JP2015530289A - バリアフィルム構築及びその作製方法 - Google Patents
バリアフィルム構築及びその作製方法 Download PDFInfo
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- JP2015530289A JP2015530289A JP2015526568A JP2015526568A JP2015530289A JP 2015530289 A JP2015530289 A JP 2015530289A JP 2015526568 A JP2015526568 A JP 2015526568A JP 2015526568 A JP2015526568 A JP 2015526568A JP 2015530289 A JP2015530289 A JP 2015530289A
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- Prior art keywords
- layer
- barrier film
- polymer layer
- base polymer
- adhesion
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Abstract
Description
本出願は、米国特許法(35 U.S.C.)119(e)条に従い、2012年8月8日出願の米国仮特許出願第61/680,963号、及び2013年3月13日出願の米国仮特許出願第61/779455号の優先権を主張する。
本開示は、概してバリアフィルム及びバリアフィルムの作成方法に関する。
比較積層構成体A及び積層構成体1〜2は、22.9cm×15.2cmバリアフィルムを、エチレンテトラフルオロエチレンポリマーシート(ETFE)(厚さ0.05mm、「NORTON ETFE」の商品名でSt.Gobain Performance Plastics(米国ニュージャージー州Wayne)から入手可能)に積層するために、厚さ0.05mmの感圧接着剤(PSA)(「3M OPTICALLY CLEAR ADHESIVE 8172P」の商品名で3M Company(米国ミネソタ州St.Paul)から得た)を使用することによって、ETFEシートに隣接するバリアフィルムの上塗りポリマー層をともなって調製された。比較積層構成体A及び積層構成体1〜2は、それぞれ、比較実施例A、及び実施例1〜2のバリアフィルムを使用して調製された。次いで、バリアフィルムのポリエチレンテレフタレート(PET)側は、厚さ0.14mm(0.0056インチ)21.6cm×14cmのポリテトラフルオロエチレン(PTFE)コーティングしたアルミホイル(「8656K61」の商品名でMcMaster−Carr(米国カリフォルニア州Santa Fe Spring)から得た)のPTFE側の上に定置された。PTFEコーティングしたアルミホイルは、それぞれの寸法がバリアフィルムより1.27cm小さいため、PETの一部が露出したままである。幅13mm(0.5インチ)の乾燥したエッジテープ(「SOLARGAIN EDGE TAPE SET LP01」の商品名でTruseal Technologies Inc.(米国オハイオ州Solon)から得た)を、積層されたバリアシートをPTFE層に固定するために、PTFEコーティングしたアルミホイルの周囲の周りに定置した。厚さ0.38cm(0.015インチ)封止材フィルム(「JURASOL」の商品名でJuraFilms(米国イリノイ州Downer Grove)から得た)をPTFEコーティングしたアルミホイルのアルミニウム側に定置した。封止材フィルムの上に積層構成体を形成するために、第1の積層したバリアシートと組成が同一の第2の積層したバリアシートのPET層が、配置された。構成体を、150℃で12分間真空積層した。
分光透過率
分光透過率は、分光計(PerkinElmer(米国マサチューセッツ州Waltham)から市販のモデル「LAMBDA 900」)を使用して測定された。分光透過率は、400nm〜700nmの間で、入射角0°で、平均透過率パーセント(Tvis)として報告された。
比較実施例A及び実施例1〜2のバリアフィルムの水蒸気透過率(WVTR)は、ASTM F−1249−06「Standard Test Method for Water Vapor Transmission Rate Through Plastic Film and Sheeting Using a Modulated Infrared Sensor」に概説される手順に基づいて、MOCON PERMATRAN−W(登録商標)Model 700 WVTR試験システム(MOCON,Inc(米国ミネソタ州Minneapolis)から得られた)を使用して測定された。約50℃の温度及び約100%の相対湿度(RH)が使用され、WVTRは、グラム/平方メートル/日(g/m2/日)で表された。試験システムの最低検出限界は、0.005g/m2/日であった。場合によっては、測定されたWVTRは、最低検出限界より低く、<0.005g/m2/日と報告された。
