JP2012510179A5 - - Google Patents

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Publication number
JP2012510179A5
JP2012510179A5 JP2011538634A JP2011538634A JP2012510179A5 JP 2012510179 A5 JP2012510179 A5 JP 2012510179A5 JP 2011538634 A JP2011538634 A JP 2011538634A JP 2011538634 A JP2011538634 A JP 2011538634A JP 2012510179 A5 JP2012510179 A5 JP 2012510179A5
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Japan
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integrated circuit
semiconductor integrated
circuit device
front surface
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JP2011538634A
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JP5620397B2 (ja
JP2012510179A (ja
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Priority claimed from US12/324,335 external-priority patent/US8388824B2/en
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Claims (1)

  1. 半導体集積回路デバイス基板におけるビア構造をメタライズするための方法であって、半導体集積回路デバイス基板は、前面、背面、ビア構造を備え、ビア構造は、基板の前面に開口部、基板の前面を内向きに伸びる側壁部、および底部を備え、前記方法は以下からなる:
    半導体集積回路デバイス基板に、(a)銅イオン源、および(b)レベラー化合物からなる電解銅沈積組成物を接触させて、前記レベラー化合物は以下の一般式(XIII)からなる:
    Figure 2012510179
    pおよびqは同じか異なる0〜6の整数で、p,qの何れかが少なくとも
    0で、Xは1〜4の整数で、Y,Zは塩素、臭素、ヨウ素、トシル、
    トリフレート、スルホネート、メシレート、ジメチルスルホネート、
    フロロスルホネート、メチルトシレート、ブロシレート、ノシレート;および
    R1〜R14は各々独立して水素、炭素数1〜6の置換または非置換アルキル、
    炭素数1〜6の置換または非置換アルキレン、置換または非置換アリールの
    何れかである。
    mは16の中の何れかの整数である。
JP2011538634A 2008-11-26 2009-11-19 ジピリジル系レベリング剤によるマイクロエレクトロニクスにおける銅の電子沈積 Active JP5620397B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/324,335 US8388824B2 (en) 2008-11-26 2008-11-26 Method and composition for electrodeposition of copper in microelectronics with dipyridyl-based levelers
US12/324,335 2008-11-26
PCT/US2009/065053 WO2010062822A2 (en) 2008-11-26 2009-11-19 Electrodeposition of copper in microelectronics with dipyridyl-based levelers

Publications (3)

Publication Number Publication Date
JP2012510179A JP2012510179A (ja) 2012-04-26
JP2012510179A5 true JP2012510179A5 (ja) 2013-01-24
JP5620397B2 JP5620397B2 (ja) 2014-11-05

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JP2011538634A Active JP5620397B2 (ja) 2008-11-26 2009-11-19 ジピリジル系レベリング剤によるマイクロエレクトロニクスにおける銅の電子沈積

Country Status (8)

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US (3) US8388824B2 (ja)
EP (1) EP2358926B1 (ja)
JP (1) JP5620397B2 (ja)
KR (1) KR101745731B1 (ja)
CN (1) CN102362013B (ja)
ES (1) ES2904299T3 (ja)
TW (2) TWI507570B (ja)
WO (1) WO2010062822A2 (ja)

