JP2009523904A - リパーゼと漂白剤触媒を含む組成物 - Google Patents
リパーゼと漂白剤触媒を含む組成物 Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38627—Preparations containing enzymes, e.g. protease or amylase containing lipase
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3902—Organic or inorganic per-compounds combined with specific additives
- C11D3/3905—Bleach activators or bleach catalysts
- C11D3/3907—Organic compounds
- C11D3/3917—Nitrogen-containing compounds
- C11D3/392—Heterocyclic compounds, e.g. cyclic imides or lactames
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3902—Organic or inorganic per-compounds combined with specific additives
- C11D3/3905—Bleach activators or bleach catalysts
- C11D3/3932—Inorganic compounds or complexes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3945—Organic per-compounds
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Abstract
Description
本出願は、米国特許法第119(e)条に基づき、米国特許仮出願第60/761,114号(2006年1月23日申請)、米国特許仮出願第60/796,269号(2006年4月28日申請)、および米国特許仮出願第60/854,840号(2006年10月27日申請)の優先権を主張するものである。
本発明は、リパーゼと漂白剤触媒を含む組成物に関するものである。さらに具体的には、本発明は、リパーゼと、ペルオキシ酸から酸素原子を受け取り、その酸素原子を酸化可能基材に受け渡すことができる漂白剤触媒を含む組成物に関するものである。本発明の組成物は典型的には、洗濯洗剤組成物として用いるのに適しており、また、とりわけ、厄介な乳製品の残留汚れ上で、優れたクリーニング性能と悪臭特性の低減をもたらす。
本組成物は、(i)リパーゼと、(ii)ペルオキシ酸から酸素原子を受け取ることができ、その酸素原子を酸化可能基材に受け渡すことができる漂白剤触媒とを含む。前記リパーゼと漂白剤触媒については、以下でさらに詳しく説明する。
本組成物はリパーゼを含む。組成物にリパーゼを組み入れることによって、洗浄性能が向上する。これに加えてリパーゼを漂白触媒と組み合わせると、組成物の悪臭特性が大きく低下する。
01759号、WO2004/101760号、およびWO2004/101763号に記載されている。
漂白剤触媒は、ペルオキシ酸および/またはその塩から酸素原子を受け取ることができ、その酸素原子を酸化可能基材に受け渡すことができる。適切な漂白剤触媒としては、イミニウムカチオンおよびポリイオン、イミニウム双性イオン、変性アミン、変性アミンオキシド、N−スルホニルイミン、N−ホスホニルイミン、N−アシルイミン、チアジアゾールジオキシド、ペルフルオロイミン、環状糖ケトン、並びに、これらの混合物が挙げられるが、これらに限らない。
本組成物には、(i)オキシベンゼンスルホネート漂白活性剤および/またはオキシベンゾイン漂白活性剤、並びに、(ii)過酸素源を含有するのが好ましい。典型的には、オキシベンゾイン酸漂白活性剤は、その塩の形状をしている。好ましいオキシベンゼンスルホネート漂白活性剤としては、以下の一般式を有する漂白活性剤が挙げられる。