比較実施例A及び実施例1〜2のバリアフィルムで調製された積層構成体を、環境チャンバ(Thermotron Industries(米国ミシガン州Holland)から得られたモデル「SE−1000−3」)内に定置し、0時間(初期)、250時間、及び500時間の間、約85℃の温度、及び約85%の相対湿度に設定した。
比較実施例A、実施例1及び実施例2のエージングしたバリアフィルムとエージングしていないバリアフィルムとが、PTFE層を剥離して除去することによって積層構成体から除去された。次いで、バリアフィルムは、幅1.0インチ(2.54cm)の切片に切断された。これらの切片は、ASTM D 1876−08「Standard Test Method for Peel Resistance of Adhesives(T−剥離試験)」に概説された手順に従って、引張り強度試験器(「INISIGHT 2 SL」の商品名でTestworks 4ソフトウェア付きでMTS(米国ミネソタ州Eden Prairie)から得た)に定置された。254mm/min(10インチ/min)の剥離速度が使用された。接着は、0.05〜5.95cmの間の4つの剥離測定の平均として、ニュートン/センチメートル(N/cm)で報告された。
バリアフィルムは、ポリエチレンテレフタレート(PET)基材フィルム(E.I.DuPont de Nemours(米国デラウエア州Wilmington)から「XST 6642」という商標で得られた)を、ベースポリマー層、無機ケイ素アルミニウム酸化物(SiAlOx)バリア層、及び上塗りポリマー層の積層体で、米国特許第5,440,446号(Shawら)及び同第7,018,713号(Padiyathら)(両者とも参照により本明細書に組み込まれる)に記載されるものと同様の真空コーター上で被覆することによって調製された。個々の層は以下のように形成された。
バリアフィルムは、接着促進材料が層2の上(すなわち、蒸気化及び凝縮)で、かつ上塗りポリマー層(層3)の堆積及び凝縮のすぐ前に堆積されたことを除いて、比較実施例Aに記載されているように調製された。バリアフィルムは、引き続いて比較実施例Aに記載するように、電子線架橋された。
バリアフィルムは、接着促進材料が(3−アクリロキシプロピル)トリメトキシシラン(Gelestから「SIA0A200.0」の商品名で得られた)であったことを除いて、実施例1に記載されているように調整された。
Claims (28)
- バリアフィルムであって、
基材と、
前記基材に隣接するベースポリマー層と、
前記ベースポリマー層に隣接する酸化物層と、
前記酸化物層に隣接する接着性調整層と、
前記接着性調整層に隣接する上塗りポリマー層と、
を備える、バリアフィルム。 - 前記基材と前記上塗りポリマーとの間に、複数の前記ベースポリマー層と前記酸化物層との交互層を更に備える、請求項1に記載のバリアフィルム。
- 前記基材が、可撓性透明フィルムを備える、請求項1又は2に記載のバリアフィルム。
- 前記ベースポリマー層が、アクリレートを含む、請求項1〜3のいずれか一項に記載のバリアフィルム。
- 前記酸化物層が、無機ケイ素アルミニウム酸化物の層を備える、請求項1〜4のいずれか一項に記載のバリアフィルム。
- 前記上塗りポリマー層に塗布される無機層を更に備える、請求項1〜5のいずれか一項に記載のバリアフィルム。
- 前記無機層が、無機ケイ素アルミニウム酸化物の層を含む、請求項6に記載のバリアフィルム。
- 前記上塗りポリマー層が、アクリレートを含む、請求項1〜7のいずれか一項に記載のバリアフィルム。
- 前記接着性調整層が、接着促進層である、請求項1〜8のいずれか一項に記載のバリアフィルム。
- 前記接着促進層がシランを含む、請求項1〜9のいずれか一項に記載のバリアフィルム。
- 前記接着性調整層が、リリース層である、請求項1〜10のいずれか一項に記載のバリアフィルム。
- 前記接着性調整層が、前記基材のうちの1つと前記ベースポリマー層との間、前記ベースポリマー層と前記酸化物材料との間、及び前記酸化物材料と前記上塗りポリマー層との間にある、請求項1〜11のいずれか一項に記載のバリアフィルム。
- バリアフィルムを作製するプロセスであって、
基材を提供する工程と、
ベースポリマー材料を前記基材に塗布する工程と、
酸化物材料を前記ベースポリマー材料に塗布する工程と、
接着性調整材料を前記酸化物材料に塗布する工程と、
上塗りポリマー層を前記接着性調整材料上に形成する工程と、