Families Citing this family (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW200632147A (ja) 2004-11-12 2006-09-16
US10221496B2 (en) 2008-11-26 2019-03-05 Macdermid Enthone Inc. Copper filling of through silicon vias
US8388824B2 (en) * 2008-11-26 2013-03-05 Enthone Inc. Method and composition for electrodeposition of copper in microelectronics with dipyridyl-based levelers
US20120027948A1 (en) * 2009-04-07 2012-02-02 Basf Se Composition for metal plating comprising suppressing agent for void free submicron feature filling
WO2012078589A1 (en) * 2010-12-07 2012-06-14 Technic Inc. Electro-depositing metal layers of uniform thickness
EP2668317B1 (en) 2011-01-26 2017-08-23 MacDermid Enthone Inc. Process for filling vias in the microelectronics
US8454815B2 (en) * 2011-10-24 2013-06-04 Rohm And Haas Electronics Materials Llc Plating bath and method
US9105628B1 (en) * 2012-03-29 2015-08-11 Valery Dubin Through substrate via (TSuV) structures and method of making the same
CN110643600A (zh) 2012-10-23 2020-01-03 基因工具股份有限公司 用于切割靶dna的系统及其用途
TWI478861B (zh) * 2012-11-22 2015-04-01 Univ Nat Chunghsing Electrodeposition of copper nanoparticles
US10214826B2 (en) * 2013-01-29 2019-02-26 Novellus Systems, Inc. Low copper electroplating solutions for fill and defect control
US20160102416A1 (en) * 2013-01-29 2016-04-14 Novellus Systems, Inc. Low copper/high halide electroplating solutions for fill and defect control
US20140262800A1 (en) * 2013-03-12 2014-09-18 Taiwan Semiconductor Manufacturing Company, Ltd. Electroplating Chemical Leveler
EP2865787A1 (en) * 2013-10-22 2015-04-29 ATOTECH Deutschland GmbH Copper electroplating method
CN105917032A (zh) 2013-11-25 2016-08-31 乐思股份有限公司 铜的电沉积
TWI710671B (zh) * 2014-09-15 2020-11-21 美商麥德美樂思公司 微電子技術中銅沈積用之平整劑
JP6539811B2 (ja) * 2014-10-09 2019-07-10 石原ケミカル株式会社 低応力皮膜形成用の電気銅メッキ浴及び電気銅メッキ方法
CN105132953B (zh) * 2015-07-24 2017-11-21 中国原子能科学研究院 一种用于直接获得锆合金燃料的乏燃料干法后处理方法
US10100420B2 (en) 2015-12-29 2018-10-16 Hong Kong Applied Science and Technology Research Institute Company Limtied Plating leveler for electrodeposition of copper pillar
CN105441994B (zh) * 2015-12-30 2017-09-19 上海新阳半导体材料股份有限公司 一种能用于提高凸点共面性的电镀液组合物
US10749278B2 (en) 2016-01-15 2020-08-18 Taiwan Semiconductor Manufacturing Co., Ltd. Method of electroplating metal into recessed feature and electroplating layer in recessed feature
KR101733141B1 (ko) * 2016-03-18 2017-05-08 한국생산기술연구원 고평탄 구리도금막 형성을 위한 전해 구리 도금용 유기첨가제 및 이를 포함하는 전해구리 도금액
CN109996785B (zh) * 2016-09-22 2021-12-28 麦克德米德乐思公司 集成电路的晶圆级封装中的铜沉积
CN109952390A (zh) * 2016-09-22 2019-06-28 麦克德米德乐思公司 在微电子件中的铜的电沉积
CN107217283B (zh) * 2017-07-25 2018-11-16 上海新阳半导体材料股份有限公司 整平剂、含其的金属电镀组合物、制备方法及应用
CN107236976B (zh) * 2017-07-25 2018-11-16 上海新阳半导体材料股份有限公司 整平剂、含其的金属电镀组合物及制备方法、应用
CN111247633A (zh) * 2017-10-19 2020-06-05 朗姆研究公司 单一金属的多浴电镀
KR20200131909A (ko) 2018-04-09 2020-11-24 램 리써치 코포레이션 비-구리 라이너 층들 상의 구리 전기충진 (electrofill)
CN109972180B (zh) * 2019-04-12 2020-12-18 博敏电子股份有限公司 2,2'-二硫代二吡啶的新用途及采用其的电镀填孔添加剂及采用该添加剂的电镀方法
US11342229B2 (en) * 2019-06-13 2022-05-24 Taiwan Semiconductor Manufacturing Co., Ltd. Method for forming a semiconductor device structure having an electrical connection structure
EP4018790A1 (en) * 2019-08-19 2022-06-29 Atotech Deutschland GmbH & Co. KG Manufacturing sequences for high density interconnect printed circuit boards and a high density interconnect printed circuit board
CN110763699B (zh) * 2019-10-12 2022-12-20 广州兴森快捷电路科技有限公司 线路板的内层互连缺陷的分析方法及线路板
US11746433B2 (en) * 2019-11-05 2023-09-05 Macdermid Enthone Inc. Single step electrolytic method of filling through holes in printed circuit boards and other substrates
JP2023533784A (ja) * 2020-07-13 2023-08-04 ビーエーエスエフ ソシエタス・ヨーロピア コバルトシード上の銅電気メッキ用組成物
CN117659393A (zh) * 2022-08-31 2024-03-08 华为技术有限公司 一种整平剂、组合物及其应用