式中、Rは、漂白活性剤が疎水性の場合に6〜12個の炭素原子、または8〜12個の炭素原子を有する、任意で分岐のアルキル基であり、Lは脱離基である。好適な脱離基の例は、ベンゾイン酸およびその誘導体、特にはその塩である。特に好ましい別の脱離基はオキシベンゼンスルホネートである。適切な漂白活性剤としては、ドデカノイルオキシベンゼンスルホネート、デカノイルオキシベンゼンスルホネート、デカノイルオキシベンゾイン酸塩、3,5,5−トリメチルヘキサノイルオキシベンゼンスルホネート、ノナノイルアミドカプロイルオキシベンゼンスルホネート、およびノナノイルオキシベンゼンスルホネート(NOBS)が挙げられる。適切な漂白活性剤はWO98/17767号にも開示されている。これらの漂白活性剤を本組成物に組み込むのは、本組成物が低レベルのゼオライトビルダーとホスフェートビルダーを含む場合に特に好ましい。特に低ビルダー(under-built)洗剤組成物(このような洗剤組成物は低濃度のゼオライトビルダーとホスフェートビルダーを含む)の中で、これらの漂白活性剤を過酸素源、および上でさらに詳細に説明されている漂白触媒、並びにリパーゼと組み合わせると、全体的な洗浄性能が向上し、ゴム製排水ホースに対する適合特性が向上し、本組成物の悪臭特性が低下することを本発明者達は見出した。
別の実施形態では、本組成物は、(i)リパーゼと、(ii)ジアシルおよび/またはテトラアシルペルオキシド種を含んでいる。上記組成物は、ゴム製排水ホースに対する優れた適合特性を呈することを本発明者達は発見した。ジアシルペルオキシド、さらにはテトラアシルペルオキシドは、ゴム、例えば、自動洗濯機のゴム製排水ホースを傷めることで知られており、これにより、複数の洗浄サイクルにわたって、ゴム製排水ホースの破損を引き起こす可能性がある。ジアシルペルオキシドおよび/またはテトラアシルペルオキシドをリパーゼと組み合わせると、ゴム製排水ホースに対する不適合性の問題が解消されることを本発明者達は発見した。
式中、R1はC6〜C18アルキル、好ましくは、少なくとも5個の炭素原子の直鎖を含んでおり、所望に応じて1つ以上の置換(例えば、−N+(CH3)3、−COOHまたは−CN)および/またはアルキルラジカルの隣接炭素原子間に挿入されている1つ以上の妨害部分(例えば、−CONH−または−CH=CH−)を含んでいるC6〜C12アルキル基を表しており、R2はペルオキシド部分と相溶性のある脂肪族基を表しており、R1およびR2には合計で8〜30個の炭素原子を含んでいる。好ましいある1つの態様では、R1およびR2は非置換の直鎖C6〜C12アルキル鎖である。R1およびR2は同一であるのが最も好ましい。ジアシルペルオキシド(R1およびR2の両方がC6〜C12アルキル基である)が特に好ましい。R基(R1またはR2)のうちの好ましくは少なくとも1つ、最も好ましくは1つのみでは、α位に、または好ましくはα位にもβ位にも、または最も好ましくはα位、β位、γ位のいずれにも、分岐またはペンダント環を含んでいない。さらに好ましいある1つの実施形態では、DAPは非対称であってよく、過酸を生成させるためにR1のアシル基の加水分解は急速であるが、R2のアシル基の加水分解はゆっくりになるようにするのが好ましい。
式中、R3はC1〜C9、好ましくはC3〜C7アルキル基を表しており、nは2〜12、好ましくは4〜10の整数を表している。
予備形成済みのペルオキシ酸(pre-formed peroxyacid)またはその塩は典型的に、ペルオキシカルボン酸もしくはその塩、またはペルオキシスルホン酸もしくはその塩のいずれかである。
2−エチルヘキシルグリシジルエーテルの調製:エピクロロヒドリン(15.62g、0.17モル)が充填されている追加の漏斗が備わっている火力乾燥済みの500mLの丸底フラスコに、2−エチルヘキサノール(16.5g、0.127モル)と塩化第2スズ(0.20g、0.001モル)を加える。反応物をアルゴン雰囲気下で保ち、油浴を用いて90℃まで加温する。エピクロロヒドリンを60分かけて攪拌溶液に滴下した後、90℃で18時間攪拌する。反応物を真空蒸留ヘッドに取り付け、1−クロロ−3−(2−エチル−ヘキシルオキシ)−プロパン−2−オルを27Pa(0.2mm Hg)で蒸留する。1−クロロ−3(2−エチル−ヘキシルオキシ)−プロパン−2−オル(4.46g、0.020モル)をテトラヒドロフラン(50mL)に溶解し、アルゴン雰囲気下の室温で攪拌する。攪拌溶液に、カリウムt−ブトキシド(2.52g、0.022モル)を加え、その懸濁液を室温で18時間攪拌する。次に、反応物を蒸発乾固し、残留物をヘキサン中に溶解させ、水(100mL)で洗う。ヘキサン相を分離させ、Na2SO4によって乾燥させ、ろ過および蒸発乾固して、粗製2−エチルヘキシルグリシジルエーテルを得、これはさらに、真空蒸留によって精製することができる。
所望の生成物は、2−ブチルオクタノールを2−ヘキシルオクタノールに置き換える以外は実施例1に従って調製する。
以下の洗濯洗剤組成物A、B、C、およびDは、本発明で用いるのに適している。典型的に、これらの組成物は、洗濯プロセス中に80g/L〜120g/Lの濃度で水中に投与する。
