) | WO2015095358A1 (ja) |
Cited By (1)
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JP7423026B1 (ja) | 2022-05-24 | 2024-01-29 | 株式会社オクト | バイオフィルムを破壊するための溶液及びその製造方法 |
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