Family Cites Families (95)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2644789A (en) * 1951-08-02 1953-07-07 Harshaw Chem Corp Electrodeposition of nickel
US2658867A (en) * 1952-03-06 1953-11-10 Harshaw Chem Corp Electrodeposition of nickel
US2839460A (en) * 1956-11-16 1958-06-17 Hanson Van Winkle Munning Co Electrolating
US3002904A (en) * 1958-09-26 1961-10-03 Hanson Van Winkle Munning Co Electrodeposition of nickel
US3152975A (en) * 1961-02-07 1964-10-13 Hanson Van Winkle Munning Co Electrodeposition of nickel
GB1202525A (en) 1966-09-28 1970-08-19 Nat Res Dev Improvements in and relating to the electrodeposition of metals
US3592943A (en) * 1967-10-25 1971-07-13 M & T Chemicals Inc Novel processes and compositions for electroplating nickel
US3591350A (en) * 1968-06-17 1971-07-06 M & T Chemicals Inc Novel plating process
GB1202497A (en) * 1968-07-18 1970-08-19 Midland Yorkshire Tar Distille Preparation of quaternary vinyl pyridine salts and polymers thereof
US3641034A (en) * 1969-09-02 1972-02-08 Polaroid Corp Polymers of dipyridyl
BE755563A (fr) * 1969-09-02 1971-03-01 Polaroid Corp Dispositif de filtrage variable de lumiere
US3694384A (en) * 1971-01-11 1972-09-26 Gen Electric Redox polymers
US3715289A (en) * 1971-02-08 1973-02-06 Stauffer Chemical Co Brightener composition for acid copper electroplating baths
DE2116389C3 (de) * 1971-03-30 1980-04-03 Schering Ag, 1000 Berlin Und 4619 Bergkamen Lösung zur Aktivierung von Oberflächen für die Metallisierung
US3919056A (en) * 1972-09-26 1975-11-11 M & T Chemicals Inc Zinc plating process and electrolytes therefor
US3821095A (en) * 1972-09-26 1974-06-28 M & T Chemicals Inc Zinc electroplating process and electrolyte therefor
US3940320A (en) * 1972-12-14 1976-02-24 M & T Chemicals Inc. Electrodeposition of copper
US3956084A (en) * 1972-12-14 1976-05-11 M & T Chemicals Inc. Electrodeposition of copper
US3956078A (en) * 1972-12-14 1976-05-11 M & T Chemicals Inc. Electrodeposition of copper
US3856714A (en) * 1973-09-07 1974-12-24 Polaroid Corp Polyviologens
US4009087A (en) * 1974-11-21 1977-02-22 M&T Chemicals Inc. Electrodeposition of copper
US4036710A (en) * 1974-11-21 1977-07-19 M & T Chemicals Inc. Electrodeposition of copper
US4024328A (en) * 1975-10-01 1977-05-17 The Dow Chemical Company Method for alkylating aminomethylacrylamide polymers
US4038161A (en) * 1976-03-05 1977-07-26 R. O. Hull & Company, Inc. Acid copper plating and additive composition therefor
DE3066786D1 (en) * 1979-02-02 1984-04-12 Ciba Geigy Ag Process for dyeing cellulose-containing fibrous materials
US4617253A (en) * 1984-06-06 1986-10-14 Polaroid Corporation Polymeric pyridinium ylides and products prepared from same
US4786746A (en) * 1987-09-18 1988-11-22 Pennsylvania Research Corporation Copper electroplating solutions and methods of making and using them
US4983508A (en) * 1987-11-18 1991-01-08 Fuji Photo Film Co., Ltd. Method for manufacturing a light-sensitive silver halide emulsion
US4841021A (en) * 1987-11-30 1989-06-20 Minnesota Mining And Manufacturing Company Polypyridinium
JP2595319B2 (ja) * 1988-07-20 1997-04-02 日本電装株式会社 化学銅めっき液及びそれを用いた銅めっき皮膜の形成方法
US5051154A (en) * 1988-08-23 1991-09-24 Shipley Company Inc. Additive for acid-copper electroplating baths to increase throwing power
US5763563A (en) * 1989-09-01 1998-06-09 The University Of Akron Poly-pyridinium salts
US5965211A (en) * 1989-12-29 1999-10-12 Nippondenso Co., Ltd. Electroless copper plating solution and process for formation of copper film