** 実施例1もしくは2に従って調製した有機触媒、またはこれらの混合物
*** ジアシルペルオキソドは、ジノナノイルペルオキシドであるのが好ましい。
Claims (19)
- (a)リパーゼ、および
(b)ペルオキシ酸から酸素原子を受け取ることができ、かつ前記酸素原子を酸化可能な基材に受け渡すことができる漂白触媒
を含む組成物。 - 前記漂白触媒が、イミニウムおよび/またはカルボニル官能基を含む、請求項1に記載の組成物。
- 前記漂白触媒が、オキサジリジニウムおよび/もしくはカルボニル官能基を含み、および/または前記漂白触媒が、酸素原子を受け取ると、オキサジリジニウムおよび/もしくはジオキシラン官能基を形成することができる、請求項1に記載の組成物。
- 前記漂白触媒が、以下の化学式に対応する化学構造を有し、
- 前記リパーゼが、アミノ酸配列を有するポリペプチドであり、
(a)フミコララヌギノーサ(Humicola lanuginosa)菌株DSM4109由来の野生型リパーゼとの同一性が少なくとも90%であり、
(b)前記野生型リパーゼと比較した場合、E1またはQ249から15Å以内の3次元構造表面における電気的に中性もしくは負に荷電したアミノ酸の正に荷電したアミノ酸による置換を含み、および/または
(c)C末端にペプチド付加物を含み、および/または
(d)N末端にペプチド付加物を含み、および/または
(e)
(i)前記野生型リパーゼのE210の位置に負のアミノ酸を含み、
(ii)前記野生型リパーゼの90〜101位に対応する領域に負に荷電したアミノ酸を含み、かつ、
(iii)前記野生型リパーゼのN94の位置に対応する位置に中性または負のアミノ酸を含み、および/または前記野生型リパーゼの90〜101位に対応する領域に負もしくは中性の正味電荷を備える、
という制限を満たす、請求項1に記載の組成物。 - 前記リパーゼが、突然変異体T231RおよびN233Rを有する、フミコララヌギノーサ(Humicola lanuginosa)リパーゼの変異体である、請求項7に記載の組成物。
- 前記組成物の5重量%未満の過酸素源を含む、請求項1に記載の組成物。
- 前記組成物の5重量%〜10重量%のカーボネートアニオン源を含む、請求項1に記載の組成物。
- 移染防止剤を含む、請求項1に記載の組成物。
- (a)前記組成物の5重量%未満のゼオライトビルダー、
(b)所望により、前記組成物の5重量%未満のホスフェートビルダー、および
(c)所望により、前記組成物の5重量%未満のシリケート塩
を含む、請求項1に記載の組成物。 - ジアシルおよび/またはテトラアシルペルオキシド種を含む、請求項1に記載の組成物。
- オキシベンゼンスルホネート漂白活性剤と過酸素源を含む、請求項1に記載の組成物。
- 予備形成されたペルオキシ酸を含む、請求項1に記載の組成物。
- (a)第1サイクルのリパーゼ(first cycle lipase)、および
(b)ジアシルおよび/またはテトラアシルペルオキシド種
を含む、請求項1に記載の組成物。 - ペルオキシ酸から酸素原子を受け取ることができ、かつ前記酸素原子を酸化可能な基材に受け渡すことができる漂白触媒を含む、請求項16に記載の組成物。
- 前記リパーゼが、アミノ酸配列を有するポリペプチドであり、
(a)フミコララヌギノーサ(Humicola lanuginosa)菌株DSM4109由来の野生型リパーゼとの同一性が少なくとも90%であり、
(b)前記野生型リパーゼと比較した場合、E1またはQ249から15Å以内の3次元構造表面における電気的に中性もしくは負に荷電したアミノ酸の正に荷電したアミノ酸による置換を含み、および/または
(c)C末端にペプチド付加物を含み、および/または
(d)N末端にペプチド付加物を含み、および/または
(e)
(i)前記野生型リパーゼのE210の位置に負のアミノ酸を含み、
(ii)前記野生型リパーゼの90〜101位に対応する領域に負に荷電したアミノ酸を含み、かつ
(iii)前記野生型リパーゼのN94の位置に対応する位置に中性もしくは負のアミノ酸を含み、および/または前記野生型リパーゼの90〜101位に対応する領域に負もしくは中性の正味電荷を備える、
という制限を満たす、請求項16に記載の組成物。 - 前記リパーゼが、突然変異体T231RおよびN233Rを有する、フミコララヌギノーサ(Humicola lanuginosa)リパーゼの変異体である、請求項18に記載の組成物。
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
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US76111406P | 2006-01-23 | 2006-01-23 | |