を含むプロセス。 - 前記ベースポリマー材料を前記基材に塗布する工程が、ベースポリマー材料を前記基材上に蒸着させて、前記蒸着させたベースポリマー材料を硬化してベースポリマー層を形成する工程を含む、請求項13に記載のプロセス。
- 前記酸化物材料を塗布する工程が、酸化物材料を前記ベースポリマー材料の上にスパッタ堆積する工程を含む、請求項13又は14に記載のプロセス。
- ベースポリマー材料を前記基材に塗布することと、酸化物材料を前記ベースポリマー材料に塗布することとを繰返して、前記ベースポリマー材料と前記酸化物材料との交互層を、前記基材と前記上塗りポリマー層との間に生成する工程を更に含む、請求項13〜15のいずれか一項に記載のプロセス。
- 前記上塗りポリマー層がアクリレートを含み、前記上塗りポリマー層を形成する工程が前記接着性調整材料及び前記アクリレートを共蒸着して前記共蒸着した接着性調整材料及びアクリレートを硬化する工程を含む、請求項13〜16のいずれか一項に記載のプロセス。
- 前記接着性調整材料及び前記上塗りポリマー層のうち少なくとも1つを硬化する工程を更に含む、請求項13〜17のいずれか一項に記載のプロセス。
- 前記ベースポリマー材料が、アクリレートを含む、請求項13〜18のいずれか一項に記載のプロセス。
- 前記酸化物材料を塗布する工程が、無機ケイ素アルミニウム酸化物の層を前記ベースポリマー層に塗布する工程を含む、請求項13〜19のいずれか一項に記載のプロセス。
- 無機材料を前記上塗りポリマー層に塗布する工程を更に含む、請求項13〜20のいずれか一項に記載のプロセス。
- 前記無機層を塗布する工程が、無機ケイ素アルミニウム酸化物の層を塗布する工程を含む、請求項21に記載のプロセス。
- 前記接着性調整層が、前記基材のうちの1つと前記ベースポリマー層との間、前記ベースポリマー層と前記酸化物材料との間、及び前記酸化物材料と前記上塗りポリマー層との間に配置される、請求項13〜22のいずれか一項に記載のプロセス。
- バリアフィルムであって、
基材と、
ベースポリマー層と、
酸化物層と、
接着性調整層と、
上塗りポリマー層と、
を備える、バリアフィルム。 - 前記接着性調整層が、前記基材のうちの1つと前記ベースポリマー層との間、前記ベースポリマー層と前記酸化物材料との間、及び前記酸化物材料と前記上塗りポリマー層との間に配置される、請求項24に記載のバリアフィルム。
- 前記接着性調整層が、前記上塗りポリマー層の上に配置される、請求項24に記載のバリアフィルム。
- 前記基材が、(コ)ポリマーフィルム又は電子デバイスから選択され、前記電子デバイスが、有機発光デバイス(OLED)、電気泳動発光デバイス、液晶ディスプレイ、薄膜トランジスタ、光起電デバイス、又はこれらの組み合わせを更に含む、請求項1〜12又は24〜26のいずれか一項に記載のバリアフィルム。
- 前記基材が、(コ)ポリマーフィルム又は電子デバイスから選択され、前記電子デバイスが、有機発光デバイス(OLED)、電気泳動発光デバイス、液晶ディスプレイ、薄膜トランジスタ、光起電デバイス、又はこれらの組み合わせを更に含む、請求項13〜23のいずれか一項に記載のプロセス。
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- 2013-07-30 CN CN201380042256.2A patent/CN104684727B/zh active Active
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WO2014025570A1 (en) | 2014-02-13 |
US10947618B2 (en) | 2021-03-16 |
US20190180968A1 (en) | 2019-06-13 |
CN104684727A (zh) | 2015-06-03 |
CN104684727B (zh) | 2017-05-17 |
TWI598224B (zh) | 2017-09-11 |
US20150213990A1 (en) | 2015-07-30 |
KR20150041062A (ko) | 2015-04-15 |
KR102126719B1 (ko) | 2020-06-25 |
EP2882587A4 (en) | 2016-04-13 |
TW201410455A (zh) | 2014-03-16 |
SG11201500934RA (en) | 2015-03-30 |
EP2882587A1 (en) | 2015-06-17 |
BR112015002840A2 (pt) | 2017-08-08 |
JP6316813B2 (ja) | 2018-04-25 |
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