US5147905A (en) * 1991-05-01 1992-09-15 The Dow Chemical Company Advanced and unadvanced compositions, nucleophilic derivatives thereof and curable and coating compositions thereof
EP0550601B1 (en) * 1990-09-25 1996-12-04 Allergan, Inc. Apparatus and method for disinfecting a contact lens and detecting the presence of an oxidative disinfectant
US5252196A (en) * 1991-12-05 1993-10-12 Shipley Company Inc. Copper electroplating solutions and processes
US5306336A (en) * 1992-11-20 1994-04-26 Monsanto Company Sulfate-free electroless copper plating baths
JPH06192418A (ja) * 1992-12-22 1994-07-12 Sagami Chem Res Center ポリカチオン系重合体
EP0676437B1 (en) * 1992-12-22 1999-09-08 Sagami Chemical Research Center Use of polycationic polymer as bactericidal/algicidal agent
US5382496A (en) * 1992-12-25 1995-01-17 Fuji Photo Film Co., Ltd. Silver halide light-sensitive material and a method for forming image using the same
JPH06289518A (ja) * 1993-04-05 1994-10-18 Fuji Photo Film Co Ltd ハロゲン化銀カラー写真感光材料
JPH0829906A (ja) * 1994-07-11 1996-02-02 Fuji Photo Film Co Ltd ハロゲン化銀乳剤
KR0155191B1 (ko) * 1994-10-05 1998-12-01 강박광 양이온 고분자 및 이의 제조방법
US5824756A (en) * 1994-10-25 1998-10-20 Reilly Industries, Inc. H2 O2 -catalyzed polymerizations for linear polyvinylpyridines
KR100307776B1 (ko) * 1995-06-06 2001-11-22 엔도 마사루 프린트배선판
JPH11142891A (ja) * 1997-11-05 1999-05-28 Nippon Oil Co Ltd エレクトロクロミックミラー
US6444110B2 (en) * 1999-05-17 2002-09-03 Shipley Company, L.L.C. Electrolytic copper plating method
US20060183328A1 (en) * 1999-05-17 2006-08-17 Barstad Leon R Electrolytic copper plating solutions
JP2001073182A (ja) * 1999-07-15 2001-03-21 Boc Group Inc:The 改良された酸性銅電気メッキ用溶液
US20040045832A1 (en) 1999-10-14 2004-03-11 Nicholas Martyak Electrolytic copper plating solutions
EP1148156A3 (en) 2000-04-11 2004-02-04 Shipley Company LLC Copper Electroplating
EP1167582B1 (en) * 2000-07-01 2005-09-14 Shipley Company LLC Metal alloy compositions and plating method related thereto
EP1182709A1 (en) * 2000-08-14 2002-02-27 IPU, Instituttet For Produktudvikling A process for depositing metal contacts on a buried grid solar cell and a solar cell obtained by the process
WO2002103753A2 (en) * 2000-11-01 2002-12-27 Myrick James J Nanoelectronic interconnection and addressing
US6776893B1 (en) * 2000-11-20 2004-08-17 Enthone Inc. Electroplating chemistry for the CU filling of submicron features of VLSI/ULSI interconnect
JP4481541B2 (ja) * 2000-12-20 2010-06-16 日本リーロナール有限会社 電解銅めっき液および電解銅めっき液の管理方法
US20030021761A1 (en) * 2001-01-18 2003-01-30 Geltex Pharmaceuticals, Inc. Ionene polymers and their use in treating mucositis
WO2002086196A1 (en) * 2001-04-19 2002-10-31 Rd Chemical Company Copper acid baths, system and method for electroplating high aspect ratio substrates
JP2003105584A (ja) * 2001-07-26 2003-04-09 Electroplating Eng Of Japan Co 微細配線埋め込み用銅メッキ液及びそれを用いた銅メッキ方法
US6572753B2 (en) * 2001-10-01 2003-06-03 Eci Technology, Inc. Method for analysis of three organic additives in an acid copper plating bath
US7316772B2 (en) * 2002-03-05 2008-01-08 Enthone Inc. Defect reduction in electrodeposited copper for semiconductor applications
US8002962B2 (en) * 2002-03-05 2011-08-23 Enthone Inc. Copper electrodeposition in microelectronics
US7450292B1 (en) * 2003-06-20 2008-11-11 Los Alamos National Security, Llc Durable electrooptic devices comprising ionic liquids
US6818313B2 (en) * 2002-07-24 2004-11-16 University Of Dayton Corrosion-inhibiting coating