US79626906P | 2006-04-28 | 2006-04-28 | |
US85484006P | 2006-10-26 | 2006-10-26 | |
PCT/US2007/001671 WO2007087258A2 (en) | 2006-01-23 | 2007-01-22 | A composition comprising a lipase and a bleach catalyst |
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JP2009523904A true JP2009523904A (ja) | 2009-06-25 |
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JP2008552348A Ceased JP2009523904A (ja) | 2006-01-23 | 2007-01-22 | リパーゼと漂白剤触媒を含む組成物 |
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US (1) | US8022027B2 (ja) |
EP (1) | EP1979457A2 (ja) |
JP (1) | JP2009523904A (ja) |
CN (1) | CN101484565B (ja) |
AR (1) | AR059153A1 (ja) |
CA (1) | CA2635946C (ja) |
WO (1) | WO2007087258A2 (ja) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2013523976A (ja) * | 2010-04-06 | 2013-06-17 | ザ プロクター アンド ギャンブル カンパニー | 洗濯洗浄剤における漂白系の最適化放出 |
JP2019502779A (ja) * | 2015-11-26 | 2019-01-31 | ザ プロクター アンド ギャンブル カンパニー | プロテアーゼを含む液体洗剤組成物及び封入リパーゼ |
Families Citing this family (233)
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PL1754781T3 (pl) * | 2005-08-19 | 2013-09-30 | Procter & Gamble | Stała kompozycja detergentowa do prania zawierająca anionowy środek powierzchniowo czynny i technologię wspomagania wapniem |
US20070191249A1 (en) * | 2006-01-23 | 2007-08-16 | The Procter & Gamble Company | Enzyme and photobleach containing compositions |
AR059156A1 (es) * | 2006-01-23 | 2008-03-12 | Procter & Gamble | Composiciones detergentes |
US20070191248A1 (en) * | 2006-01-23 | 2007-08-16 | Souter Philip F | Detergent compositions |
US20070179074A1 (en) * | 2006-01-23 | 2007-08-02 | Souter Philip F | Detergent compositions |
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AR059153A1 (es) | 2008-03-12 |
CN101484565A (zh) | 2009-07-15 |
WO2007087258A2 (en) | 2007-08-02 |
CA2635946C (en) | 2012-09-18 |
EP1979457A2 (en) | 2008-10-15 |
CN101484565B (zh) | 2011-12-14 |
US8022027B2 (en) | 2011-09-20 |
US20070173429A1 (en) | 2007-07-26 |
CA2635946A1 (en) | 2007-08-02 |
WO2007087258A3 (en) | 2008-12-04 |
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