JP3850772B2 (ja) * 2002-08-21 2006-11-29 富士通株式会社 レジストパターン厚肉化材料、レジストパターンの製造方法、及び半導体装置の製造方法
EP1422320A1 (en) 2002-11-21 2004-05-26 Shipley Company, L.L.C. Copper electroplating bath
KR20040073974A (ko) * 2003-02-14 2004-08-21 롬 앤드 하스 일렉트로닉 머트어리얼즈, 엘.엘.씨. 전기도금 조성물
US20050072683A1 (en) * 2003-04-03 2005-04-07 Ebara Corporation Copper plating bath and plating method
JP2004346381A (ja) * 2003-05-23 2004-12-09 Hitachi Ltd プリント配線基板、その製造方法、電気銅めっき方法、及び電気銅めっき液
US7128822B2 (en) * 2003-06-04 2006-10-31 Shipley Company, L.L.C. Leveler compounds
JP2005029818A (ja) * 2003-07-09 2005-02-03 Ebara Corp めっき方法
WO2005009928A2 (en) * 2003-07-24 2005-02-03 The Queen's Medical Center Preparation and use of alkylating agents
KR100539392B1 (ko) * 2003-08-12 2005-12-27 (주)해은켐텍 습도센서 감습막용 전해질 고분자 조성물, 그로부터제조되는 전해질 고분자 잉크 및 잉크젯 인쇄방식을이용하여 감습막을 형성하는 습도센서 제조방법
US20050092611A1 (en) * 2003-11-03 2005-05-05 Semitool, Inc. Bath and method for high rate copper deposition
US7186326B2 (en) * 2004-05-27 2007-03-06 Eci Technology, Inc. Efficient analysis of organic additives in an acid copper plating bath
TW200613586A (en) * 2004-07-22 2006-05-01 Rohm & Haas Elect Mat Leveler compounds
JP4973829B2 (ja) * 2004-07-23 2012-07-11 上村工業株式会社 電気銅めっき浴及び電気銅めっき方法
TWI303832B (en) * 2004-08-30 2008-12-01 Shinetsu Polymer Co Conductive composition and conductive cross-linked product, capacitor and production method thereof, and antistatic coating material, antistatic coating, antistatic film, optical filter, bnd optical information recording medium
JP4583860B2 (ja) * 2004-10-04 2010-11-17 富士通株式会社 レジストパターン厚肉化材料、レジストパターンの形成方法、並びに、半導体装置及びその製造方法
US20060246217A1 (en) * 2005-03-18 2006-11-02 Weidman Timothy W Electroless deposition process on a silicide contact
US7651934B2 (en) * 2005-03-18 2010-01-26 Applied Materials, Inc. Process for electroless copper deposition
US20060246699A1 (en) * 2005-03-18 2006-11-02 Weidman Timothy W Process for electroless copper deposition on a ruthenium seed
WO2006102180A2 (en) * 2005-03-18 2006-09-28 Applied Materials, Inc. Contact metallization methods and processes
US20060243599A1 (en) * 2005-04-28 2006-11-02 Taiwan Semiconductor Manufacturing Company, Ltd. Electroplating additive for improved reliability
EP1741804B1 (en) * 2005-07-08 2016-04-27 Rohm and Haas Electronic Materials, L.L.C. Electrolytic copper plating method
US20070012576A1 (en) * 2005-07-13 2007-01-18 Rohm And Haas Electronic Materials Llc Plating method
WO2007035880A2 (en) * 2005-09-21 2007-03-29 Applied Materials, Inc. Method and apparatus for forming device features in an integrated electroless deposition system
JP4652197B2 (ja) * 2005-09-29 2011-03-16 富士フイルム株式会社 染料含有ネガ型硬化性組成物、カラーフィルタ及びその製造方法
TWI328622B (en) * 2005-09-30 2010-08-11 Rohm & Haas Elect Mat Leveler compounds
US20070099422A1 (en) * 2005-10-28 2007-05-03 Kapila Wijekoon Process for electroless copper deposition
US8012334B2 (en) * 2007-04-03 2011-09-06 Rohm And Haas Electronic Materials Llc Metal plating compositions and methods
TWI341554B (en) * 2007-08-02 2011-05-01 Enthone Copper metallization of through silicon via
KR20110046439A (ko) * 2008-07-24 2011-05-04 코비오 인코포레이티드 알루미늄 잉크 및 이의 제조 방법, 알루미늄 잉크 증착 방법 및 알루미늄 잉크의 인쇄 및/또는 증착에 의해 형성된 필름
US7998859B2 (en) * 2008-09-25 2011-08-16 Enthone Inc. Surface preparation process for damascene copper deposition
US8388824B2 (en) * 2008-11-26 2013-03-05 Enthone Inc. Method and composition for electrodeposition of copper in microelectronics with dipyridyl-based levelers

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